Handbook Scientific Branch of Applied Physics Department of Physics, Chemistry and Biology (IFM) SOS Alarm (emergency only) (0)112 Security officer (013-28) 4087, 5888 Head of security (013-28) 1733 House manager Akademiska Hus (013-36) 4545 House manager, local at IFM, Bengt Andersson (013-28) 1285 Handling of waste, local support at IFM, Petra Hagstrand (013-28) 1049 Revised 2010-12-08 / Jeanette Nilsson, Stefan Klintström The Scientific area Applied Physics have seven divisions. This handbook cover the following six divisions: Applied Physics Biomolecular and Organic Electronics Molecular Physics Molecular Surface Physics and Nanoscience Applied Optics Biosensors and Bioelectronics As we in this handbook uses the denomination Applied Physics we mean the six divisions above. PREFACE This handbook is intended to give an overview of the organization at Applied Physics, and it should also clarify some rules and routines regarding safety and practical laboratory work. It should be regarded as a complement to the general regulations that are listed in the department handbook: http://cms.ifm.liu.se/intranet/institutionshandboken/ The general rules for IFM also applies to the Division of Applied Physics if not otherwise stated. Anyone who is about to perform laboratory work at Applied Physics must first understand the relevant parts of this handbook. If there is anything that needs to be changed or updated, please contact Jeanette Nilsson. It is especially important that the information in this handbook is examined together with guests and students working in our laboratories. Supervisors and teachers are responsible for their students, master students and project workers. It is your responsibility to learn which regulations and laws that govern your work. Your responsibilities increase with your knowledge and experience! Stefan Klintström SAFETY FIRST! The safety of yourself, your colleagues and our guests shall always be a primary concern. Bear in mind the interdisciplinary nature of Applied Physics. Your neighbor does not necessarily understand the danger that can be involved in your research. Most incidents with fretting compounds are actually caused by spill from co-workers. Please do not rush the laboratory work, too many accidents are caused by stress. 2 TABLE OF CONTENTS ORGANIZATION____________________________________________________ 5 Scientific area/Divisions ____________________________________________ 6 Management Group _______________________________________________ 6 Administrators ____________________________________________________ 6 Research Engineers _______________________________________________ 6 WHO HAS THE RESPONSIBILITY? ____________________________________ 7 Laws and regulations ______________________________________________ 7 Local information __________________________________________________ 7 Routines for purchasing ____________________________________________ 7 GENERAL RULES AND RESTRICTIONS ________________________________ 8 When something is not working_______________________________________ 8 If an accident or incident occurs ______________________________________ 8 Work alone ______________________________________________________ 8 Children _________________________________________________________ 8 Smoking ________________________________________________________ 8 Recyclable items __________________________________________________ 8 LABORATORIES AT APPLIED PHYSICS ________________________________ 9 LABORATORIES, PRESENTATION ___________________________________ 10 CHEMISTRY LAB (STEFAN KLINTSTRÖM) _____________________________ 10 Analytical scales _________________________________________________ 10 Wet silanization __________________________________________________ 10 Radioactivity ____________________________________________________ 10 Ellipsometric ____________________________________________________ 10 Scriber _________________________________________________________ 10 Gloves _________________________________________________________ 10 SURFACE CHEMISTRY LAB (BO LIEDBERG, KAJSA UVDAL) ______________ 11 Avoid contamination ______________________________________________ 11 Gamma counter__________________________________________________ 11 SURFACE ANALYSIS LAB (BO LIEDBERG, KAJSA UVDAL) ________________ 11 Equipments _____________________________________________________ 11 General ________________________________________________________ 11 WASHING UP (BO THUNÉR, JEANETTE NILSSON) ______________________ 11 TL1 and TL2 ____________________________________________________ 11 Dishwasher _____________________________________________________ 11 PROCESS LAB (BO LIEDBERG, BO THUNÉR) __________________________ 12 Evaporation (Bo Thunér) _________________________________________ 12 Bonding/Welding (Mike Andersson) _________________________________ 12 WORKSHOP (BO THUNÉR) _________________________________________ 12 General ________________________________________________________ 12 ELECTRONIC LAB (HANS SUNDGREN) _______________________________ 12 SENSOR LAB (MATS ERIKSSON) ____________________________________ 12 Gas-mixing systems ______________________________________________ 12 TONGUE & NOSE LAB (FREDRIK WINQUIST) __________________________ 12 Experimental set ups ______________________________________________ 12 SCANNING PROBE LAB (RAGNAR ERLANDSSON, JÖRGEN BENGTSSON) __ 13 Veeco Dimension 3100 ____________________________________________ 13 Veeco Enviroscope _______________________________________________ 13 Nanonics Multiview 1000 ___________________________________________ 13 Nanoscope Multimode ____________________________________________ 13 3 POLYMER LAB (OLLE INGANÄS) _____________________________________ Photovoltaic experiments __________________________________________ Evaporation _____________________________________________________ Glovebox _______________________________________________________ APPLIED OPTICS LAB (HANS ARWIN) ________________________________ General ________________________________________________________ Ellipsometers ____________________________________________________ Sample preparation _______________________________________________ Optical analysis __________________________________________________ LABORATORY RULES, IN GENERAL __________________________________ Before start working in the lab _______________________________________ Borrow equipment ________________________________________________ Eat or drink _____________________________________________________ Label/content, date and owner ______________________________________ Keep clean _____________________________________________________ Teaching activities and other guests at the laboratory ____________________ HAZARDOUS WORK _______________________________________________ Risk analysis/risk assessment _______________________________________ Material Safety Data Sheet _________________________________________ Flammable products/materials ______________________________________ Organic solvents _________________________________________________ Ethanol ________________________________________________________ Toxic and/or corrosive compounds ___________________________________ Hydrofluoric acid, HF ______________________________________________ Chemical waste __________________________________________________ Radioactivity ____________________________________________________ Genetically modified material _______________________________________ Blood products __________________________________________________ Syringes and injection needles ______________________________________ Pipettes ________________________________________________________ Sharp objects and contaminated waste________________________________ Glue Epoxy and thermosetting plastic _________________________________ Laser __________________________________________________________ Gas tubes ______________________________________________________ Electric mains powered equipment ___________________________________ Work with electricity_______________________________________________ Welding ________________________________________________________ Glass waste from lab ______________________________________________ Protective clothing/protection equipment _______________________________ 4 13 13 13 13 14 14 14 14 14 15 15 15 15 15 15 15 16 16 16 16 16 16 16 16 17 17 17 17 17 17 17 18 18 18 18 18 18 18 18 ORGANIZATION A large portion of the research at Applied Physics is interdisciplinary and staffs include engineers, physicists, chemists, biologists and others. Several projects are chosen in the areas between physics and chemistry, and physics and biology. Yet, the research is also indeed intra disciplinary, primarily within surface physics. Many projects are run in collaboration with other laboratories at IFM and with external collaborators. The doctoral programme Forum Scientium is administered at Applied Physics. Applied Physics has some 60-70 employees divided into several research divisions/groups (organization chart below). The scientific branch is run by the management group (the division leaders). The research activities are supported by a number of technicians and administrators. Scientific area Applied Physics Division of Applied Physics Division of Biosensors and Bioelectronics Division of Applied Optics Division of Molecular Physics Division of Molecular Surface Physics and Nanoscience Division of Biomolecular and Organic Electronics Division of Biotechnology 5 Scientific area/Divisions Scientific area Applied Physics Bo Liedberg Divisions Applied Physics Biosensors and Bioelectronics Molecular Physics Molecular Surface Physics and Nanoscience Biomolecular and Organic Electronics Applied Optics Biotechnology1 Stefan Klintström Anthony Turner Bo Liedberg Kajsa Uvdal Olle Inganäs Hans Arwin Carl-Fredrik Mandenius Management Group Bo Liedberg Leader Scientific Area Division leader Division leader Division leader Division leader Division leader Division leader Division leader Scientific mentor Stefan Klintström Anthony Turner Kajsa Uvdal Olle Inganäs Hans Arwin Carl-Fredrik Mandenius Ingemar Lundström Administrators Susann Årnfelt Scientific area Applied Physics Divisions Applied Physics Molecular Surface Physics and Nanoscience Molekylär Physics Applied Physics Anita Spetz group Biomolecular and Organic Elektronics Applied Optics Biotechnology1 Anna Maria Uhlin Pia Blomstedt Therese Dannetun Mikael Amlé Susann Årnfelt Anna Sundin Research Engineers Bo Thunér Technical infrastructure of laboratories Gas handling CAD Evaporation Representative for the working environment Resource person regarding handling of waste Representative for environmental issues Computer related issues Purchase of Computer Software Scanning Probe Microscopy Resource person for purchase of chemicals and common lab ware Registry of chemicals in KLARA Jeanette Nilsson Jörgen Bengtsson Anke Suska 1 See separate handbook at http://www.ifm.liu.se/biotech/ 6 WHO HAS THE RESPONSIBILITY? Laws and regulations The working environment in Sweden is carefully regulated in Arbetsmiljölagen and Arbetsmiljöverkets författningssamling, AFS. These are available at http://www.av.se and should be consulted if necessary. Local copies are also available in Technical Service supply in room M225. Local information The employer, Linköping University, is always responsible for the working environment. The Rector of the University has delegated the responsibility at IFM to the Head of the Department. The Head of IFM has then delegated the responsibility for the working environment to the employer representatives in the management group at Applied Physics. At IFM we also have a coordinator for environmental issues, Petra Hagstrand. She is an expert within environmental issues, handling of chemicals and waste, and handling of gases. Bo Thunér is a resource person for the infrastructure at all laboratories at Applied Physics except for Applied Optics and Division of Biotechnology. Furthermore, each individual research laboratory has personnel how is responsible for the research details, risk analysis and for the practical laboratory work. For sensitive equipment there may be appointed equipment responsible persons, indicated by a sign posted next to the instrument. There is an independent control of the working environment at Applied Physics performed by the representative for the working environment that is appointed by the employer representative and the Labour Union. Deficiencies in the working conditions in a research laboratory shall primarily be reported to the person who is responsible for that specific laboratory or to the representative for the working environment or alternatively to Lokala Samverkansgruppen, LSG. Routines for purchasing Purchasing (over certain sums) are regulated according to the rules for governmental activity in Sweden. Consult the regulations in the University handbook before placing an order: https://cms.ifm.liu.se/intranet/institutionshandboken/upphandling/. Always consult your supervisor and administrator before placing an order. A copy of the purchase order shall be sent to your administrator and to Peter Alm, who is taking care of your parcel when it arrives. Purchases of chemicals shall always be done by Anke Suska. 7 GENERAL RULES AND RESTRICTIONS When something is not working If you identify errors that are related to ventilation, heating, electrical supply, cooling water, fume hoods, doors, etc., then report to: The House Manager, Akademiska Hus 013-364545 or local representative at IFM, Bengt Andersson (013-28)1285. Upon burglary or vandalism, call University Security officer (013-28) 4087, 5888. All other errors at the laboratories shall be reported to Bo Thunér (013-28) 5661. If an accident or incident occurs Accidents/injuries shall be reported as soon as possible on a special form “Anmälan om arbetsskada”. The form can be obtained from the staff intendant at IFM or download from http://www.fk.se. The form shall be filled in via collaboration between the injured person and the person who is employer representative for the specific laboratory. The representative for the working environment and the employer representative shall sign the form. The form shall be sent back to the staff intendant. Injuries shall also be reported to “AFA Försäkringar”. The form can be download from http:/afaforsakring.se. The form shall be sent back to the staff intendant. Incidents that could have caused injury on personnel or serious economic damage shall be reported on yet another form “Anmälan om tillbud”. The form can be obtained from the staff intendant at IFM or download from: http://cms.ifm.liu.se/intranet/institutionshandboken/blanketter/ The procedure for this form is the same as for injuries. Work alone You are not allowed to work alone after normal working hours (normal weekdays 8.00 to 18.00). Weekdays during summer and other holiday seasons are considered as after normal working hours. However, working alone is allowed if the working alone alarm system is used. Exceptions from using the alarm system could be a very short visit at the laboratory to check an instrument. The alarm units and instructions for how to use them are found in the IFM mailroom. Guests and students that work for a shorter period at IFM Applied Physics shall not work alone. Children Children under the age of 12 do not have access to the laboratories, not even under supervision. Smoking Smoking is prohibited in the entire building, as well for the balcony in Zenit. You are recommended to go outside the building. Recyclable items Most of the waste we throw away can be recycled (glass, plastic, batteries, light bulbs, office paper, magazines, newspapers, carton, corrugated cardboards etc.) IFM has a recycling-room in the basement. Close to the containers there are labels that tells you how to sort the waste. Broken instruments/computers shall be hand over to Peter Alm. If any questions contact Jeanette Nilsson. 8 LABORATORIES AT APPLIED PHYSICS Table 1: List of the laboratories at Applied Physics LABORATORY ROOM WORKING ENVIRONMENT RESPONSIBLE Stefan Klintström RESEARCH DETAILS Stefan Klintström PRACTICAL LABORATORY WORK Stefan Klintström Stefan Klintström Stefan Klintström Anke Suska Stefan Klintström Ragnar Erlandsson Jörgen Bengtsson Bo Thunér Jeanette Nilsson Anke Suska Jeanette Nilsson Chemistry L202-205 Chemical Storage L210 Scanning Probe L214, L 215 vä Washing-up L209 Stefan Klintström N203 Stefan Klintström Optical Biosensors N208, N210 Stefan Klintström Daniel Filippini Daniel Filippini Gas Storage P101 Stefan Klintström Bo Thunér Bo Thunér Workshop P205 Stefan Klintström Bo Thunér Bo Thunér Tongue & Nose P204 Mats Eriksson Fredrik Winquist Fredrik Winquist Electronic P206 Mats Eriksson Hans Sundgren Hans Sundgren Sensor P207 Mats Eriksson Mats Eriksson Mats Eriksson Process L213 Bo Liedberg Bo Thunér Bo Thunér Light Emision L216 Bo Liedberg Thomas Ederth Thomas Ederth Surface Chemistry L215, hö Bo Liedberg Bo Liedberg Tobias Ekblad Surface Chemistry N204 Bo Liedberg Bo Liedberg Emma Ericsson Surface Analysis IR XPS N205-207 Bo Liedberg Kajsa Uvdal Bo Liedberg Kajsa Uvdal Bo Liedberg Kajsa Uvdal Optical Measurement N209 Bo Liedberg Bo Liedberg Bo Liedberg Biosensors N211 Bo Liedberg Bo Liedberg Bo Liedberg Optics SPR N213 Bo Liedberg Bo Liedberg Pitsiri Sukkaew Storage Common lab ware ---------- Anke Suska BIA N212 Bo Liedberg Bo Liedberg Emma Ericsson Bo Liedberg Polymer- Alvastra Electronics M204,M207 Olle Inganäs Olle Inganäs Niclas Sohlin Polymer- Skänninge Electrochemistry M206,M208 Olle Inganäs Olle Inganäs Niclas Sohlin Applied Optics M205, L210, L206-8 Hans Arwin Hans Arwin Hans Arwin Roger Magnusson 9 LABORATORIES, PRESENTATION CHEMISTRY LAB (Stefan Klintström) Analytical scales Many people are using the analytical scales. Always wipe up spilled chemicals and always note the substance in the logbook when you are finished. This may be important information for the next user. Wet silanization Inside the laboratory there is an area reserved for wet silanization. Please follow the posted protocols carefully during silanization and keep the door to this area closed. The glassware used during the silanization is forever contaminated and shall be treated as such. That is, it shall never leave the silanization room as other than waste. Always keep the door to the room closed. It is absolutely forbidden to put silanized lab ware in the dishwasher! Radioactivity We have permission to work with a limited amount of radioactivity. However, you always have to clear with Stefan Klintström before you handle any radioactive material in the laboratory. Ellipsometric Before planning extensive experiments requiring ellipsometric analyses, please study the calendar next to the instruments to make sure the instruments are not reserved. Approved personnel may only reserve ellipsometers. Contact Stefan Klintström. Scriber The Scriber instrument (used for cutting silicon wafers) is a sensitive instrument that requires proper instructions before use. Please ask for help before attempting to use it, contact Bo Thunér. Always note in the logbook, what you have cut. Gloves At this laboratory we primarily use gloves to protect ourselves, not our samples. Please discard the gloves as soon as they are no longer needed to avoid spreading of contamination. Don’t throw used gloves in the wastepaper-bin, instead use the special waste container. 10 SURFACE CHEMISTRY LAB (Bo Liedberg, Kajsa Uvdal) Avoid contamination At this laboratory it is extremely important to avoid surface contamination. Therefore, all the glasswares in this lab is only for use within the Surface Chemistry Lab. Tools and glasswares cannot be borrowed for usage outside the lab. If you are uncertain about the cleanliness of glassware – don’t utilize it. Never bring glassware from other labs. It is absolutely forbidden to bring in things that have been in contact with silanez. Gamma counter We have permission to work with a limited amount of radioactivity. However, you always have to clear with Stefan Klintström before you handle any radioactive material in the laboratory. SURFACE ANALYSIS LAB (Bo Liedberg, Kajsa Uvdal) Equipments In this laboratory there are UHV- XPS system, ellipsometer and equipment for contact angle measurements. General The laminar flow hood is only for handling and mounting of XPS samples and cleaning of UHV components. This area is restricted only for ultra-pure work, prior to UHV analysis. No liquids are allowed. Tools on the blue tool pad and on the desk close to it are only for UHV equipment. Please respect this. It is of major importance that these tools not get in contact with grease and lubricants to avoid contamination of the UHV system. The XPS instrument is not for common use. If you need XPS analysis, please contact Kajsa Uvdal. The desks at the ellipsometer and equipment for contact angle measurements should always be clean and tidy. Please, never leave old samples in or beside the instruments. Avoid if possible bringing incubation solutions and solvents into the room. When this is necessary, please bring them back to the wet chemistry lab immediately after use. For questions regarding ellipsometer and contact angle measurements contact Tobias Ekblad. WASHING UP (Bo Thunér, Jeanette Nilsson) TL1 and TL2 The hoods in this laboratory are intended for standard semiconductor cleaning procedures (TL1 and TL2) only. Please follow the posted instructions carefully and put the waste where intended. For handling TL2 one has to be introduced to the process to get an authorization. This is for minimizing the damage, from the acid, on fume hood and ventilation shaft. Contact Jeanette Nilsson. Dishwasher There are too dishwashers; one for the IR group and one common, respect that. Please rinse the utensils to be washed-up carefully before placing them next to the “dirty” sign or in the dishwasher. It is absolutely forbidden to put silanized lab ware in the dishwasher. 11 PROCESS LAB (Bo Liedberg, Bo Thunér) Evaporation (Bo Thunér) The evaporation equipments “Valfrid” and “Agneta” require proper training before use, contact Bo Thunér. Bonding/Welding (Mike Andersson) The bond- and weld equipment are not for common use. Contact Mike Andersson if you need help. WORKSHOP (Bo Thunér) General Of course you have to know how to handle tools before start working here. Here you can find tools, drilling-machine, ultrasound washer, vacuum cleaner etc. There are also a bench where you can carry out smaller works. ELECTRONIC LAB (Hans Sundgren) Bear in mind that there is a risk for exposed main power supplies at this laboratory. SENSOR LAB (Mats Eriksson) Gas-mixing systems At the Sensor lab, at S-SENCE, there are a number of gas-mixing systems. They are normally used to test gas sensors in controlled mixtures of different gases. Please, note that there are important instructions for the handling of the gas mixing systems in a binder at the entrance of the Sensor lab. Always contact Mats Eriksson before working in the lab. TONGUE & NOSE LAB (Fredrik Winquist) Experimental set ups The X-Y table, electronic tongue systems (3) and electronic nose systems (3) are not for common use. 12 SCANNING PROBE LAB (Ragnar Erlandsson, Jörgen Bengtsson) Veeco Dimension 3100 Versatile AFM (Atomic Force Microscope) instrument that requires special training to be used. Contact Jörgen Bengtsson in order to get a driving license for the instrument. Those who are certified users should use the Timebook systemet https://timebook.ifm.liu.se/login.php which is used for booking and charging money. Veeco Enviroscope AFM instrument specially designed to allow measurements where it is required to modify the environment around the sample. It is possible to measure in liquid, vacuum, controlled gas atmosphere, enhanced temperature etc. The instrument requires special training to be used. Contact Jörgen Bengtsson in order to get a driving license for the instrument. Nanonics Multiview 1000 Scanning Nearfield Optical Microscope (SNOM). This instrument is meant to be used for specific research tasks, and cannot be booked for individual measurements. The idea is that this instrument should have a small number of expert users who use it a lot. Nanoscope Multimode Our oldest AFM instrument. Those who use this instrument should be registered in the Timebook system. In order to use this system it is required that one is trained by an experienced user. POLYMER LAB (Olle Inganäs) Photovoltaic experiments Use of the dedicated experimental set ups for photovoltaic experiments (determination of internal monochromatic quantum efficiency, solar simulator) for light emitting diodes (emission spectrometer, LED photometer) requires introduction by Fengling Zhang prior to use. Evaporation The evaporation equipment “Malte” requires proper training before use, contact Bo Thúner. The use of vacuum evaporation requires permission from Fengling Zhang. Glovebox The Glovebox is used only for organic solar cell fabrication in a water and oxygen free atmosphere. Contamination of the glovebox will be avoided and thus only limited number of materials may exist inside the box. The Glovebox may only be used by authorized people. For training and permission, contact Fengling Zhang, Mattias Andersson or Kristofer Tvingstedt. 13 APPLIED OPTICS LAB (Hans Arwin) The information below concerns five small connected rooms with names Rogers room/Woollam (L206), Azzam (L208), Schubert (L201) and Aspnes (M205). General All eating and drinking are forbidden. During weekends and after 17.00 weekdays is only data analysis at the computer and changing samples on ellipsometers allowed. All doors must be locked during weekends and after 17.00 weekdays. Ellipsometers There are five ellipsometer systems (VASE1, VASE2, M88, IRSE and RC2) which all require license. Hans Arwin will answer questions about licences. Booking of an instrument is done through the booking calendar on the home page of Applied Optics. When using an instrument, the logbook must be filled in. Sample preparation There is hood and a bench for sample preparations in Rogers room (L206). The routines for chemical work are the same as for Applied Physics, e.g. for using hoods, waste handling, cleaning up, purchase of chemicals, etc. Samples and other items which not are marked with the users name will be removed by the laboratory responsible person if left on the sample preparation areas. Optical analysis For analysis of optical data there is a computer with the software WVASE in Rogers room (L206). This computer can be booked through the booking system and booking gives priority over non-booked users. In the room there is also a software key to the program to be inserted in the parallel port. Using this it is possible to perform analysis on ones own computer. This license is intended for short term use (not more than 2 days) and must be booked. For more extensive analysis it is possible to borrow a license during a longer time. Hans Arwin will answer questions related to program licenses. 14 LABORATORY RULES, IN GENERAL Before start working in the lab As a general rule, you shall always clear with the person who is responsible for a specific laboratory before you are allowed to work in that laboratory. Before starting to work in any laboratory, introduce yourself, your work and the potential dangers to your colleagues at the laboratory. Also have them to explain their work to you. Always make sure that you know where the emergency shower, eye rinse and fire extinguishers are located, and that you are capable of operating them. If an accident occurs there is no time to read the instructions. Borrow equipment You shall always ask for permission before you borrow any equipment from any laboratory. If you have moved equipment (after permission), please leave a note with information on the new location of the equipment. Eat or drink You are not allowed to eat or drink at the laboratories. Label/content, date and owner All glassware and other utensils shall be marked with content, date and owner. It is also allowed to temporarily store harmless unmarked utensils in a suitable box on the desk, if the owner is identified on the box. Empty boxes can be found in the lab L213, or contact Bo Thunér. All potentially dangerous chemicals shall be labelled with appropriate warning labels. Labels are available where the chemicals are stored and in the Technical Service store M225. Keep clean Each laboratory bench and fume hood shall have a sign where it is posted who is responsible for that specific area. Labels, notes and signs shall always be understandable also for the English speaking staff and guests. Generally, you shall keep the desks and other laboratory areas as clean as possible. Never store your stuff on the lab benches or in the fume hoods. The lab space is limited. Teaching activities and other guests at the laboratory Short-time guests shall work under careful supervision by a member of the research group. Use the form: https://cms.ifm.liu.se/intranet/institutionshandboken/arbetsmiljo/laboratoriesaker het/rutiner_och_instruktioner/ Supervisors and teachers are responsible for their students, master students and project workers. Perform a safety briefing before any laboratory assignment with students. Remember that teaching activities also require a risk analysis. This is the responsibility of the course leader. 15 HAZARDOUS WORK Risk analysis/risk assessment All new experiments/processes, including teaching activities, shall be subject for a risk analysis/risk assessment. Risk analysis is a dynamic process. You are encouraged to report to the responsible person if you identify potentially hazardous activities. Form and further information is available at: http://cms.ifm.liu.se/intranet/institutionshandboken/arbetsmiljo/laboratoriesakerh et/ The risk assessments should be stored in a register easily available in the current lab. Material Safety Data Sheet Before handling any unknown chemical you must first read and understand the specific Material Safety Data Sheet (MSDS) that is delivered with the chemical and shall be stored in an easily available register in the current lab, next to where the chemicals are stored. If you take the last of some chemical or utensil please be sure to always refill the supplies or inform Anke Suska. Flammable products/materials Flammable products/materials shall of course never be exposed to open flames or electric engines etc where sparks could ignite the compounds. Bear in mind that some flammable organic solvents have the nasty habit of forming fumes that can “crawl” out of a ventilated hood. Furthermore, it is very important that you know how to handle spill of the specific flammable before you use it. Spill of some flammables may burst into flames spontaneously. More information at: http://cms.ifm.liu.se/intranet/institutionshandboken/arbetsmiljo/laboratoriesakerh et/rutiner_och_instruktioner/ Organic solvents Organic solvents shall be used under hood and are stored in a specific locker in Chemical store L210. Smaller amounts may also be temporary stored in ventilated cabinets. Ethanol Access to ethanol is restricted. Contact Jeanette Nilsson if you need ethanol in your research. Toxic and/or corrosive compounds Toxic and/or corrosive compounds shall always be handled in fume hoods. Toxic compounds shall be stored in a special locker in Chemical store L210. Acids and bases have two separate lockers in L210. When diluting strong acids, the acid must always be put into the water, not the vice versa. Hydrofluoric acid, HF HF etching involves especially nasty hazards. At IFM, working with HF is limited. Before start working with HF you need permission from your super visor. After having that take contact with Jeanette Nilsson for authorization. 16 Chemical waste Pack the chemical in an appropriate container and seal it properly. Mark the container with its content, date, your name and what lab it comes from. Place the container in the cupboards for waste in Chemistry lab L202. Waste labels can be found at the outside of the cupboards. Containers and waste labels can also be purchased in Technical Service store M225. Never (ever!) leave waste unattended, even if it is water only. Other users or cleaning personnel does not know that it is harmless. If you have any questions regarding the handling of waste, or suggestions for purchasing of specific waste labels, containers etc., please turn to Jeanette Nilsson or Petra Hagstrand. More information at: http://cms.ifm.liu.se/intranet/institutionshandboken/arbetsmiljo/laboratoriesakerhet/rutiner _och_instruktioner/ Radioactivity We have permission to work with a very limited amount of radioactivity. Contact Stefan Klintström before planning to use or ordering any radioactive material. Genetically modified material All work with genetically modified material is restricted. Contact Carl-Fredrik Mandenius for more information. Blood products Generally, the blood and other human body fluids (or products derived there from) that are being used at Applied Physics have passed the standard blood bank testing. Yet they shall always be treated as capable of transmitting infectious diseases. Always use gloves when handling blood, blood plasma or blood serum (except if you are performing experiments with samples of your own blood) and disposable lab ware. Blood to be wasted shall be sealed carefully and put in the containers for contaminated waste. Contact Anke Suska if you have questions about this. Syringes and injection needles Syringes and injection needles shall be stored in locked compartments. Waste shall be put into special container. Pipettes You are not allowed to use your mouth as an aid when filling pipettes with liquids. Use pipette fillers instead. Sharp objects and contaminated waste Sharp objects like razor- and knife blades, injection needles etc. shall be thrown in a special container. Label container with content. Place filled container in the chemical waste cupboards in chemistry lab L202. Contaminated utensils, not classified as risk waste, such as gloves, pipettes tips, paper tissues, tops, small pieces of silicon wafers and glass etc. shall be thrown in a special container. Label container with content. Place the filled container in the container for combustible waste in the recycling-room located in the basement. Empty containers can be found in Applied Physics store N203. Never (ever!) put sharp and/or contaminated waste in the regular waste-paper basket, regarding to the cleaning personnel! 17 Glue Epoxy and thermosetting plastic If you use certain glues/plastics, more than three times a year there is a recommendation that you attend a special course. Some use of this glue may require that you go through a medical examination. Contact Petra Hagstrand. Laser The use of lasers is accompanied by strict regulations. Always contact Bo Thunér before using any laser equipment. Gas tubes Gas tubes shall be chained to a support to avoid them from overturning. The protective cover must be applied before you move the tubes, even if it is just inside a laboratory. If the gas is toxic, the tube must be stored in a ventilated cupboard or hood. Applied Physics has a gas store in the basement. Contact Bo Thunér for purchase or returning tubes. For more information: http://cms.ifm.liu.se/intranet/institutionshandboken/arbetsmiljo/laboratoriesakerh et/rutiner_och_instruktioner Electric mains powered equipment You are not allowed to perform any modifications, maintenance or any other kind of work inside/outside equipment intended for connection to the electric mains. This applies to new designs of equipment as well as existing equipment. Contact your boss if you find any need for maintenance or alterations on electric mains powered equipment. Work with electricity A risk assessment must always be carried out before working with electric circuits. The risk assessment must be approved and signed by the responsible senior. However, if it is clear that none of the following values can be exceeded: 50V, 10A or 200W a risk assessment is not needed for electric reasons exclusively. Welding Welding is only allowed at certain locations where proper ventilation is available. Glass waste from lab Empty glass bottles (ethanol, acid etc.) for recycling shall be rinsed very carefully and thrown away in the containers in the recycling-room in the basement. This does not apply for beakers, pipettes etc. from lab, those shall be thrown in a special container located in the basement in corridor M101-113. Protective clothing/protection equipment Protective clothing and other relevant protection equipment shall always be worn when handling chemicals, refer to the safety document for each specific chemical. Use proper eye protection if there is a risk for splashes. Note that this also applies for your neighbours at the laboratory if there is a reasonable risk that they may become exposed to splashes from your work. 18