Effects of Thermal Damage on the Strength Properties of 7050-T7451 and 7075-T7351 Aluminium Alloys Jaime Calero and Suzana Turk Air Vehicles Division Defence Science and Technology Organisation DSTO-TR-2104 ABSTRACT This report presents experimental test data that quantify the effects of thermal damage on the strength properties of 7050-T7451 and 7075-T7351 aluminium alloys. The test results indicate that there is a direct relationship between hardness and strength properties that can be used to determine residual strength of these alloys at room temperature after thermal damage. This relationship can be expressed as a function of hardness number by the use of exponential equations. RELEASE LIMITATION Approved for public release Published by Air Vehicles Division DSTO Defence Science and Technology Organisation Fishermans Bend, Victoria 3207 Australia Telephone: (03) 9626 7000 Fax: (03) 9626 7999 © Commonwealth of Australia 2008 AR-014-106 February 2008 APPROVED FOR PUBLIC RELEASE Effects of Thermal Damage on the Strength Properties of 7050-T7451 and 7075-T7351 Aluminium Alloys Executive Summary An extensive test program was conducted to quantify the effects of thermal damage on the strength properties of 7050-T7451 and 7075-T7351 aluminium alloys. The program was initiated in response to the need to provide comprehensive experimental data on thermal damage. These data could be used to quantify room temperature residual strength properties of airframe structures and components that have been exposed to temperatures above 205°C. The data show that both alloys have a similar response to thermal damage and that there is a direct relationship between hardness and strength properties. This relationship can be expressed by the use of exponential equations of the hardness number and strength data. As a result it was possible to use hardness and electrical conductivity testing to estimate the residual strength at room temperature after thermal damage had occurred. The test results also revealed that exposure at 315°C for more than 60 minutes eventually results in partial recovery of strength following the initial decrease in strength properties. A similar phenomenon was observed in the specimens tested at 350°C. It is expected however that this trend will revert as other factors that affect the strength of the alloy evolve. This behaviour should not be interpreted as an indication of recovery of properties but instead as a sign of possible severe thermal damage. It is envisaged that calculations based on these data could be used in structural integrity models to estimate room temperature residual strength properties of damaged structures and components made from these alloys. Contents 1. INTRODUCTION............................................................................................................... 1 2. OBJECTIVES........................................................................................................................ 2 3. TEST DETAILS.................................................................................................................... 2 4. TEST RESULTS ................................................................................................................... 5 4.1 7050-T7451 Aluminium alloy - Test Results ........................................................ 5 4.1.1 Sub-size Tension (SST) Specimens .......................................................... 5 4.1.2 Round Tension (RT) Specimens .............................................................. 9 4.2 7075-T7351 Aluminium alloy - Test results.......................................................... 9 4.2.1 Sub-size Tension (SST) Test Specimens.................................................. 9 4.2.2 Round Tension (RT) Test Specimens .................................................... 13 5. DISCUSSION .................................................................................................................... 13 6. FURTHER COMMENTS ................................................................................................. 19 7. CONCLUSIONS................................................................................................................ 19 8. ACKNOWLEDGEMENT................................................................................................. 20 9. REFERENCES .................................................................................................................... 20 APPENDIX A: TABLES ...................................................................................................... 21 DSTO-TR-2104 1. Introduction Two of the most extensively used materials in aircraft structures are 7050-T7451 and 7075-T7351 aluminium alloys. However, exposure to temperatures above the specified ageing temperature of these alloys (Table 1) has deleterious effects on their mechanical properties. The extent of any damage caused by excessive heating after heat treatment is primarily dictated by the exposure time and temperature that the affected component/area experiences. When thermal damage is suspected, assessment of affected areas might be required to assess the structural integrity or to design a repair process for the affected area. For this purpose, hardness and electrical conductivity tests have generally been used to estimate residual strength properties of aircraft structures and components affected by thermal damage [1, 2, 3]. Thermal damage assessment is achieved by measuring the relative changes in hardness and electrical conductivity of affected areas and comparing them with reference values measured at unaffected areas; these results are subsequently correlated to strength properties. However, data on thermal damage are limited to specific conditions. Consequently, a test program that covers a wide range of exposure conditions was set up to quantify the effects of thermal damage on the strength properties of these alloys. The test program used hardness and electrical conductivity testing as a means of quantifying the residual strength properties of these alloys at room temperature after thermal damage had occurred. This report is part of a series of tests conducted to quantify the effects of thermal damage on hardness and electrical conductivity, fatigue life, fracture toughness and the microstructure of these alloys. Table 1. Recommended age-hardening heat treatment for 7050-T7451 and 7075-T7351 aluminium plates (from W51 1 condition before ageing) [4] Alloy Solution Heat Treating Temperature (°C) 7050 7075 1st Step 2nd Step Temperature (°C) Time (Hrs) Temperature (°C) Time (Hrs) 471 to 482 116 to 127 3 to 6 157 to 168 24 to 30 460 to 499 * 102 to 113 6 to 8 157 to 168 24 to 30 * For plates over 101.6 mm thick, a maximum temperature of 488°C is recommended to avoid eutectic melting. W51: Solution heat-treated, this is an unstable temper and applies specifically to plate, to rolled or cold-finished rod and bar, to die or ring forgings, and to rolled rings. 1 1 DSTO-TR-2104 2. Objectives The objectives of the tests presented in this report are (i) to quantify variations in strength properties (at room temperature) resulting after thermal damage at temperatures above 205ºC; and (ii) to explore the ability of hardness and eddy current electrical conductivity tests to estimate room temperature residual strength after thermal damage. It is envisaged that calculations based on these data might be used in structural integrity calculations to manage affected areas of service components. These data can also be linked to fatigue life [5, 6 ] in the same way that hardness is linked to strength properties. 3. Test Details Testing for determination of yield (Fty) and ultimate tensile (Ftu) strengths were performed on round tension (RT) (12.5 mm diameter) and sub-size tension (SST) (6 mm square section) test specimens (Figure 1) to ASTM B 557M – 94, Standard Test Methods of Tension Testing Wrought and Cast Aluminium – and Magnesium – Alloy Products [7]. Testing was conducted using an Instron 50 KN tensile test machine. Machining of the specimens to final dimensions was performed after thermal damage. All testing was conducted at room temperature in a laboratory controlled environment. The round tension specimens were introduced to explore the possibility of variations in the test results caused by a larger-cross section compared to that of the sub-size tension specimens. Figure 1. Schematic of (Top) round tension and (bottom) sub-size tension test specimens. Drawings not to scale, all dimensions in millimetres 2 DSTO-TR-2104 The specimens, cut in the longitudinal direction, were manufactured from rolled aluminium alloy plate 7050-T7451 (127 mm thick) to AMS 4050 and from 7075-T7351 (50.8 mm thick) to QQ-A-250/12. Table 2 presents the mechanical properties and Table 3 the chemical composition of the plates as specified in the respective certificates of conformity. Table 2. Mechanical properties of aluminium alloy plates used to manufacture the tension test specimens. Results are as specified in the respective certificate of conformity Property 7050-T7451 7075-T7351 Ftu, MPa 530.8 – 533* 489.5 – 496* Yield, MPa 474 – 478* 418.5 – 424* Hardness, HRB N/A N/A % Elongation 10.00* Electrical conductivity, 41.3 – 41.64 %IACS * Properties in the longitudinal direction. 6* 40.7 – 40.9 Table 3. Aluminium alloy composition in weight percentage Element Silicon Chromium Copper Iron Magnesium Manganese Bismuth Titanium Zinc Zirconium Others, each Others, Total Aluminium 7050 7075 Certificate of conformity AMS 4050H Certificate of conformity QQ-A-250/12F <0.1 2.2 0.08 2.0 0.01 0.03 0.03 6.4 0.11 0.05 0.15 Remainder 0.12 max 0.04 max 2.0-2.6 0.15 max 1.9-2.6 0.10 max --0.06 max 5.7-6.7 0.08-0.15 0.05 max 0.15 Remainder 0.08 --1.6 0.31 2.5 0.03 --0.02 5.6 ------Remainder 0.40 max 0.18-0.28 1.2-2.0 0.50 max 2.1-2.9 0.30 max --0.20 max 5.1-6.1 --0.05 max 0.15 max Remainder Because hardness and electrical conductivity properties are the basis of thermal damage assessment, it was necessary to assess whether significant variations in these properties existed within each plate. To test this, Rockwell hardness test2 B scale (HRB) and eddy current electrical conductivity 3 tests through the thickness of the aluminium alloy plates cross section were performed. The test results revealed that minimum hardness and maximum electrical conductivity values were measured at the core of the plates (Table 4). In contrast, the opposite was true for the surface of the plates. Variations of these properties, from surface to the core of Performed using a Wilson Rockwell Hardness Tester Series 500 machine. Performed using a SIGMATEST D 2.068 eddy current electrical conductivity test unit (Software Version 3.0). 2 3 3 DSTO-TR-2104 the plates, were attributed to mechanical work and to the solidification process and heat treatment, which produced a significantly larger grain size and less optimum distribution of secondary phases in the core material. Table 4. DSTO test results. Minimum hardness and maximum electrical conductivity values were measured at the core of the plates. Test Hardness, HRB Electrical conductivity, %IACS 7050-T7451 82.7 - 89.43 39.9 – 40.8 7075-T7351 84.1 – 88.67 40.0 – 40.95 The test matrix showing the number of 7050-T7451 and 7075-T7351 aluminium alloy specimens tested is presented in Table 5. A fluidised bed furnace was used to induce thermal damage in the specimens. In addition, to allow for through thickness homogeneous temperature, the exposure time started four minutes after the specimens were loaded into the furnace. Steady air-cooling was used to cool down the specimens to room temperature. Table 5. Test matrix showing the number of specimens and the exposure conditions Exp Temp, °C 205 (450°F) 232 (450°F) 260 (500°F) 315 (599°F) 350 (662°F) Total 4 7050 7075 Exp Time (minutes) Round Tension Sub-size Tension Round Tension Sub-size Tension --- 3 2 3 3 10 30 60 300 10 30 60 300 10 30 60 300 10 30 60 300 10 30 60 300 3 3 3 3 2 3 3 3 26 --3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 59 3 3 3 3 3 3 2 3 3 29 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 51 DSTO-TR-2104 4. Test Results 4.1 7050-T7451 Aluminium alloy - Test Results 4.1.1 Sub-size Tension (SST) Specimens The test results (Table 6 Appendix A) showed that as the exposure temperature increases above 205°C, the yield and ultimate tensile strengths rapidly decrease. The higher the exposure temperature and exposure time the greater the reduction in strength properties. However, following the initial decrease, an increase in strength was measured after 60 minutes exposure at 315°C. Beyond this exposure condition, the strength properties begin to increase slightly; suggesting that the alloy is partially recovering its strength. For example, the room temperature ultimate tensile strength measured after 300 minutes exposure at 350°C (denoted as ’A’ in Figure 2) was slightly higher than that measured in specimens exposed at 232°C for 300 minutes (denoted as ‘B’ in Figure 2). In comparison, the yield strength was lower than that measured after 232°C for 300 minutes (denoted as ‘A’ in Figure 3), but still higher than that measured after exposure at 260°C (denoted as ‘B’ in Figure 3). It is interesting to note that different exposure conditions resulted in an equivalent degree of deterioration. The exposure condition where a partial recovery in properties is observed has also been called the ‘inversion point’ [1]. 7050-T7451 Aluminium Alloy SST Specimens Ultimate Tensile Strength (Ftu), MPa 500 o 400 (A) 350 C, 369.63 MPa o (B) 232 C, 352.94 MPa 300 o 205 C PC 200 o o 232 C o 315 C 260 o 350 C 100 0 50 100 150 200 Exposure time, minutes 250 300 Figure 2. Ultimate tensile strength at room temperature after thermal damage as noted. Exponential curve fits are applied to these data. 5 DSTO-TR-2104 7050-T7451 Aluminium Alloy SST Specimens 500 o PC 205 C o o 232 C 260 C Yield Strength (Fty), MPa o o 315 C 350 C 400 300 o (A) 232 C, 243.93 MPa o 350 C, 199.63 MPa 200 o (B) 260 C, 185.79 MPa 100 0 50 100 150 200 250 300 Exposure time, minutes Figure 3. Yield strength at room temperature after thermal damage as noted. Exponential curve fits are applied to these data. The recovery in strength beyond the inversion point is also manifested, as expected, in an increase in hardness. For example in Figure 4, the data show that hardness at the room temperature after 300 minutes exposure at 350°C (denoted as ‘A’) is higher than that measured after 60 minutes at 315°C (denoted as ‘B’). 100 7050-T7451 Aluminum Alloy SST Specimens 90 PC o 232 C o 315 C Hardness, HRB 80 o 205 C o 260 C o 350 C 70 0 (A) 350 C (58.65 HRB) 60 50 40 0 (B) 315 C (28.2 HRB) 30 20 0 50 100 150 200 250 300 Exposure time, minutes Figure 4. Hardness number at room temperature after thermal damage at indicated conditions. Exponential curve fits are applied to these data. 6 DSTO-TR-2104 The inversion point of this alloy is better visualised when electrical conductivity is plotted against hardness number (Figure 5). The partial recovery of properties creates a loop in the value measured and as a consequence, beyond the inversion point the same electrical conductivity could correspond to two different hardness numbers (e.g. points ‘A’ and ‘B’ in Figure 5). Similarly, a comparable hardness number could correspond to two different electrical conductivity vales (e.g. points ‘A’ and ‘C’ in Figure 5). 100 7050-T7451 Aluminum Alloy SST Specimens PC (B) (41.5 %IACS, 84.43 HRB) Hardness Number, HRB 80 (A) (41.5 %IACS, 58.65 HRB) (C) (45.5 %IACS, 58.6 HRB) 60 40 20 o 205 C o 260 C o 232 C o 315 C o 350 C 0 39 40 41 42 43 44 Electrical Conductivity, %IACS 45 46 47 Figure 5. Electrical conductivity and hardness number at room temperature after thermal damage at the indicated conditions. The arrow indicates increasing temperature and exposure time. C is an estimated datum. The loop in properties (and the ambiguous results) is also observed when strength properties are plotted against electrical conductivity (Figure 6) and hardness number (Figure 7). In this case, the same electrical conductivity could correspond to two significantly different strength levels. For example in Figure 6, an electrical conductivity of 41.50 %IACS (denote as ‘A’) could correspond to an ultimate tensile strength of 371 MPa or 501 MPa (denoted as ‘B’). In the case of hardness number versus strength properties, the data shows that hardness and strength properties rapidly decrease with increasing exposure temperature (Figure 7). It also shows a small recovery in properties once the inversion point has been passed. For example, the strength measured at room temperature after exposure at 315°C for 10 minutes (denoted as ‘A‘ in Figure 7) was lower than that measured after exposure at 350°C for 30 minutes (denoted as ‘B‘ in Figure 7). However, ambiguous results beyond the inversion point were not as significant as in the case of the electrical conductivity. Equivalent thermal exposure condition, beyond the inversion point, that resulted in comparable hardness number showed similar strength levels. The good correlation between hardness and strength levels, even beyond the inversion point allows fitting of exponential curves to test data. 7 DSTO-TR-2104 600 7050-T7451 Aluminum Alloy SST Specimens PC 80 (B) 501.6 MPa 60 400 300 (A) 371.3 MPa 40 200 o o 205 C 232 C o 41.5 %IACS Ultimate Tensile Strength, ksi Ultimate Tensile Strength, MPa 500 o 260 C 315 C o 350 C 20 100 40 41 42 43 44 45 46 Electrical Conductivity, %IACS Figure 6. Strength properties at room temperature after thermal damage at the indicated conditions. The arrow indicates increasing temperature and exposure time. 200 160 140 Hardness Number, HV 120 100 90 80 70 600 PC 7050-T7451 Aluminum Alloy SST Specimens 80 Colour Code: 500 o o 205 C 232 C o o 260 C 315 C o 60 400 Strength, ksi Strength, MPa 350 C Ftu Fty 300 40 (A) 10 minutes, 21.65 HRB, 145.47 Mpa 200 20 (B) 300 minutes, 58.65 HRB, 199.63 Mpa 100 100 80 60 40 20 0 Hardness Number, HRB Figure 7. Strength properties at room temperature after thermal damage at indicated conditions. The direction of the arrows indicates increasing temperature and time. 8 DSTO-TR-2104 4.1.2 Round Tension (RT) Specimens The test results for the round tension specimens are presented in Figure 8 and Table 7 Appendix A. The results for these specimens were similar to those of the sub-size tension specimens. The main difference was that the strength of the round tension specimens (in the pristine condition and after thermal damage) showed lower hardness and strength than those measured for the sub-size tension specimens in similar condition. An explanation for these differences is that the round tension specimens were cut from areas near to or at the core of the plate (The core of the plate shows the lowest strength and hardness [8]). A limited number of round tension specimens were tested; hence it was not possible to reach the conditions where the inversion point is observed. 200 160 140 Hardness Number, HV 120 100 90 80 70 600 7050-T7451 Aluminum Alloy RT Specimens PC 80 Colour Code: 500 o 205 C o 260 C o 232 C o 315 C 350 C 60 400 Ftu Fty 300 Strength, ksi o 40 200 20 100 100 80 60 40 20 0 Hardness Number, HRB Figure 8. Strength properties at room temperature after thermal damage at indicated conditions. Exponential curves fit have been applied to these data. PC= Pristine condition. 4.2 7075-T7351 Aluminium alloy - Test results 4.2.1 Sub-size Tension (SST) Test Specimens The test results for the sub-size tension test specimens are presented in Table 8 Appendix A. The results showed that changes in ultimate tensile (Figure 9) and yield (Figure 10) strengths and hardness (Figure 11) caused by thermal damage are quantitatively and qualitatively similar to those of the 7050-T7451 aluminium alloy. Consequently, the residual strength properties of the alloy at room temperature after thermal damage can also be expressed as a function of hardness number by exponential equations. 9 DSTO-TR-2104 600 7075-T7351 Aluminium Alloy SST Specimens Ultimate tensile Strength, MPa 500 400 300 200 o o 205 C o 260 C o 350 C 100 232 C o 315 C PC 0 0 50 100 150 200 Exposure time, minutes 250 300 Figure 9. Ultimate tensile strength at room temperature after thermal damage at indicated conditions 600 7075-T7351 Aluminium Alloy SST Specimens Yield Strength, MPa 500 o o 205 C o 260 C o 350 C 400 232 C o 315 C PC 300 200 100 0 0 50 100 150 200 Exposure time, minutes 250 300 Figure 10. Yield strength at room temperature after thermal damage at indicated conditions 10 DSTO-TR-2104 100 7075-T7351 Aluminium Alloy SST Specimens 90 o 205 C o 260 C o 350 C Hardness Number, HRB 80 o 232 C o 315 C PC 70 60 50 40 30 20 0 50 100 150 200 Exposure time, minutes 250 300 Figure 11. Hardness test results at room temperature after thermal damage at indicated conditions Figure 12 shows the inversion point (circled area) and the ambiguity in the results measured for electrical conductivity and ultimate tensile strength beyond the inversion point (similar trend is observed in the yield strength, see Table 8 for results). Figure 13 presents the hardness number versus strength properties with exponential curves fitted to these data. These data show a sharp decrease in strength properties and hardness with increasing temperature, e.g. points ‘A’ and ‘B’ in Figure 13. It also shows a small recovery in properties (after the initial drop) once the inversion point has been passed. For example, the ultimate tensile strength measured at room temperature after exposure at315°C for 30 minutes (denoted as ‘B’ in Figure 13) was lower than that measured after exposure at 350°C for 30 minutes (denoted as ‘C’ in Figure 13). 11 DSTO-TR-2104 600 7075 Aluminum Alloy SST Specimens 80 PC o o 205 C o o 260 C 315 C o 350 C 60 400 300 40 Ultimate Tensile Strength, ksi 500 Ultimate Tensile Strength, MPa 232 C 200 20 100 38 39 40 41 42 43 44 45 Electrical Conductivity, %IACS Figure 12. Ultimate tensile strength properties at room temperature after thermal damage at indicated conditions. The arrow indicates increasing temperature and exposure time. 200 Hardness Number (HV) 100 90 150 80 70 600 7075-T7451Aluminum Alloy SST Specimens PC 80 Colour Code: o (A) 232 C, 30 minutes 500 o 205 C 77.2HRB, 449.57 MPa o 260 C o 232 C o 315 C o 60 (C) 350 oC, 30 minutes: 400 41.08HRB, 318.48 MPa Strength, ksi Strength, MPa 350 C Ftu Fty 300 40 (B) 315 oC, 30 minutes 200 30.08 HRB, 281.64 MPa 20 100 100 80 60 40 20 0 Hardness Number (HRB) Figure 13. Tension test results at room temperature after thermal damage at indicted conditions. Exponential curves have been fitted to these data. The direction of the arrows indicates increasing temperature and time. 12 DSTO-TR-2104 4.2.2 Round Tension (RT) Test Specimens The test results for the round tension test specimens are shown in Table 9 Appendix A and Figure 14. The hardness and strength properties test results for the round tension test specimens were higher than those measured for the sub-size tension specimens in similar condition. The differences could be attributed to the fact that the round tension test specimens were taken from or near to the surface of the plate used in the manufacturing of the specimens. The hardness and strength properties of the plate are higher near the surface than those found in the core of the plate [8]; consequently, the round tension test specimens exhibited higher initial properties. Hardness Number (HV) 200 150 100 90 80 70 600 PC 7075-T7351 Aluminum Alloy RT Specimens o 205 C 500 o 260 C 80 o 232 C o 315 C o 60 Ftu Fty 400 Strength, ksi Strength, MPa 350 C 300 40 200 20 100 100 80 60 40 20 0 Hardness Number (HRB) Figure 14. Room temperature strength properties after thermal damage at indicated conditions. Exponential curves have been fitted to these data. 5. Discussion The test results indicate that both aluminium alloys have qualitatively and quantitatively comparable responses to thermal damage, and that the room temperature residual strength properties after thermal damage can be expressed as a function of hardness number by exponential equations. The test data clearly shows that exposure above 205°C results in rapid deterioration of strength properties. These changes are accompanied by measurable decrease in hardness and an increase in electrical conductivity values that are, regardless of the exposure conditions, indicative of the strength level of these alloys. The data also show that different combinations 13 DSTO-TR-2104 of exposure time and exposure temperature (i.e. equivalent exposure conditions) can result in similar strength levels. The good strength-to-weight ratio exhibited by these alloys is owed 4 to the presence of semicoherent η′ phase (and non coherent η phase). The amount, size and distribution of these phases determine the strength properties and provide the alloys with characteristic hardness and electrical conductivity values. However, thermal damage induces further phase transformations, which changes the balance of these precipitates to negatively affect the strength properties, which in turn affects the hardness and electrical conductivity values. Nonetheless, the resulting hardness and electrical conductivity values are still characteristic of the strength level of the alloys. Hence, hardness and electrical conductivity tests can be used to estimate residual strength properties at room temperature after thermal damage. The current test data show that increasing the temperature at which thermal damage was applied resulted in faster and more significant deterioration of strength properties. This was expected as the phase transformations (i.e. dissolution of η’ and formation of η phase) resulting from thermal damage occur through a process of atomic diffusion (atom movement), which is dependent on temperature. Therefore, diffusivity of the atoms will be faster at higher temperatures (Equation 1). That is, higher exposure temperatures result in faster and more significant deterioration of strength properties. The diffusion rate is given by the following equation: Equation 1 D = D0 e ⎛ E ⎞ −⎜ ⎟ ⎝ kT ⎠ Where D is the diffusion rate, D0 is a constant (particular to each material); E is the activation energy for atomic movement at the conditions considered (it is not temperature or concentration dependent), k is the gas constant and T is temperature. Furthermore, the test results show that for longer exposure times the rate of deterioration of strength properties slowed down as the phase transformations that drive the changes are completed and the alloys approach a state of equilibrium at the exposure conditions. A simplistic way to explain this behaviour is to consider only the main phase transformation (i.e. dissolution of semi-coherent η’ -MgZn2- to form the non-coherent η -MgZn2- phases). According to the first-order reaction rate (Equation 2), the reaction rate of the main phase transformation will be proportional to the concentration of reactants (i.e. η’ and η) multiply by a rate constant. Thus, as the main phase transformation progresses and the reactions at the exposure condition are completed (η’ decreases and η increases) changes to the strength properties will slow down in time as the alloys move towards a state of equilibrium (e.g. annealed condition). The First-order reaction rate equation is given by: 4 Other factors such as chemical composition and method of manufacturing also influence the mechanical properties. 14 DSTO-TR-2104 Equation 2 − d [c ] = k1 × c dt Where c is the concentration of reactant (i.e. η’), k is the rate constant of reaction and t is time. Equation 2 could also be written like: Equation 3 [c] = [c]0 × e − kt Equation 3 means that the concentration of c (i.e. η’) decreases exponentially as a function of time. Therefore, according to Equation 1 and Equation 2, thermal damage is temperature and time dependent and it should follow an exponential law. The test results indicate that the time required to induce a given degree of deterioration in the strength properties is inversely proportional to the exposure temperature. Previous work conducted [2, 3] on thermal damage assessment shows that significant deterioration of hardness and strength properties takes place within the first five minutes of thermal exposure. However, in the current study an inversion point is observed after exposure at 315°C for more than 60 minutes (A similar phenomenon was observed in the specimens tested at 350°C). Above this exposure condition, the strength and hardness of the alloys increased (after the initial drop), whilst at the same time the electrical conductivity decreased. This phenomenon is attributed to a process of re-tempering [1] or re-ageing [9] where solute elements (i.e. zinc and magnesium) that have returned to solid solution (due to an increased solubility of solute element in the matrix resulting from exposure to elevated temperatures) do not completely diffuse out of the matrix during rapid cooling. As a consequence, the solute atoms that remain in solid solution produce the re-ageing or retempering effect. Hence, the increase in hardness and strength and the decrease in electrical conductivity observed beyond the inversion point. It is expected however that this trend of increasing strength will eventually revert as other factors such as grain growth and coarsening of precipitates evolve. Further reduction in strength properties will occur if formation of eutectoid structures or incipient melting at grain boundaries takes place during thermal exposure. In addition, it was observed that beyond the inversion point two different electrical conductivity values could show similar hardness number and vice versa; this translated in ambiguous strength values. That is two different strength levels could correspond to a single electrical conductivity value; however, unlike the electrical conductivity, the difference between two strength levels showing a similar hardness number was very small. Nonetheless, regardless of the exposure conditions, there is only one combination of electrical conductivity and hardness number that are characteristic of a given strength level. Therefore, both electrical conductivity and hardness tests should be used in conjunction to determine the strength of the alloys. An interesting observation, which will require further analysis, is that the test results for the ultimate tensile strength for exposures at 350°C were located above the curve fit applied to the 15 DSTO-TR-2104 Ftu data; whereas the yield strength values were below that predicted by the curve fit applied to the Fty data. To facilitate further analysis of the data, the test results were converted to a percentage of the pristine strength properties at room temperature. Subsequently, exponential curves (Equations 4 to 7) were fitted using Igor Pro 5.04B software. In addition, prediction bands representing the region within which the results from the curve fit were expected to fall (plus random errors) have been included; they represent a 95 % confidence level. The following equations present the exponential curve fit that can be used to estimate the percentage of initial strength at room temperature after thermal damage. 7050-T7451 Aluminium alloy (SST specimens): Equation 4 Ultimate tensile Strength, Ftu = 36.5 + 9.1× e ( 0.022×HRB ) Equation 5 Yield strength, Fty = 20.2 + 4.9 × e ( 0.032×HRB ) 7075-T7351 Aluminium alloy SST specimens: Equation 6 Ultimate tensile Strength, Ftu = 37.0 + 11.0 × e ( 0.021×HRB ) Equation 7 Yield strength, Fty = 14.2 + 8.7 × e ( 0.027×HRB ) The data clearly show that both 7050-T7451 (Figure 15) and 7075-T7351 (Figure 16) aluminium alloys have qualitatively and quantitatively similar responses to thermal damage. Per cent of initial room temperature Strength 180 110 160 Hardness Number, HV 120 100 90 140 100 80 72 7050-T7451 Aluminium Alloy SST Specimens Ftu Fty 90 80 70 60 50 40 30 20 90 80 70 60 50 Hardness Number, HRB 40 30 20 Figure 15. Residual strength properties at room temperature after thermal damage in percent of initial values 16 DSTO-TR-2104 180 110 160 Hardness Number (HV) 120 100 140 90 80 7075-T7351 Aluminum Alloy SST Specimens Per cent of initial room temperature Strength 100 Ftu Fty 90 80 70 60 50 40 30 20 90 80 70 60 50 40 30 20 Hardness Number (HRB) Figure 16. Residual strength properties at room temperature after thermal damage in percent of initial values Regarding the results for the round tension and sub-size tension specimens, the differences in the results were attributed to variations in properties within the plates (e.g. specimens that were taken close to or from the core of the plate presented lower strength, lower hardness and higher electrical conductivity). However, the most important observation regarding the differences in the test results is that both sets of results showed similar (and almost identical) rates of strength deterioration. For example in the case of 7050-T7451 aluminium alloy, curve fits applied to the round tension and sub-size tension test specimens were almost the same despite the initial higher hardness (and strength) of the sub-size tension specimens (Figure 17). Similar results were observed for 7075-T7351 aluminium alloy in the temperature range tested (Figure 18). These findings suggest that the rate of deterioration due to thermal damage is almost independent of the initial condition for these two alloy tempers. 17 DSTO-TR-2104 180 160 140 120 Hardness Number (HV) 100 90 80 72 110 Per cent of inital room temperature Tensile Strenght 7050-T7451 Aluminum Alloy Tension Specimens 100 SSTspecimen Ftu SSTspecimen Fty 90 RT specimen Ftu RT specimen Fty 80 70 60 50 40 30 20 80 60 Hardness Number (HRB) 40 20 Figure 17. Comparison of residual strength properties of sub-size tension (SST) and round tension (RT) test specimen at room temperature after thermal damage. Markers have been added for better visualisation. Hardness Number (HV) 180 160 140 120 100 90 80 110 7075-T7351 Aluminum Alloy Tension Specimens Per cent of initial room temperature Strength 100 90 SST specimen Ftu RT specimen Ftu 80 70 60 50 SST specimen Fty RT specimen Fty 40 30 20 80 60 Hardness (HRB) 40 20 Figure 18. Comparison of residual strength properties of sub-size tension (SST) and round tension (RT) test specimen at room temperature after thermal damage. Markers have been added for better visualisation. 18 DSTO-TR-2104 6. Further Comments The data on the effects of thermal damage on the strength properties of 7050-T7451 and 7075T7351 aluminium alloys presented in this report assume uniform thermal exposure of an affected area, which in most instances of thermal damage of structures and components is not the case. Therefore, predictions based on these data might be conservative. However, a conservative approach is necessary when thermal damage assessment is performed as in most instances the exposure conditions of the affected areas are unknown. Furthermore, partial recovery of properties within a thermally damaged area should not be interpreted as a partial recovery of all properties; instead, it should be considered as an indication of possible severe thermal damage. The difficulty in attempting an estimation of residual strength beyond the inversion point is that other factors such as grain growth, precipitation of particles at grain boundaries, formation of eutectic structures and ultimately incipient melting at grain boundaries (if present) cannot be accounted for by hardness or electrical conductivity tests alone. Consequently, any prediction based on these tests might produce results that overestimate the strength of affected areas. In addition to the obvious concerns regarding the effects of thermal damage on the strength of these alloys, other factors such as creep rupture and creep properties as well as corrosion resistance of these alloys might also be affected (these aspects are not part of the DSTO test program). Fatigue life and fracture toughness are also affected. 7. Conclusions Based on the tests conducted on thermally damaged specimens made from of 7050-T7451 and 7075-T7351 aluminium alloys, it is concluded that: 1. Both alloys showed qualitatively and quantitatively similar response to thermal damage. 2. Regardless of the thermal exposure conditions, the level of deterioration in the strength properties caused by thermal damage is characterised by a unique combination of hardness number and electrical conductivity values that can be used to estimate the remaining strength level. 3. The residual strength of these alloys at room temperature after thermal damage can be expressed as a function of hardness number by exponential equations. 4. There was an increase in strength, measured at room temperature, after the initial drop was recorded for both materials after exposure at 315°C for more than 60 minutes. This point marks the beginning of a partial recovery of strength. A similar phenomenon was observed in specimens tested at 350°C. It is however expected that this trend will revert, as other factors that affect the strength of the alloy evolve (e.g. precipitation of particles at grain boundaries). 5. Different combinations of exposure temperature and time (i.e. equivalent exposure conditions) can result in similar strength levels. 19 DSTO-TR-2104 6. The time required for changes in strength properties is inversely proportional to the temperature. 8. Acknowledgement The authors would like to acknowledge the technical support and contribution of DSTO staff and in particular to Nicholas Athiniotis, Simon Barter, Charles Brady, Greg Cunningham, Noel Goldsmith, Bruce Grigson, David Holmes, Robert Pell, Kevin Phibbs and Michael Ryan. Without their support and collaboration this work could not have come to fruition. 9. References 1. Hagemaier, D, ‘Evaluation of Heat Damage to Aluminium Aircraft Structures’. Materials Evaluation, Vol. 40, No. 9, p. 962-969, Aug. 1982. 2. Holmes, D, ‘Assessing properties of heat damaged aluminium 7075-T73’. Aeronautical Engineering Support Facility, Australia, 1996. Directorate General of Technical Airworthiness, Royal Australian Air Force. 3. Clark, B, ‘Overaging of alloys used in airframe construction resulting from accidental exposure to heat’. University of Ballarat, Nov. 1997. 4. Department of Defence. Military Specification MIL-H6088G (1991), ‘Heat Treatment of Aluminium Alloys’, Department of Defence United States of America. 5. Calero, J. (2006), ‘Study of the Effects of Thermal Damage on the Fatigue Life of AA7050T7451 Aluminium Alloy’. International Conference on Structural Integrity and Failure (SIF2006). Melbourne, Australia. 6. Calero, J. (2007), ‘Effects of Thermal Damage on the Mechanical Properties of 7050-T7451 Aluminium Alloy’. International Committee on Aeronautical Fatigue (ICAF 2007), 24th ICAF Symposium. Naples, Italy. 7. ASTM B 557M – 94, ‘Standard Test Methods of Tension Testing Wrought and Cast Aluminium – and Magnesium – Alloy Products’. 8. Barter, S. Air Vehicles Division, Defence Science and Technology Organisation Melbourne, Australia, not published. 9. Wu X. J., Koul A. K., Zhao L, ‘A New Approach to Heat Damage Evaluation for 7XXX Aluminium Alloy’, Canadian Aeronautics and Space Journal, volume 42, No. 2, 1996, pp 93-101. 20 DSTO-TR-2104 Appendix A: Tables Table 6. Test results for 7050-T7451 aluminium alloy sub-size tension (SST) test specimens Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% --- 40.50 89.4 89.0 89.8 536 485 17.20 --- 40.80 87.7 87.6 87.9 519 464 13.72 205 30 41.55 84.6 84.1 84.9 510 429 18.8 205 30 41.50 84.4 83.6 85.2 494 425 17.1 205 30 41.50 83.7 83.4 83.9 497 421 14.9 205 60 40.90 84.4 83.9 84.9 486 427 16.13 205 60 40.90 83.2 82.9 83.6 493 429 13.89 205 60 41.43 81.6 80.8 82.5 483 412 17.73 205 300 44.10 69.0 68.4 69.5 415 316 17.4 205 300 44.60 68.7 67.6 70.1 412 313 16.5 205 300 44.50 66.7 66.0 67.1 402 308 17.8 232 10 41.10 84.7 84.0 85.3 532 456 13.4 232 10 41.50 80.9 80.2 81.7 502 420 14.5 232 10 42.70 75.1 73.5 75.7 458 362 14.7 232 30 40.20 84.9 84.8 85.0 506 436 19.10 232 30 42.70 75.7 74.9 76.2 441 353 17.10 232 30 42.70 72.8 71.9 73.3 421 327 18.68 232 60 43.10 73.6 73.2 73.9 431 337 19.63 232 60 43.10 72.9 72.3 73.4 420 327 16.51 232 60 43.60 70.4 70.0 70.8 409 311 18.87 232 300 45.50 56.5 55.8 56.9 353 244 19.63 232 300 45.50 56.1 55.6 56.5 349 239 19.51 232 300 45.55 55.4 54.2 55.9 348 240 17.20 260 10 43.20 71.8 70.4 72.9 431 329 19.1 260 10 43.50 70.2 69.2 71.3 407 305 17.8 260 10 43.50 68.8 68.1 69.4 406 304 17.8 260 30 44.10 56.6 55.9 57.0 363 261 17.27 260 30 44.30 55.8 55.4 56.2 357 255 15.78 260 30 44.60 54.8 54.6 55.0 354 256 17.38 260 60 45.20 55.6 54.6 56.6 346 229 19.4 260 60 44.60 53.1 51.7 53.9 346 225 18.9 Exp Temp (ºC) Pristine Condition (PC) - Room temp Pristine Condition (PC) - Room temp (Continued) 21 DSTO-TR-2104 Table 6. Test results for 7050-T7451 aluminium alloy SST test specimens (Continued) Exp Temp (ºC) Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% 260 300 45.50 39.1 38.2 39.7 296 179 19.20 260 300 45.60 38.9 37.9 39.9 300 186 19.91 260 300 45.70 37.3 36.7 37.7 297 182 18.90 315 10 45.40 36.6 36.1 36.8 290 174 20.19 315 10 45.60 36.6 36.2 37.0 289 173 19.69 315 10 44.53 35.5 34.5 36.1 289 167 18.09 315 30 44.50 32.4 31.8 33.1 286 160 18.38 315 30 44.45 31.7 31.0 32.5 287 161 20.77 315 315 315 30 60 60 45.20 44.60 45.40 31.0 28.2 23.4 30.8 27.7 22.6 31.5 28.7 24.3 279 290 271 158 159 150 19.80 18.32 19.82 315 60 45.50 21.9 20.3 24.3 264 148 17.99 315 300 43.63 40.1 39.2 40.6 334 179 16.52 315 300 43.63 38.2 37.2 38.7 321 174 315 300 45.00 21.7 21.2 21.8 274 145 18.57 350 10 43.10 45.2 44.4 45.9 351 196 13.06 350 10 43.70 40.3 38.9 41.6 330 179 14.58 350 10 45.00 24.5 23.9 25.1 274 148 19.53 350 30 42.70 51.9 51.4 52.1 359 190 17.32 350 30 42.90 49.8 49.5 50.4 341 177 18.76 350 30 44.70 31.8 31.2 32.5 288 145 22.93 350 60 43.85 37.6 35.0 40.1 306 157 17.8 350 60 44.75 36.1 35.5 36.7 298 173 19.5 350 300 41.50 58.7 58.1 59.1 371 200 20.77 350 300 41.20 58.1 57.1 59.2 381 210 19.73 350 300 41.70 56.6 56.1 57.0 370 199 14.30 Table 7. 14.47 Test results for 7050-T7451 aluminium alloy round tension (RT) test specimens Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% --- 39.9 84.4 82.8 86.8 489 460 13 --- 40.3 83.0 82.2 83.4 491 418 13 --- 40.0 82.7 82.2 83.0 483 413 13 205 10 40.1 83.6 82.9 84.1 484 412 14 205 10 39.8 83.1 82.2 84.1 478 403 13 205 10 40.1 82.4 81.6 83.0 487 415 13 205 60 39.9 80.8 79.3 81.6 478 402 14 Exp Temp (ºC) Pristine Condition (PC) - Room temp Pristine Condition (PC) - Room temp Pristine Condition (PC) - Room temp (Continued) 22 DSTO-TR-2104 Table 7. Test results for 7050-T7451 aluminium alloy RT test specimens. (Continued) Exp Temp (ºC) Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% 205 60 40.1 80.7 80.5 81.0 468 387 14 205 60 40.3 78.6 78.2 79.1 458 373 15 232 10 40.1 82.4 82.0 82.8 484 411 15 232 10 39.9 82.3 81.8 83.0 486 414 15 232 10 39.7 79.2 78.5 79.5 471 392 15 232 60 41.6 69.0 68.9 69.0 398 298 17 232 60 42.0 65.0 64.5 65.3 380 276 15 232 60 41.9 64.8 64.1 65.8 382 279 17 260 10 42.1 66.1 65.9 66.4 388 286 17 260 10 42.0 65.9 65.6 66.1 383 280 17 260 60 42.8 51.8 51.0 52.4 324 209 19 260 60 43.0 50.3 49.6 50.9 323 208 13 260 60 42.9 49.1 48.8 49.4 322 206 13 315 60 45.1 27.5 25.6 29.7 266 142 12 315 60 45.6 26.7 26.5 26.8 259 140 12 315 60 42.6 26.6 25.1 28.0 265 133 13 350 30 41.3 34.8 34.0 35.4 290 152 13 350 30 41.5 33.7 32.5 35.0 298 148 14 350 30 41.8 29.0 28.8 29.3 288 141 14.0 Table 8. Test results for 7075-T7351 aluminium alloy sub-size tension (SST) test specimens Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% --- 40.0 84.9 84.7 85.3 499 424 16 --- 40.0 84.7 83.7 85.8 497 422 15 --- 40.2 84.1 83.5 84.6 496 418 15 205 30 39.7 81.9 81.3 82.6 482 397 17.2 205 30 39.7 81.5 81.2 81.8 481 390 17.0 205 60 39.9 81.7 81.3 82.1 481 403 17.32 205 60 39.9 80.2 79.8 80.4 468 385 16.35 205 60 40.7 78.2 77.8 78.4 452 366 15.89 205 300 42.7 68.9 68.4 69.7 405 293 16.7 Exp Temp (ºC) Pristine Condition (PC) - Room temp Pristine Condition (PC) - Room temp Pristine Condition (PC) - Room temp (Continued) 23 DSTO-TR-2104 Table 8. Test results for 7075-T7351 aluminium alloy SST test specimens (Continued). Exp Temp (ºC) Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% 205 300 42.7 68.6 67.9 69.2 408 295 16.4 205 300 42.7 68.4 67.7 69.3 403 291 18.5 232 10 40.7 77.1 76.4 77.5 453 350 17.2 232 10 40.7 75.9 75.4 76.3 451 347 15.0 232 30 40.4 80.3 79.2 80.9 472 387 16.27 232 30 40.4 79.2 78.0 80.1 463 380 15.99 232 30 40.7 77.2 76.8 77.5 450 357 16.60 232 60 40.6 77.3 75.7 78.4 445 350 13.13 232 60 40.9 76.7 75.4 77.8 443 347 16.71 232 60 41.1 74.6 73.9 75.3 431 330 16.69 232 300 43.2 52.5 52.3 52.6 336 221 17.37 232 300 43.2 51.9 50.7 52.6 335 220 16.75 232 300 43.2 51.6 51.1 52.2 335 220 17.31 260 10 41.5 68.1 67.6 69.2 404 288 16.8 260 10 41.5 68.0 67.7 68.4 403 287 17.0 260 10 41.5 62.4 61.7 62.9 384 262 16.4 260 30 42.2 54.0 53.6 54.5 346 229 17.39 260 30 42.2 54.0 53.2 54.4 343 225 17.52 260 30 42.6 53.1 52.4 53.6 343 227 17.25 260 60 43.1 51.0 50.5 51.2 337 210 17.0 260 60 43.0 48.9 48.4 49.2 336 207 17.2 260 60 43.0 48.6 47.3 50.1 331 206 17.0 315 10 42.3 33.1 32.7 33.5 292 157 19.68 315 10 42.4 32.5 31.7 33.3 286 157 19.13 315 10 42.4 30.9 30.4 31.4 238 151 19.47 315 30 42.1 32.5 31.5 33.9 291 153 20.10 315 30 42.5 30.1 29.5 30.5 282 148 20.15 315 30 42.7 30.0 29.5 30.6 283 149 20.56 315 60 41.8 37.6 37.1 38.2 310 158 19.28 315 60 41.8 35.1 28.1 37.9 309 157 21.44 315 60 42.5 29.8 29.1 30.3 283 145 21.39 350 10 40.9 44.9 44.2 46.3 331 169 19.98 350 10 40.8 44.3 43.9 44.8 330 169 20.27 (Continued) 24 DSTO-TR-2104 Table 8. Test results for 7075-T7351 aluminium alloy SST test specimens (Continued) Exp Temp (ºC) Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% 350 10 41.1 43.6 43.2 43.9 331 170 20.39 350 30 41.3 41.7 40.9 42.6 321 162 19.37 350 30 41.3 41.1 40.6 41.6 318 161 20.23 350 30 41.6 36.3 35.8 36.8 305 154 20.76 350 60 41.2 43.2 42.1 44.1 334 168 19.7 350 60 41.1 37.9 37.8 38.1 312 152 19.8 Table 9. Test results for 7075-T7351 aluminium alloy RT tension test specimens Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% --- 40.3 88.7 88.5 88.9 525 480 15.9 --- 40.9 86.7 86.3 87.0 513 466 12.5 --- 41.0 86.3 86.0 86.9 518 465 13.5 205 10 40.2 88.4 88.0 89.2 520 476 15.7 205 10 40.1 87.8 87.3 88.3 520 477 14.9 205 10 40.0 86.9 86.4 87.4 513 465 15.7 205 60 41.7 80.9 80.7 81.2 470 400 15.2 205 60 41.3 80.6 80.5 80.8 482 416 11.2 205 60 42.5 76.3 75.8 76.6 457 389 12.7 232 10 40.0 87.1 86.3 87.5 516 470 15.6 232 10 40.8 85.7 85.0 86.2 516 460 12.8 232 10 40.9 82.5 82.5 82.6 492 430 12.3 232 60 42.2 77.8 77.5 78.4 454 377 13.2 232 60 42.9 74.1 73.9 74.2 432 348 14.0 232 60 43.2 72.2 71.8 72.7 417 330 260 10 43.2 74.5 74.2 74.8 423 336 16.7 260 10 41.3 70.3 69.8 71.0 411 313 14.5 260 10 43.8 69.4 68.2 70.3 408 324 14.0 260 60 45.0 56.8 56.5 56.9 336 228 16.3 260 60 45.1 56.5 56.0 57.2 338 230 16.7 260 60 45.3 51.6 51.3 52.1 333 237 15.1 315 10 42.8 31.9 30.7 32.6 278 152 16.2 Exp Temp (ºC) Pristine Condition (PC) - Room temp Pristine Condition (PC) - Room temp Pristine Condition (PC) - Room temp (Continued). 25 DSTO-TR-2104 Table 9. Test results for 7075-T7351 aluminium alloy RT tension test specimens. (Continued) Exp Temp (ºC) Exp Time (minutes) %ICAS Hardness (HRB) HRB MIN HRB MAX Ftu (MPa) Fty (MPa) Elongation, 2% 315 10 42.9 31.5 30.3 33.3 277 151 16.0 315 60 44.9 28.8 28.2 29.4 269 145 15.1 315 60 45.1 28.7 28.1 29.5 265 144 16.9 315 60 44.7 28.3 27.3 29.8 273 147 15.7 350 30 43.5 41.2 40.8 41.5 321 162 18.8 350 30 43.6 41.1 40.4 42.3 334 173 15.2 350 30 43.3 41.0 39.9 41.8 322 163 20.3 26 Page classification: UNCLASSIFIED DEFENCE SCIENCE AND TECHNOLOGY ORGANISATION DOCUMENT CONTROL DATA 2. TITLE 1. PRIVACY MARKING/CAVEAT (OF DOCUMENT) 3. SECURITY CLASSIFICATION (FOR UNCLASSIFIED REPORTS THAT ARE LIMITED RELEASE USE (L) NEXT TO DOCUMENT CLASSIFICATION) Effects of Thermal Damage on the Strength Properties of 7050-T7451 and 7075-T7351 Aluminium Alloys Document Title Abstract (U) (U) (U) 4. AUTHOR(S) 5. CORPORATE AUTHOR Jaime Calero and Suzana Turk DSTO Defence Science and Technology Organisation 506 Lorimer St Fishermans Bend Victoria 3207 Australia 6a. DSTO NUMBER 6b. AR NUMBER 6c. TYPE OF REPORT 7. DOCUMENT DATE DSTO-TN-2104 AR-014-106 Technical Report February 2008 8. FILE NUMBER 9. TASK NUMBER 10. TASK PONSOR 11. NO. OF PAGES 12. NO. OF REFERENCES 2006/1056002 AIR 06/022 DGTA 26 9 13. URL on the World Wide Web 14. RELEASE AUTHORITY http://www.dsto.defence.gov.au/corporate/reports/DSTO-TR2104.pdf Chief, Air Vehicles Division 15. SECONDARY RELEASE STATEMENT OF THIS DOCUMENT Approved for public release OVERSEAS ENQUIRIES OUTSIDE STATED LIMITATIONS SHOULD BE REFERRED THROUGH DOCUMENT EXCHANGE, PO BOX 1500, EDINBURGH, SA 5111 16. DELIBERATE ANNOUNCEMENT No Limitations 17. CITATION IN OTHER DOCUMENTS 18. DSTO Yes Research Library Thesaurus Thermal damage, 7050 aluminium alloy, 7075 aluminium alloy, hardness, electrical conductivity, strength 19. ABSTRACT This report presents experimental test data that quantify the effects of thermal damage on the strength properties of 7050-T7451 and 7075-T7351 aluminium alloys. The test results indicate that there is a direct relationship between hardness and strength properties that can be used to determine residual strength of these alloys at room temperature after thermal damage. This relationship can be expressed as a function of hardness number by the use of exponential equations. Page classification: UNCLASSIFIED