Novel Silicon Stripixel Detectors on High Resistivity p-type Magnetic Czochralski Silicon Wafers for USATLAS Upgrade Zheng Li, D. Lissauer, D. Lynn, P. O’Connor, and V. Radeka Abstract—a new Si detector system based on a number of novel aspects of detector structure and detector material is proposed here for the US ATLAS Upgrade Project. The novel aspects in this Si detector system include: 1) a novel Si stripixel detector structure developed at BNL will be used, which provides 2d position sensitivity with single-sided process; 2) high resistivity magnetic Czochralski (MCZ) Si wafer will be used, which provides naturally high concentration of oxygen for improved radiation hardness to charged particles; and 3) p-type MCZ substrates are used, for which single-sided process is retained and fast electron collection is presented, and which experiences no space charge sign inversion to ensure partial depletion mode operation at extremely high radiation fluences. In the first detector design layout, strip pitches in both y and u directions have been fixed at 80 µm, with a stereo angle of 4.6° between them. The strip length is 3 cm and the detector chip size is 2.56 cm×6.0 cm, with 2 halves of 2.56 cm×3.0 cm sensitive areas without dead space between them. Both y and u strips will be read out by the sides perpendicular to the strips. Simulations on detector processing as well as the electric properties before and after radiation by charged particles up to 1.0×1016 neq (1 MeV neutron equivalent)/cm2 have been done. Simulation results show that up to 2.0×1015 neq/cm2 of charged particle irradiation, the highest fluence for the inter-medium region for strip detector in the SLHC, the new detector with a thickness of 200 µm can still be fully depleted at a bias of 400 volts. I. INTRODUCTION Recently, a novel detector structure based on interleaved pixel electrodes arranged in a projective x-y readout has been developed at BNL [1-2]. With this novel detector structure, named as “stripixel”, a 2d-position sensitive detector can be Manuscript received on October 18, 2004. This research was supported by the U.S. Department of Energy: contract No: DE-AC02-98ch10886 Zheng Li is with Brookhaven National laboratory, Upton, NY 11973-5000, USA (telephone: 631-344-7604, e-mail: zheng@bnl.gov). D. Lissauer is with Brookhaven National laboratory, Upton, NY 11973-5000, USA (telephone: 631-344-4864, e-mail: lissauer@bnl.gov). D. Lynn is with Brookhaven National laboratory, Upton, NY 11973-5000, USA (telephone: 631-344-4560, e-mail: lynn@rcf.rhic.bnl.gov). P O’Connor is with Brookhaven National laboratory, Upton, NY 11973-5000, USA (telephone: 631-344-7577, e-mail: Oconnor2@bnl.gov). V. Radeka is with Brookhaven National laboratory, Upton, NY 11973-5000, USA (telephone: 631-344-4266, e-mail: Radeka1@bnl.gov). made with single-sided process using double-metal technology. Two prototypes of stripixel detectors had been fabricated at BNL for the PHENIX Upgrade at RHIC [3-5]. Laser, electron source and beam tests on these prototype detectors have shown 2d-position sensitivity with resolutions of 25 µm in both x and u directions (both are 80 µm in pitch, and a stereo angle of 4.6°) [4]. For applications in SLHC, where the luminosity will be increased by a factor of 10, the stripixel detector may be a good candidate in the inter-medium strip detector region. Since in this region in the SLHC, the detector strip length may be limited to a few cm’s in length due to occupancy requirement. This is an excellent fit for the stripixel detectors since short strip length will compensated the increase in strip capacitance due to the interleaving scheme in stripixel structure [2]. The simplicities in processing, assembly, and readout in the stripixel detector can result in significant reductions in costs in material, processing and readout scheme. Another key issue for the SLHC with increased luminosity is the radiation hardness of the detectors. The highest charged particle fluence in the inter-medium region for strip detectors is about 2.0×1015 neq (1 MeV neutron equivalent)/cm2. One of the main research approaches to improve Si sensor radiation hardness is to oxygenate Si by introducing oxygen into Si during the detector processing [610]. With its natural high oxygen concentration (over 1018 /cm3), high resistivity (≥ 1 kΩ⋅cm) Magnetic Czochralski (MCZ) Si detectors are a candidate for more improved radiation hardness [11-12]. In this work, a new detector system using the novel stripixel structure with p-type MCZ Si substrate is proposed for the US ATLAS Upgrade for SLHC. With p-type substrate, the single-sided process advantage in stripixel processing is preserved (as compared to n on n, which is two-sided process). In addition, electrons will be collected with fast rate, no space charge sign inversion will take place at any radiation level, and detectors can work in partial depletion mode after extremely high fluence radiation. Moreover, recent date on oxygenated p-type strip detectors have shown improved charge collection efficiency, by a factor of more than 2, over its n-type counterpart [13]. Detector design, detector chip and bonding layout, as well as simulations in detector processing and electric properties before and after irradiation will be given. II. DETECTOR DESIGN AND CHIP LAYOUT 0-7803-8701-5/04/$20.00 (C) 2004 IEEE As shown in Fig. 1, the basic stripixel concept is to divide an ordinary pixel into two parts: the x (or u)-pixel and y-pixel and read x and y pixels by x and y strips in a projective way. In order to ensure a signal in both x and y pixel when a particle passing through the detector, the two parts within a pixel should be interleaved in such a way that the maximum distance between them any where should be smaller than the full width at half maximum (FWHF) for diffusion cloud during the drifting of the induced charge [2]. For the single cell design for US ATLAS Upgrade, the pixel pitches are 620 µm in x and 50 µm in y. The y-strip pitch and u-strip pitch are both 50 µm. The stereo angle between u and y strips is 4.6°. The line widths for both x and y-pixels are 5 µm, with a gap of 3.33 µm between them. The maximum distance between x and y pixels is thus 8.33 µm, less than FWHM = 9 µm for the diffusion cloud [2]. The detector is to be made on p-type MCZ Si with resistivity of about 3 kΩ-cm. Fig. 2 shows the schematics of detector processing and processing parameters. A uniform field (or spray) p+ implant will be made on the front side to provide channel separation between the n+ pixels to be implanted later. With this field implant, only five mask steps are needed for the detector processing of this new detector system. u (or Y)-strips X-strips u (or Y)-strip Stereo angle X-strip X-pixel pitch Y-pixel pitch Fig. 1 Schematics of the stripixel Si detector system for US ATLAS Upgrade 2 µm 3000 Å 4500 Å 1000 Å 2000 Å half are separated, there is no guard ring between them; therefore there is no dead space. There are 512 u strips and 512 X strips in each half. Both u and X strips are read out from the side using the same double metal process technology already existed in the stripixel processing (no 3rd metal needed). The readout lines are grouped in 128 strip bunches, with 48 µm bonding pitch with stacked bonding pads of 80 µm× 300 µm in size. III. n+ implant: 1014/cm2 p+ implant: 1012/cm2 Fig. 2 Schematics a parameters for the processing for the stripixel Si detector system for US ATLAS Upgrade Fig. 3 shows the schematic of the wafer layout. On a 4”diameter wafer, there are two detector chips with the size of 2.56cm x 6.0cm each. Each detector chip consists of two halves, each with a size of 2.56cm x 3.0cm. Strips (both X and u) in two halves are not connected, which results in a strip length of about 3.0 cm for both X and u strips in each half. However, the gap between the two halves is the same as that between X strips (and that between u strips) at 3.33 µm. Shown in Fig. 4 is the left half of a detector chip with chip size of 2.56 cm × 3.0 cm. The right half of the chip is a mirror image of the left along the mirror line indicated in the figure. Although the strips in the left half and those in the right DETECTOR SIMULATIONS Simulations before irradiation and after irradiation by charged particles up to 1.0×1016 neq/cm2 have been performed on novel stripixel Si detectors made on p-type high resistivity MCZ wafers. The introduction rate of radiation-induced negative space charges is obtained from ref. [12]. Fig. 4 shows the detector electrical properties after being irradiated charged particles to 2.0×1015 neq/cm2, the highest fluence for the strip detectors in the inter-medium region in SLHC. It is clear that, even after such high fluence of irradiation by charged particles, the detector can still be fully depleted at a modest bias voltage of 400 volts. Further simulations have shown that, for higher fluences than 2.0×1015 neq/cm2, the detector may be deleted at higher bias voltages (<1000 volts). However, micro breakdown along the surface may occur before such biases being reached. In this case, the detector can be operated at partial depletion mode with lower biases (400 volts<V<1000 volts) with significant fraction of sensitive volume. However, 0-7803-8701-5/04/$20.00 (C) 2004 IEEE at fluences close to 1.0×1016 neq/cm2, the trapping effect will dominate, and is the limiting factor for detector charge collection efficiency (CCE), and other approaches may be needed in addition to the approach proposed here. 3cm (48 × 620µm) u (Y)-strips 2.56 cm (512 × 50µm) Chip #1 Chip #2 X-strips 3.33 µm No dead space 100 mm dia. Fig. 3 Detector wafer layout for the stripixel Si detector system for US ATLAS Upgrade. The gap between left and right halves on a detector chip is only 3.33 m to eliminate dead space (shown bigger in the figure for better viewing) IV. DETECTOR DESIGN There are five mask steps in the double metal processing for the prototype stripixel detectors for US ATLAS Upgrade. Shown in Fig. 6 is the mask design layout of one detector chip (half wafer). Both u and Y strips are routed to the top and bottom sides for wire bonding. 16 readout chips with 128 channels each will be used to read out all u and Y strips. As shown in Fig. 7, the bonding pads are 48 µm in pitch and stacked in two rows to get the maximum pad width of 70 µm. The length of the bonding pads is 300 µm. Fig. 8 shows the contact vias for both u and X strips between the 1st Al layer and the 2nd Al layer. The insulation layer used between the 2 Al layers will be polyimide with a thickness of about 2 µm. Note here that the width of the via is only about 5 m, extremely small taking into account the polyimide thickness. Therefore, extreme caution and special care should be taken during the processing: if the etching time of polyimide is too short, then the via may not be open all the way to the 1st Al, and there will be no contact made to the strips; if the etching time is too long, then the size of the via may be too large, resulting in the shorting of u and X strips. In our experience, the difference between the short time and the long time is not much, and we do not have too much margin of error to play with. Shown in Fig. 9 is the detailed connection scheme between the Y pixels in the formation of u-strips. While X pixels in the same row are connected by the 1st Al layer to form the X strip, the Y pixel in one row is connected to the Y pixel in the row above it and the next column on the right. In this way, a stereo angle of 4.6º is formed between X and u strips. The connection between the two adjacent Y pixels is made by a connector made by the 2nd Al through the via on each Y pixel. The connection line is made with minimum length (about 10µm in current design) to minimized unwanted additional capacitance. V. DETECTOR PROCESSING PLAN By the end of July 2004, the design of the full mask set has been completed. The mask set was ordered, and it was delivered in the beginning of September, 2004. The 0-7803-8701-5/04/$20.00 (C) 2004 IEEE preparation for the fabrication of the first batch of the prototype stripixel detectors for US ATLAS Upgrade is now underway, which includes the oxidation of MCZ Si wafers and the generation of a detector processing receipt. The actual processing will begin in the beginning of November 2004, with a delivery date of detectors set for the end of January 2005. Electrical tests, including current-voltage and capacitance-voltage measurements on test structures and stripixel detectors will be carried on soon after. Charge collection tests on the first batch prototype Si stripixel detectors for US ATLAS Upgrade will be made using a laser (transient current technique) and by an electron source, before and after proton radiation. Test results will be published elsewhere. Improvement will be made on the design of the second prototype batch base on the test results, and the processing of the second prototype will probably start in the Summer of 2005. Quarter wafer Side bonding pads ---- zero dead space between two chips X-bonding pads u-strips X-strips u-bonding pads Fig. 4 Detector chip and readout layout for the stripixel Si detector system for US ATLAS Upgrade US ATLAS Upgrade Electric simulation on the Novel n on p and n on n 2d-sensitive Si Stripixel detectors on MCZ wafers For US-ATLAS Upgrade After 2x1015 neq/cm2 radiation X-strip 1st Al Pixel #2 400 volts Hole concentration Pixel #3 620 µm Potential profile 400 volts Fully depleted at 400 volts 50 µm Electric field Pixel #1 Pixel #4 Y-strip 2n Al Fig. 5 Detector electrical simulations after irradiation for the stripixel Si detector system for US ATLAS Upgrade 0-7803-8701-5/04/$20.00 (C) 2004 IEEE Detector Chip (half wafer) Connections between the Y pixels for the formation of u-strips US ATLAS Stripixel Detector: 2 halves of 48×512 array of 620 µm×50 µm pixels Interleaving pitch: 8.33 µm, 5 µm line width 512 u and 512 X strips/half with 50 µm pitch and 4.6 stereo angle Detector size: 6.37 cm×2.98 cm Sensitive area: 5.97 cm×2.58cm X Pixel Y Pixels u connectors X strip contacts Left half Right half Fig. 6 ACAD mask design layout of one detector chip for the stripixel Si detector system for US ATLAS Upgrade Fig. 9 Connection scheme between adjacent Y pixels for the formation of u strips. V. REFERENCES 70 µm [1] [2] 300 µm 7 µm 130 µm Z. Li, BNL Internal Report, BNL #67527, June 10, 2000 Z. Li, “Novel Silicon Stripixel Detector: Concept, Simulation, Design, and fabrication”, BNL 71393-2003JA, Nucl. Instr. & Meth. A 518, Vol. 3, (2004) pp738-753. [3] Z. Li et al., “Novel Silicon Stripixel Detector for PHENIX Upgrade”, presented on 9th Pisa Meeting on Advance Detectors, May 25-31, 2003, La Biodola, Isola d’Elba, Italy, Nucl. Instr. & Meth. A 518 (2004) 300304. [4]. J. Tojo et al., “Development of a Novel Silicon Stripixel Detector for RHIC-PHENIX Detector Upgrade”, presented on IEEE Nucl. Sci. Symp., October 19-25, 2003, Portland, Oregon, to be published in IEEE Trans. Nucl. Sci. [5] Z. Li et al., “Development of 2nd prototype of Novel Silicon Stripixel Detector for PHENIX Upgrade”, presented on 10th Vienna Conference on instrumentation, Feb. 16-21, 2004, Vienna, Austria, accepted by Nucl. Instr. & Meth. A. 270 µm [6] 48 µm Fig. 7 Design layout of the bonding side bonding pads for the stripixel Si detector system for US ATLAS Upgrade [7] Contact vias for strips between 1st and 2nd Al layers u strip contacts [8] [9] Z. Li, H. W. Kraner, E. Verbitskaya, V. Eremin, A. Ivanov, M. Rattaggi, P. G. Rancoita, F. A. Rubinelli, S. J. Fonash, C. Dale, and P. Marshall, “Investigation of the Oxygen-Vacancy (A-Center) Defect Complex Profile in Neutron Irradiated High Resistivity Silicon Junction Particle Detectors”, IEEE Trans. Nucl. Sci., Vol. 39, No. 6, (1992) pp 1730-1738. A. Ruzin and CERN Rd48 Collaboration, “Recent results from the RD48 (ROSE) Collaboration” Nucl. Instrum. & Meth. A447, (2000) pp116-125 RD48 Status Report, CERN/LHCC 2000-009, December 1999. G. Lindstroem, and CERN RD48 Collaboration, “Radiation hard silicon detectors––developments by the RD48 (ROSE) collaboration”, Nucl. Instrum. & Meth. A466, (2001) pp308-326. [10] G. Lindström, “Radiation Damage in Siliocon Detectors”, Nucl. Instrum. & Meth. A512 (2003) pp30-43. [11] J. Harkonen et al., on MCZ. [12] Z. Li et al, “Radiation Hardness of High Resistivity Magnetic Czochralski Silicon Detectors after Gamma, Neutron and Proton Radiations”, IEEE Trans. Nucl. Sci. Vol. 51, No. 4, August (2004) pp1901-1908. X strip contacts Fig. 8 Contact vias and routing of X and u strips [13] G. Casse et al., “Performances of miniature microstrip detectors made on oxygen enriched p-type substrates after very high proton irradiation”, presented at the Vienna Conference of Instrumentation, 2004, submitted to NIM A. 0-7803-8701-5/04/$20.00 (C) 2004 IEEE