UNIVERSITY of CALIFORNIA Santa Barbara Understanding material and process limits for high breakdown voltage AlGaN/GaN HEMTs A dissertation submitted in partial satisfaction of the requirements for the degree of Doctor of Philosophy in Electrical and Computer Engineering by Yuvaraj Dora Committee in charge: Professor Umesh K. Mishra, Chair Professor Robert A. York Professor James S. Speck Dr. Sten Heikman Dr. Sriram Chandrasekaran March 2006 The dissertation of Yuvaraj Dora is approved: Chair March 2006 Understanding material and process limits for high breakdown voltage AlGaN/GaN HEMTs Copyright 2006 by Yuvaraj Dora iii Curriculum Vitæ Yuvaraj Dora EDUCATION Bachelor of Technology in Electrical Engineering, Indian Institute of Technology, Chennai, India, March 2001. Bachelor’s thesis work,“Simulation of Resonant Tunneling Diodes by solving Poisson and Schrodinger equations iteratively using Airy functions” done under the guidance of Prof. Amitava DasGupta. Doctor of Philosophy in Electrical and Computer Engineering, University of California, Santa Barbara, March 2006 (expected). Doctoral thesis work,“Understanding material and process limits for high breakdown voltage AlGaN/GaN HEMTs” done under the guidance of Prof. Umesh K. Mishra. PUBLICATIONS Y.Dora, A. Chakraborty, L. McCarthy, S. Keller, S. P. Denbaars, U. K. Mishra, “High breakdown voltage achieved in AlGaN/GaN HEMTs with trench gates”. submitted to IEEE Electron Device Letters. Y.Dora, A. Chakraborty, S. Heikman, L. McCarthy, S. Keller, S. P. Denbaars, U. K. Mishra, “The effect of ohmic contacts on buffer leakage in GaN transistors”.submitted to IEEE Electron Device Letters. Y. Dora, S. Han, D. Klenov, P. J. Hansen, K. Noc, U. K. Mishra, S. Stemmer, J. S. Speck, “ZrO2 gate dielectrics Produced by Ultraviolet Ozone Oxidation for GaN and AlGaN/GaN Transistors”, J. Vac. Sci. Technol. B, 24, pp 575, 2006. Y. Dora, C. Suh, A. Chakraborty, S. Heikman, S. Chandrasekaran, V. Mehrotra, U. K. Mishra, “Switching Characteristics of High Breakdown Voltage AlGaN/GaN HEMTs”. Device Research Conference Digest, 2005, DRC 2005, iv 63rd , vol.1, pp 191-192, June 20-22, 2005 Huili Xing, Y. Dora, A. Chini, S. Heikman, S. Keller, U. K. Mishra, “High breakdown voltage AlGaN-GaN HEMTs achieved by multiple field plates,” IEEE Electron Device Letters, vol 25, no 4, pp 161-163, April 2004. v Abstract Understanding material and process limits for high breakdown voltage AlGaN/GaN HEMTs by Yuvaraj Dora The breakdown voltage in AlGaN/GaN HEMTs is known to be triggered by the gate leakage caused by the electric field crowding at the drain-side edge of the gate. The effect of gate leakage on breakdown is mitigated by relieving the peak electric field at the drain-side edge of the gate and by decreasing the tunnelling probability with the use of gate dielectrics. Multiple field-plates were used to split the single electric field peak into several smaller peaks without compromising the frequency response too much. As predicted by the device simulations, this increased the breakdown voltage of the fabricated devices to 900 V with two field-plates. A technique yielding an integrated field-plate self-aligned with the gate (trench gate technology) was devel- vi oped, in which the SiNx passivation was deposited before the gates, followed by trenches being etched in the passivation and gate metal deposited in the trenches. The profile of the etched trench wall could be controlled to shape the electric field profile. Zirconium oxide produced by ozone oxidation shows promise as a high-k gate dielectric for GaN. Increasing the Fe-doping in the buffer was shown to reduce the buffer leakage and enhance the breakdown voltage. Furthermore, alloyed ohmic contacts were identified as a source of buffer leakage. Beyond 400 V, the parasitic breakdown of air was identified to be limiting the device breakdown voltage. Devices made with trench gate technology, when immersed in Fluoroinert liquid, had a breakdown voltage of more than a kilo-volt (up to 1900 V was measured). Switching measurements were done on the diced devices wirebonded to a compact switching test setup. A 5.5mm wide device switched 2.4 A at 150 V with a turn-off time of less than 20 ns. The measured switching speed is still limited by the gate drive speed. The on-resistance is limited by the wirebond resistance and the increase in access resistance of the device due to some amount of dispersion. This study has helped to give definitive direction in developing AlGaN/GaN HEMTs for power applications. vii Contents List of Figures xi List of Tables xiv 1 Introduction 1 1.1 Figures of Merit for the switching transistors . . . . . . . . . . . 2 1.2 Advantages of GaN material system over other materials . . . . 4 1.3 Particular advantages of AlGaN/GaN HEMTs for power switching 6 1.4 Research background of high breakdown voltage AlGaN/GaN HEMTs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 1.5 Synopsis of this dissertation . . . . . . . . . . . . . . . . . . . 8 References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 2 Increasing Breakdown in AlGaN/GaN HEMTs Plates 2.1 Introduction . . . . . . . . . . . . . . . . . 2.2 The need for Field Plates . . . . . . . . . . 2.3 Simulations . . . . . . . . . . . . . . . . . 2.4 Device Fabrication and results . . . . . . . 2.5 Discussion . . . . . . . . . . . . . . . . . . 2.6 Summary . . . . . . . . . . . . . . . . . . References . . . . . . . . . . . . . . . . . . . . . using Mutiple Field . . . . . . . 13 13 14 16 22 26 29 29 3 Gate Leakage in AlGaN/GaN HEMTs 3.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3.2 The origin of gate leakage . . . . . . . . . . . . . . . . . . . . 31 31 32 viii . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3.3 Reducing gate leakage . . . . . . . . . . . . . . . . . . . . . . 3.3.1 Reducing gate leakage by using trench gates . . . . . . 3.3.2 Literature survey of reducing gate leakage in GaN devices using dielectrics . . . . . . . . . . . . . . . . . . 3.3.3 Reducing gate leakage by using in-situ grown dielectrics 3.3.4 Reducing gate leakage by using ZrO2 dielectric . . . . . 3.4 Leakage from field-plates: . . . . . . . . . . . . . . . . . . . . 3.5 Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36 36 38 40 42 53 56 57 4 Buffer Leakage in GaN Transistors 4.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4.2 Test Structures . . . . . . . . . . . . . . . . . . . . . . . . . . 4.3 Effect of Fe-doping level on the buffer leakage . . . . . . . . . . 4.4 Effect of ohmic contacts on buffer leakage . . . . . . . . . . . . 4.4.1 Observation of differences in buffer leakage . . . . . . . 4.4.2 Interpretation of Electrical data . . . . . . . . . . . . . 4.4.3 Interpretation for Morphology . . . . . . . . . . . . . . 4.4.4 Ways to reduce the effect of ohmics on buffer leakage in HEMTs . . . . . . . . . . . . . . . . . . . . . . . . . . 4.5 Conducting SiC substrate for GaN transistors . . . . . . . . . . 4.6 Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60 60 61 63 65 65 69 71 5 Kilo-Volt breakdown voltage devices and wide periphery devices 5.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . 5.2 Trench gate process : Self-aligned field-plates . . . . . . . . . 5.2.1 Controlling the profile of the trench . . . . . . . . . . 5.2.2 Controlling the field-plate extension . . . . . . . . . . 5.2.3 The Effect of Source-side dispersion . . . . . . . . . . 5.2.4 Frequency response of the trench-gates . . . . . . . . 5.3 Kilo-Volt breakdown voltage devices . . . . . . . . . . . . . . 5.3.1 Identifying the parasitic breakdown . . . . . . . . . . 5.3.2 Kilo-Volt breakdown measurements . . . . . . . . . . 5.4 What is limiting the breakdown voltage ? . . . . . . . . . . . 80 80 81 81 83 85 89 91 92 95 96 ix . . . . . . . . . . 73 74 78 78 5.5 Wide periphery devices . . . . . . . . . . . . . . . . . . . . . . 100 5.6 Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 104 6 Switching measurements 6.1 The need for switching measurements . . . . . . . . . . . . . 6.2 Switching setup schematic and waveforms . . . . . . . . . . . 6.3 The need for compact test setup . . . . . . . . . . . . . . . . 6.4 Measurements with a compact test setup . . . . . . . . . . . . 6.5 Issues with switching measurements . . . . . . . . . . . . . . 6.5.1 Gate drive speed . . . . . . . . . . . . . . . . . . . . 6.5.2 High Von . . . . . . . . . . . . . . . . . . . . . . . . 6.5.3 Heat sinking the devices . . . . . . . . . . . . . . . . 6.5.4 Ongoing improvements with switching measurements 6.6 Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105 105 108 110 111 116 116 118 120 122 123 123 7 Conclusions and future work 125 7.1 Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . 125 7.2 Future Work . . . . . . . . . . . . . . . . . . . . . . . . . . . . 127 A ATLAS code for simulating AlGaN/GaN HEMTs 129 B SiNx deposition conditions 134 C Specifics of Processing 135 x List of Figures 1.1 1.2 Figure of merit: theoritical limits of material systems . . . . . . Epitaxy and Device schematic of AlGaN/GaN HEMT . . . . . . 2.1 2.2 2.3 2.4 2.5 2.6 2.7 2.8 2.9 2.10 2.11 2.12 Schematic of the devices . . . . . . . . . . . . . . . . . . . . Simulated Potential contours . . . . . . . . . . . . . . . . . . Electric field profiles . . . . . . . . . . . . . . . . . . . . . . E-field profiles with applied voltage . . . . . . . . . . . . . . E-field profiles with thickness of dielectric beneath field-plates E-field profiles with lateral shift of field-plates . . . . . . . . . Epitaxial structure and Fabricated Device schematic . . . . . . Pulsed-IV before and after passivation . . . . . . . . . . . . . SEM cross-section of the fabricated device . . . . . . . . . . . High breakdown voltage achieved with two field-plates . . . . Breakdown voltage with processing steps . . . . . . . . . . . Small signal frequency response after three field-plates . . . . 3.1 3.2 3.3 3.4 3.5 3.6 3.7 3.8 3.9 The dependence of Gate Leakage with Lgd and Wg . . . . . . . Leakage is not through the SiNx layer . . . . . . . . . . . . . . Gate Leakage in HEMTs grown on LEO GaN template . . . . . Gate leakage reduction using trench-gate process . . . . . . . . In-situ MOCVD dielectrics . . . . . . . . . . . . . . . . . . . . Process flow for HEMTs with ZrO2 . . . . . . . . . . . . . . . TEM characterization of ZrO2 film . . . . . . . . . . . . . . . . Gate leakage reduction using zirconium oxide underneath the gate Controlled experiment to show that the reduction is due to ZrO 2 xi . . . . . . . . . . . . 5 7 15 17 18 19 20 21 22 23 24 25 26 28 33 34 35 37 41 43 45 47 49 3.10 3.11 3.12 3.13 Problems with integrating ZrO 2 into the HEMT process flow. An Approach to integrate ZrO2 into the HEMT process flow. Leakage from fieldplate through passivation layer. . . . . . . Leakage from fieldplate through different passivation layers. 4.1 4.2 4.3 4.4 Epitaxial structure of a HEMT and MESFET . . . . . . . . . . Effect of Fe-doping level on buffer leakage . . . . . . . . . . . Buffer Leakage test structures to study the effect of ohmic contacts Optical microscope picture and AFM scan-section of the ohmic regions after stripping the alloyed metals . . . . . . . . . . . . . Morphology explains the difference in buffer leakage . . . . . . Removal of spiky ohmics translates to higher device breakdown Effect of Fe on buffers grown on n-SiC substrate . . . . . . . . Pulsed-IV amd Power measurements in HEMTs grown on n-SiC substrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Removal of spiky ohmics gave reduced buffer leakage in HEMTs on n-SiC substrate . . . . . . . . . . . . . . . . . . . . . . . . . 4.5 4.6 4.7 4.8 4.9 5.1 5.2 5.3 5.4 . . . . . . . . 50 52 54 55 62 64 66 67 68 74 75 76 77 Profile of the etched trench . . . . . . . . . . . . . . SEM picture of the trench-gate . . . . . . . . . . . . Effect of source side dispersion . . . . . . . . . . . . Explanation for IV-curves of devices with dispersion side only and source-side only. . . . . . . . . . . . . 5.5 Small signal characteristics and pulsed-IV . . . . . . 5.6 Load-pull power measurements at 4GHz . . . . . . . 5.7 Effect of etched mesa wall on breakdown . . . . . . 5.8 Breakdown voltage of 1400 V measured . . . . . . . 5.9 Dependence of Breakdown voltage with Lgd spacing 5.10 Dependence of Breakdown voltage with Lsg spacing 5.11 Picture of a flip-chip bonded device . . . . . . . . . . . . . . . 82 . . . . . . 84 . . . . . . 86 on drain. . . . . . 87 . . . . . . 90 . . . . . . 91 . . . . . . 92 . . . . . . 95 . . . . . . 96 . . . . . . 99 . . . . . . 101 6.1 6.2 6.3 6.4 . . . . Switching test setup and waveforms The need for compact test setup . . Compact switching test setup . . . . Gate transition times . . . . . . . . xii . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 107 110 111 112 6.5 6.6 6.7 6.8 6.9 6.10 Switching measurements with high speed gate drive High current turn-off characteristic . . . . . . . . . Current and Voltage waveform crossover locus . . The gate drive schematic . . . . . . . . . . . . . . Effect of source side parasitic resistance on Von . . High current switching . . . . . . . . . . . . . . . xiii . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 113 114 116 117 120 121 List of Tables 1.1 Physical properties of various semiconductors relevant to highvoltage applications . . . . . . . . . . . . . . . . . . . . . . . xiv 6 Acknowledgements I would like to thank my advisor Prof. Umesh Mishra for providing me an oppurtunity to participate in the research in his group. It is my pleasure to have worked in one of the leading groups for research in GaN devices. I also thank Prof. Mishra for providing me the financial aid during my graduate school. I would like to thank all my committee members for their guidance and feedback. I would like to thank Prof. Robert York for letting me use the microwave lab facilities. I would like to thank Prof. James Speck and Prof. Susanne Stemmer for helping me with the work on zirconium oxide gate dielectrics and helping me with the material characterization. I would like to thank Sten for guiding me on the project and growing many samples in attempts to understand the buffer leakage. I appreciate the amount of time he spent in growing samples for this project. I would like to thank Sriram and Vivek for their help in doing the switching measurements. I am grateful for the time that Sriram spent on designing a compact switching test setup and teaching me the concepts of gate drivers. This project involved intensive use of the Nanofab facilities at UCSB. I thank the efforts of the Nanofab engineers Bob, Brian, Don, Jack, Louis, Mike, Neil, xv Ning to keep the lab running smoothly. This work would not have been possible if not for the expertise and the time commitment of the people in the MOCVD lab. I would like to thank Arpan, Gia, Lee, Nick, Stacia, Sten and Prof. DenBaars for their help. The data storage and analysis would not have been possible if not for the help and guidance of Chris, Mike, Eric, Val, John, Guylene and Ken. I would like to thank all the members of Mishra-York group for their contribution to maintain the high quality of the microwave lab. I thank Ajay, Ale, Arpan, Carl, Chang-soo, Chris Sanabria, Chris Schaake, Dario, Felix, Hongtao, Huili, Ilan, Jaehoon , Lal, Lee, Likun, Manhoi, Mike, Mishra, Nadia, Nick, Pete, Siddharth, Srabanti, Stacia, Sten, Raj, Tomas, Val, Yenyun, Yipei and York for their cooperation. I thank Dmitri, Pete, and Soo-yeon for their help in characterizing the zirconia film, Hisashi and James for their help in wirebonding and Navin for his help with the SEM. I would like to thank Jim-Ping, Mark for their help with AFM and SEM. I would like to thank Prof. Evelyn Hu, Prof. Mark Sherwin, Carey and Dario from whom I learnt various experimental techniques. I would like to acknowledge the help that I received regarding paperwork from Laura, Lee Baboolal, Lynn, Mike, Val and others. Finally, I would like to thank all the friends, who made my stay here pleasant and educative . xvi Dedicated to xvii 1 Introduction D URING the past few years, enormous progress has been made in the development of Gallium Nitride (GaN) and its family of material alloys for both electronics and opto-electronics applications. For electronics applications, a number of devices take advantage of both the high critical breakdown field associated with the large bandgap of GaN as well as its high saturated electron velocities. These devices are intended to fulfill the growing demands for high power at high frequency electronic components as well as for high voltage power switches operating at higher frequencies. Improvements in AlGaN/GaN high electron mobility transistors (HEMTs) [1] and heterojunction bipolar transistors (HBTs) [2] continue to be reported, and microwave GaN HEMTs have been commercialized. This dissertation will focus on the improvements in high breakdown voltage 1 CHAPTER 1. INTRODUCTION AlGaN/GaN HEMTs with low Ron for power switching applications. The primary focus of the work was to improve the device design, to identify the parameters critical to the device breakdown and to develop the processing techniques for the fabrication of devices with high breakdown voltage. The use of multiple field-plates enabled high breakdown voltages without sacrificing the frequency response too much. Several dielectric materials were also tried to be used as gate dielectric to reduce the gate leakage in AlGaN/GaN HEMTs. The alloyed ohmic contacts were identified as an additional source of buffer leakage. High breakdown voltage measurement techniques were developed. Switching measurements were done to characterize the large signal frequecy response of the devices. As a whole, this work has also contributed to the overall understanding of AlGaN/GaN HEMTs, and a number of the techniques developed for the fabrication of high breakdown voltage HEMTs could potentially be beneficial in other areas of GaN technology. 1.1 Figures of Merit for the switching transistors The devices used for switching applications need a breakdown voltage of atleast twice the operating voltage in order to accomodate peak surges. The drain 2 CHAPTER 1. INTRODUCTION voltage to gate control voltage ratio should be very high to reduce the power consumption by the driver circuits. The on-resistance of the switch should be as low as possible to reduce the conduction losses during the on-period of the switch. Assuming that the power losses are solely due to conduction losses during the on-state, Baliga [3] derived a figure of merit (BFOM) for vertical devices Vbr2 /Ron ∼ · µ · Ec3 , applicable for low frequency operation. Here µ is the mobility and Ec is the critical electric field. The rise time and fall time should be as low as possible to reduce the switching losses. This is especially important for power switching at higher frequencies. The power converter losses at higher frequencies consist of the switching losses and the conduction losses. The conduction losses can be reduced by increasing the device area. But increasing the device area increases the capacitive charging and increases the switching losses. Hence for a given switching frequency the total loss must be minimized by choosing the optimum area of the device, Plossmin ∼ √ √ f /( µ · Ec ) leading to a high frequency figure of merit [4][5][6]. Here f is the switching frequency. For any given area of the device, the switching losses increase steadily with increased switching frequency. Still the high frequency operation is preferred be- 3 CHAPTER 1. INTRODUCTION cause the size of the passive components scale down, leading to compact packaging of power supplies. Hence it is critical for switches operating at higher frequencies to have very low turn-on and turn-off times, so that the switching losses can be kept at tolerable limits. 1.2 Advantages of GaN material system over other materials Two of the most important requirements for switching devices are a large breakdown voltage Vbr and a low on-resistance Ron . Silicon has long been the dominant semiconductor for high voltage power switching devices, most commonly making use of structures like the double-diffused metal-oxide-semiconductor (DMOS), UMOS etc, [7]. However, silicon power devices are rapidly approaching theoretical limits for performance [Figure 1.1]. There have been efforts to push beyond limits of Si by novel device structures like the SuperJunction MOSFET [8][9]. At the same time, wide bandgap materials, particularly GaN and SiC, have at- 4 2) Specific On-Resistance (ohm-cm ( CHAPTER 1. INTRODUCTION 1 10 RPI '00 Lateral RESURF MOSFETs Purdue '98 Lateral DMOSFET Navy '99 Kansai '98 Kansai '00 N-G '97 Lateral RESURF UMOSFET SIAFET UMOS MOSFETs Cree’02 4H SiC DMOS Purdue NCSU '99 '98 Siemens '00 Planar Denso '97 Cree’02 VJFET ACCUFET ACCUFET SiC BJT 0 10 -1 10 -2 10 -3 10 Si Limit SC '00 UCSB '01 GaN MOS-HFET GaN HEMT -4 10 Al.22Ga.78N-GaN HEMT Limit SiC Limit -5 10 10 2 10 3 10 4 Breakdown Voltage (V) Figure 1.1: The theoritical limits of the figure of merit for various material systems. tracted much attention because they offer a number of potential advantages over silicon. These potential advantages arise from the fundamental physical properties of the material [Table 1.1]. GaN has projected saturated electron velocities of 2.5×107 cm/s [10] and a 3.4 eV bandgap that leads to a critical breakdown field of 3.3 MV/cm, as well as stability at high temperatures. Additionally, the ability to form a high density two-dimensional electron gas (2DEG) in the GaN near the AlGaN/GaN heterointerface by polarization doping, allows for very high electron mobility µ n while maintaining a high channel charge ns . A High 5 CHAPTER 1. INTRODUCTION Property Eg [eV] ni [cm−3 ] εr µn [cm2 /V·s] vsat [107 cm/s] Ecrit [MV/cm] ΘK [W/cm·K] Si GaN AlN 4H-SiC Diamond 1.1 1.5×1010 11.8 1350 1.0 0.3 1.5 3.39 1.9×10−10 9.0 1500 2.5 3.3 1.3 6.1 ∼10-31 8.4 1100 1.8 11.7 2.5 3.26 8.2×10−9 10 700 2.0 3 4.5 5.45 1.6×10−27 5.5 1900 2.7 5.6 20 Table 1.1: Physical properties of various semiconductors relevant to highvoltage applications µn ·ns product in devices results in low on-resistances R on . Table 1.1 compares some of the fundamental physical properties of GaN to those of other major semiconductors. 1.3 Particular advantages of AlGaN/GaN HEMTs for power switching AlGaN/GaN HEMTs typically have a high electron mobility (µ=1500 cm 2 /V·s). Mobilities of µ=2000 cm 2 /V·s by using thin AlN interlayers have been realised [11]. High electron concentration can be realised in AlGaN/GaN due to polarization doping (ns =1×1013 cm−2 )[Figure 1.2]. These in turn yield a high ns .µ product which contributes to a low Ron . High Ec (> 3MV/cm) enables high breakdown 6 CHAPTER 1. INTRODUCTION 2Deg 29nm AlGaN Source Source 1.3um GaN:UID Gate Gate SiN x Drain Drain AlGaN AlGaN 0.5um GaN:Fe nucleation substrate (a) Epi GaN GaN (b) Device schematic Figure 1.2: AlGaN/GaN HEMT - a) epitaxial structure and b) device schematic. voltages to be sustained in smaller device regions thereby reducing the R on .The wide Band Gap of the GaN material system permits high temperature operation up to 400◦ C. The operating temperature is only limited by the extrinsic materials like the reliablity of the SiNx passivation layer, Schottky metal stability etc,. 1.4 Research background of high breakdown voltage AlGaN/GaN HEMTs Zhang et al. at UCSB has done the preliminary work on high breakdown voltage AlGaN/GaN HEMTs [12]. In their work the overlapping gate technology was used to increase the breakdown voltage. Their work led to the understanding that gate leakage is limiting the breakdown voltage. Their work involved using several gate dielectrics like Jet vapour Deposited (JVD) SiO 2 and combi- 7 CHAPTER 1. INTRODUCTION nations of sputtered SiNx and E-beam deposited SiOx to achieve higher breakdown voltage as well as reduced dispersion. However those devices still had frequency dispersion in their IV-curves. To achieve high breakdown voltage in AlGaN/GaN HEMTs without sacrificing the large signal frequency response was an issue that remained to be addressed. 1.5 Synopsis of this dissertation This dissertation focuses on the development of the AlGaN/GaN HEMTs for high voltage switching applications. The primary objective was the demonstration of a device with both a very large breakdown voltage and a low on-resistance without losing the large signal frequency performance. There was considerable focus on the development of the device process as well as gaining an understanding of device operation and the parameters that affect device performance. Chapter 2 presents the intial efforts directed towards reducing the peak electric field at the drain edge of the gate to achieve higher breakdown voltage without affecting the large signal frequency performance. Device simulations showed that with multiple field plates a single peak electric field can be split into several smaller electric field peaks thereby permitting a much larger voltage to be 8 CHAPTER 1. INTRODUCTION withstood by the device. A strategy for optimizing the design parameters is presented. The fabrication of the devices with field-plates and the high breakdown voltage device results are presented. In Chapter 3, the investigation of the origin of gate leakage in AlGaN/GaN HEMTs is presented. Several dielectrics were tried as gate dielectrics for AlGaN/GaN HEMTs. By the improved processing technique of ‘trench gates’ the dielectrics could be incorporated into the AlGaN/GaN HEMT process, without compromising the SiNx passivation that is used to eliminate the DC-RF dispersion. The leakage from the field plates was characterized and a two layer passivation dielectric lead to a reduction in the leakage from the field plates. In Chapter 4, a study of the buffer leakage with different Fe doping levels in the buffer for SiC substrates is presented. This study verified that the Fe doping of the buffer indeed reduces the buffer leakage. By a series of controlled experiements the alloyed ohmic contacts were identified as another source of buffer leakage. Techniques to reduce the effect of these alloyed ohmic contacts is discussed. Finally the HEMTs grown on n-SiC substrates with Fe-doped buffers showed considerable performance. Chapter 5 presents the details of the trench gate process technology. Field 9 CHAPTER 1. INTRODUCTION plates self-aligned with the gate were fabricated. Various parasitic weak points which could prevent the device from reaching a kilo-volt breakdown were investigated. As recognized by researchers in the power devices field, arcing through air was of concern and AlGaN/GaN devices made with the trench gate technology, when tested immersed in the liquid Fluoroinert, withstood more than a kilo-volt. Wide-periphery devices were implemented with the flip-chip process having a current capacity of 10 A. Finally, in Chapter 6, the role of switching measurements in the large signal frequency characterization of the large breakdown voltage device is presented. The switching measurements were done with the help of Dr. Sriram Chandrasekaran and Dr. Vivek Mehrotra at Rockwell Scientific, Thousand Oaks. The need for compact switching setup is shown. A compact switching test setup designed and built there showed a gate drive speed of less than 50ns. A large current of 2.4 A was switched at Vdc =150 V in a turn-off time of less than 20 ns. Various issues with the switching measurements were identified and investigated. 10 CHAPTER 1. INTRODUCTION References [1] Robert Coffie. Characterizing and Suppressing DC-to-RF Dispersion in AlGaN/GaN High Electron Mobility Transistors. PhD thesis, University of California, Santa Barbara, 2003. [2] H. Xing, L. McCarthy, S. Keller, S. P. DenBaars, and U. K. Mishra. High current gain GaN bipolar junction transistors with regrown emitters. Proceedings of the IEEE Twenty-Seventh International Symposium on Compound Semiconductors, pages 365–9, 2000. [3] B. J. Baliga,“Semiconductors for high-voltage, vertical channel field-effect transistors,”. Journal of Applied Physics, Volume 53, Issue 3, pp. 1759-1764, Mar 1982. [4] B. J. Baliga,“Power semiconductor device figure of merit for high-frequency applications,”. Electron Device Letters, IEEE , vol.10, no.10, pp.455-457, Oct 1989. [5] A. Q. Huang,“New unipolar switching power device figures of merit,” Electron Device Letters, IEEE, vol.25, no.5, pp. 298- 301, May 2004. [6] Yifeng Wu, CREE-Santa Barbara Technology Center, Personal communication. [7] B. J. Baliga,“Trends in power semiconductor devices,”. Electron Devices, IEEE Transactions on , vol.43, no.10, pp.1717-1731, Oct 1996. [8] T. Fujihira,“Theory of Semiconductor Superjunction Devices”.Japanese Journal of Applied Physics,Vol. 36 Part1 (1997) , No. 10, pp.6254-6262. [9] W. Saito, I. Omura, S. Aida, S. Koduki, M. Izumisawa, H. Yoshioka, T. Ogura, “Over 1000V semi-superjunction MOSFET with ultra-low onresistance below the Si-limit”. Power Semiconductor Devices and ICs, 2005. Proceedings. ISPSD ’05. The 17th International Symposium on , pp. 27- 30, 23-26 May 2005. [10] O. Ambacher. Growth and applications of group III-nitrides. Journal of Physics D, 31(20):2653–710, 1998. 11 CHAPTER 1. INTRODUCTION [11] Likun Shen , “Advanced Polarization-Based Design of AlGaN/GaN HEMTs”. PhD thesis, University of California, Santa Barbara, 2004. [12] Naiqian Zhang , “High Voltage GaN HEMTs with Low on-resistance for Switching Applications”. PhD thesis, University of California, Santa Barbara, 2002. 12 2 Increasing Breakdown in AlGaN/GaN HEMTs using Mutiple Field Plates 2.1 Introduction G aN has emerged as a promising material for the high speed, high power device applications. The large bandgap and the high electron velocity make it suitable for high power microwave applications [1]. Factors that limit GaN transistor performance are primarily dispersion and gate leakage. Electric field lines which concentrate at the drain-side edge of the gate cause charge injection into the surface traps. This reduces the field concentration at the drainside edge of the gate, but leads to high-frequency current dispersion because the surface traps respond slowly to gate bias. Dispersion is eliminated by an effective surface passivation which leads to electric fields concentrating at the 13 CHAPTER 2. MUTIPLE FIELD PLATES drain-side edge of the gate [2]. Hence low dispersion and high field concentration and hence high gate leakage are linked. Engineering low gate leakage while maintaining low dispersion is critical and conveniently achieved by the field-plate technology. 2.2 The need for Field Plates It is known that when the device is at pinch-off the maximum electric field occurs at the drain side edge of the gate [2][3]. Before passivation the surface states adjacent to the gate fill up with elecrons thereby extending the depletion region width. This reduces the peak electric field that is seen at the edge of the gate thus enhancing the breakdown voltage [Figure 2.1]. However there is dcto-rf dispersion in the IV curves as the surface states do not respond fast to the changes in gate bias. The high frequency dispersion is eliminated by passivating the surface with SiNx film. After passivation the electric field lines peak at the drain side edge of the gate thereby reducing the breakdown voltage. To break this trade-off between speed and breakdown voltage, it would be appropriate if the peak electric field is spread out not by the slow responding 14 CHAPTER 2. MUTIPLE FIELD PLATES No Field-Plate Before Passivation Source Gate Gate Drain Source Gate Gate AlGaN AlGaN GaN GaN SiNx Drain SiNx Drain Two Field-Plates One Field-Plate FP2 FP1 Source Gate Gate FP1 SiNx Drain Source Gate Gate AlGaN AlGaN GaN GaN Figure 2.1: Various device schematics surface states but by some external means so that the electric field can be tailored in a controlled fashion without compromising the speed too much. Such an advantage is given by a field-plate [4]. A field-plate is a metal electrode which offers an additional edge for the electrical field lines to terminate at higher drain bias [Figure 2.1]. This leads to the reduction in the peak electric field at the gate edge. Since the field-plate is a metal electrode the response time is much faster than that of the surface states. The field-plate can be electrically connected either to the source or to the gate. The field-plates electrically connected to the source 15 CHAPTER 2. MUTIPLE FIELD PLATES have an advantage over that of those connected to the gate. The charging and discharging of the field-plate to drain capacitance can be faster if it is connected to the source. The advantage with gate connected field-plates is that it enables to make them self-aligned to the gate and it allows a better control in tailoring the electric field as presented in Chapter 5. By using multiple (n) field plates each with increasing lateral extension from the gate and increasing vertical distance from the AlGaN surface the single electric field peak at the gate edge can be split into (n+1) smaller peaks for the same applied drain bias. This enables a much higher drain bias to be supported without exceeding the critical electrical field at which breakdown happens. 2.3 Simulations Qualitative simulations were done using Silvaco ATLAS device simulation software to study the electric field profiles. These simulations confirm that the potential contours [Figure 2.2] and the electric field profile can be engineered by changing the lateral shift and the vertical height of the field-plates. The code of the program used is shown in Appendix-A. 16 CHAPTER 2. MUTIPLE FIELD PLATES 0 50. Distance y (um) 0.8 Potential 0.6 Contours 40. -6. 0.4 s1 0.2 0 70. s2 t2 t1 AlGaN GaN -10. -0.2 0 0.5 60. 80. 10. 90. 20. 30. 1 1.5 2 Distance x (um) 2.5 3 Figure 2.2: The simulated potential contours of a device with two field-plates and applied drain bias of 100 V. Figure 2.3 shows the simulation of the E-field strength at a lateral cross section in the AlGaN region of the device in the off-state. The first curve shows the electric field strength of a device with only the gate for an applied drain bias of 100 V. The second curve with two peaks shows that for the same maximum electric field permitted in the system, a higher drain bias of 240 V can be supported with one field-plate. This is possible because of the increase in the depletion region width leading to an increase in the area under the E-field vs. distance curve. With two field-plates, for the same maximum electric field that can be permitted 17 CHAPTER 2. MUTIPLE FIELD PLATES Sectional view of Electric Field Normal gate With first fieldplate With second fieldplate 6M 5M E-field (V/cm) 4M 3M 2M 400V 1M 100V 240V 0 0 1 2 3 4 5 6 Distance (um) Figure 2.3: For the same peak electric field values, the voltage that can be supported by the devices with field-plates is larger due to the increasing area under the E-field vs. distance curve (t1,t2=120nm). in the system, a much higher drain bias of 400 V can be supported. The lateral shift of the field-plates and vertical thickness of the dielectric beneath them can be optimized to obtain E-field peaks of equal magnitude, each smaller than the critical field, to maximize the permissible drain bias of the device. This section shows a strategy for optimizing the parameter space of the field- 18 CHAPTER 2. MUTIPLE FIELD PLATES E-field vs. applied voltage (Vds) t1, t2 = 120 nm s1, s2 = 0.4 um 20v t2 t1 50v 100v s2 s1 Figure 2.4: The simulated electric field profiles of a device with two field-plates shows that the electric field terminating on the field-plates increases with increasing drain bias. plates. The first point to observe is that the E-field lines terminating at the fieldplates increase in magnitude with increasing drain bias [Figure 2.4]. So the optimization of the parameter space should be aimed for the maximum drain bias seen by the device during the peak surges and not for the nominal operating voltage. Also the electric field stress on the schottky gate can be relieved by the field-plates at higher drain biases. Another point to note is that with smaller thickness of the dielectric which supports the field-plates (t1,t2 as defined in 19 CHAPTER 2. MUTIPLE FIELD PLATES E-field vs. SiNx thickness (t1, t2) t1, t2 = 60, 100, 120 nm 60nm 100nm 120nm Figure 2.5: The simulated electric field profiles of a device with two field-plates shows that the electric field terminating on the field-plate can be increased by decreasing the thickness of the dielectric beneath it. Figure 2.4) the electric field terminating on the field-plates can be increased [Figure 2.5]. So to increase the electric field stress on a particular field-plate it is enough to reduce the thickness of the dielectric beneath it. Another observation is that increasing the lateral shift of the field-plates (s1,s2 as defined in Figure 2.4) reduces the magnitude of the electric-field peaks in the system for the same applied drain bias. However beyond a certain point, increasing the lateral shift does not lead to reduced electric field peaks for the same applied bias 20 CHAPTER 2. MUTIPLE FIELD PLATES E-field vs. fieldplate shifts (s1, s2) t1, t2 = 120 nm s1, s2 = 0.4 um and s1, s2 = 0.5 um 0.4 um 0.5 um Figure 2.6: The simulated electric field profiles of a device with two field-plates shows that with increasing the lateral spacing leads to the peaks spatially seperated. because thereafter the electric field peaks get spatially seperated. The intermediate regions between the peaks do not significantly contribute to the potential supported, but they contribute to the additional gate capacitance [Figure 2.6]. 21 CHAPTER 2. MUTIPLE FIELD PLATES Gate Source Source 2Deg 29nm AlGaN 1.8um GaN:UID 0.5um GaN:Fe nucleation substrate Drain Figure 2.7: The epitaxial structure of the HEMT and the layout of the fabricated devices. 2.4 Device Fabrication and results The AlGaN/GaN HEMT epitaxial structure was grown by Metal Organic Chemical Vapour Deposition(MOCVD) on a c-plane Sapphire substrate. The epitaxial growth was initiated with a 50 nm AlN nucleation layer followed by a 0.7µm Fe-doped GaN layer. This was followed by a 1.8µm thick unintentionally doped(UID) GaN layer and a 29 nm thick AlGaN heterostructure. The sample was capped with an insitu grown 4nm thick SiN x as gate dielectric to reduce gate leakage. Hall measurements at room temperature showed a channel carrier concentration of 8.59×1012 cm−2 and mobility of 1310 cm 2 /V·s. 22 CHAPTER 2. MUTIPLE FIELD PLATES 800m dc 80us 700m 600m 600m Ids (A/mm) 500m Ids (A/mm) dc 80us 700m 400m 300m 200m 100m 500m 400m 300m 200m 100m 0 0 0 5 10 15 20 25 30 35 0 5 10 15 20 25 30 35 Vds (V) Vds (V) Figure 2.8: (a) Before passivation there is significant dispersion between dc and pulsed-80µsIV curves (b) After passivation the dispersion is eliminated. The AlGaN/GaN HEMTs made in this run used a T-shape layout [Figure 2.7] with a gate of width 2×25µm. The gate length used was 1.5µm and 2µm and the gate-drain distance varied from 4µm to 28µm. First, Ti/Al/Ni/Au(20/120/30/50nm) ohmic metals were deposited and annealed at 870 ◦C in a RTA chamber to get ohmic source and drain contacts. The devices were then mesa-isolated by etching in a Cl2 reactive ion etcher. Ni-Au-Ni(30/400/30nm) gates were deposited by a lift-off process. Devices were then tested using tek370A curve tracer. They were found to have RF dispersion and the three terminal breakdown voltage increased with increasing gate-drain spacing. For Lgd =24µm the breakdown voltage was between 300-400 V. This breakdown voltage decreased to about 250V 23 CHAPTER 2. MUTIPLE FIELD PLATES FP3 FP2 FP1 Gate Figure 2.9: SEM picture of the cross-section of the fabricated device with three field-plates. after a surface passivation done by depositing about 120 nm SiN by Plasma Enhanced Chemical Vapour Deposition (PECVD). The current-voltage(I-V) characteristics measured at DC and 80µs are shown in Figure 2.8. The devices showed high current density (700 mA/mm) with no dispersion at the measured frequency. By shifting the gate layer mask towards the drain the lithography for the first field-plate was patterned. The field-plate (Ni/Au 30/400 nm) is connected to the gate at the gate pad region. The field-plate extension was s1=0.5-0.7µm. On top 24 CHAPTER 2. MUTIPLE FIELD PLATES Figure 2.10: With two field-plates a breakdown voltage of 900V was achieved on a device with Lg =2µm and Lgd =24µm of this another 120nm thick SiN was deposited by PECVD. An increase in the breakdown voltage was observed. Devices with Lgd =24µm had a three terminal breakdown voltage of 600-700 V. This process was repeated to get the second field-plate shifted further towards the drain [Figure 2.9]. The extension of the second field plate was s2=0.5-0.7µm and the device was capped with another 120 nm thick layer of SiNx deposited by PECVD. After this step the breakdown voltage increased further. Devices with Lgd =24µm showed a three terminal breakdown voltage of 900 V as shown in Figure 2.10. The measured three ter- 25 CHAPTER 2. MUTIPLE FIELD PLATES Breakdown Voltage (V) 1000 Lg = 1.5 um Lgd = 24 um 900 800 700 600 500 400 300 200 100 0 after gate passvtn 1st FP 2nd FP 3rd FP Measurements Figure 2.11: Breakdown voltage was measured with different processing steps. minal breakdown voltages at various processing steps is shown in Figure 2.11. After applying the field-plates no significant change was observed in the DC and pulsed-80µs I-V measurments. 2.5 Discussion It has been reported that the gate breakdown occurs at the drain-side edge of that gate electrode due to the high electric field peak, via avalanche breakdown and thermally assisted tunneling [5]. In the presence of dispersion the surface 26 CHAPTER 2. MUTIPLE FIELD PLATES traps are negatively charged at pinch-off. This extends the effective gate length and reduces the peak electric field at the drain side edge of the gate. Due to this mitigation of the electric field before passivation, devices show higher breakdown voltage (>350 V). But they also show dispersion due to the slow response of the surface traps. When dispersion is removed by surface passivation the peak electric field at the drain side edge of the gate increases drastically. This extremely large electric field peak can cause local Schottky-barrier breakdown at lower drain bias. Thus electric field engineering in the proximity of the gate is necessary to improve the device performance. The multiple field-plates technique is effective in alleviating the electrical field crowding at the drain-side edge of the gate. As simulations and experiments have demonstrated the multiple field-plates technique is effective in extending the drain depletion region and replacing the single peak electric field with n+1 peaks with smaller electric field strength (n is the number of field-plates). Since the field-plates increase the effective gate capacitance it leads to slight degradation of the high frequency performance. For devices with Lg =0.7µm, the ft is typically about 20 GHz. From this, for Lg=2µm an f t = 7 GHz is expected, but the measured ft is only about 4.5 GHz due to the additional capacitance from 27 CHAPTER 2. MUTIPLE FIELD PLATES Magnitude 10 |h21| |U| 1 ft=4.5 GHz fmax=12 GHz 100M 1G Frequency (Hz) 10G Figure 2.12: Small signal measurements of a device with L gd =20µm, Lg =2µm, s1=0.5µm, s2=0.5µm, s3=1µm at a bias of Vds=15 V, Ids=280 mA/mm the field-plates [Figure 2.12]. However this technique is especially attractive for power electronics application below 1 GHz range. This technique of using multiple field-plates over the passivation dielectric uses simple and well controlled processing steps. The active device area is protected from possible damages in the subsequent processing steps by the passivation dielectric, thereby not affecting the processing yield. 28 CHAPTER 2. MUTIPLE FIELD PLATES 2.6 Summary The need for using multiple field plates to achieve both high breakdown voltage and high frequency operation was presented. Simulations showed the expected trends in the electric field profiles in the presence of field-plates. A strategy for optimizing the parameter space for the field-plates was presented. Fabricated devices with field-plates showed a higher breakdown voltage than the devices without field-plates. With two field-plates a breakdown voltage of 900 V was obtained. The field-plates lead to a slight degradation in the frequency response due to the additional capacitance contributed by the field-plates. References [1] U. K. Mishra, P. Parikh, Y. Wu,“AlGaN/GaN HEMTs - An Overview of Device Operation and Applications”.Proceedings IEEE, 90, pp 1022 (2002). [2] R. Vetury, N. Q. Zhang, S. Keller, and U. K. Mishra,“The impact of surface states on the DC and RF characteristics of AlGaN/GaN HFETs”. IEEE Electron Device Letters, vol 48, pp 560-566, March 2001. [3] Robert Coffie ,“Characterizing and Suppressing DC-to-RF Dispersion in AlGaN/GaN High Electron Mobility Transistors”. PhD thesis, University of California, Santa Barbara, 2003. [4] S. Karmalkar, U. K. Mishra,“Enhancement of breakdown voltage in AlGaN/GaN high electron mobility transistors using a field plate”, Electron Devices, IEEE Transactions on , vol.48, no.8 pp.1515-1521, Aug 2001. 29 CHAPTER 2. MUTIPLE FIELD PLATES [5] R. J. Trew, U. K. Mishra,“Gate breakdown in MESFETs and HEMTs”.IEEE electron device letters, 12(10), 524 (1991). 30 3 Gate Leakage in AlGaN/GaN HEMTs 3.1 Introduction G aN has emerged as a promising material for the high speed, high power device applications. The large bandgap and the high electron velocity make it suitable for high power microwave applications [1]. However, GaN metal semiconductor field-effect transistor (MESFET) and AlGaN/GaN high electron mobility transistor (HEMT) devices suffer from high gate leakage current which reduces the reliability and efficiency of the devices. High gate leakage current prevents the GaN MESFETs from reaching their potential for high power levels [2]. Field effect transistors require low gate leakage current for low noise and improved reliability. Considerable interest in this issue has initiated the exploration of dielectrics to reduce the gate leakage in the GaN materials 31 CHAPTER 3. GATELEAKAGE system. As discussed in §2.2 dc-to-rf dispersion in GaN transistors is normally addressed by surface passivation employing PECVD deposited SiN x . It is necessary that the gate dielectrics explored for GaN transistors should incorporate surface passivation to maintain high power performance. 3.2 The origin of gate leakage Solving the problem of gate leakage needs an understanding of where exactly the leakage happens. Gate leakage is measured after passivation as a twoterminal measurement between gate and drain with source left floating. Gate leakage does not depend on the Lgd spacing as shown in Figure 3.1. Gate leakage scales faithfully with device width. The linear fit of the data shows that the leakage is happening throughout the width of the device. The y-intercept seen could be either the parasitic leakage in the mesa regions and in the region where the gate feed runs over the mesa wall or it could arise out of measurement scatter from device to device. Gate leakage does not change with gate length (from 0.7µmto 2µm). This shows that the leakage though occuring throughout the 32 CHAPTER 3. GATELEAKAGE Ig vs L gd 1m 100µ Lgd= 2um Lgd= 15um Lgd= 20um 10µ 5V 2.5 10V 15V 20V 25V Vdg (V) linear fit R=0.998 2.0 1.5 1.0 0.5 0.0 0.0 1µ 0V Ig vs W g scaling 3.0 Ig (mA) at V ds=25V GateLeakage (A/mm) 10m Ig(mA) = 0.5 0.26 + 1.1xWg(mm) 1.0 1.5 Wg (mm) 2.0 2.5 Figure 3.1: (a)Gate Leakage does not change with different Lgd spacing (b)Gate leakage scales faithfully with device width Wg . width of the gate is not occuring throughout the length of the gate. This implies that the leakage is happening at the drain end of the gate where the E-field is higher than the other regions of the gate. A possible source of gate leakage is that the passivating SiN x layer could be conducting. To study the leakage in the passivating layer, a controlled experiment was performed in which the leakage path in the SiN x was isolated. This was done by etching trenches in the SiNx by shifting the gate lithography [Figure 3.2]. The distance of these isolation trenches were varied to study their effect on leakage. Devices with these isolation trenches in SiN x showed a gate leakage similar to the device without the isolation trenches. This experiment shows that 33 CHAPTER 3. GATELEAKAGE SiNx Isolation at 1.1um SiNx Isolation at 1.6um 1.1um Source SiNx Gate 1.6um Drain Source AlGaN AlGaN GaN GaN Drain AlGaN GaN GateLeakage (A/mm) SiNx Gate Drain Gate L eakage with Sx iN isolated 10m Standard Device Source SiNx Gate 1m 100µ Normal device I solation at 1.6um I solation at 1.1um 10µ 1µ 0 5 10 15 Vdg (V) 20 25 Figure 3.2: Controlled experiments to check if the gate leakage is through the passivating SiN layer. Leakage remains the same after isolating the SiN layer by etching trenches of 0.7µmlength. the leakage path is not through SiNx . The above experiments show that the leakage path is through the AlGaN layer at the drain end of the gate. To study whether the leakage in the AlGaN is occuring at the dislocation sites, a HEMT was grown on a double-LEO GaN substrate which had lower dislocation density (1×10 7 cm−2 ). The HEMT made on this sample had a similar gate leakage of 1 mA/mm as seen in a standard HEMT made on other substrates (with dislocation density of 1×10 9 cm−2 ). If the 34 CHAPTER 3. GATELEAKAGE 1m 100µ 10µ 1µ after passivation before passivation 100n 10n Drain Current (mA/mm) GateLeakage (A/mm) 10m 1k 200ns 80us dc 800 Max.Vg = 1V Del.Vg= -1V 600 400 200 0 0 5 10 15 20 0 25 Vdg (V) 2 4 6 8 10 12 14 16 Drain V oltage (V) Figure 3.3: After passivation the gate leakage in HEMTs grown on LEO GaN template is about 1 mA/mm (comparable to those devices on ordinary templates). dislocation density is known, one could estimate the current that the dislocations have to support. Assuming a dislocation density of 1×10 7 cm−2 , a high E-field region of 0.1µm length and a width of 1 mm, the number of dislocations present in this area can be estimated as 10. This means that if dislocations were the only paths of gate leakage, then these 10 dislocations must pass 1mA of current which turns out to be a very high current density. So it could be argued that the gate leakage could occur in AlGaN even without the aid of dislocations, due to the high electric field peak at the drain side of the gate edge. This is controversial because Yu et al.[3] have shown that the dislocations are the source 35 CHAPTER 3. GATELEAKAGE of gate leakage on an unpassivated AlGaN/GaN sample grown by MOCVD. The exact mechanism of gate leakage in the AlGaN is not clearly understood. 3.3 Reducing gate leakage 3.3.1 Reducing gate leakage by using trench gates One processing variation that reduced the gate leakage in the HEMTs even without the use of any dielectric is the trench gate process. In this process technology the passivation is done before the gates and trenches as defined by the gate lithography are etched in the passivation using Reactive Ion Etching(RIE conditions: 20 mT chamber pressure, 20/2 sccm CF 4 /O2 gas flow). Gates are deposited in these trenches using the same lithography in a self-aligned way. Also during the metal evaporation the angle at which the sample receives the metal flux could be changed to get a self-aligned field-plate intimately connected to the gate. Also the shape of the profile of the SiNx trench walls could be changed by changing the etch conditions. For example a high chamber pressure (20 mT) during the etch yields a considerable flux of reactive ions in the RIE sideways 36 CHAPTER 3. GATELEAKAGE 10m Source Gate SiNx Drain AlGaN GaN Trench gate Source Gate Gate AlGaN GaN SiNx Drain GateLeakage (A/mm) Standard Gate 1m 100µ std gates trench gates 10µ 1µ 0 5 10 15 Vdg (V) 20 25 Figure 3.4: Gate leakage is reduced by a factor of 5 by using the trench-gate process, in which the passivation is done first and the gate is deposited in the trench etched in the passivation layer. and this yields a sloping trench wall. Also by changing the CF 4 /O2 gas ratio the rate of etch of the Photoresist relative to the etch rate of the passivation layer could be changed thereby allowing another parameter to control the trench wall profile. By varying the angle of E-beam gate metal evaporation the extension of the self-aligned field-plate could also be controlled. Gate leakage was reduced by atleast a factor of 5 by using trench gates. Figure 3.4 shows the comparison of the gate leakage of devices with normal gates and devices with trench gates. This reduction in gate leakage could be due to 37 CHAPTER 3. GATELEAKAGE the formation of a self-aligned field-plate on the sloping trench wall by using an angled gate metal evaporation. This field-plate reduces the peak E-field yielding a reduced gate leakage. An additional advantage with the trench gate process is that it yielded an improved passivation. The trench gate process in presented in detail in §5.2. 3.3.2 Literature survey of reducing gate leakage in GaN devices using dielectrics Various dielectric materials have been tried as an insulator underneath the gate to reduce gate leakage in HEMTs. Chini et al. have used a thin film of SiN x grown in situ by MOCVD to reduce gate leakage in GaN MESFETs [2]. 4 nm of SiNx was deposited on the sample surface by flowing disilane and ammonia inside the MOCVD chamber at a temperature of 980◦ C. Chini et al. attributed the reduction in gate leakage with the SiNx film to reduced conduction through the dislocations or due to increased Schottky barrier height. In §3.3.3 the results of various dielectrics grown by MOCVD is presented. SiO 2 deposited by plasmaenhanced chemical vapor deposition (PECVD) under the gate has been shown 38 CHAPTER 3. GATELEAKAGE to reduce gate leakage by six orders of magnitude in an AlGaN/GaN HEMT structure [4]. However the low dielectric constant of SiO2 (r = 3.9) leads to a larger pinch-off voltage and reduced gate control in the HEMT. A combination of sputtered SiNx and Ebeam-evaporated SiOx films have been tried as gate dielectric to reduce gate leakage [5]. However the devices with that dielectric showed considerable high frequency dispersion. In two separate studies Hansen et al. have reported the use of (Ba,Sr)TiO3 (BST) [6] and LiNbO3 [7] thin films deposited by rf-magnetron sputtering as possible dielectrics for GaN and AlGaN/GaN devices. Hansen et al. performed a blanket deposition of the films just before the gate metallization step. However they observed that the surface was damaged by the high ion energies associated with the sputtering process which resulted in reduced electron density and reduced electron mobility in the two-dimensional electron gas (2DEG) at the AlGaN/GaN interface. Oxides such as crystalline gadolinium oxide (Gd 2 O3 ) and amorphous gadolinium gallium oxide Ga 2 O3 (Gd2 O3 ) have been tried in GaN devices using molecular beam epitaxy to achieve low interface state density between the dielectric and the substrate [8]. MgO and Sc2 O3 deposited by RF plasma-assisted molecular beam epitaxy have been tried as high-k gate di- 39 CHAPTER 3. GATELEAKAGE electrics for AlGaN/GaN devices [9]. The pulsed-IV curves reported in these studies show reduced DC-to-RF dispersion [10]. Thin metallic Zr and Hf films have been oxidized by ozone to yield high-k gate oxide dielectrics for Si and Si-Ge material system [11]. The ozone is generated by exposure of oxygen gas to ultraviolet (UV) radiation from a Hg vapor lamp. A high dielectric constant, large bandgap (Eg 5.8 eV), large conduction band offset with Si ( Ec 1.4 eV) and reduced charge trapping make these oxides very promising dielectrics for Si [12]. ZrO2 is also reported to have breakdown fields above 3 MV/cm [13] making it a potential candidate as a dielectric for large bandgap, high power material system like GaN. The low energy deposition of Zr followed by the UV-ozone oxidation at relatively lower temperatures could enable this film to be easily incorporated into the GaN process flow. In §3.3.4 the use of ZrO2 as a high-k dielectric for the GaN material system is presented. 3.3.3 Reducing gate leakage by using in-situ grown dielectrics Various dielectric materials grown by MOCVD were tried as candidates for a gate dielectric for GaN transistors. These dielectrics were grown at high temper- 40 CHAPTER 3. GATELEAKAGE Std. HEMT 0.5nm SiNx 2nm SiNx 4nm SiNx 6nm SiNx Buried SiNx 4nm AlOx 031005FA 031005FB 031005FC 031006FB 031006FA 031014FA 031016OH Before passivation Gate Leakage Vds = 18V; Vgs = -6V; 2T-GD Breakdown 0.133 uA/mm 3 uA/mm 30 uA/mm 200 uA/mm 0.7 uA/mm 14 uA/mm 0.03 uA/mm 150V 120V 150V 130V 210V 130V 160V 670 uA/mm 330 uA/mm 500 uA/mm 1000 uA/mm 100 uA/mm 830 uA/mm 67 uA/mm 100V 60V 70V 50V 50V 80V 60V After passivation Gate Leakage Vds = 18V; Vgs = -6V; 2T-GD Breakdown Figure 3.5: Gate leakage of devices made on HEMT samples with in-situ MOCVD grown dielectrics. ature (> 950◦ C) in the MOCVD reactor. They were grown in-situ in MOCVD reactor after finishing the growth of HEMT epitaxy. The samples had SiN x of various thicknesses and AlOx on the surface of the HEMT expitaxy. The SiNx was deposited on the sample surface by flowing di-silane and ammonia inside the MOCVD chamber at a temperature of 980◦ C. One sample had a buried SiNx layer 4 nm beneath the surface of the HEMT epitaxy which was achieved by 41 CHAPTER 3. GATELEAKAGE interupting the AlGaN growth, depositing SiN x and growing 4 nm of AlGaN on top of it. The AlOx was deposited on the sample surface by flowing tri-methyl aluminum and oxygen inside the MOCVD chamber at a temperature of 900 ◦ C. The data, summarized in Figure 3.5, was not conclusive. One issue with these dielectrics was that these films cracked during the 870 ◦C ohmic anneal step during processing. These cracks were seen in the ohmic regions. The uniformity of these films is also an issue. Devices next to each other sometimes had differing gate leakage values. This could also be due to the cracking of the film during the 870◦ C anneal. To use such dielectrics improved deposition conditions need to be employed. 3.3.4 Reducing gate leakage by using ZrO2 dielectric Zirconium Oxide was tried as a high-k gate dielectric for GaN transistors. The deposition process for the ZrO2 film was optimized by the analysis of metal oxide semiconductor capacitor (MOSCAP) structure made on GaN and with surface characterization techniques. This work was done at UCSB by Sooyeon Han, Dr. Peter J. Hansen and Dr. Dmitri O. Klenov. Atomic Force Microscopy 42 CHAPTER 3. GATELEAKAGE AlGaN AlGaN GaN GaN Source Drain AlGaN AlGaN GaN GaN ZrO2 Source Drain AlGaN AlGaN (b) Transistor Layout GaN GaN ZrO2 Source Gate Gate Drain AlGaN AlGaN GaN GaN ZrO2 Source Gate Gate SiNx AlGaN AlGaN Drain GaN GaN (c) CV pattern (a) Process flow Figure 3.6: HEMT process flow incorporating Zro2 as gate dielectric. The layout of the transitor and the circular CV-pattern are also shown. (AFM) study of the surface showed that UV-ozone process appeared to produce a thin uniform conformal oxide. The optimized film was applied to AlGaN/GaN HEMTs and the compatibility and performance of the film as a gate dielectric was tested in an actual device operation. The optimized conditions for ZrO 2 on the MOS structures were used for the AlGaN/GaN structures. The HEMTs had the following layer structure: Al 0.22 Ga0.78 N 43 CHAPTER 3. GATELEAKAGE (29 nm)/unintentionally-doped GaN (UID GaN, 1.8 µm)/GaN:Fe (0.5 µm)/AlN (50 nm)/Sapphire Substrate. Room temperature Hall measurements on the HEMT samples showed a 2DEG carrier concentration of 8×1012 cm−2 and a mobility of 1700 cm2 /V·s. The HEMT fabrication started with the liftoff of the Ti/Al/Ni/Au (20/120/30/50 nm) ohmic contact metallization and annealing at 870 ◦ C in an N2 environment for 30 sec in the RTA. Isolation of the devices was achieved by etching a mesa to a depth of about 120 nm by Cl2 -based reactive ion (RIE) etching. The sample surface was then cleaned by an O2 plasma de-scum followed by a dip in HCl:DI = 1:2 for 30 sec to remove any native gallium oxide and a DI rinse. The samples were pumped overnight in the electron beam evaporator to a pressure of 9×10−7 torr. A 4 nm Zr film was electron beam deposited. The samples were quickly transferred to the UV-ozone oxidation chamber with Hg-lamps and a heated stage. The Hg vapor lamp emits wavelengths of 185 and 254 nm which are close to the bond energy of O2 . This radiation interacts with oxygen gas to produce oxygen radicals and ozone. This activated oxygen enhances the kinetics of oxidation compared to natural oxidation, resulting in better oxidation even at room temperature [14]. The samples were oxidized by the UV-ozone oxidation 44 CHAPTER 3. GATELEAKAGE Glue Glue ZrO2 ZrO2 AlGaN AlGaN (a) (b) Figure 3.7: The high resolution Transmission electron Microscope images a)HRTEM and b)HAADF-STEM. This characterizatin was done by Dr. Dmitri O. Klenov at UCSB. method for 30 min at 300◦ C. Ni/Au/Ni gates were defined by lift-off. In the AlGaN/GaN HEMT samples, after the gate metallization the surface was passivated with PECVD grown SiNx of thickness 120 nm to remove dispersion. A schematic of the HEMT process flow is shown in Figure 3.6a. The test structures on the HEMT samples consisted of the HEMT devices (Figure 3.6b) and circular CV pattern with a guard ring (Figure 3.6c). The gate width and gate length of the transistors measured were 150 µm and 0.7 µm, respectively. The source-to-drain spacing was 3.4 µm. Electrical characteriza- 45 CHAPTER 3. GATELEAKAGE tion included CV, gate leakage, pulsed-IV and load-pull power measurements. Capacitance-voltage measurements were performed with a Keithley-590 CV meter at 1 MHz. The leakage current measurements were made using a HP 4145 semiconductor parameter analyzer. The load-pull power measurements on the HEMTs were performed on a Maury 2-18 GHz load-pull system. Cross-sectional TEM micrographs done by Dmitri O. Klenov showed that 4 nm of evaporated Zr resulted in an uniform thickness of the ZrO 2 film of approximately 5 nm. Both High Resolution Transmission Electron Microscope (HRTEM) and High-Angle Annular Dark Field Scanning Transmission Electron Microscopy (HAADF-STEM) images showed that the ZrO 2 was amorphous. In addition, no crystallization was observed by nanodiffraction. However, some degree of nanocrystallinity could not be excluded [15]. HRTEM images (Figure 3.7a) showed an abrupt interface between AlGaN and ZrO2 and no reaction layer was found. The HAADF-STEM images (Figure 3.7b) showed the absence of any reaction layer between AlGaN and ZrO2 though a greater roughness of the AlGaN surface was observed than expected, which may be due to some degree of oxidation of the AlGaN during ozone oxidation. Direct evidence of the oxidation of AlGaN is not available. 46 CHAPTER 3. GATELEAKAGE Standard Gate Gate with ZrO2 ZrO2 Gate Source SiNx Drain Source AlGaN GaN GaN 100pF 80pF 100µ Capacitance (F) Gate L eakage (A/mm) 1m 10µ 1µ 100n 10n 1n standard gates gates with Z rO2 (300°C) 10p 0V 5V SiNx AlGaN 10m 100p Gate Gate 10V 15V 20V Drain standard gates gates on Z r2O 60pF 40pF 20pF 0F -6 -4 -2 0 2 Voltage (V) Vdg (V) Figure 3.8: Gate leakage is reduced by 2 orders using zirconium oxide dielectric(oxidized at 300◦ C). In AlGaN/GaN HEMTs, PECVD deposition of SiNx (performed at 250◦C) passivates the surface of the AlGaN. Therefore to achieve a high quality of passivation, it is necessary that the temperature and the time for which the AlGaN surface is subjected to oxidation should be limited to as close to 250 ◦ C as possible. So an optimum temperature of 300 ◦ C and a time of 30 min for the UV oxidation step were chosen for all the AlGaN/GaN HEMT samples so that the passivation would not be seriously affected. 47 CHAPTER 3. GATELEAKAGE The gate leakage in the AlGaN/GaN HEMTs was reduced by at least two orders of magnitude with ZrO2 as a gate dielectric [Figure 3.8] in comparison to the Schottky gates. All gate leakage measurements were performed after the devices were passivated with SiNx. After passivation, the DC-to-RF dispersion was reduced, but the peak electric field increased because all the electric field lines terminate at the drain edge of the gate. Thus, measurements of gate leakage after passivation ensured that the high electric field at the drain side of the gate was the same as in the high frequency high power operation of HEMTs. Figure 3.8 compares the CV measurements with and without ZrO 2 under the gate. By comparing the capacitance values at a gate bias for which there is still an undepleted 2DEG, the relative dielectric constant for the ZrO 2 layer was extracted to be r =23 . This value of dielectric constant agreed with the numbers reported by others for amorphous ZrO2 [16]. The absence of any significant shift in the CV curve between the positive and negative sweeps demonstrated that the ZrO2 -AlGaN interface had insignificant charge trapping. The global shift in the CV curve by about 1V towards the right, exhibiting a reduced pinch-off voltage, is attributed to the reduction in the 2DEG concentration (delta n s = 2.5×1012 cm−2 ) at zero gate bias after the oxidation process, suggesting a change in sur- 48 CHAPTER 3. GATELEAKAGE Surface oxidized with Zr film 10m 1m Source Gate Gate SiNx Drain AlGaN GaN Surface oxidized without Zr film Surface oxide Source Gate Gate SiNx Drain AlGaN GateLeakage (A/mm) ZrO2 100µ 10µ 1µ 100n 10n 1n without oxidation oxidized without zr oxidized with zr 100p 10p -5V GaN 0V 5V 10V 15V 20V 25V Vdg (V) Figure 3.9: Controlled experiment performed by UV-Ozone oxidation of devices with zirconium film deposited on AlGaN and devices without zirconium film on AlGaN show that the reduced gate leakage is due to the zirconium oxide and not due to the surface oxidation of AlGaN. face fermi-level position at the AlGaN/ZrO2 interface. However the reduction in the zero bias 2DEG concentration did not affect the device performance, because with ZrO2 the device could be biased to more positive voltages, thus inducing additional 2DEG concentration. To verify whether the gate leakage reduction was due to ZrO2 or due to surface oxidation of AlGaN, a controlled experiment was performed. One of the samples was partially shadow masked during the electron beam evaporation of Zr. Thus part of the sample had Zr deposited on it and the rest had the bare AlGaN 49 800 1m 200 ns 80 us dc max V g = 1 V del V g = -1 V 100µ GateLeakage (A/mm) Drain Current (mA/mm) CHAPTER 3. GATELEAKAGE 600 400 200 0 0 2 4 6 8 10 10µ 1µ 100n 10n 1n fresh device after pulsed-IV after 15V V ds power 100p 10p 12 0V Drain V oltage (V) 5V 10V 15V 20V 25V Vdg (V) Figure 3.10: Using ZrO2 leads to dispersion as shown in these pulsed-IV curves. The gate leakage reduction gradually degrades with pulsed-IV measurements and finally with 4GHz load-pull power measurements. surface. The entire sample was oxidized by the UV-ozone oxidation method at 300◦ C for 30 min. Gates were deposited in both the regions and SiN x passivation was performed to reduce dispersion. Figure 3.9 shows the comparison of gate leakage for the AlGaN surface, oxidized with and without Zr. This controlled experiment clearly showed that the leakage reduction was due to ZrO 2 and not due to surface oxidation of AlGaN. Two challenges for using ZrO2 as gate dielectric for AlGaN/GaN HEMTs were observed. One was the effectiveness of the SiNx passivation in the AlGaN/GaN HEMTs in the presence of a gate dielectric. Figure 3.10a shows the 50 CHAPTER 3. GATELEAKAGE high frequency pulsed-IV curves showing knee-walkout compared to the DC IV curves, commonly referred to as dispersion. Due to the poor thermal conductivity of the sapphire substrate, a well-passivated AlGaN/GaN HEMT grown on sapphire substrate is expected to have a peak pulsed-current at least 10% above that of the peak DC-current. The pulsed-IV curves show lower current level than the DC current level indicating the presence of dispersion. Another issue is the stability of the gate dielectric in device operation. Figure 3.10b shows that the gate leakage degraded after pulsed-IV measurements and 4 GHz load-pull power measurements at a bias of Vds = 15 V. To address the issues of dispersion and the dielectric stability, the fabrication process of the AlGaN/GaN HEMT was changed as shown in Figure 3.11a. Instead of passivating the HEMT after the gate metal deposition, SiN x was deposited first. Using the gate lithography, trenches were etched in the SiN x and the photoresist was removed. After solvent cleaning, Zr was blanket deposited and oxidized as described earlier. Finally with another gate lithography aligned towards the drain side wall of the trench, the gate metal was deposited, simultaneously introducing a field-plate effect [17][18]. The pulsed-IV curves shown in Figure 3.11b demonstrate improved passiva- 51 CHAPTER 3. GATELEAKAGE Std. Gate with ZrO2 Trench gate with ZrO2 ZrO2 ZrO2 1k 200 ns 80 us dc 800 SiNx Source Drain AlGaN GaN GaN 400 200 4 Drain 1m 0 2 SiNx 10m Max V g = 1 V del V g = -1 V 600 0 Gate Gate AlGaN GateLeakage (A/mm) Drain Current (mA/mm) Source Gate Gate 100µ 10µ 1µ 100n fresh after after after after 10n 1n 100p device pulsed-IV 15V V ds power 25V V ds power 35V V ds power 10p 6 8 10 12 14 16 Drain V oltage (V) 0V 5V 10V 15V 20V 25V Vdg (V) Figure 3.11: The HEMT process flow was modified by which the SiN x passivation was done first and gates were deposited in the trenches etched in SiN x using the gate lithography in a self-aligned way. tion. The 200 ns pulsed current was 20% higher than the dc current level showing very good passivation for a AlGaN/GaN HEMT on a substrate which has a poor thermal conductivity. Power measurements at 4 GHz showed a peak power of 3.8 W/mm at a bias of Vds = 25 V for a HEMT on sapphire substrate. The power added efficiency (PAE) for this power was 58%. The high power and PAE results at 4 GHz are another indication of insignificant high frequency dispersion in the devices. Collectively, these results confirm the applicability of ZrO 2 as 52 CHAPTER 3. GATELEAKAGE gate dielectric for high frequency operation. Figure 3.11c shows that the gate leakage reduction did not degrade until the power measurements at Vds bias of 35 V. We believe that the improvement in the gate leakage degradation is caused by a reduced field peaking, due to the fieldplate effect caused by the alignment of the gate edge over the wall of the SiNx trench. After the device showed degradation in the gate leakage, the pulsed-IV and load-pull measurements were performed. After the degradation, however the current levels and the power levels in the devices did not change. However, the gate leakage was significantly higher after the degradation, but was on the same order as a device without any dielectric under the gate. This leads us to believe that the dielectric degraded under very high field operation. Further investigation is necessary to improve the high-field reliability of this dielectric. 3.4 Leakage from field-plates: The leakage through the field-plates was quantified by a device structure without a gate, but with a field-plate sitting on top the passivation dielectric as shown in Figure 3.12. Such a structure allows for the measurement of the leakage 53 CHAPTER 3. GATELEAKAGE Gate leakage test structure Field-Plate leakage test structure FP Source Gate Gate SiNx SiNx Source Drain AlGaN AlGaN GaN GaN Drain Figure 3.12: The test structure used to quantify the leakage from field-plates through the passivation layer is shown. from the field-plate through the passivation layer and the AlGaN to the 2-DEG. The leakage was measured by grounding the field-plate and applying a positive sweep on the drain. The source contact was left floating. The leakage from the field-plate is about 100µA/mm as opposed to the 1 mA/mm leakage from the gate which is shown in Figure 3.13. The E-field that terminates at the field-plates increases steadily with the applied drain bias. Hence it is possible that the leakage from the field-plate could play a critical role for breakdown voltage, especially for devices with very high breakdown voltage. Therefore the SiNx passivation layer deposited under a different chemistry was studied to see its effect on passivation and on the gate leakage and the field-plate leakage. SiNx film deposited by an Inductive Coupled Plasma(ICP) [Appendix-B] deposition system was used because the film 54 CHAPTER 3. GATELEAKAGE pulsed IV curves S td.SiNx trench gate S td.SiNx field plate 1m 100µ 10µ 1µ 100n 2-layerSiNx trench gate 2-layerSiNx field plate 10n 0 5 10 15 20 Drain Current (mA/mm) GateLeakage (A/mm) 10m 1k 800 200ns 50ohmLL 200ns 165ohmLL dc 600 MaxVg = 1V del Vg= -1V 400 200 0 0 25 Vdg (V) 5 10 15 20 25 Drain Voltage (V) 30 Figure 3.13: Leakage from field-plates through different passivation layers is shown. The bottom set of curves show the gate leakage and field-plate leakage of the two-layer passivation and the top set of curves show the gate leakage and field-plate leakage of the standard passivation. The pulsed-IV curves of the device passivated with two-layer dielectric show little dispersion upto 165ohm loadline. deposited using this high density plasma is supposed to give a denser film. But the devices with this passivation had a reduced current of about 1/10th of the Imax . Exposing the AlGaN surface to this dense plasma seems to have damaged the surface leading to a reduced current. So a two layer passivation dielectric was tried in which the first layer of SiNx of 60 nm thickness was depsoited by PECVD and on top of this a second layer of SiNx of 60 nm thickness was deposited by ICP. 55 CHAPTER 3. GATELEAKAGE Figure 3.13 compares the leakage from the field plates between two passivation dielectrics. The standard SiNx passivation had gate leakage of 1 mA/mm and field-plate leakage of 0.1 mA/mm. Devices passivated with the two layer dielectric had a gate leakage of 0.05 mA/mm and a field-plate leakage of about 0.005 mA/mm. This shows that the field-plate leakage through the two layer dielectric is insignificant and this dielectric would be useful for devices operating at high voltages. The pulsed-IV curves of devices passivated with the two layer dielectric is shown Figure 3.13. For 200 ns pulses there is no dispersion for a 50 ohm load-line. For a 165 ohm load-line there is little dispersion. These devices were made using the trench gate process. Further characterization of this passivation was done by doing power measurements at 4GHz, the details of which are presented in §5.2.4. 3.5 Summary The source of gate leakage was studied. The experiments presented show that the leakage occurs through the AlGaN layer throughout the width of the gate and at the drain end of the gate. The exact mechanism of leakage in the AlGaN 56 CHAPTER 3. GATELEAKAGE is not well understood. Various dielectric films were tried as candidates for gate dielectrics in GaN transistors. In-situ high temperature grown dielectrics have to deal with the problem of uniformity and compatibility with AlGaN/GaN HEMT processing. However these high temperature grown dielectrics seem to be reliable. Zirconium oxide film made by UV-ozone oxidation of deposited zirconium film was optimized to serve as a high-k dielectric for GaN transistors. Improved processing technique enabled the compatibility of ZrO 2 as a gate dielectric without compromising passivation. The degradation of this dielectric at high power operation is an issue. Trench gate processing technique reduced the gate leakage by a factor of 5. Finally the leakage through the field-plates was studied. References [1] U.K. Mishra, P. Parikh, Y. Wu,“AlGaN/GaN HEMTs - An Overview of Device Operation and Applications”. [2] A. Chini, J. Wittich, S. Heikman, S. Keller, S.P. DenBaars, U.K. Mishra,“Power and linearity characteristics of GaN MISFETs on sapphire substrate”.IEEE Electron Device Letters, 25, 55 (2004). [3] E.J. Miller, X.Z. Dang, E.T. Yu,“Gate leakage current mechanisms in AlGaN/GaN heterostructure field-effect transistors”.Journal of Applied Physics, 88, 5951 (2000). [4] M.A. Khan, X. Hu, A. Tarakji, G. Simin, J. Yang, R. Gaska, M.S. Shur,“AlGaN/GaN metal-oxide-semiconductor heterostructure field-effect transistors on SiC substrates”.Applied Physics Letters, 77, 1339 (2000). 57 CHAPTER 3. GATELEAKAGE [5] Naiqian Zhang , “High Voltage GaN HEMTs with Low on-resistance for Switching Applications”. PhD thesis, University of California, Santa Barbara, 2002. [6] P. J. Hansen, L. Shen, Y. Wu, A. Stonas, Y. Terao, S. Heikman, D. Buttari, T. R. Taylor, S. P. DenBaars, U. K. Mishra, R. A. York, J. S. Speck,“AlGaN/GaN metal-oxide-semiconductor heterostructure field-effect transistors using barium strontium titanate”.J. Vac. Sci. Technol. B, vol 22(5), pp 2479, Sep 2004. [7] P. J. Hansen, Y. Terao, Yuan Wu, R. A. York, U. K. Mishra, J. S. Speck,“LiNbO/sub 3/ thin film growth on (0001)-GaN”.J. Vac. Sci. Technol. B, vol 23(1), pp 162-167, Jan 2005. [8] B.P. Gila, K.N. Lee, W. Johnson, F. Ren, C.R. Abernathy, S.J. Pearton, M. Hong, J. Kwo, J.P. Mannaerts, K.A. Anselm,“A comparison of gallium gadolinium oxide and gadolinium oxide for use as dielectrics in GaN MOSFETs”IEEE-Cornell Conference on High performance Devices, 182 (2000). [9] R. Mehandru, B. Luo, J. Kim, F. Ren, B.P. Gila, A.H. Onstine, C.R. Abernathy, S.J. Pearton, D. Gotthold, R. Birkhahn, B. Peres, R. Fitch, J. Gillespie, T. Jenkins, J. Sewell, D. Via, A. Crespo, “AlGaN/GaN metal-oxidesemiconductor high electron mobility transistors using Sc2 O3 as the gate oxide and surface passivation”. Appl. Phys. Lett. 82, 2530 (2003). [10] B. Luo, J.W. Johnson, J. Kim, R.M. Mehandru, F. Ren, B.P. Gila, A.H. Onstine, C.R. Abernathy, S.J. Pearton, A.G. Baca, R.D. Briggs, R.J. Shul, C. Monier, J. Han,“Influence of MgO and Sc2 O3 passivation on AlGaN/GaN high-electron-mobility transistors”. Appl. Phys. Lett. 80, 1661 (2002). [11] S. Ramanathan, P.C. McIntyre, S. Guha, E. Gusev,“Charge trapping studies on ultrathin ZrO2 and HfO2 high-k dielectrics grown by room temperature ultrviolet ozone oxidation” Appl. Phys. Lett. 84, 389 (2004). [12] G.D. Wilk, R.M. Wallace, J.M. Anthony,“High-k dielectrics: Current status and materials properties considerations”. J. Appl. Phys. 89, 5243 (2001). [13] J. Shappir, A. Anis, I. Pinsky,“Investigation of MOS Capacitors with Thin ZrO2 layers and various gate materials for advanced DRAM applications”. IEEE Trans Electron Devices, 33, 442 (1986). 58 CHAPTER 3. GATELEAKAGE [14] S. Ramanathan, G.D. Wilk, D.A. Muller, C.M. Park, P.C. McIntyre,“Growth and characterization of ultrathin zirconia dielectrics grown by ultraviolet ozone oxidation”. Appl. Phys. Lett. 79, 2621 (2001). [15] M.-Y Ho, H. Gong, G.D. Wilk, B.W. Busch, M.L. Green, P.M. Voyles, D.A. Muller, M. Bude, W.H. Lin, A. See, M.E. Loomans, S.K. Lahiri and P.I. Ralsanen,“Morphology and crystallization kinetics in HfO2 thin films grown by atomic layer deposition” J. Appl. Phys. 93, 1477 (2003) [16] S. Ramanathan, C. Park, P.C. McIntyre,“Electrical properties of thin film zirconia grown by ultraviolet ozone oxidation”, J. Appl. Phys., 91, 4521 (2002). [17] A. Chini, D. Buttari, R. Coffie, L. Shen, S. Heikman, A. Chakraborty, S. Keller, and U. K. Mishra, “Power and linearity characteristics of field-plated recessed-gate AlGaN-GaN HEMTs”. IEEE Electron Device Letters, vol 25, pp 229-231, May 2004. [18] Huili Xing, Y. Dora, A. Chini, S. Heikman, S. Keller, U. K. Mishra, “High breakdown voltage AlGaN-GaN HEMTs achieved by multiple field plates,” IEEE Electron Device Letters, vol 25, no 4, pp 161-163, April 2004. 59 4 Buffer Leakage in GaN Transistors 4.1 Introduction G aN-based transistors are very promising devices for high power and high frequency applications. High power levels at microwave-frequencies [1][2] and high breakdown voltages [3][4] have been demonstrated. To achieve high performance in lateral devices it is important to have a highly resistive buffer underneath the conducting channel of the transistor. AlGaN/GaN High Electron Mobility Transistors (HEMTs) and GaN MEtal Semiconductor Field Effect Transistors (MESFETs) are made on semi-insulating GaN buffers grown on substrates like Sapphire, SiC, bulk grown GaN, Si etc,. Thicker GaN buffers are grown on these substrates to reduce the threading dislocation density which yields channels with high mobility. In order to achieve 60 CHAPTER 4. BUFFERLEAKAGE higher breakdown voltage and high power added efficiency it is necessary that the leakage through the underlying GaN buffer be as low as possible. Residual donors, presumably oxygen, in the unintentionally doped(UID) GaN, have been identified as a source of buffer leakage [5][6]. Techniques like incorporating Fe-doping in Metal-organic chemical vapour deposition(MOCVD) grown GaN buffers [6] and C-doping in Molecular Beam Epitaxy(MBE) grown GaN buffers [7] are commonly used to reduce the buffer leakage. The effect of varying the Fe-doping on the buffer leakage is presented in § 4.3. Alloyed ohmic contacts are identified as another cause of buffer leakage as described in §4.4. The effect of ohmic contacts on the leakage in the underlying GaN buffer and its effect on the breakdown voltage of AlGaN/GaN HEMTs is also presented. 4.2 Test Structures The epitaxial layer structure used for the GaN devices were grown by MOCVD on sapphire and 4H-SiC substrates. The epitaxial growth was initiated with a 100 nm thick nucleation layer followed by a 0.5µm thick Fe-doped layer and an 61 CHAPTER 4. BUFFERLEAKAGE 2Deg 29nm AlGaN Gate Pad Region 200nm GaN:Si Source Source 1.3um GaN:UID 0.5um GaN:Fe nucleation substrate (a) Epi 1.3um GaN:UID 0.5um GaN:Fe nucleation substrate Drain (b) Layout Figure 4.1: (a) Epitaxial structure of a HEMT and MESFET and (b) Layout of the test structure UID GaN layer of about 1.3µm as shown in Figure 4.1(a). The device structure on top of this UID GaN consisted of a 200 nm thick Si-doped (5 × 10 17 cm−3 ) GaN channel for MESFETs and a 29 nm thick Al0.22 GaN heterostructure layer for HEMTs. Device fabrication commenced by defining source and drain metallization(Ti/Al/Ni/Au - 20/120/30/50 nm) by lift-off. The samples were annealed at 870 o C in a Rapid Thermal Annealer(RTA) system to achieve alloyed ohmic contacts for source and drain. Devices were then mesa-isolated by etching away the material to about 100 nm below the active channel(300 nm in MESFETs and 130 nm in HEMTs, as shown in Figure 4.3(a,b). Next, Ni/Au/Ni(30/250/50 nm) gates were defined by liftoff metallization followed by the deposition of 120 nm of SiN x by 62 CHAPTER 4. BUFFERLEAKAGE PECVD at 250o C for passivation. Bondpads were then formed by etching away the passivating layer on the contact regions. The transistor layout consisted of a gate with two fingers each of 75µm width as shown in Figure 4.1(b). The gate length was 0.7µm. The Buffer leakage test pattern used the same layout, but without the gate and with the channel between the source-drain contacts etched during the mesa isolation step. Buffer leakage is measured just after the mesa isolation and before the SiNx passsivation process. Higher leakage values were observed after passivation but the trends were preserved. The HEMTs had an Imax ∼1 A/mm, ft ∼20 GHz and fmax ∼50 GHz. 4.3 Effect of Fe-doping level on the buffer leakage The technique of doping the unintentionally-doped(UID) GaN with Fe yields semi-insulating buffer for the GaN transistors. The Fe-doping is believed to introduce traps which affects the high frequency performance of the devices [6]. This drawback is overcome by stopping the Fe-flow after sometime during the growth and growing UID GaN of about 1µm thickness above the Fe-doped GaN buffer. The profile of the Fe has been observed not to be abrupt, exhibiting a tail 63 CHAPTER 4. BUFFERLEAKAGE 600 Voltage @ 1mA/mm 500 buffleak 3t-BD bp 400 300 200 Normal Fe 1/4 Fe 1/10 Fe 1/40 Fe 100 0 5 10 15 s-d distance(um) 20 Figure 4.2: Effect of Fe-doping level on the buffer leakage and on the breakdown voltage of the HEMTs. into the UID GaN grown subsequent to turning off the Fe-flow [6]. The effect of the concentration of Fe on the buffer leakage was studied. The flow of the Fe-source (normal flow was 26 sccm) was varied in a series of samples. The plot summarises the dependence of buffer leakage on Fe-flow level for various source-drain spacings. The voltage at which the buffer leakage reaches 1mA/mm is taken as a benchmark for comparing values. With increasing source-drain spacing the withstanding voltage under which the leakage can be kept below 1 mA/mm, increased steadily. The withstanding voltage increased with increasing Fe-doping for all the source-drain spacings. After completing 64 CHAPTER 4. BUFFERLEAKAGE the HEMT fabrication the three terminal breakdown voltage of the HEMTs was measured for the samples with different Fe-doping. The breakdown voltage increased with increasing Fe-doping only for devices with shorter spacing [Figure 4.2]. For devices with larger spacing the amount of Fe-doping did not show any consistent difference. 4.4 Effect of ohmic contacts on buffer leakage 4.4.1 Observation of differences in buffer leakage It was observed that for the same underlying GaN epitaxial growth, the buffer leakage for the HEMTs was higher than MESFETs [Figure 4.3(a,b,c)]. To investigate whether this difference comes from the epitaxial growth of the AlGaN heterostructure or due to the characteristics of device processing, a controlled experiment was performed, in which a MESFET with a thin channel of 30 nm was grown, imitating a HEMT with respect to the distance of the surface to the buffer. This thin-MESFET had a higher buffer leakage [Figure 4.3(b,c,d)] compared to the MESFET with thick channel, thus eliminating the heterostructure 65 CHAPTER 4. BUFFERLEAKAGE Drain Source 130 nm 29nm AlGaN 3.4 um Drain 300 nm 3.4 um Source 200nm GaN:Si 2Deg GaN:UID GaN:UID (b) MESFET (a) HEMT hemt 600µ Drain 130 nm 1m 800µ 3.4 um thin mesfet recessed mesfet 30nm GaN:Si GaN:UID (d) Thin-MESFET 400µ mesfet 0 0 20 40 60 80 Vds (V) (c) Buffer Leakage Source 160 nm 3.4 um 200µ 300 nm BufferLeakage (A/mm) Source Drain 100 200nm GaN:Si GaN:UID (e) Recessed-ohmic MESFET Figure 4.3: (a)HEMT (b)MESFET (with normal surface ohmics) (c)Buffer Leakage for various device structures with identical underlying buffer (d)Thinchannel MESFET imitating HEMT in channel distance (e)MESFET with recessed ohmics growth as a reason. To identify the characteristic of device processing which is causing this difference, the impact of alloying on the semiconductor was studied. This was done by etching away the alloyed metal and scanning the resulting surface with Atomic Force Microscopy (AFM). The etch was performed by dipping the sample in two solutions (HF:HNO3 =1:1) and (HCl:HNO3 =3:1 aqua regia) alternately for varying periods of time, until all the alloyed metal has been etched away. The 66 0 -50 -100 Height (nm) 50 CHAPTER 4. BUFFERLEAKAGE 0 2 4 6 8 Scan length (um) 10 2 4 6 8 Scan length (um) 10 0 -50 -100 Height (nm) 50 (a) HEMT 0 (b) MESFET Figure 4.4: Optical microscope picture and AFM scan-section(10µm) of the ohmic regions after stripping the alloyed metals a) HEMTs b) MESFETs. The scan for the HEMTs show upto 100 nm deep pits after the removal of the alloyed metal. In MESFETs though deep spikes are absent there are smaller peaks and the alloy reaction proceeds to a depth of about 25∼30 nm into GaN. optical picture of the resulting surface is presented in Figure 4.4. In the HEMTs a trace of the ohmic regions could be seen due to the uneven morphology of the resulting semiconductor surface. In the MESFETs the trace of the ohmic regions was barely visible. The resulting surface when scanned with AFM reflected the morphology of the alloyed reaction into the semiconductor as only the alloyed regions were 67 CHAPTER 4. BUFFERLEAKAGE Drain Source 29nm AlGaN 3.4 um Drain 300 nm 3.4 um 130 nm Source 200nm GaN:Si 2Deg GaN:UID GaN:UID (b) MESFET (a) HEMT 3.4 um 30nm GaN:Si Source 160 nm Drain 300 nm 130 nm Source 3.4 um Drain GaN:UID GaN:UID (c) Thin-MESFET 200nm GaN:Si (d) Recessed-ohmic MESFET Figure 4.5: Morphology of the ohmic contacts explains the difference in buffer leakage in (a)HEMTs (b)MESFETs (with normal surface ohmics) (c)thin MESFETs imitating the HEMTs (d)MESFETs with recessed ohmics. In HEMTs the deep spikes are not screened by the 2DEG. In MESFETs deep spikes are absent but there are smaller sharp projections and these are screened well by the Si doping only in the case of mesfet with surface ohmics. etched in the acid. In the case of HEMTs 100 nm deep pits were observed with spiky features [Figure 4.4(a)]. These spiky features could correspond either to the physical spiking down of the alloyed metal or due to the change in the crystalline material in those pits which leads to it being etched away by the alloy-etch solutions. In MESFETs no deep pits were observed in all the cases studied and the alloyed reaction proceeded in a seemingly uniform manner to a depth of about 25 ∼ 30 nm into the GaN with shallow pits [Figure 4.4(b)]. 68 CHAPTER 4. BUFFERLEAKAGE 4.4.2 Interpretation of Electrical data To interpret the electrical data, another controlled experiment was performed in which the distance between the ohmic metals and the bottom edge of the thick channel of the MESFET was varied. This was done by recessing the ohmic regions after ohmic lithography in a portion of the wafer. The RIE recess etch removed about 160 nm of the channel which was originally grown to be 200 nm thick. The buffer leakage of the devices with normal surface-ohmics and the devices with recessed-ohmics were compared [Figure 4.3(b)(e)]. The devices with recessed-ohmics had a higher buffer leakage than the devices with ohmics deposited on the surface. The higher buffer leakage current in the HEMTs compared to the MESFETs can be explained as follows. It is plausible that the electric field lines concentrate at the spikes due to the lack of screening from the 2DEG [Figure 4.5(a)]. This field acts on the material that is within and in the vicinity of the spikes which could be weaker than crystalline GaN. Hence local injection of carriers into the neighbouring GaN is possible causing the increased buffer leakage. In normal MESFETs the electric field lines do not concentrate because the sharp points 69 CHAPTER 4. BUFFERLEAKAGE from the alloying process are screened by the Si-doping [Figure 4.5(b)]. Hence the reduced buffer leakage in normal MESFETs. Deep spikes are not necessary to cause this effect. Even if deep spikes are absent, the region where the alloy-GaN interface lies has an effect on the buffer leakage. In the case of MESFETs, even though there are no deep spikes like that of the HEMTs, there are smaller sharp points. Depending on whether the alloyGaN interface lies in a doped region or not, it affects the buffer leakage. In the normal MESFET case, the alloy depth of 30 nm is screened by the underlying Si doping layer which seems to remove any local E-field peaking. In the case of the thin-MESFET [Figure 4.5(c)] and in the recessed-ohmic-MESFET [Figure 4.5(d)], the alloy reaction depth of 30 nm makes the alloy-GaN interface to reach the undoped region. Since there is no underlying Si-doping to screen any local E-field peaking at the sharp points, it presumably leads to local avalanche of carriers. 70 CHAPTER 4. BUFFERLEAKAGE 4.4.3 Interpretation for Morphology An interpretation is presented to explain why the deep etched spikes are present only in HEMTs and not in MESFETs. This difference in the alloying behaviour could be either due to the presence of Si dopants in MESFET channel or due to the presence of Al in the AlGaN layer of the HEMT. To study the effect of Si-doping on the morphology of the ohmic contacts, two MESFETs - one with higher doping density of 2 × 10 18 cm−3 than the normal doping of 5 × 1017 cm−3 and another with a lighter doping of 1 × 10 17 cm−3 were processed. An intermediate channel thickness of 60 nm was chosen for these samples to see if this thickness is enough to screen the electric-field. If the presence of Si were to change the behaviour of the alloying reaction, then the alloy depth in channels with different dopings would be expected to be different. This series of samples showed that MESFETs with Si doping of 2 × 10 18 cm−3 and 1 × 1017 cm−3 did not have deep spikes and had a very similar alloying depth of about 25∼30 nm. This implies that the presence of Si did not contribute to the change in morphology of the ohmic alloy. Buffer leakage for both the dopings in these MESFETs of intermediate thickness was comparable to the MESFET 71 CHAPTER 4. BUFFERLEAKAGE with 200 nm thick channel. This shows that a channel thickness of 60 nm and a doping density of 1 × 1017 cm−3 are sufficient to screen the E-field peaks. The presence of deep spikes in the AlGaN/GaN HEMT is reflective of the localized reactions in the AlGaN layer rather than the uniform reaction observed in MESFETs. This could be due to a combination of strain in the AlGaN causing increased reactivity of the dislocations to the alloy-metal stack, and stronger bond-strength of the AlGaN causing reduced reactivity in the non-dislocated regions. The nature of the TDs participating in these enhanced reaction is unclear since the densities of pure-edge TDs and TDs with screw components are each about 5 × 108 cm−2 [8] (AlGaN and GaN layers have the same dislocation densities), whereas the ohmic spike density is about 1 × 10 7 cm−2 . Since the size of the ohmic spikes are typically large (100∼500 nm), it is probable that several dislocations participate in each spiking event explaining the discrepancy in the densities. Further investigation is needed to clarify the mechanism of the ohmic spikes in HEMTs. 72 CHAPTER 4. BUFFERLEAKAGE 4.4.4 Ways to reduce the effect of ohmics on buffer leakage in HEMTs One way in which the spikes in the ohmic alloy in a HEMT were removed was to anneal the ohmic metals in the presence of ammonia gas. This eliminated the spikes under the alloyed ohmic contacts which was confirmed by stripping the ohmic alloy and scanning the surface using AFM. The buffer leakage on these devices was much lower than the devices where the ohmic regions were annealed under normal conditions which result in spiking [Figure 4.6(a)]. The reduced buffer leakage translates to an increase in the breakdown voltage of the HEMTs as shown in Figure 4.6(b). To ensure that the enhancement of breakdown was not a parasitic effect of enhanced dispersion [3][9], pulsed-IV measurements were performed on these devices. The 200 ns pulsed-IV curves were similar for both these HEMTs. Also it should be noted that there were no field-plates on these devices [3]. Though occasionally yielding ohmic contacts to HEMTs without spiky features and thus helping to verify our hypothesis, the ammonia anneal process was not reproducible and neither was a full understanding developed. Techniques 73 CHAPTER 4. BUFFERLEAKAGE 100m Vgs = hemt std. anneal 2m hemt NH 3 anneal 1m -7, -5, -3, -1 (V) 80m Ids (A/mm) BufferLeakage (A/mm) 3m 60m hemt NH3 anneal 40m 20m 0 0 0 20 40 60 80 100 120 0 20 40 60 80 100 120 140 160 Vds (V) Vds (V) Figure 4.6: (a)Buffer Leakage reduced in HEMTs by the removal of spikes in ohmic contacts by using NH 3 during the anneal (b)Breakdown voltage of HEMTs increased from 100 V to about 145 V by the removal of alloy-spikes. such as non-alloyed contacts to n+ cap-layers and implanted regions show more promise and need to be explored. The removal of the effect of alloyed ohmic contacts would lower the buffer leakage in the lateral devices and the vertical leakage in CAVET like vertical GaN transitors [10]. 4.5 Conducting SiC substrate for GaN transistors Doped Silicon Carbide (n-SiC) can be used as a substrate to grow GaN transistors. n-SiC has the advantage that it is available at a much cheaper cost than the 74 Back-to-Front Current (A) CHAPTER 4. BUFFERLEAKAGE 040312FD2 hemt 1m mesfet:Fe 040417AA 040417AB 100µ mesfet:NoFe 10µ 1µ 100n 10n 1n 100p 10p 1p 100f -40 -30 -20 -10 0 10 20 30 BackGate Voltage Vg (V) 1m 100µ 10µ 1µ 100n 10n 1n 100p 10p 1p 100f 40 Figure 4.7: The back-to-front leakage of MESFETs grown on n-SiC substrate is reduced in the presence of HEMTs. However for HEMTs grown with the same buffer as the MESFET with Fe the back-to-front leakage is higher. semi-insulating SiC. Additionally the conducting SiC could be used as a backside field-plate modulating the electric field from the backside [11].The buffer for transistors on such a substrate was investigated. To characterize the buffer grown on n-SiC, the leakage from backside-tofrontside was measured. This was done by placing a dot of Indium metal on the backside along the edges to make contact and the leakage between this backside gate and the frontside ohmic contact was measured. A controlled experiment was done to study the effect of Fe on the back-to-front leakage [Figure 4.7]. 75 CHAPTER 4. BUFFERLEAKAGE PULSED IV 30 0.6 Vg = +1V del Vg= -1V 0.4 0.2 0.0 Pout Gt 25 2 4 6 8 10 Drain Voltage (V) 30 PAE 15 20 10 10 5 4GHz; Vds=30V; Wg=150um 0 12 50 40 20 0 0 5.1 W/mm Eff 0.8 200ns 80us dc Pout (dBm), Gt (dB) Drain Current (A/mm) 1.0 5 10 15 Pin (dBm) 0 20 Figure 4.8: Pulsed-IV curves of HEMTs grown on n-SiC show slight dispersion at 50ohm load-line. Load-Pull power measurements at 4 GHz done on this sample showed a power density of 5 W/mm Two MESFET samples were grown on n-SiC substrate with an identical epitaxial structure except that in one sample the Fe in the buffer was absent. This experiment showed that the presence of Fe reduces the back-to-front leakage by three orders of magnitude[Figure 4.7]. A HEMT sample grown with this amount of Fe-doping in the buffer had a back-to-front leakage similar to that of the MESFET without Fe. The buffer leakage of this HEMT structure was about 1mA/mm at 55 V. The fabricated HEMT showed IV-characteristics similar to the HEMTs grown on semi-insulating SiC. The pulsed-IV curves show slight dispersion [Figure 4.8]. These devices were 76 CHAPTER 4. BUFFERLEAKAGE -40 2.0m BufferLeakage (A/mm) BacktoFront Current (A) MOCVD anneal std.RTA anneal 100µ 10µ 1µ -20 0 20 40 HEMT on n-SiC (ohmics without spikes) 1.5m 1.0m 500.0µ 0.0 0 60 20 40 60 80 100 120 Vds (V) BackGate Voltage (V) Figure 4.9: Buffer Leakage reduced in HEMTs grown on n-SiC susbstrate by the removal of spikes in ohmic contacts by using NH 3 during the anneal. The contacts made on this sample however were not fully ohmic and had slight nonlinearity made with normal gates where the passivation is done after the gate metal deposition. Power measurements done at 4 GHz yielded a maximum power of 5.1 W/mm at a bias of Vds=30 V [Figure 4.8]. After understanding the effect of ohmic contacts on buffer leakage, the effect of alloyed ohmic spikes on back-to-front leakage was studied. A HEMT grown on n-SiC was fabricated by annealing the ohmic contacts in the MOCVD chamber in the presence of ammonia. The back-to-front leakage was compared with the devices on a control piece annealed by the standard RTA anneal process. 77 CHAPTER 4. BUFFERLEAKAGE The sample annealed in MOCVD chamber was not ohmic as it was difficult to obtain ohmic contacts without spikes in a repeatable fashion. The back-to-front leakage is reduced in the sample that had no spikes in the ohmic contacts as shown in Figure 4.9. The buffer leakage on this sample also reduced to a value of 1 mA/mm at 100 V [Figure 4.9]. 4.6 Summary The leakage occuring in the buffer region of the GaN transistors was studied. The buffer leakage is reduced by increasing the concentration of Fe-flow during the growth. The spikes in the ohmic contacts were identified as another source of the buffer leakage. Conducting SiC substrate was tried as the substrate for growing AlGaN/GaN HEMTs and performance similar to the HEMTs on the Semi-Insulating SiC substrate was obtained at 4 GHz. References [1] A. Chini, D. Buttari, R. Coffie, L. Shen, S. Heikman, A. Chakraborty, S. Keller, and U. K. Mishra, “Power and linearity characteristics of field-plated recessed-gate AlGaN-GaN HEMTs”. IEEE Electron Device Letters, vol 25, pp 229-231, May 2004. [2] Y.-F. Wu, A. Saxler, M. Moore, R. P. Smith, S. Sheppard, P. M. Chavarkar, T. 78 CHAPTER 4. BUFFERLEAKAGE Wisleder, U. K. Mishra, P. Parikh, “30-W/mm GaN HEMTs by field plate optimization”IEEE Electron Device Letters, vol 25, pp 117-119, March 2004. [3] Huili Xing, Y. Dora, A. Chini, S. Heikman, S. Keller, U. K. Mishra, “High breakdown voltage AlGaN-GaN HEMTs achieved by multiple field plates,” IEEE Electron Device Letters, vol 25, no 4, pp 161-163, April 2004. [4] Naiqian Zhang , “High Voltage GaN HEMTs with Low on-resistance for Switching Applications”. PhD thesis, University of California, Santa Barbara, 2002. [5] C. Wetzel, T. Suski, J.W.Ager III, E. R. Weber, E. E. Haller, S. Fischer, B. K. Meyer, R. J. Molnar, P. Perlin, “Pressure induced deep gap state of oxygen in GaN”. Physical Review Letters, vol 78, pp 3923-3926, May 1997. [6] S. Heikman, S. Keller, S. P. DenBaars, U. K. Mishra,“Growth of Fe doped semi-insulating GaN by metalorganic chemical vapor deposition”. Applied Physics Letters, vol 81, pp 439-441, July 2002. [7] C. Poblenz, P. Waltereit, S. Rajan, S. Heikman, U. K. Mishra, J. S. Speck,“Effect of carbon doping on buffer leakage in AlGaN/GaN high electron mobility transistors”. J. Vac. Sci. Technol. B, vol 22(3), pp 1145-1149, May 2004. [8] X. H. Wu, L. M. Brown, D. Kapolnek, S. Keller, B. Keller, S. P. DenBaars and J. S. Speck,“Defect structure of metal-organic chemical vapor deposition-grown epitaxial (0001) GaN/Al2 O3 ”, J. Appl. Phys., vol 80(6), pp 3228, Sep 1996. [9] R. Vetury, N. Q. Zhang, S. Keller, and U. K. Mishra,“The impact of surface states on the DC and RF characteristics of AlGaN/GaN HFETs”. IEEE Electron Device Letters, vol 48, pp 560-566, March 2001. [10] Ilan Ben-Yaacov , “AlGaN/GaN Current Aperture Vertical Electron Transistors”. PhD thesis, University of California, Santa Barbara, 2004. [11] W. Saito, Y. Takada, M. Kuraguchi, K. Tsuda, T. Omura, T. Ogura,“600V AlGaN/GaN power-HEMT: design, fabrication and demonstration on high voltage DC-DC converter”. Electron Devices Meeting, 2003. IEDM ’03 Technical Digest. IEEE International, vol., no.pp. 23.7.1- 23.7.4, 8-10 Dec. 2003 79 5 Kilo-Volt breakdown voltage devices and wide periphery devices 5.1 Introduction T he use of multiple field-plates to achieve higher breakdown voltage was demonstrated in Chapter 2. This chapter presents an improved processing technique to achieve the effect of multiple field-plates. This processing technique involves realizing the multiple field-plates as fabricated in a self-aligned fashion with the gate. This chapter also presents some of the issues identified in measuring breakdown voltage. Also presented are wide-periphery devices with high current capacity fabricated by the flip-chip process. The results of the devices made by the flip-chip process are presented. 80 CHAPTER 5. KILO-VOLT DEVICES 5.2 Trench gate process : Self-aligned field-plates Chapter 2 showed the use of multiple field-plates in increasing the breakdown voltage of the devices. In those devices the passivation is done after the gate and the field-plates were achieved by shifting the gate lithography after each dielectric deposition step. An improved processing technique, referred as ‘trench gate process’, was identified which yeilded not only better passivation but also the ability to obtain field-plates self-aligned with the gate. This improved process involves doing the SiNx passivation step before the gate step. Trenches defined by the gate lithography were etched in the SiNx passivation layer using CF4 /O2 RIE system. Using the same lithography gate metal was deposited in the trenches by E-beam evaporation. 5.2.1 Controlling the profile of the trench The gate lithography was achieved by using a double-layer photoresist (Appendix C) which yielded a lift-off profile with significant overhang. Due to this profile of the lithography, the flux reactive ions in the RIE in the normal direction leads to a higher etch rate for the SiNx lying under the opening of the 81 CHAPTER 5. KILO-VOLT DEVICES 100 -50 -100 0 150 200 AFM scan of the trench (trench zoomed-in) 50 0 Height (nm) Height (nm) 100 direct angled angled ion flux -50 100 1 2 3 4 Distance (um) drain ohmics GaN GaN trench SiN x AlGaN AlGaN 0 SiN x SiN x Source 50 source ohmics 0.3um Height (nm) 0.7 um Drain Source PR2 PR1 AFM scan of the trench 150 double-layer PhotoResist 5 AFM scan of the trench Profile of trench wall in x:y=1:1 scale 0 -100 -100 1000 1500 2000 2500 Distance (nm) -200 2200 3000 2300 2400 2500 Distance (nm) 2600 Figure 5.1: Schematic of the double layer photoresist used and the AFM scan of the trench etched in the SiNx passivation layer. lithography. The SiNx lying underneath the overhang of the liftoff profile sees a lower flux of the reactive ions coming at an angle to the normal and hence has a lower etch rate. This leads to a step-like profile of the etched trench. By varying the chamber pressure in the RIE the flux of the ions in directions other than the normal can be varied. Lower pressures (<5 mT) leads to a flux mostly in the normal direction giving a vertical wall of the etch without any significant etch of 82 CHAPTER 5. KILO-VOLT DEVICES the SiNx beneath the overhang regions. However it should be noted that at very low pressures (<2 mT) the etch rate is also significantly reduced and also it is difficult to obtain a sustainable plasma in RIE3 system at UCSB-Nanofab used for this experiment. At higher chamber pressures (∼20 mT) there is a significant flux in the directions other than the normal direction which leads to a significant etch of the SiNx beneath the overhang regions. This yields a step-like profile of the etched trench as shown in the AFM scans [Figure 5.1]. These scans were done by stripping the photoresist after the trench etch to show the profile of the trench that will be exposed to the metal evaporation. 5.2.2 Controlling the field-plate extension The gate metal evaporation is done in a E-beam evaporator. The sample is loaded in a rotating chuck whose surface is kept at an angle to the direction of the incident metal flux. Since there is an overhang of the liftoff profile of the photoresist, the angled evaporation enables the gate metal to cover the sidewall of the etched trenches. This yields a field-plate self-aligned with the gate in a single process step. By changing the angle of the chuck with respect to the 83 CHAPTER 5. KILO-VOLT DEVICES Figure 5.2: SEM picture shows the metal evaporated at an angle to the normal on the sample mounted on a rotating chuck. The trench gate metal covers the step in the etched trench yielding a field-plate self-aligned with the gate. direction of the incident flux the extension of the self-aligned field-plate could be changed. For an angle of about 10∼15 degrees and a photoresist height of 1.8µm a field-plate extension of about 0.2µm can be expected. Figure 5.2 shows an extension of about 0.2µm measured using an SEM. It should be noted that the angled evaporation done on the sample on a rotating 84 CHAPTER 5. KILO-VOLT DEVICES chuck leads to a field-plate extension on the source-side too. This contributes to an increase in the gate-source capacitance leading to a slight reduction in f t and fmax . One way to avoid the source-side extension is to do metal evaporation on a chuck at normal angle and then to repeat the evaporation again on a chuck at an angle oriented towards the drain and without rotation. However this approach is not suitable to device layouts with interdigitated source-drain fingers where the source and drain alternately serve two branches in both directions and also not suitable to any closed geometry devices like circular layouts and winding gate layouts. However the beneficial effects of the source-side extension of the field-plate could be understood if one looks at the effect of the surface states in the source-side on dispersion. The effect of surface states in the source-side on dispersion is presented in the next section. 5.2.3 The Effect of Source-side dispersion To study the effect of the surface states in the source-side on dispersion the effect of surface states in the drain-side needs to be decoupled or removed. A controlled experiment was performed in which the angle of the evaporation of 85 CHAPTER 5. KILO-VOLT DEVICES drain-side disp. SiNx source-side disp. Drain 200 GaN GaN 0 PULSED IV 800 600 200ns 80us dc MaxVg = 1V del Vg= -1V 400 200 0 0 2 4 SiNx GaN Drain Current (mA/mm) Drain Current (mA/mm) 400 Gate Gate Source AlGaN MaxVg = 1V del Vg= -1V 600 Drain AlGaN 200ns 80us dc 800 SiNx AlGaN PULSED IV 1k Gate Source Trench gate 6 8 10 12 14 16 Drain Voltage (V) Drain PULSED IV Drain Current (mA/mm) Source Gate 800 600 200ns 80us dc MaxVg = 1V del Vg= -1V 400 200 0 0 2 4 6 8 10 12 14 16 Drain Voltage (V) 0 2 4 6 8 10 12 14 16 Drain Voltage (V) Figure 5.3: The schematic of the devices used in the controlled experiment to study the effect of source-side dispersion. the metal for the trench gates were controlled. After etching the trench, metal evaporation was done on a few dies (shadow masking the rest) with the sample loaded on a non-rotating chuck with metal flux oriented towards the drian-side. This yielded devices with dispersion only on source-side. The metal evaporation was repeated on few other dies (shadow masking the rest) with the sample loaded on a non-rotating chuck with metal flux oriented towards the source-side. This yielded devices with dispersion only on the drain-side. The metal evaporation was repeated on a few other control dies (shadow masking the rest) with the sample loaded on a rotating chuck with an angle of about 10 degrees to the 86 CHAPTER 5. KILO-VOLT DEVICES d drain-side disp. Gate Source SiNx Rsc Drain velocity saturation GaN delayed space-charge region Gate Source di AlGaN SiNx Drain AlGaN g space-charge region GaN si Drain Current (mA/mm) Drain Current (mA/mm) MaxVg = 1V del Vg= -1V 600 Rsc s PULSED IV 200ns 80us dc 800 g velocity saturation s PULSED IV 1k d source-side disp. 400 200 0 800 600 200ns 80us dc MaxVg = 1V del Vg= -1V 400 200 0 0 2 4 6 8 10 12 14 16 Drain Voltage (V) 0 2 4 6 8 10 12 14 16 Drain Voltage (V) Figure 5.4: Explanation for IV-curves of devices with dispersion on drain-side only and source-side only. The equivalent circuit model is also shown. direction to the flux. This yielded devices with field-plate extension on both sides and therefore devices with practically no dispersion to yield contol data. The pulsed-IV curves of these devices are presented in Figure 5.3. The devices with dispersion only on the drain-side shows significant knee-walkout and increased Ron due to increased access resistance. The devices with dispersion only on the source-side shows increased Ron due to increased access resistance. These devices do not show knee-walkout. The control devices with field-plate 87 CHAPTER 5. KILO-VOLT DEVICES extension on both sides have the 200 ns pulsed-IV curves matching the DC-IV curves. Current saturation in a Field Effect Transistor is caused by the channel pinchoff near the gate-drain edge and the velocity saturation of the electrons happening there. The current gets saturated after this drain voltage which is referred to as ‘knee voltage’. During dispersion the charging-up of surface states causes the channel below those surface states to be depleted leading to the formation of a space-charge region [1]. In a device with drain-side dispersion, this spacecharge region comes between the gate and the drain. The applied drain bias is partially dropped across this space-charge region leading to lower intrinsic drain bias. The gate-drain pinch-off is delayed due to the voltage drop at the spacecharge region and is no longer sharp with the applied drain bias. In other words, the space-charge region in this case leads not only to increased access resistance but also to the knee-voltage walkout. An equivalent circuit model representing this is shown in Figure 5.4. In a device with source-side dispersion, this spacecharge region does not come between the gate and the drain. The applied drain bias, after accomodating the low channel resistance(∼500 ohms-square), is seen by the channel below the gate. This leads to sharp gate-drain pinch-off and hence 88 CHAPTER 5. KILO-VOLT DEVICES an abrupt knee voltage. The space-charge region appears between the gate and the source causing an increased source access resistance and a reduced gm . In other words, the space-charge region in this case leads only to the increased access resistance but not to the knee-voltage walkout. An equivalent circuit model representing this is shown in Figure 5.4. This controlled experiment shows that the surface states on the source-side contribute to the increase in access resistance. If a slight reduction of frequency can be tolerated it would be beneficial to have field-plate extension on the sourceside too. 5.2.4 Frequency response of the trench-gates The small signal performance of the devices with trench gates are presented in Figure 5.5. These devices had field-plate extension on both sides. The measured ft and fmax of these devices are 18.5 GHz and 64 GHz. The pulsed-IV measurements performed at loadline of 50ohms showed no dispersion. The pulsedIV measurements done at a higher loadline of 165ohms also showed insignificant dispersion [Figure 5.5]. The load-pull power measurements done at 4 GHz 89 CHAPTER 5. KILO-VOLT DEVICES 100 Magnitude 10 Drain Current (mA/mm) pulsed IV curves |h21| |U| 1 ft=18.5 GHz fmax=64 GHz 0.1 100M 800 200ns 50ohmLL 200ns 165ohmLL dc 600 MaxVg = 1V del Vg= -1V 1k 400 200 0 1G 10G Frequency (Hz) 100G 0 5 10 15 20 25 Drain Voltage (V) 30 Figure 5.5: Small signal measurements show an f t =18.5 GHz and fmax =64 GHz. The large signal 200 ns pulsed-IV measurements show no dispersion at 50 ohms. At a higher loadline of 165 ohms there is little dispersion. yielded a power density of 6.7 W/mm and a power-added-efficiency of 64% at a bias of 35 V [Figure 5.6]. This is comparable to the values (6.3 W/mm) reported by Chini et al. at a bias of 30 V [2]. At a higher drain bias of 55 V the device yielded a power density of 8.8 W/mm and power-added-efficiency of 48% [Figure 5.6]. 90 CHAPTER 5. KILO-VOLT DEVICES 60 6.7 50 W/mm 25 PAE 40 20 Pout (dBm), Gt (dB) 30 35 70 30 15 20 4GHz; Vds=35V; Wg=200um 10 0 5 10 30 60 50 48% 40 25 PAE 30 20 20 15 10 4GHz ; Vds=55V; Wg=200um 10 10 15 8.8W/mm Pout Gt Eff (%) 64% Pout Gt Eff Pout (dBm), Gt (dB) 35 0 5 10 15 0 20 Pin (dBm) Pin (dBm) Figure 5.6: The load-pull power measurements done at 4GHz shows high power densities. This confirms that the devices with trench gates have good high frequency large signal behaviour. 5.3 Kilo-Volt breakdown voltage devices High breakdown voltage of up to 900 V was achieved in AlGaN/GaN HEMTs by using multiple field-plates as was described in Chapter 2. However HEMTs made on other wafers did not show such a high breakdown voltage. Even with the aid of a number of field-plates (two to four), the devices tend to break at about 500 V. The breakdown voltage occasionally was about 800 V on devices made on some samples but it was not repeatable. This behaviour suggested that there is a parasitic element that breaks down before the intrinsic device breakdown has been reached. This prompted an investigation to identify the parasitic element in 91 CHAPTER 5. KILO-VOLT DEVICES Figure 5.7: The effect of etched mesa wall on breakdown was studied. The device on left shows the gate feed at the mesa wall susceptible to electric field lines terminating on it; With a layout on the right, the gate feed climbs at the mesa wall at the backside so that the electric field lines terminating on it remains limited once the 2-DEG is depleted on the side. the device which is causing the premature breakdown. 5.3.1 Identifying the parasitic breakdown The HEMT fabrication involved either laying down the gates after the mesa isolation etch or laying down the trench gates after the mesa isolation etch. In both of these processes the feed-line of the gate and the gate bond-pad lie not on the AlGaN but on the GaN which is exposed by the mesa-isolation etch. To check whether this MESFET-like parasitic part of the device is causing the 92 CHAPTER 5. KILO-VOLT DEVICES breakdown, the etched mesa regions were filled with SiOx dielectric. This was done by the E-beam evaporation of SiOx after the mesa isolation etch. The evaporation was done by a liftoff process using the same mesa lithography in a selfaligned fashion. This change in the process did not lead to an improvement in the breakdown voltage. This confirms that the feed regions are not causing the premature breakdown. This also confirms the expectation that the peak electric field on the gate feed line should be low because the GaN beneath it is un-itentionally doped. This UID-GaN has almost no carriers and the depletion region has to be quite wide leading to low electric field peak at the feed line. The HEMT process used involves using mesa etch for device isolation. The gate feed runs in the etched regions and climbs over the wall of the mesa to continue as the gate in the active region of the device. The wall of the mesa where the gate feed climbs over was suspected as a possible cause of premature breakdown. In order to reduce the magniturde of the electric field lines terminating on the gate feed at the mesa wall, the gate feed was made to climb over the wall far behind the active region of the device as shown in Figure 5.7. By doing this though there was improvement on some devices (up to V br =800 V), the breakdown voltage was not uniform over many devices and the devices would not 93 CHAPTER 5. KILO-VOLT DEVICES reach 1 kV even with four field-plates. The air which surrounds the fabricated device during the breakdown voltage measurements was suspected to be triggerring the breakdown beyond a certain drain voltage. A study of various high breakdown voltage measurements that have been reported in the literature was done. Those devices with more than a 1 kV breakdown voltage predominantly have vertical geometry in which the drain is in the back side of the substrate (various DMOS structures). In these devices the semiconductor itself is the dielectric between electrodes at vastly different potentials [3]. Devices on Si with lateral geometry that have been reported with very high breakdown voltage have large source-drain spacing(>70µm) [4][5]. However all the lateral geometry devices on a high bandgap material like SiC have been reported to have been tested with Fluorinert, though it is never stated why it is so [6]. Testing the fabricated AlGaN/GaN HEMTs immersed in the inert liquid called Fluorinert (FC-77) showed that the devices could withstand more than a 1 kV on the drain. These breakdown voltage results were consistent and reproducible. 94 CHAPTER 5. KILO-VOLT DEVICES Figure 5.8: With devices immersed in Fluorinert liquid a breakdown voltage of 1400 V was measured on a device with trench gates and Lgd =15µm, Lg =1µm, Lsg =1µm, Wg =200µm. 5.3.2 Kilo-Volt breakdown measurements AlGaN/GaN HEMTs immersed in the Fluorinert liquid could reach a breakdown voltage of more than a kilovolt [Figure 5.8]. These devices were made with the trench-gate process where the self-aligned field-plate (shift=0.25µm) and the gate are achieved in a single process step as was shown in §5.2. This means that the trench gate is sufficient to obtain such high breakdown voltages. These measurements were repeatable and these results were consistently obtained over dif- 95 CHAPTER 5. KILO-VOLT DEVICES 2000 OFF-state IV curves Trenchgates withF Trenchgates withoutF Beforepassiv withF 1800 1600 20.0m Vbr = (86.7 * Lgd) - 3.7 1200 Vbr (V) Vgs = -7V to -1V delVgs = +2V 15.0m Current (A) 1400 1000 800 600 10.0m 5.0m 400 200 0.0 0 0 5 10 15 20 0 400 800 1200 1600 2000 Voltage (V) Lgd (um) Figure 5.9: The breakdown voltage versus Lgd measured with and without Fluorinert at various process steps. Lsg =1µm; Lg =1µm; Wg =200µm. ferent processing runs. Furthermore, the breakdown voltage increased linearly with increasing gate-drain spacing. 5.4 What is limiting the breakdown voltage ? Gate leakage was thought to be critical and limiting the breakdown voltage as reported by Zhang et al. [7]. Based on that work it was believed that the presence of a gate dielectric is critical to achieve a kilo-volt breakdown voltage in AlGaN/GaN HEMTs. But it is shown in this work that even for high gate 96 CHAPTER 5. KILO-VOLT DEVICES leakage values of 1 mA/mm, a kilo-volt was obtained with trench gates and with device immersed in Fluorinert. To explain the high breakdown voltage results and to study the limits of breakdown voltage in AlGaN/GaN HEMTs a device fabrication run was carried out in which the breakdown voltage was monitored in the presence of Fluorinert after each process step. The breakdown voltage of devices before passivation measured in the presence of Fluorinert followed a linear increase with Lgd spacing [Figure 5.9]. Without fluorinert the breakdown voltage was limited to a maximum of about 400∼500 V. After passivation the breakdown voltage measured in the presence of Fluorinert showed a reduced breakdown voltage to which the presence or absence of fluorinert did not make a difference. After passivation the devices with trench gates measured with Fluorinert showed a linear increase in breakdown voltage [Figure 5.9]. Without Fluorinert the breakdown voltage in these devices gets clamped around 500 V [Figure 5.9]. The results of this experiment can be summarized as follows. If the peak electric field is not alleviated the devices break early whether they are in the presence of air or fluorinert. If the peak electric field at the drain edge of the gate is alleviated either by surface states before passivation or by the using the trench 97 CHAPTER 5. KILO-VOLT DEVICES gates which provide an integrated field-plate, the breakdown follows a linear trend as shown in linear fit in Figure 5.9. From this linear trend, supposing that the electric field is constant between the gate and drain an electric field strength of 86 V/µm∼0.86 MV/cm could be calculated. Given that the breakdown field strength of GaN is about 3 MV/cm, these devices could be at the inherent limits of the material system involved. To determine if the parasitic breakdown of the Fluorinert liquid is yielding this linear trend, metal pads with varying spacings were deposited on an insulating sapphire substrate. In the presence of Fluorinert, the metal pads could be biased to 1600 V for a 4µm spacing and more than 2000 V for spacings greater than 7µm. The breakdown voltages of the devices with these spacings [Figure 5.9] are much lower than these numbers, thereby eliminating the parasitic breakdown of Fluorinert. The linear trend in the results could be due to the depletion region extending and reaching the drain contacts [8]. As seen in §4.3, the Fe-doping level seems to change the slope of the Vbr vs. Lgd . The linear trend in the results could also be possible if the Fe-doped buffer underneath the device is reaching its limits of insulating behaviour. A controlled experiment was done to see the effect of Lsg spacing on break- 98 CHAPTER 5. KILO-VOLT DEVICES 2000 Trenchgates withF Trenchgates withoutF Beforepassiv withF 1800 1600 Vbr = (86.7 * Lgd) - 3.7 1400 Vbr (V) 1200 2_1_14 1000 4_1_12 800 600 400 200 0 0 5 10 15 20 Lgd (um) Figure 5.10: The breakdown voltage reduced with increasing L sg spacing. On a device with fixed Lsd =17µm, by keeping Lsg =2µm and 4µm respectively, the Lgd becomes 14µm and 12µm. The reduced breakdown voltage fits into the V br vs. Lgd linear fit. This shows that Lsg spacing does not affect breakdown voltage. down voltage. The gate lithography was shifted on a device with fixed L sd =15µm by 1µm and 3µm respectively. This yielded devices with L sg -Lg -Lgd spacings of 2-1-14µm and 4-1-12µm respectively. The breakdown voltage of these devices were lower than the device with normal 1-1-15µm spacing. However these values fit into the linear plot of the Vbr vs. Lgd plot [Figure 5.10]. This shows that the reduction in breakdown voltage is due to the reduction in L gd spacing and 99 CHAPTER 5. KILO-VOLT DEVICES the increase in the Lsg spacing did not affect breakdown voltage. An experiment to probe this issue further was done in which the fabricated device was covered with 1µm thick dielectric (ICP deposited SiOx ). Covering the device with this dielectric showed no change in the breakdown voltage in the presence of Fluorinert, indicating that an appropriate passivation to ultimately eliminate the need for Fluorinert needs to be pursued. 5.5 Wide periphery devices Devices with wide-periphery and hence large current capacity were made to do switching measurements in an actual power converter-like environment and also to eventually incorporate them into a switched power converter module. The first generation devices had a linear geometry with 1∼2 mm wide active region. Many such devices were wirebonded to get a wider device (up to 5.5 mm wide) with a current capacity of 5 A. However combining such discrete devices by wirebonding posed difficulties. The reliability of the wirebonds was an issue and the access resistance was limited by the wirebonds themselves. In the next generation devices, twenty short (500µm) device fingers were 100 CHAPTER 5. KILO-VOLT DEVICES Figure 5.11: Wide periphery(10mm) device with interdigitated fingers. The source fingers get connected during the flip-chip bonding. made adjacent to each other. The drain contacts of the fingers were tied together at one side. The interdigitated gate feeds of the fingers were tied at the opposite side. The source fingers were brought out at the gate feed side to be connected. The source connections need to be made by crossing over the gate feeds either by dielectric/air bridges or by external connections like wirebonds or flip-chip bonding. The bond pads on source and drain contacts were made of 6µm thick Au deposited by Ebeam. The contact patterns on the flip-chip substrate also had 101 CHAPTER 5. KILO-VOLT DEVICES 6µm thick Au pads which after bonding leads to 12µm thick metal connections. The details for the flip-chip process are given in apendix-C. The flip-chip process has an additional advantage in that the flip-chip substrate provides an additional heat sink to the device [9]. Also if AlGaN/GaN HEMTs were grown on cheaper substrates like Si which has low thermal conductivity, doing a flip-chip bond of the device onto a substrate with higher thermal conductivity would enhance the thermal budget of the device. Also since the flip-chip substrate gives mechanical support the original substrate could be lapped and thinned to enhance the thermal conduction if a double-sided heat sink were implemented. The layout used for the flip-chip devices is show in Figure 5.11. The source and drain pad lengths were intentionally kept longer (about 50µm) because of the alignment tolerance of the flip-chip bonder at UCSB-Nanofab which is +/10µm. This increased the die area by a large factor. If the bondpad dimensions were optimized it would lead to reduction in the die size by atleast four times. The actual die area of the completed device is shown in Figure 5.11. The device has 20 interdigitated fingers of 500µm width contributing to a total width of 10 mm and hence a current capacity of 10 A. The electrodes are brought out into wide area metal pads which enable easy wirebonding. These pads are wide 102 CHAPTER 5. KILO-VOLT DEVICES enough so that the device can be soldered directly to the contacts of a switching test set-up or a power converter module. Many such compact modules could be put together to achieve higher current capacity. 5.6 Summary The chapter presents improvements in the processing of high breakdown voltage devices and in the high voltage measurements. The trench gate technology was observed to have advantages over the standard process for AlGaN/GaN HEMTs. It also allows for obtaining field-plates self-aligned with the gate in a single process step. The parasitic breakdown voltage which was causing the device to break prematurely was identified. Using Fluorinert liquid breakdown voltages of up to 1900 V was measured on AlGaN/GaN HEMTs. Possible reasons which could explain the linear increase of breakdown voltage with L gd spacing was discussed. Wide periphery devices with large current capacity were made. These devices were improved by using the flip-chip technology. 103 CHAPTER 5. KILO-VOLT DEVICES References [1] Robert Coffie , “Characterizing and Suppressing DC-to-RF Dispersion in AlGaN/GaN High Electron Mobility Transistors”. PhD thesis, University of California, Santa Barbara, 2003. [2] A. Chini, D. Buttari, R. Coffie, L. Shen, S. Heikman, A. Chakraborty, S. Keller, and U. K. Mishra, “Power and linearity characteristics of field-plated recessed-gate AlGaN-GaN HEMTs”. IEEE Electron Device Letters, vol 25, pp 229-231, May 2004. [3] A. K. Agarwal, J. B. Casady, L. B. Rowland, S. Seshadri, R. R. Siergiej, W. F. Valek, C. D. Brandt,“700-V asymmetrical 4H-SiC gate turn-off thyristors (GTO’s),”.Electron Device Letters, IEEE, vol.18, no.11pp.518-520, Nov 1997 [4] S. Merchant, E. Arnold, H. Baumgart, R. Egloff, T. Letavic, S. Mukherjee, H. Pein,“Dependence of breakdown voltage on drift length and buried oxide thickness in SOI RESURF LDMOS transistors,”. Power Semiconductor Devices and ICs, 1993. ISPSD ’93. Proceedings of the 5th International Symposium on, pp.124-128, 18-20 May 1993. [5] S. Hardikar, R. Tadikonda, D. W. Green, K. V. Vershinin, E. M. S. Narayanan,“Realizing high-voltage junction isolated LDMOS transistors with variation in lateral doping,”. Electron Devices, IEEE Transactions on , vol.51, no.12pp. 2223- 2228, Dec. 2004. [6] J. Spitz, M. R. Melloch, J. A. Cooper, Jr., M. A. Capano,“2.6 kV 4H-SiC lateral DMOSFETs,”. Electron Device Letters, IEEE, vol.19, no.4pp.100-102, Apr 1998. [7] Naiqian Zhang , “High Voltage GaN HEMTs with Low on-resistance for Switching Applications”. PhD thesis, University of California, Santa Barbara, 2002. [8] W. R. Frensley,“Power-limiting breakdown effects in GaAs MESFET’s,” Electron Devices, IEEE Transactions on , vol.28, no.8, pp. 962- 970, Aug 1981. [9] Jian Xu , “AlGaN/GaN High-Electron-Mobility-Transistors Based Flip-chip Integrated Broadband Power Amplifiers”. PhD thesis, University of California, Santa Barbara, 2000. 104 6 Switching measurements 6.1 The need for switching measurements A lGaN/GaN HEMTs with high breakdown voltages have been demonstrated in Chapters 2 and 5. The breakdown versus speed trade-off is overcome by using field-plates. Using the trench gate process technology, breakdown voltage of kilovolt has been demonstrated. Small signal measurements of devices made with this technology and with a L g =0.7µm showed an ft =18.5 GHz and fmax =64 GHz [Chapter 5]. To characterize the devices for large signal response, pulsed-IV with pulsewidth upto 200 ns were done. The pulsed-IV measurements were done at a 50 ohm load-line upto a bias of 15 V and at a 165 ohm load-line upto a bias of 30 V. For measurements done at 165 ohm load-line the pulsed-IV showed 105 CHAPTER 6. SWITCHING MEASUREMENTS increased dispersion compared to the 50 ohm measurement though still insignificant [Chapter 5]. So it is expected that the pulsed-IV done at larger loadlines typical in switching application may show greater dispersion. However microwave power measurements at 4GHz done on devices with trench gates (Lg =0.7µm) showing a power density of 8.8 W/mm for a V ds bias of 55 V [Chapter 5] indicate that this may not be excessive. Devices with large breakdown voltages operate at a much higher load-lines. These load-lines are usually not purely resistive. For example, in a switched power converter the switching device is subjected to inductive and capacitive loading which leads to non-linear load-lines. To characterize the frequency response of the devices with large breakdown voltages, larger load-lines are needed and dc-power supplies with larger voltage and power capacities are needed. The standard pulsed-IV measurement system could not be used because the dc-power supply used could only go upto 60 V and it could accomodate only resistive loadlines. So the best means to characterize these devices is to have a switching test system imitating the load-lines and the waveforms that the device sees in an actual switching application. This is achieved by having a two-pulse switching setup with inductive load [1][2]. During the first pulse the inductor is charged 106 off-state on-state freewheeling charging CHAPTER 6. SWITCHING MEASUREMENTS Vgs Iind Id Iind Isw Turn on Turn off Isw Id waveforms time Figure 6.1: Schematic of the switching test set-up and the waveforms during different phases of the double-pulse signal with a certain current which is made to free-wheel in a diode. During the second pulse the device under test is subjected to this current. The transient response of the device to this current gives a measure of the high frequency performance of the device. 107 CHAPTER 6. SWITCHING MEASUREMENTS 6.2 Switching setup schematic and waveforms A schematic of the test setup is shown in Figure 6.1. An inductive load is added in series to the switch under test. A free-wheeling diode is connected in parallel to the inductive load to bypass the current in the inductor when the device is in the off-state. A Gate drive circuit controls the Vgs voltage. The switching measurements were done with the help of Dr. Sriram Chandrasekaran and Dr. Vivek Mehrotra at Rockwell Scientific, Thousand Oaks. The various waveforms of the double-pulse switching measurement is as shown in Figure 6.1. In the begining the switch is kept off and the applied dc-bias appears across the device. There is no current in the circuit. When the gate is first turned on during the charging period, the switch conducts (I sw ) and the voltage across the device (Vsw ) drops. As the difference in voltage appears across the inductor the inductor current increases continuously. When the switch is turned-off in the free-wheeling period the current in the inductor is pushed into the free-wheeling diode. The voltage across the switch in this period is the sum of Vdc and Vdiode−drop . The forward voltage drop of the diode (∼0.7V) appears across the inductor and the inductor current falls off slowly. When the switch is 108 CHAPTER 6. SWITCHING MEASUREMENTS turned on again in the on-state period, the inductor current is taken by the switch and voltage across the device falls to Von . Thus a current which was originally established in the circuit is switched by the device from another branch of the circuit to itself. This transistion which imitates the actual transition in a power converter is defined as ’turn-on’. The diode gets reverse biased and undergoes reverse recovery. The current for the reverse recovery passes through the switch. The difference between the Vdc and Von of the device appears across the inductor and the inductor current continuously increases from its original value. At the off-state period the switch is turned-off and the voltage across the switch increases. After the voltage across the switch reaches the sum of Vdc and Vdiode−drop , the diode turns on and the current in the inductor is bypassed into the branch of the circuit with the diode. This transition, defined as ’turn-off’, imitates the actual power converter where the current through the switch is sent into another branch when the switch is turned-off. The inductor current being opposed by the diode-drop slowly decays to zero. 109 CHAPTER 6. SWITCHING MEASUREMENTS 100 V / 570 mA TURN-ON Id 100 60 400 40 300 200 Id 150 600 Vds 200 50 0 -200 100 0 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 Vgs 0 Vgs 0 1.2 400 100 Id (mA) 500 Id (mA) 80 20 800 600 Vgs and Vds (V) Vds Vgs and Vds (V) 100 V / 570 mA TURN-OFF 700 120 0.4 0.6 0.8 1.0 1.2 1.4 1.6 Time (µs) Time (µs) Figure 6.2: The need for compact test setup. Devices probed on dc-probestation showed a lot of ringing. The turn-on and turn-off characterisitic of a 2 mm wide device with two field-plates and Lg=1.5µm, Lgd=15µm. 6.3 The need for compact test setup The preliminary switching measurements were done on devices made with multiple field plates as described in Chapter 2. These devices did not have large bondpads and the bondpads would peel-off during the wirebonding process. So these devices were probed on-wafer with the dc-probe station needles that were connected by bnc-cables to the test setup. These measurements showed a lot of ringing due to the parasitics involved in the probing process. The waveforms of the devices measured in this way is shown in Figure 6.2. The gate pulse did not have fast transitions (turn-on duration was about 0.5µs) due to the parasitics of the cables and probes. 110 CHAPTER 6. SWITCHING MEASUREMENTS V dc Current Sensor Inductor, L gate source High Speed gate driver Capacitor Bank drain Diode, Df GaN HEMT 1 inch Switching signal generator Diced and wirebonded device Figure 6.3: Compact switching test setup and the diced and wirebonded device. A 1.5mm wide device wirebonded to the circuit board is shown. 6.4 Measurements with a compact test setup A compact test setup comprising of the double-pulse signal generator, gate drive circuit, the capacitor bank and switch in series with the inductor and freewheeling diode was designed and built at Rockwell Scientific. The picture of the test setup is shown in Figure 6.3. Dies having the wide devices were diced and wirebonded to the circuit board which interfaces with the test setup as shown in Figure 6.3. This compact test setup with the wirebonded devices enabled the gate transition to less than 50 ns. The gate transition time was verified by doing switching 111 CHAPTER 6. SWITCHING MEASUREMENTS Vds ton 50ns Vgs toff 30ns Vds Vgs Figure 6.4: Gate turn-on and turn-off times verified by resistive loading. Vdc =150 V, Rload =560 ohms, Vgon =2 V, Vgof f =-11 V measurements on the device under resistive loading. A 1mm wide device with Lg=1.5µm, Lgd=15µm with two field-plates was used in this measurement. The turn-on and turn-off characteristic with resistive loading is shown in Figure 6.4. The turn-on gate pulse changes in less than 50 ns and the turn-off gate pulse changes in less than 30 ns. Switching measurements were then done with inductive loading. An inductor of 680µH was used to charge the circuit with current and a Si p-i-n diode (MUR1100E) was used as the free-wheeling diode. A device with Wg =1 mm, Lg=1.5µm, Lgd=15µm and two field-plates was used as the switch for this measurement. The waveforms captured during the duration of the double pulse is 112 CHAPTER 6. SWITCHING MEASUREMENTS 800mA Reverse recovery Turn ON Turn OFF charging isw vsw vg Von increase Figure 6.5: Switching measurements with compact test setup and inductive loading. Wg =1 mm, Lg =1.5µm, Vdc =120 V, Lload =680 µH, Vgon =2V, Vgof f =-11 V shown in Figure 6.5. The switch conducts current during the initial charging period. When the switch is turned off the current through the switch drops to zero and the inductor current is bypassed by the free-wheeling diode. When the switch is turned on again, the current in the free-wheeling circuit is drawn by the device and the V sw drops driving the diode into reverse bias. The reverse bias depletion region of the diode is setup by the reverse recovery current which is carried by the device. 113 CHAPTER 6. SWITCHING MEASUREMENTS Vgs=2v to -10v Isw=2.4A Vsw=150v 20ns Figure 6.6: High current turn-off characteristic shows a turn-off time less than 20 ns, which is still limited by the gate transition speed. W g =5.5 mm, Lg=1.5µm, Vdc =150 V, Lload =680µH, Vgon =2 V, Vgof f =-11 V The sharp peak observed in the current at turn-on is due to the reverse recovery of the diode. Once the reverse depletion region of the diode has been setup, the reverse recovery component of the current goes to zero. The current thereafter carried by the switch is the current that was free-wheeling in the diode. The voltage drop in the inductor continues to increase the current in the switch in the on-state period. When the device is turned-off the current through the device goes to zero and the current setup in the inductor starts to free-wheel through the 114 CHAPTER 6. SWITCHING MEASUREMENTS diode. From the waveforms, turn-on and turn-off times of about 25 ns were observed. The on-state voltage drop across the device was higher than expected. Also the Von increased with increasing current in the device as seen in Figure 6.5. § 6.5.2 discusses the possible reasons for the high values of V on observed in the switching measurements. Switching measurements were also perfomed on devices with high current capacity. Three devices in a die were wirebonded together to achieve a 5.5 mm wide device with a peak current capacity of 5 A. These devices switched a current of 2.4 A at a Vdc=150 V. The turn-off characterisitic is shown in Figure 6.6. The turn-off time was less than 20 ns. The gate transition time was about 20 ns. This shows that the switching speed is still limited by the gate transition and not by the intrinsic performance of the switch. 115 CHAPTER 6. SWITCHING MEASUREMENTS Voltage (V) 25 Vsw 20 Isw 15 3.0 3.0 2.5 2.5 2.0 2.0 1.5 Isw (A) turn-off turn-on Current (A) 30 1.5 10 1.0 5 0.5 0.5 0.0 0.0 0 0 250n 500n 750n turn-on turn-off 1.0 0 1µ time (s) 5 10 15 20 Vsw (V) 25 30 Figure 6.7: The current and voltage waveform cross-over at each transition leads to energy loss. The cross-over of V and I curves during turn-on and turn-off is evident in the I-V locus. The energy loss can be reduced if the switching time is reduced. 6.5 Issues with switching measurements 6.5.1 Gate drive speed As mentioned in §1.1, power switching at higher frequencies is desired because the passive components scale down in size yielding compact power supplies. However, the switching losses increase with frequeny because now there are more transitions for the same time duration. The losses during the switching occur because of the cross-over of the current and voltage waveforms [Fig- 116 CHAPTER 6. SWITCHING MEASUREMENTS Figure 6.8: The schematic block diagram of the gate drive circuit used in the compact switching test setup. ure 6.7]. The energy loss in each switching transistion is given by integrating i(t)×v(t) product with time. To minimize the switching losses the turn-on and turn-off times should be kept as low as possible [3][4]. As observed in the measurements described in the previous section the switching speed is limited by the transition time of the gate drive circuit. The gate driver used for power switching at higher frequency should also be capable of driving the gate as fast as possible. The schematic of the compact gate 117 CHAPTER 6. SWITCHING MEASUREMENTS driver circuit used at Rockwell Scientific is shown in Figure 6.8. The doublepulse signals are generated by a monostable multi-vibrator circuit. The doublepulse signal is coupled by an opto-coupler to an isolated dc-supply for the driver. The opto-coupler also serves to shift the signal levels. The driver consists of a current buffer which is made of npn and pnp structure connected as shown in Figure 6.8. When the gate voltage needs to be increased the npn transistor at the top is turned-on while the pnp transistor at the bottom is turned-off thus causing the gate to charge up. When the gate voltage needs to be decreased the above process is reversed. In order to increase the gate drive speed the a faster optocoupler needs to be used. Or in the place of the optocoupler a faster galvanic isolator can be used. Increasing the slew rate of the transistors in the current buffer would also improve the gate drive speed. 6.5.2 High Von The Von of the switch during the switching measurements was higher than the intrinsic device values. The Von also increased with increasing switching 118 CHAPTER 6. SWITCHING MEASUREMENTS current (Isw ) [Figure 6.5]. The effect of parasitic source-side resistance (Rwb , the wirebond resistance) on Von was investigated. Simulations were done on Agilent’s Advanced Design System (ADS) to see the effect of Rwb on Von . The simulation results are summarized in Figure 6.9. With the increase of current in the transistor the parasitic Rwb decreases the effective Vgs seen by the device leading to the depletion of the channel. This leads to an increase in the voltage drop in the device (both intrinsic V ds and the Vd in the external circuit). This effect gets pronounced especially in the regions close to the saturation region of the FET. The plots of Vgs , Vds , Vd versus Isw with increasing parasitic Rwb parameter is shown in Figure 6.9. Preliminary switching measurements were done on the wide-periphery devices made by flip-chip process. Figure 6.10 shows a high current of 3.6 A switching at 30 V. This measurement was done on a device with L sg =1µm, Lg =1µm, Lgd =5µm. The Imax of this device was about 0.7 A/mm. This device had interdigitated gate fingers in which the source-to-drain regions were oriented in both directions. Since the metal for the trench gates on this device was deposited at a fixed angle, half of the device had source-side dispersion and the other half had the drain-side dispersion. Hence there is a considerable in- 119 CHAPTER 6. SWITCHING MEASUREMENTS Vgs Vd Vds Figure 6.9: ADS simulations of the effect of source side parasitic resistance on Von . Schematic used in the simulation and the parametric plot of V gs , Vds , Vd versus Isw with Rwb as the parasitic wirebond resistance. crease in Von with increasing current [Figure 6.10]. Devices made with proper trench gates by mounting the sample on a rotating chuck would not have this issue. Switching measurements on such devices needs to be done. 6.5.3 Heat sinking the devices Heat-sinking the devices during the switching measurements is also a critical factor. Devices that were initially mounted on Printed circuit board (PCB) with- 120 CHAPTER 6. SWITCHING MEASUREMENTS 40 2 20 1 10 Voltage (V) Isw 0 0 0 250n 500n 750n 5 Imax=4.3A Vsw Current (A) Voltage (V) 50 3 Vsw 30 4 4 30 3 Isw 20 2 10 1 0 1µ 0 0 time (s) Current (A) Imax=3.6A 40 250n 500n 750n 1µ time (s) Figure 6.10: High current switching measurements on devices made with flipchip process. Measured device had Lsg =1µm, Lg =1µm, Lgd =5µm, Wg =10 mm. The device was subjected to Imax =3.6 A and 4.3 A at 30 V and 40 V respectively. out any heat sink broke at an earlier voltage than when they were tested on a metal chuck. For example, devices which withstood a voltage of 550 V when tested on a metal chuck would break at 300 V when mounted on PCBs without any heat sinking. So the compact test setup must incorporate means to heat sink the devices. 121 CHAPTER 6. SWITCHING MEASUREMENTS 6.5.4 Ongoing improvements with switching measurements Work is in progress to build a switching test setup at UCSB. The pulsedIV setup is being modified to enable switching measurements to be done with inductive loads. Preliminary measurements show that gate transition speeds as low as 10 ns can be achieved. The wide-periphery devices made using the flip-chip process have big metal pads coming out on the carrier substrate. This enables them to be mico-soldered directly to the test electrodes instead of using wirebonds. This should reduce the parasitic contact resistance. These devices have a periphery of 10 mm and have a current capacity of 10 A. Many such devices could be put together at the circuit board level to build a high power switching converter. The off-state leakage in the measured devices is about 1 mA/mm. At high voltage operation this leakage leads to heating. Since the duty cycle of devices is usually kept low the device is in the off-state for a major duration of time. This leads to significant leakage losses when the width of the device is increased to reduce the Ron . Devices with the gate regions implanted with Flourine ions has shown reduced gate leakage on microwave and digital-logic transistors. This 122 CHAPTER 6. SWITCHING MEASUREMENTS technology shows promise in making devices with low off-state leakage and should be incoporated in power devices as well. 6.6 Summary The need for the switching measurements to characterize the high breakdown voltage devices was presented. The preliminary measurements showed the need for compact test setup. Using a compact test setup built at Rockwell scientific gate drive speed less than 50 ns was achieved. High current switching measurements performed switched 2.4 A at Vdc=150 V at a turn-off time of less than 20 ns. Various issues with the switching measurements were identified and investigated . References [1] Naiqian Zhang , “High Voltage GaN HEMTs with Low on-resistance for Switching Applications”. PhD thesis, University of California, Santa Barbara, 2002. [2] W. Saito, Y. Takada, M. Kuraguchi, K. Tsuda, T. Omura, T. Ogura,“600V AlGaN/GaN power-HEMT: design, fabrication and demonstration on high voltage DC-DC converter”. Electron Devices Meeting, 2003. IEDM ’03 Technical Digest. IEEE International, vol., no.pp. 23.7.1- 23.7.4, 8-10 Dec. 2003. [3] W. Saito, Y. Takada, M. Kuraguchi, K. Tsuda, I. Omura, T. Ogura, H. Ohashi,“High breakdown voltage AlGaN-GaN power-HEMT design and high 123 CHAPTER 6. SWITCHING MEASUREMENTS current density switching behavior,”.Electron Devices, IEEE Transactions on , vol.50, no.12pp. 2528- 2531, Dec. 2003. [4] W. Saito, M. Kuraguchi, Y. Takada, K. Tsuda, I. Omura, T. Ogura,“High breakdown Voltage undoped AlGaN-GaN power HEMT on sapphire substrate and its demonstration for DC-DC converter application”. Electron Devices, IEEE Transactions on , vol.51, no.11pp. 1913- 1917, Nov. 2004. 124 7 Conclusions and future work 7.1 Conclusions T HIS dissertation has focused on the improvement of the AlGaN/GaN HEMTs with emphasis on those devices with high breakdown voltage. Initial efforts were aimed at reducing the peak electric field at the drain edge of the gate by using multiple field plates. Thus high breakdown voltage was achieved without sacrificing the frequency performance too much. In addition, the origin of the gate leakage current was investigated. Several dielectric materials were tried as gate dielectrics to reduce the gate leakage in AlGaN/GaN HEMTs. The leakage from the field-plates through the SiN x was characterized and the leakage was found to reduce with the two layer SiNx passivation layer. The buffer leakage was characterized by using buffer leakage test 125 CHAPTER 7. CONCLUSIONS AND FUTURE WORK patterns with different spacings. The effect of Fe-doping on buffer leakage in HEMTs grown on SiC was verified which showed that the highest amount of Fe normally used yielded the lowest buffer leakage. After a series of controlled experiments alloyed ohmic contacts were identified as another source of buffer leakage. One way to reduce the buffer leakage was to anneal the ohmic metals in MOCVD chamber in the presence of NH3 and this yielded ohmic contacts without spiky features and also improved breakdown voltage on microwave HEMTs. An improved processing technique which yields field-plate self-aligned with the gates was developed. The parasitic weakpoints in the devices which prevented the HEMTs to reach a kilovolt breakdown voltage were investigated. The HEMTs with kilovolt breakdown voltage were obtained when these devices were tested immersed in Fluorinert liquid. Switching measurements were done with the help of Dr. Sriram Chandrasekaran and Dr. Vivek Mehrotra at Rockwell Scientific, Thousand Oaks. A compact setup was designed and built which yielded a gate drive speed less than 50 ns. High current switching measurements were performed by combining several devices in parallel. Devices with turn-off time of less than 20 ns were measured. The switching time is still limited by the gate drive speed. The effect of parasitic source-side wirebond resistance on Von was 126 CHAPTER 7. CONCLUSIONS AND FUTURE WORK studied. 7.2 Future Work The exact mechanism which is limiting the breakdown and why the breakdown is linear with Lgd needs to be investigated. If the breakdown is limited by the depletion region reaching the drain, then a channel with higher charge should yield higher breakdown voltages since the depletion region should extend slower then. If the buffer is limiting the breakdown then devices made with slighlty lower Fe in the buffer should yield reduced breakdown voltages. The trench gates could be optimized to obtain better performance in removing dispersion at higher load-lines. The dielectrics grown at high temperature in-situ in the mocvd chamber should be investigated to get a reliable gate dielectric for GaN devices. The gate leakage can also be reduced by implanting the gate regions with Fluorine ions. The implantation and n + capped ohmic contacts need to be incorporated into the HEMT process to reduce the buffer leakage. Devices made on cheaper n-SiC substrates show promise and the buffer for this should be optimized. Switching measurements need to be done with a gate driver ca- 127 CHAPTER 7. CONCLUSIONS AND FUTURE WORK pable of switching at higher speeds. The Von needs to be reduced by reducing the parasitic resistances. The wide-periphery devices made with flip-chip process need to be characterized by the switching measurements. Several of these devices can be put together to build a switching power converter operating at high(>10 MHz) frequencies. 128 A ATLAS code for simulating AlGaN/GaN HEMTs # version.1 ####### from Karmalkar’s email file ###### ### Field plate # go atlas # set label1=t1s1fp2 # t1=1200A s1=0.4um # ####### SECTION 1: Mesh Input 129 APPENDIX A. ATLAS CODE FOR SIMULATING ALGAN/GAN HEMTS # mesh nx=69 ny=80 # x.m n=1 l=0.0 r=1.0 x.m n=50 l=2.0 r=1.0 x.m n=69 l=3.1 r=1.0 # # y.m n=1 l=-0.9 r=1.0 y.m n=10 l=-0.4 r=1.0 #y.m n=4 l=-0.17 r=1.0 y.m n=30 l=0.0 r=1.0 y.m n=40 l=0.015 r=1.0 y.m n=50 l=0.02 r=1.0 y.m n=60 l=0.025 r=1.0 y.m n=70 l=0.045 r=1.0 y.m n=80 l=0.2 r=1.0 # # ###### SECTION 2: Structure specification # region num=1 material=GaAs y.min=0.02 region num=2 material=AlGaAs y.max=0.02 x.composition=0.3 region num=3 sapphire x.min=0.1 x.max=3.0 y.min=0.0195 y.max=0.02 region num=4 oxide y.min=-0.9 y.max=0 # # elec num=1 name=source x.min=0.0 x.max=0.0 y.min=0.0 y.max=0.05 elec num=2 name=gate x.min=0.5 x.max=1.0 y.min=-0.4 y.max=0.0 elec num=2 name=gate x.min=0.5 x.max=1.4 y.min=-0.4 y.max=-0.120 elec num=2 name=gate x.min=0.5 x.max=1.8 y.min=-0.4 y.max=-0.240 elec num=3 name=drain x.min=3.1 x.max=3.1 y.min=0.0 y.max=0.05 # # doping uniform y.min=0.0 y.max=0.02 n.type conc=1e16 130 APPENDIX A. ATLAS CODE FOR SIMULATING ALGAN/GAN HEMTS doping uniform y.min=0.02 n.type conc=1e15 doping uniform x.min=0.0 x.max=0.05 y.min=0.0 y.max=0.04 n.type conc=1e18 doping uniform x.min=3.05 x.max=3.1 y.min=0.0 y.max=0.04 n.type conc=1e18 # # interface x.min=0.1 x.max=3.0 y.min=0.0197 y.max=0.0203 qf=10e12 # # ###### SECTION 3: Material models # material material=AlGaAs mun=600 mup=10 affinity=3.82 eg300=3.96 copt=9.75e10 taun0=1e-9 taup0=2e-8 permittivity=9.5 nc300=2.07e18 nv300=1.16e19 arichp=72 arichn=23 edb=0.025 eab=0.16 material material=GaAs mun=900 mup=10 eg300=3.4 vsat=2.0e7 copt=6.84e10 taun0=1.0e-9 taup0=2.0e-8 permittivity=9.5 nc300=2.07e18 nv300=1.16e19 arichp=72 arichn=23 edb=0.025 eab=0.16 material align=0.8 material material=oxide permittivity=7.5 # # model fldmob srh b.electr=1 b.holes=1 # # impact selb an1=2.9e8 bn1=3.4e7 ap1=2.9e8 bp1=3.4e7 an2=2.9e8 bn2=3.4e7 ap2=2.9e8 bp2=3.4e7 egran=1.0e6 betan=1 betap=1 # # contact name=gate workfun=5.2 # # ###### SECTION 4: Bias Gate # # method gummel newton itlim=20 trap maxtrap=6 output con.band val.band 131 APPENDIX A. ATLAS CODE FOR SIMULATING ALGAN/GAN HEMTS # # my addition solve vgate=0.0 name=gate save outf=$”label1” zero.str tonyplot $”label1” zero.str -set pot contour.set # # solve vgate=-0.1 vstep=-0.5 vfinal=-6.6 name=gate # save outf=$”label1” pinch.str tonyplot $”label1” pinch.str -set pot contour.set # # # SECTION 5: Drain Ramp # log outf=fp1.log master # method newton trap itlim=35 maxtrap=6 solve vdrain=0.05 vstep=0.05 name=drain vfinal=0.3 solve vdrain=0.50 vstep=0.25 name=drain vfinal=4.5 solve vdrain=5.0 vstep=1.0 name=drain vfinal=20 compl=30e-5 e.comp=3 save outf=$”label1” 20v.str tonyplot $”label1” 20v.str -set efield.set solve vdrain=20 vstep=2.0 name=drain vfinal=50 compl=30e-5 e.comp=3 # save outf=$”label1” 50v.str tonyplot $”label1” 50v.str -set efield.set # solve vdrain=50 vstep=2.0 name=drain vfinal=80 compl=30e-5 e.comp=3 save outf=$”label1” 80v.str tonyplot $”label1” 80v.str -set efield.set # 132 APPENDIX A. ATLAS CODE FOR SIMULATING ALGAN/GAN HEMTS solve vdrain=80 vstep=2.0 name=drain vfinal=100 compl=30e-5 e.comp=3 save outf=$”label1” 100v.str tonyplot $”label1” 100v.str -set efield.set # #tonyplot -overlay d2N.6a3.str d2N.6c3.str -set # hemtex02 0.set #tonyplot -overlay d2N.6b1.log d2N.6b2.log -set # hemtex02.set tonyplot fp1.log -set idvd.set # quit # 133 B SiNx deposition conditions 1. PECVD: SiH4 =200 sccm, N2 = 200 sccm, NH3 =2.0 sccm, 250◦ C, pressure=600 mT, plasma power=22 W 2. ICP: SiH4 (2%)=315 sccm, N2 = 4 sccm, Ar=20 sccm, 250◦ C, pressure=15 mT, bias power=5 W, ICP power=400 W. 134 C Specifics of Processing Making Ohmic contacts to HEMTs 1. Standard Clean: Acetone and Isopropanol soak in Ultrasonic for 3 min each and DI water rinse 2. 120◦ C dehydration bake for 2-3 min; cool it 3. Apply HMDS, wait for 20 sec and spin it off. (If the sample has a dielectric 135 APPENDIX C. SPECIFICS OF PROCESSING on it, the PR will not stick to it. Otherwise HMDS can be skipped.) 4. OCG825 at 5 krpm for 30 sec 95◦ C hotplate for 1min 5. SPR950-0.8 at 3.5 krpm for 30 sec 6. 90◦ C hotplate for 1 min (total thickness of about 1.8µm PhotoResist PR) 7. Expose in stepper for 1.8 sec 8. Post exposure bake in 100◦ C for 2 min. 9. Develop for 1 min and 40 sec in MF701:DI=2:1 10. DI rinse for 2 min. 11. O2 descum clean for 30 sec. 12. HCl:DI=1:3 dip for 40sec 13. Ohmic metallization in EBeam#4 (Ti/Al/Ni/Au-20/120/30/50 nm) Isolation of devices by Mesa etch 14. Lithography for Mesa layer, using lithography as mentioned in steps 1-10. 136 APPENDIX C. SPECIFICS OF PROCESSING 15. Native Oxide removal in RIE5 machine BCl3 -10 sccm flow, pressure10mT, power-100W, time-1 min. 16. Native Oxide removal in RIE5 machine Cl2 -10 sccm flow, pressure-10mT, power-100W, time-2 min (etch rate∼1 nm/sec). 17. PR stripped by acetone soak and sample subjected to a standard clean. Gate metallization 18. Gate Lithography, using lithography as mentioned in steps 1-10. 19. Gate metals deposited in Ebeam#4 Ni/Au/Ni-30/250/30nm. 20. Metal lift-off by acetone soak and sample subjected to a standard clean. SiNx Passivation 21. PECVD chamber cleaned by CF4 /O2 clean at 300W power. 22. O2 descum clean for 30 sec. 23. HCl:DI=1:3 dip for 40sec 24. Sample loaded in PECVD and SiNx of about 120nm deposited at 250 ◦ C. 137 APPENDIX C. SPECIFICS OF PROCESSING Bondpad formation 25. Bondpad Lithography using lithography as mentioned in steps 1-10. 26. SiNx etched in descum machine with CF4 300mT/200W for 150 sec. 27. HCl:DI=1:3 dip for 40sec 28. Bondpad metals deposited in Ebeam#3 Ti/Au-30/250 nm. 29. Metal lift-off by acetone soak and sample subjected to a standard clean. Trench gate process 30. Bondpad Lithography using lithography mentioned in steps 1-10. 31. Etch SiNx in RIE#3, CF4 /O2 =20/2 sccm flow, chamber pressure-20mT, Bias Voltage=100 V, etch time∼14min. 32. HCl:DI=1:3 dip for 40sec 33. Sample loaded on a rotating chuck kept at about 15 ◦ angle to the incident metal flux in Ebeam#3 (Ni/Au/Ni-30/250/30 nm). 34. Metal lift-off by acetone soak and sample subjected to a standard clean. 138 APPENDIX C. SPECIFICS OF PROCESSING Thick bond pad formation and flip-chip bonding 35. solvent clean, dehydration bake, HMDS spin as steps 1-3. 36. Spin AZ4620 at 4 krpm for 100 sec. 37. 110◦ C 90 sec bake 38. Flood expose for 30 sec in contact aligner 39. AZ4210 4 krpm 60 sec spin 40. 95◦ C 60 sec bake 41. Expose pattern in stepper 3 sec time 42. Develop 60∼75 sec in freshly mixed AZ400k:DI=1:4 mixture 43. DI rinse 2 min 44. Look for liftoff profile. Resist should be atleast 8µm thick in dektak. 45. Deposit 5∼6µm thick Au in Ebeam#1 and liftoff by acetone soak 46. Dice the devices. 47. Standard clean. 139 APPENDIX C. SPECIFICS OF PROCESSING 48. Align the device wafer and carrier wafer in Flip-chip bonder. 49. Bond at pressure of 10kg and at 200◦ C. 140