Progress Toward Mini and Micro Magnetic Undulators Ololade Oniku, William Patterson, Alexandra Garraud, Evan Shorman, Paul Ryiz, David P. Arnold University of Florida Dept. Electrical & Computer Engineering Interdisciplinary Microsystems Group Brock Peterson, Florian Herrault, Mark G. Allen Georgia Institute of Technology School of Electrical and Computer Engineering MicroSensors and MicroActuators Group HBEB San Juan, Puerto Rico March 27, 2013 Overview State-of-the-art undulator - Pole pitch (λu ~ 5-50 mm) Peak field (B0 ~ 0.1-1 T) Large total system size Manual assembly High costs (material and labor) Micromachined Undulator - Pole-pitch (λu ~ 5-50 µm) Peak field (B0 > 0.2 T) Hard X-rays at lower beam energies Microfabrication advantages • Photolithgraphic resolution • Wafer-level mass production • More complex patterns (3D?) 2 Overview 3 Scale-dependent approaches Thin-Film Electroplating & Sputtering Thick-Film Micro Powder Processing Bulk COTS Sintered Magnets Outline Laser-micromachined SmCo “Mini” undulators Electroplated CoPt film “Micro” undulators Characterization - Scanning Hall Probe - Magneto-optical imaging Collaborations - Pulsed-wire characterization (UCLA) - Photon-generation tests (Michigan) 4 Laser-Cut Magnets Process Overview Bulk SmCo ~300 µm thick (unmagnetized) Laser-cut into comb structures Magnetize out-of-plane Assemble and polish 5 Interlocking Array Segments 6 single PM comb-arrays assembled 6 Micro-Assembly 7 Comb array assembly (magnetically self-aligned) Top and bottom arrays assembled into frame Polished to final thickness 20 mm SEM of half an undulator (Period = 500 µm) Laser-machined SmCo undulator array with 200-µm thick, 2-mm long poles, 400-µm period and 50 periods Assembled Prototype Undulator 8 Undulator assembly - Two magnet arrays sandwiched with spacers Estimated ~0.23 T peak B-field Magnetized and assembled SmCo arrays (400 µm period). The vertical gap between the PM plates was set at 200 µm. High-Resolution Field Mapping High-resolution Hall effect sensor (1 µm x 1 µm area) 3-axis stage with 100 nm step size (x, y axes) Currently implementing automatic scan height control Sensor module Sample platform x- y- and zstages 9 Scanning Hall Probe Stage 1 µm x 1 µm sensing area 10 Scanning Hall Probe system Example field maps at ~100 µm scan height Peak-to-peak: 0.1 T Measured period: 400 µm 11 Simulation vs. Experiment 12 Simulation and experimental data at different heights for a single array Simulation Very good agreement Measurement B0 ~ 0.1 T peak, 100 µm above Film Magnets Process Overview 13 Electroplate films (CoPt) 5-20 µm thick Soft magnetic magnetizing head Hard magnetic film (5 – 20 µm) Pre-magnetize the film uniformly “UP” Si substrate Use magnetizing head to selectively reverse areas “DOWN” Hext Selective magnetic patterning using magnetizing heads Electroplated Co80Pt20 Films 14 Co-Rich Co80Pt20 on silicon substrates Top view Out-of-plane properties: - Remanent flux density: Br=1.0 T - Intrinsic coercivity: Hci=330 kA/m (4.1 kOe) - Energy density: BHmax=134 kJ/m3 (17 MGOe) 30 µm Cross section Selective magnetization 15 Laser-cut magnetizing head from bulk Fe Pattern Co80Pt20 using the magnetizing head Characterization: magneto-optical imaging and scanning Hall probe Laser-micromachined Fe magnetizing head 200 µm 200 µm Electroplated Co-Pt film (5 - 10 µm) Si substrate 400 µm Laser-machined Fe magnetizing head Magneto-optical image at surface Scanning Hall data 100 µm above surface Selective magnetization 16 Further down-scaling 200 µm period 120 µm period 65 µm period Selective magnetization: complex patterns Magnetizing mask (Fe sheet) Magnetic pattern 17 Magnetic Properties of L10 CoPt 18 L10 CoPt (50:50 ratio) on silicon substrates Annealed @ 700 °C Coercivity ~2.5x higher than Co80Pt20 films 500 µm Out-of-plane properties: - Remanent flux density: Br=1.15 T - Intrinsic coercivity: Hci=800 kA/m (10 kOe) - Energy density: BHmax=220 kJ/m3 (28 MGOe) Magnetic Properties 19 Micromagnets compared to bulk Sputtered NdFeB 40 μm (collaborator) Plated L10 CoPt 15 μm Plated Co80Pt20 15 μm UCLA: pulsed-wire measurements Magnetic characterization of the full undulator Side view Schematic of the setup 20 UCLA: Pulsed-wire measurements 21 Undulator - full length = 20 mm - period = 400 µm - gap = 200 µm Wire - diameter = 25-50 µm Hanging mass ~ 30-80 g Electron “kick” but no detectable undulations Work in progress - estimation of the displacement of the e-beam Michigan: Photon-generation tests eprofile Fiducial Array (100µm W wires, 1.25 mm spacing) ~140 cm 110 cm Micro-Undulator on Hexapod (400 µm gap, 2 cm long) 5 cm Magnet (0.75T) Light shield/ Laser block Deflected (25 µm Al) Direct detection X-ray camera (Andor) LANEX or Filter Pack (300 µm Mylar + 2 µm Al) Electron Beam e- spec 22 F/20 OAP Beam (~100 TW, ~22 µm spot) Gas cell (10mm) Michigan: Photon-generation tests Initial results indicate that: - e-beam is not mono-energetic enough (dE/E > 10%) New gas cells have been fabricated - 10 mm gas cell: monoergenetic shots at ~400 MeV 3 consecutive shots 23 Ongoing Efforts Halbach magnetization patterns for higher magnetic fields Further development of electroplated L10 CoPt and FePt (50:50 ratio) for superior magnetic properties Exploration of limits of selective magnetization using magnetizing heads - Goal: 50-µm period undulator Collaboration with UCLA and Michigan for lasermicromachined undulator characterization - Open to other collaboration opportunities 24 Acknowledgments 14 AXiS Project #N6601-11-1-4198 Uniform Magnetization Patterned Magnetization 26 Towards shorter laser-machined undulators Undulator with shorter periods successfully fabricated Magnetized and assembled SmCo arrays: (a) 300-µm period (b) 250-µm period (c) 230-µm period 27 Summary of Designs 28 Undulator period (#) Undulator gap Magnetic material 400 µm (50) 200 µm Laser-cut Bulk SmCo 0.25 T 1 0.010 50 µm (50) 20 µm Plated L10 CoPt 0.13 T 2 0.00065 1 measured with the SHP 2 estimated from simulation B-field (peak, midgap) K (cm.T)