SMRE - Reliability Project Title: Tensile Strength of Fibers Author: Brian Russell Date: November 20, 2008 Objective: Using data provided by “Reliability Modeling, Prediction, and Optimization”, Case 2.6, “Tensile Strength of Fibers” I will explore the tensile strength of silicon carbide fibers after extraction from a ceramic matrix. Description of System: This experiment is an attempt to estimate fiber strength after incorporation into the composite, rather than modeling composite strength and estimating each component separately, which is the usual approach in estimating composite strength. The difficulty with the latter is that it is necessary to account for the interaction between the two materials in determining strength (see Fox and Walls, 1997). Fiber strength is measured as stress applied until fracture failure of the fiber. The objective of the experiment was to determine the distribution of failures as a function of gauge length of the fiber after incorporation into the composite. Data from “Reliability Modeling, Prediction, and Optimization”, Case 2.6 0.36 0.50 0.57 0.95 0.99 1.09 1.09 1.33 1.33 1.37 1.38 1.38 1.39 1.41 1.42 265 1.93 1.96 1.97 1.99 2.04 2.06 2.06 2.08 2.11 2.26 2.27 2.27 2.38 2.39 2.47 1.25 1.50 1.57 1.85 1.92 1.94 2.00 2.02 2.13 2.17 2.17 2.20 2.23 2.24 2.30 Fiber length (mm) 25.4 2.81 1.96 2.82 1.98 2.90 2.06 2.92 2.07 2.93 2.07 3.02 2.11 3.11 2.22 3.11 2.25 3.14 2.39 3.20 2.42 3.20 2.63 3.22 2.67 3.26 2.75 3.29 2.75 3.30 2.75 12.7 3.29 3.30 3.36 3.39 3.39 3.41 3.41 3.43 3.52 3.72 3.96 4.07 4.09 4.18 4.13 5 2.36 2.40 2.54 2.67 2.68 2.69 2.70 2.77 2.77 2.79 2.83 2.91 3.04 3.05 3.06 3.81 3.88 3.93 3.94 3.94 3.94 3.70 4.04 4.07 4.08 4.08 4.16 4.18 4.22 4.24 1.42 1.45 1.49 1.50 1.56 1.57 1.57 1.75 1.78 1.79 1.79 1.82 1.83 1.86 1.89 1.90 1.92 2.48 2.73 2.74 2.33 2.42 2.43 2.45 2.49 2.51 2.54 2.57 2.62 2.66 2.68 2.71 2.72 2.76 2.79 2.79 2.80 3.34 3.35 3.37 3.43 3.43 3.47 3.61 3.61 3.62 3.64 3.72 3.79 3.84 3.93 4.03 4.07 4.13 2.89 2.93 2.95 2.96 2.97 3.00 3.03 3.04 3.05 3.07 3.08 3.13 3.20 3.22 3.23 3.26 3.27 4.14 4.15 4.29 3.24 3.27 3.28 3.34 3.36 3.39 3.51 3.53 3.59 3.63 3.64 3.64 3.66 3.71 3.73 3.75 3.78 4.35 4.37 4.50 Methodology used for Analysis: Data was imported to Minitab so that mathematical manipulation could be performed to produce transfer functions. Based on the amount of data, Monte Carlo simulations will be performed to simulate a larger population Equations will be manipulated using Maple to produces the appropriate Reliability functions and display the data graphically. Expected Outcome: The data will show if there is a significant difference in the strength of carbon fibers after extraction of different lengths. References: Reliability Modeling, Prediction, and Optimization, Wallace R. Blischke and D.N. Prabhakar Murthy, published 2000 by Wiley-Interscience Publication Minitab Project Report For Fiber Length 265 mm Distribution ID Plot: C1 Goodness-of-Fit Distribution Weibull Lognormal Exponential Normal Anderson-Darling (adj) 0.924 2.112 22.663 0.630 Correlation Coefficient 0.969 0.913 * 0.988 Table of Percentiles Percent 1 1 1 1 Percentile 0.439830 0.664794 0.0116532 0.456895 Standard Error 0.100323 0.0648694 0.0013559 0.151184 95% Normal CI Lower Upper 0.281274 0.687764 0.549071 0.804908 0.0092769 0.0146382 0.160579 0.753211 Weibull Lognormal Exponential Normal 5 5 5 5 0.741634 0.860701 0.0594737 0.824807 0.113691 0.0677524 0.0069202 0.119756 0.549164 0.737646 0.0473458 0.590089 1.00156 1.00428 0.0747082 1.05953 Weibull Lognormal Exponential Normal 10 10 10 10 0.934107 0.987750 0.122164 1.02094 0.113298 0.0690738 0.0142146 0.104864 0.736469 0.861236 0.0972520 0.815410 1.18478 1.13285 0.153457 1.22647 Weibull Lognormal Exponential Normal 50 50 50 50 1.70863 1.60536 0.803692 1.7128 0.0897044 0.0860398 0.0935155 0.0763479 1.54155 1.44528 0.639803 1.56316 1.89381 1.78317 1.00956 1.86244 Distribution Weibull Lognormal Exponential Normal Table of MTTF Distribution Weibull Lognormal Exponential Normal Mean 1.71903 1.72489 1.15948 1.71280 Standard Error 0.084254 0.095243 0.134914 0.076348 95% Normal CI Lower Upper 1.56158 1.89235 1.54796 1.92204 0.92304 1.45649 1.56316 1.86244 Probability Plot for Length of 265 LSXY Estimates-Complete Data Weibull 99 90 90 50 P er cent P er cent C orrelation C oefficient Weibull 0.969 Lognormal 0.913 E xponential * N ormal 0.988 Lognormal 99.9 10 50 10 1 0.5 1.0 C1 1 2.0 1 E xponential N ormal 99.9 99 90 90 50 P er cent P er cent 10 C1 10 50 10 1 0.01 0.10 1.00 10.00 1 0 C1 1 2 3 C1 The graphs show that Weibull, Lognormal and Normal distributions are good fits to the data. Distribution Overview Plot: C1 Goodness-of-Fit Distribution Weibull Anderson-Darling (adj) 0.924 Correlation Coefficient 0.969 Distribution Overview Plot for Length of 265mm LSXY Estimates-Complete Data P robability D ensity F unction Table of S tatistics S hape 3.11972 S cale 1.92163 M ean 1.71903 S tDev 0.603230 M edian 1.70863 IQ R 0.844805 F ailure 50 C ensor 0 A D* 0.924 C orrelation 0.969 Weibull 99.9 90 50 P er cent P DF 0.6 0.4 0.2 0.0 1 2 10 1 3 0.5 1.0 C1 C1 S urv iv al F unction H azard F unction 100 4.5 Rate P er cent 2.0 50 3.0 1.5 0 0.0 1 2 3 1 C1 2 3 C1 Probability Plot of C1 Weibull - 95% CI 99.9 Shape Scale N AD P-Value Percent 99 90 80 70 60 50 40 3.119 1.922 50 0.773 >0.250 30 20 10 5 3 2 1 0.1 1.0 C1 10.0 This Minitab plot shows that the response at length 265 mm fits a Weibull well with Shape of 3.119 and scale of 1.922. The scale parameter is: a = 1.992 The shape parameter is: b = 3.119 So the Weibull function that fits this data is F=1-exp (-(t/a) ^b) F:=1-exp(-(t/1.992)^3.119) To perform the Monte Carlo Simulation in Excel, this expression is first transformed to: t=-1.992*ln(1-3.119(F)) Minitab Project Report For Fiber Length 25.4 mm Distribution ID Plot: 25.4 Goodness-of-Fit Distribution Weibull Lognormal Exponential Normal Anderson-Darling (adj) 0.391 0.696 36.043 0.342 Correlation Coefficient 0.997 0.980 * 0.996 Table of Percentiles Percent 1 1 1 1 Percentile 1.20572 1.52980 0.0183122 1.26452 Standard Error 0.127267 0.0947980 0.0018304 0.169025 95% Normal CI Lower Upper 0.980397 1.48284 1.35484 1.72735 0.0150542 0.0222752 0.933232 1.59580 Weibull Lognormal Exponential Normal 5 5 5 5 1.68599 1.81960 0.0934589 1.72884 0.124415 0.0896237 0.0093417 0.133828 1.45896 1.65215 0.0768315 1.46654 1.94836 2.00401 0.113685 1.99114 Weibull Lognormal Exponential Normal 10 10 10 10 1.95506 1.99590 0.191972 1.97637 0.117821 0.0863227 0.0191885 0.117142 1.73725 1.83368 0.157818 1.74677 2.20017 2.17247 0.233518 2.20596 Weibull Lognormal Exponential Normal 50 50 50 50 2.88037 2.76578 1.26295 2.84953 0.0873777 0.0880059 0.126238 0.0851665 2.71411 2.59856 1.03825 2.68261 3.05682 2.94376 1.53627 3.01645 Distribution Weibull Lognormal Exponential Normal Table of MTTF Distribution Weibull Lognormal Exponential Normal Standard Error 0.083858 0.092411 0.182122 0.085167 Mean 2.84712 2.85686 1.82205 2.84953 95% Normal CI Lower Upper 2.68742 3.01632 2.68136 3.04385 1.49788 2.21637 2.68261 3.01645 Probability Plot for 25.4 LSXY Estimates-Complete Data C orrelation C oefficient Weibull 0.997 Lognormal 0.980 E xponential * N ormal 0.996 Lognormal 99.9 99.9 90 99 50 90 P er cent P er cent Weibull 10 50 1 10 0.1 0.1 1 1 2 2 5 .4 5 2 E xponential N ormal 99.9 99.9 90 99 50 90 P er cent P er cent 5 2 5 .4 10 1 50 10 1 0.1 0.001 0.010 0.100 2 5 .4 1.000 10.000 0.1 1.0 Goodness-of-Fit Anderson-Darling (adj) 0.391 4.0 2 5 .4 Distribution Overview Plot: 25.4 Distribution Weibull 2.5 Correlation Coefficient 0.997 5.5 Distribution Overview Plot for 25.4 LSXY Estimates-Complete Data P robability D ensity F unction 0.6 90 50 P DF P er cent 0.4 0.2 0.0 10 1 1 2 3 0.1 4 1 2 2 5 .4 2 5 .4 S urv iv al F unction 5 H azard F unction 6 100 4 Rate P er cent Table of S tatistics S hape 4.86156 S cale 3.10592 M ean 2.84712 S tDev 0.669072 M edian 2.88037 IQ R 0.918007 F ailure 64 C ensor 0 A D* 0.391 C orrelation 0.997 Weibull 99.9 50 0 2 0 1 2 3 4 1 2 2 5 .4 3 4 2 5 .4 Probability Plot of 25.4 Weibull - 95% CI Percent 99.9 99 Shape Scale N AD P-Value 90 80 70 60 50 40 30 20 4.862 3.106 64 0.178 >0.250 10 5 3 2 1 0.1 5 0. 6 0. 7 8 9 0 0. 0 . 0 . 1. 5 1. 25.4 0 2. 0 3. 0 4. 0 5. This Minitab plot shows that the response at length 25.4 mm fits a Weibull well with shape of 4.862 and scale of 3.106. The scale parameter is: a = 3.106 The shape parameter is: b = 4.862 So the Weibull function that fits this data is F=1-exp(-(t/a)^b) F:=1-exp(-(t/3.106)^4.862) To perform the Monte Carlo Simulation in Excel, this expression is first transformed to: t=-3.106*ln(1-4.862(F)) Minitab Project Report For Fiber Length 12.7 mm Distribution ID Plot: 12.7 Goodness-of-Fit Distribution Weibull Lognormal Exponential Normal Anderson-Darling (adj) 1.234 1.084 30.193 0.851 Correlation Coefficient 0.974 0.977 * 0.983 Table of Percentiles Percent 1 1 1 1 Percentile 1.51695 1.83419 0.0196892 1.59493 Standard Error 0.138867 0.109073 0.0022165 0.179155 95% Normal CI Lower Upper 1.26780 1.81507 1.63240 2.06093 0.0157909 0.0245499 1.24380 1.94607 Weibull Lognormal Exponential Normal 5 5 5 5 2.00419 2.12373 0.100487 2.03343 0.130730 0.100300 0.0113121 0.142080 1.76366 1.93597 0.0805909 1.75496 2.27751 2.32970 0.125294 2.31191 Weibull Lognormal Exponential Normal 10 10 10 10 2.26652 2.29632 0.206408 2.26720 0.122440 0.0951671 0.0232359 0.124531 2.03881 2.11717 0.165540 2.02312 2.51966 2.49063 0.257364 2.51127 Weibull Lognormal Exponential Normal 50 50 50 50 3.12730 3.02507 1.35792 3.0918 0.0899931 0.0920098 0.152864 0.0909962 2.95579 2.85001 1.08906 2.91345 3.30875 3.21089 1.69315 3.27015 Distribution Weibull Lognormal Exponential Normal Table of MTTF Distribution Weibull Mean 3.08449 Standard Error 0.087560 95% Normal CI Lower Upper 2.91756 3.26096 Lognormal Exponential Normal 3.09585 1.95906 3.09180 0.095292 0.220537 0.090996 2.91461 1.57118 2.91345 3.28837 2.44270 3.27015 Probability Plot for 12.7 LSXY Estimates-Complete Data Weibull 99.9 99 90 90 50 P er cent P er cent C orrelation C oefficient Weibull 0.974 Lognormal 0.977 E xponential * N ormal 0.983 Lognormal 10 50 10 1 2 3 4 1 5 2 1 2 .7 E xponential 4 5 N ormal 99.9 99 90 90 50 P er cent P er cent 3 1 2 .7 10 50 10 1 0.01 0.10 1.00 1 2 .7 10.00 1 2 Distribution Overview Plot: 12.7 Goodness-of-Fit Distribution Weibull Anderson-Darling (adj) 1.234 Correlation Coefficient 0.974 3 1 2 .7 4 5 Distribution Overview Plot for 12.7 LSXY Estimates-Complete Data P robability D ensity F unction Table of S tatistics S hape 5.85190 S cale 3.32943 M ean 3.08449 S tDev 0.611609 M edian 3.12730 IQ R 0.829597 F ailure 50 C ensor 0 A D* 1.234 C orrelation 0.974 Weibull 99.9 90 P er cent P DF 0.6 0.4 0.2 0.0 2 3 1 2 .7 50 10 1 4 2 S urv iv al F unction 4 H azard F unction 100 6 Rate P er cent 3 1 2 .7 50 4 2 0 0 2 3 1 2 .7 4 2 Distribution Overview Plot: 12.7 Goodness-of-Fit Distribution Lognormal Anderson-Darling (adj) 1.084 Correlation Coefficient 0.977 3 1 2 .7 4 5 Distribution Overview Plot for 12.7 LSXY Estimates-Complete Data P robability D ensity F unction Table of S tatistics Loc 1.10693 S cale 0.215072 M ean 3.09585 S tDev 0.673604 M edian 3.02507 IQ R 0.880738 F ailure 50 C ensor 0 A D* 1.084 C orrelation 0.977 Lognormal 99 0.6 P er cent P DF 90 0.4 0.2 0.0 50 10 2 3 4 1 5 1 2 .7 2 3 1 2 .7 4 S urv iv al F unction H azard F unction 5 100 Rate P er cent 2 50 0 1 0 2 3 4 5 2 3 1 2 .7 4 5 1 2 .7 Probability Plot of 12.7 Weibull - 95% CI 99.9 Shape Scale N AD P-Value Percent 99 90 80 70 60 50 40 30 20 10 5 3 2 1 1.5 2.0 3.0 12.7 4.0 5.0 5.852 3.329 50 0.911 >0.250 Probability Plot of 12.7 Lognormal - 95% CI 99 Loc Scale N AD P-Value 95 90 1.107 0.2151 50 0.873 >0.250 Percent 80 70 60 50 40 30 20 10 5 1 2 3 12.7 4 5 6 The Minitab plot shows that the response at length 12.7 mm fits a Lognormal plot well with a correlation value of .977, but also fits a Weibull distribution with a correlation value of .974 and shape of 5.82 and scale of 3.329. The scale parameter is: a = 3.32943 The shape parameter is: b = 5.85190 So the Weibull function that fits this data is F=1-exp(-(t/a)^b) F:=1-exp(-(t/3.32943)^5.85190) To perform the Monte Carlo Simulation in Excel, this expression is first transformed to: t=-3.32943*ln(1-5.85190(F)) Distribution ID Plot: 5 For Fiber Length 5 mm Goodness-of-Fit Distribution Anderson-Darling (adj) Correlation Coefficient Weibull Lognormal Exponential Normal 0.775 1.280 33.879 0.924 0.980 0.974 * 0.983 Table of Percentiles Percent 1 1 1 1 Percentile 1.96488 2.30149 0.0215009 2.13513 Standard Error 0.163005 0.110021 0.0023790 0.162786 95% Normal CI Lower Upper 1.67002 2.31181 2.09565 2.52756 0.0173090 0.0267080 1.81607 2.45418 Weibull Lognormal Exponential Normal 5 5 5 5 2.46466 2.59024 0.109733 2.53343 0.142729 0.0984042 0.0121418 0.129089 2.20021 2.40438 0.0883391 2.28042 2.76090 2.79047 0.136308 2.78644 Weibull Lognormal Exponential Normal 10 10 10 10 2.72409 2.75870 0.225400 2.74576 0.128618 0.0920145 0.0249401 0.113138 2.48332 2.58412 0.181456 2.52401 2.98821 2.94507 0.279987 2.96751 Weibull Lognormal Exponential Normal 50 50 50 50 3.53976 3.44533 1.48287 3.49476 0.0826591 0.0845028 0.164076 0.0826535 3.38140 3.28362 1.19376 3.33276 3.70553 3.61499 1.84198 3.65676 Distribution Weibull Lognormal Exponential Normal Table of MTTF Distribution Weibull Lognormal Exponential Normal Mean 3.48921 3.49753 2.13932 3.49476 Standard Error 0.081561 0.086448 0.236712 0.082653 95% Normal CI Lower Upper 3.33296 3.65279 3.33214 3.67114 1.72223 2.65742 3.33276 3.65676 Probability Plot for 5 LSXY Estimates-Complete Data Weibull 99 90 90 50 P er cent P er cent C orrelation C oefficient Weibull 0.980 Lognormal 0.974 E xponential * N ormal 0.983 Lognormal 99.9 10 50 10 1 2 3 5 4 1 5 2 3 E xponential 5 N ormal 99.9 99 90 90 50 P er cent P er cent 4 5 10 50 10 1 0.01 0.10 1.00 10.00 1 2 5 Goodness-of-Fit Anderson-Darling (adj) 0.775 4 5 Distribution Overview Plot: 5 Distribution Weibull 3 Correlation Coefficient 0.980 5 Distribution Overview Plot for 5 LSXY Estimates-Complete Data P robability D ensity F unction Table of S tatistics S hape 7.19240 S cale 3.72481 M ean 3.48921 S tDev 0.571679 M edian 3.53976 IQ R 0.765493 F ailure 50 C ensor 0 A D* 0.775 C orrelation 0.980 Weibull 99.9 90 P er cent P DF 0.6 0.4 0.2 0.0 2 3 4 50 10 1 5 5 2 3 5 4 S urv iv al F unction H azard F unction 5 100 Rate P er cent 6 50 4 2 0 0 2 3 4 5 2 3 5 4 5 5 Probability Plot of 5 Weibull - 95% CI 99.9 Shape Scale N AD P-Value Percent 99 90 80 70 60 50 40 7.192 3.725 50 0.512 >0.250 30 20 10 5 3 2 1 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 5 This Minitab plot shows that the response at length 5. mm fits a Weibull well with shape of 7.192 and scale of 3.725. The scale parameter is: a = 3.72481 The shape parameter is: b = 7.19240 So the Weibull function that fits this data is F=1-exp(-(t/a)^b) F:=1-exp(-(t/3.72481)^7.19240) To perform the Monte Carlo Simulation in Excel, this expression is first transformed to: t=-3.72481*ln(1-7.19240(F)) Next, enter the cumulative distribution function (F(t)) for each value of length into Maple and solve for all of the reliability functions. The following results are obtained: For Fibers of length 265mm > > > > > > > > For Fibers of length 265mm > > > > > > > > For Fibers of length 12.7mm > > > > > > > > For Fibers of length 5mm > > > > > > > > Combined Analysis in Maple: > > > > > > > > > > > > > > > The data shows that as the fiber length increases, the Mean Time To Failue (MTTF) decreases. A fiber of length 5mm has a MTTF of 3.5 seconds compared to a fiber of length 2.65 inches has a MTTF of 1.8 seconds. Monte Carlo analysis was performed using the following equations in Excel: 265 25.4 F:=1-exp(-(t/1.992)^3.119) t=-1.992*ln(1-3.119(F)) 12.7mm F:=1-exp(-(t/3.106)^4.862) t=-3.106*ln(1-4.862(F)) 1.784042003 2.817144112 5mm F:=1-exp(-(t/3.32943)^5.85190) t=-3.32943*ln(1-5.85190(F)) F:=1-exp(-(t/3.72481)^7.19240) t=-3.72481*ln(1-7.19240(F)) 3.081436469 The MTTF values in Excel match the values calculated in Maple. Fiber Length (mm) 265 25.4 12.7 5 Maple 1.781963 2.847213 3.084489 3.489212 Excel Monte-Carlo 1.779479205 2.893593614 3.081029868 3.482595755 From this information, a conclusion can be drawn that as the length of composite fibers increases from 5 mm to 265 mm, the tensile strength decreases. 3.486495448