COURSE PLAN Instrumental analysis: Scanning electron microscopy, 5 credits Valid for the period 2014 Course plan developed Elisaveta Potapova, 2012-09-20 Revised 2014-02-04 Education level Third cycle Grade Subject Passed/Failed Chemical Technology Division Chemical Engineering Department Civil, Environmental and Natural Resources Engineering Requirement Course participants should be accepted for post-graduate studies. Special requirement Goal/Expected result After the course the participants should be able to: - understand the physics and the instrumentation behind the scanning electron microscopy (SEM) methods, as well as the capabilities and limitations of the methods; - understand the effect of different parameters on the measurement result; - to chose the correct measurement set up depending on the type of measurement to be carried out. Course content - SEM image formation and magnification, electron-specimen interactions, interaction volume, backscattered electrons, secondary electrons, detectors; - Contrast, electron gun, electron lenses, aberration, astigmatism, resolution; - Imaging modes, STEM, sample preparation; - Energy dispersive spectroscopy, wavelength dispersive spectroscopy. Realization The course consists of six lectures covering the theoretical part of the course and an obligatory laboratory exercise. Literature Scanning electron microscopy and x-ray microanalysis, Volume 1, J. Goldstein, D.E. Newbury, D.C. Joy, C.E. Lyman, P. Echlin, E. Lifshin, L. Sawyer, and J.R. Michael, Kluwer Academic / Plenum, New York, 2003/2007, ISBN 978-0-306-47292-3. Examination - an approved laboratory report; - passed written examination. Examiner Bärbar/SBN/kursplan doktorandkurs ver 120413 Assoc. Prof. Johanne Mouzon, Division of Chemical Engineering johanne.mouzon@ltu.se, tel. +46(0)920491960 For more information contact Dr. Elisaveta Potapova, Division of Chemical Engineering elisaveta.potapova@ltu.se, tel. +46(0)920491776 Bärbar/SBN/kursplan doktorandkurs ver 120413