Assiut University Faculty of Engineering Mining and Metallurgical Engineering Department B. Sc. Project Ore Reserve Estimation Using Computer Aided – A Case Study of Mahamid Phosphate Mine By Baligh Hamdy et.al. Supervisors Prof. Dr. Prof. Dr. Dr. Dr. M. R. El-Tahlawi M. Zaki Rashad Gamal Y. Boghdady SaMeH S. Ahmed A dissertation submitted as part of the B.Sc. Degree in Mining and Metallurgy Engineering To Assiut University July 2004 Abstract Abstract The Phosphate deposits in Egypt represent one of the most economic deposits with a yearly production of …million tons. Those highly production are covered the local market and about…..% of its …….. to several countries among there India, and…………. The quality of the reserves is measured directly by its P2O5 %. The World wide percentage should be above …..% P2O5 , The Egyptian phosphate has ….% in average. This deposit are locality in the Eastern Desert at Kharga , Dakhla and Abu-Tartour platue and distributed at the Eastern Desert at the Red Sea in Hamarwien , Qusier , and around the Nile Valley at Sibaia and El Mahamid . This study is focused in estimation of ore reserve at Eastern Mahamid district-using computes facilitates, getting advantages of its fast accurate and easy way of calculation. The principles of calculation are based upon the triangulation method where the sampling area is divided into a triangulation net with known X, Y and measured of P2O5 of ore at each location. Two ways have been implemented to conduct the calculations, the first is using Excel software to determining the lengths of each triangle in the net from the coordinates, and average thickness, and average assay of the ore, and thus estimate the average thickness and assay of the ore in the study area. The same variables (average thickness of the ore and average assay) have been determined using Kriging technique. This study reviews the geological and geophysical aspects of the phosphate at the study area and addresses the main mining method of ore extraction using surface mining. Results of ore reserve estimation at Eastern Mahamid showed that the average thickness of the ore deposit …and average P2O5. 340 sampling points taken from the area under study at El Mahamid district, Eastern Desert of Egypt Were used to estimate the ore reserves of phosphate deposits and the average thickness and average P2O5 content. The study has focused on applying an approach supported with statistically steps that lead to an accurate and logic estimation. The phosphate mining in Egypt represents one of the largest mining investments with annual production of 56 million tons. These highly production are covered the local market and about 80% of it exported to several countries, among them Ukraine and India. The quality of the phosphate ores is mainly determined by it percentage of P 2O5. The accepted grade in the industry is 22%. Fortunately, the Egyptian phosphate has 25% in average. The use of computer facilities has become widely increased in different areas. Mining engineering in general and ore reserve evaluation in particular are among these applications. This project aims to determine the phosphate ore reserves at El Mahamid area. Several factors have been taken into considerations during the calculations using Excel software, such as providing robust, accurate, and easy use tool that would assist the mining industry. The calculations have conducted based on the Triangular method, statistical analysis of the raw sampling data. Giving X, Y, Z and one ore more variable, for a certain area and with sufficient samples, the software has the capability of determine the total area, volume, ore reserves, distribution of the variable under study and point estimation for any un-sampled point within the entire area. The results are i Abstract introduced as tables, figures, contour maps, and three-dimensional representation of the variables. On the other hand, the students have prepared a database for El Mahamied phosphate mine to be added to the "Mining Information System (MIS.. ii Acknowledgements Acknowledgements All gratitude is to God who guided and helped us to bring this work forward. Sincere and heartfelt gratitude are expressed to the many individuals who have helped to complete this work. Supervisory committee members gave us generous portions of their time, their technical expertise, their support, and their encouragements. We would like to express our deep gratitude to Prof. M. R. El-Tahlawi, Professor of Mining Geology in Mining Engineering Department, Assiut University, for his sincere help, valuable advice, guidance and continual assistance. Grateful thanks are due to Prof. Mohamed Zaki Rashad, Professor of Mining Engineering and Head of the Department, Assiut University, for his interest, supports, and all efforts. Grateful thanks are due to Dr. Gamal Yahia Boghdady, assistant Professor of Structure Geology, Assiut University, for his help, and advice especially through the mapping part. We also desire to express our special and sincere gratitude to Dr. Sameh S. Ahmad, assistant Professor of Mining and Environmental Engineering, Assiut University, for his interest, effort, advice, and helpful remarks. Our acknowledgment is extended to the people at the computer centre, library and all workers in the department. Finally, we would like to thank everyone who helped in one way or another in making this work feasible. The Students: 1. Ahmed Abdo Abbas 2. Ahmed Abdel Aleem Ahmed 3. Ahmed Abde Wahed Ahmed 4. Assma Abdel Azeem Mohamed 5. Ahmed Abdo Abbas 6. Ahmed Abdo Abbas 7. Ahmed Abdo Abbas 8. Ahmed Abdo Abbas 9. Ah Mahmoud Ali 11. Riad Gamal Riad 12. Maged Hanna Fangary 13. Mohammed Usama Ali 14. Samy Ebied Ewida 15. Riad Gamal Riad 16. Riad Gamal Riad 17. Riad Gamal Riad 18. Riad Gamal Riad 19. iii Table of Contents Table of Contents 1.1 Introduction .......................................................................................................... 2 1.1.1 Classification of Phosphate Rocks ................................................................. 3 1.1.1.1 Classification according to its grade: ........................................................... 3 1.1.1.2 Classification according to its gangue minerals: .......................................... 3 1.1.2 Production Costs and Phosphate Availability .............................................. 3 1.2 Objectives .............................................................................................................. 4 1.3 Research Approach .............................................................................................. 5 1.4 Dissertation Organisation .................................................................................... 5 2.1 Introduction .......................................................................................................... 8 22 Geological Studies ................................................................................................ 9 221 Occurrence and origin of the world phosphate rock ................................... 9 2. 2. 2 Chemical and Physical Properties of Phosphate .................................... 11 2 .2 .2 .1 Colors ...................................................................................................... 11 2 .2 .2.2 Hardness ................................................................................................... 11 2. 2.3 Phosphate in Egypt .................................................................................. 11 2.2.4 Nile Valley Phosphate ................................................................................... 13 2.2.4.1 The Location and the topography .............................................................. 13 2.2.4.3 Geological setting....................................................................................... 13 2.2.4.4 The main features of the productive carbonate-phosphorite ...................... 14 2.3 Geophysical Investigation ............................................................................. 18 2.3.1 Importance of some logging methods ............................................................. 19 2.3.1.1 The GL method .......................................................................................... 19 2.3.2 Radioactivity logging .................................................................................... 20 2.3.3 Interpretation of gamma logging measurements ....................................... 20 2.3.3.1 Methods of interpretation ........................................................................... 21 2.3.4 Conclusions .................................................................................................... 21 3.1 Introduction ........................................................................................................ 24 3.2 Conventional Methods ....................................................................................... 24 3.2.1 3.3 Triangular Method ....................................................................................... 24 3.3.1 Geostatistics Techniques .................................................................................... 26 Variogram Modelling.................................................................................... 27 3.3.2 Kriging ........................................................................................................... 31 3.3.2.1 Equations for the Kriging system without and with a known mean ........... 32 3.3.2.2 Advantages of Kriging technique................................................................ 34 4.1 Introduction ........................................................................................................ 35 4.2 Summary Statistics for Area I............................................................................ 36 iv Table of Contents 4.2.1 Summary Statistics for whole area .................................................................... 36 4.2.1.1 Summary Statistics for P2O5 .................................................................... 36 4.2.1.2 Summary Statistics for “t” ...................................................................... 38 4.2.2 Summary Statistics for Part I. a ........................................................................ 39 4.2.2.1 Summary Statistics for P2O5 .................................................................... 39 Percentiles for P2O5 ................................................................................................... 40 4 2 2 2 Summary Statistics for “t” ........................................................................... 41 Percentiles for “t” ...................................................................................................... 41 4.2.3 Summary Statistics for Part I. b ........................................................................ 43 4.2.3.1 Summary Statistics for P2O5 .................................................................... 43 Percentiles for P2O5 ................................................................................................... 43 4.2.3.2.Summary Statistics for “t” ................................................................................. 44 Percentiles for “t” ........................................................................................................... 45 4.2.4 Summary Statistics for Part I.c .......................................................................... 46 4.2.4.1 Summary Statistics for P2O5 .............................................................................. 46 Percentiles for P2O5 ........................................................................................................ 46 4 2.4 2 Summary Statistics for “t” ................................................................................. 48 Percentiles for “t” ........................................................................................................... 48 4.3 Summary Statistics for Area II .......................................................................... 49 4.3.1 Summary Statistics for whole area .................................................................... 49 4.3.1.1 Summary Statistics for P2O5 ........................................................................ 49 Percentiles for P2O5 ................................................................................................... 50 4.3.1.2. Summary Statistics for "t" ......................................................................... 51 Percentiles for “t” ...................................................................................................... 51 4.3.2 Summary Statistics for Part II.d ........................................................................ 53 4.3.2.1 Summary Statistics for P2O5 .............................................................................. 53 Percentiles for P2O5 ........................................................................................................ 53 4.3.2.2 Summary Statistics for “t” ................................................................................. 54 Percentiles for "t" ......................................................................................................... 55 4.3.3 Summary Statistics for Part II.e. ....................................................................... 56 4.3.3.1 Summary Statistics for P2O5 .............................................................................. 56 4.3.3.2 Summary Statistics for “t” ................................................................................. 58 Percentiles for "t" ......................................................................................................... 58 4.3.4 Summary Statistics for Part II.f......................................................................... 59 4.3.4.1 Summary Statistics for P2O5 .............................................................................. 59 v Table of Contents Percentiles for P2O5 ............................................................................................... 60 4.3.4.2 Summary Statistics for “t” ................................................................................. 61 Percentiles for t............................................................................................................... 61 4.3.5 Summary Statistics for Part II.g. ....................................................................... 63 4.3.5.1 Summary Statistics for P2O5 .............................................................................. 63 Percentiles for P2O5........................................................................................................ 63 4.3.5.2 Summary Statistics for “t” ................................................................................. 64 Percentiles for "t" ......................................................................................................... 65 4.3.6 Summary Statistics for Part II-h. ...................................................................... 66 4.3.6.1 Summary Statistics for P2O5 .............................................................................. 66 Percentiles for P2O5........................................................................................................ 66 4.3.6.2 Summary Statistics for “t” ................................................................................. 68 Percentiles for “t”........................................................................................................... 68 4.4 Summery of the Statistical Analysis and Discussion ........................................ 70 4.4.1 Analysis for the Overall Data ....................................................................... 70 4.4.2 Comments on the Results ............................................................................. 70 5.1 Introduction ........................................................................................................ 72 5.2 Original Sampling Data for Mahamied Phosphate Mine ................................ 73 5.3 Results of Triangular Method ........................................................................... 75 5.3.1 Upper Phosphate Seam ................................................................................. 76 5.3.2 Main Phosphate Seam .................................................................................. 82 5.4 5.4.1 Results of Ordinary Kriging Technique ............................................................ 83 Upper Phosphate Seam ................................................................................. 84 Main Phosphate Seam .............................................................................................. 86 5.5 Validation of the Results .................................................................................... 86 6.1 Introduction ........................................................................................................ 87 6.2 Surface Mining Method ..................................................................................... 88 6.2.1 General .......................................................................................................... 88 6.2.2 Advantages of surface mining ...................................................................... 88 6.2.3 Disadvantages ................................................................................................ 89 6.2.4 Factors favouring surface mining: .............................................................. 89 6.3 6.3.1 Surface or Underground Mining Methods? ..................................................... 89 6.4 Calculation of Stripping Ratio ..................................................................... 90 6.4.1 Height of bench .................................................................................................. 91 Height of bench due to stability of the face slope ....................................... 91 vi Table of Contents 6.4.1.1 6.4.1.2 The Maximum height of the vertical face ............................................... 91 The limiting height of a vertical face ...................................................... 91 6.4.2 Height of bench due to safety of working place ............................................. 91 6.4.3 6.5 Height of bench calculated from the efficiency of work place .................. 91 Development schemes and mine trenches ......................................................... 92 6.5.1 Type of trenches ............................................................................................ 92 6.5.2 Shape of trenches: ......................................................................................... 93 6.6 Calculation of height of bench .......................................................................... 94 6.7 Drilling................................................................................................................ 95 6.7.1 Method of borehole drilling.......................................................................... 95 6.7.1.1 Rotary blast hole diameter: ..................................................................... 95 6.7.1.2 Percussive blast hole drilling for surface mining .................................... 96 6.8 Blasting ............................................................................................................... 97 6.8.1 Calculation of burden and spacing for 4 inch. borehole diameter: .......... 97 6.8.2 Calculation of burden and spacing for 2 inch borehole diameter: ........... 98 6.9 Loading and Unloading ..................................................................................... 99 6.10 Equipment ........................................................................................................ 100 6.10.1 Trucks ...................................................................................................... 100 6.10.2 Drag Line Specifications ......................................................................... 101 7.1 Conclusions ...................................................................................................... 104 7.2 Recommendations ............................................................................................ 105 W. M. Telford et al, 1974 "Applied Geophysics", Cambridge University. 860 P. ..... 108 I.1 X, Y Coordinates,"t"and P2O5 of Sampling Points at Mahamid ................... 109 II.1 X, Y Coordinates,"t" and P2O5 of Sampling Points ....................................... 112 III.1 Calculated tonnage and average assay at area II ........................................... 116 vii List of Figures List of Figures FIGURE 1.1: A DIAGRAM EXPLAINS THE OBJECTIVES OF THE PROJECT ................................................... 7 FIGURE (2.1) THE BELT OF THE PHOSPHATE ....................................................................................... 12 FIGURE 2.2 THE LOCATION MAP OF EL MAHAMID . ............................................................................. 17 FIGURE 2.3: A DIAGRAM OF GL & LCL. ................................................................................................... 19 FIGURE2.4................................................................................................................................................... 21 FIGURE 2.5. ................................................................................................................................................. 21 FIGURE 3.2: TRIANGULAR MODEL SHOWING DRILL HOLE LOCATIONS AT CORNERS OF TRIANGLES, AND AVERAGE VALUE FOR THE HOLES. THE GRADE FOR EACH TRIANGULAR PRISM-SHAPED AREA IS FOUND BY AVERAGING THE THREE VALUES AT THE CORNERS. ................................................... 25 FIGURE 3.3: VARIOGRAM PARAMETERS ................................................................................................ 28 FIGURE 3.4: COMMON VARIOGRAM MODELS, (AFTER, AHMED 2001) ................................................. 31 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART I) ................................................................................ 37 FIGURE 4.2.B: HISTOGRAM FOR P2O5 (PART I) ..................................................................................... 37 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART I) .................................................................................. 38 FIGURE 4.2.B: HISTOGRAM FOR “T” (PART I) ....................................................................................... 39 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART I. A) ............................................................................ 40 FIGURE 4.2.B: HISTOGRAM FOR P2O5 (PART I. A) ................................................................................. 41 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART I. A) .............................................................................. 42 FIGURE 4.2.B: HISTOGRAM FOR “T” (PART I. A) ................................................................................... 42 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART I.B) ............................................................................. 43 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART I.B) ................................................................................. 44 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART I.B) ............................................................................... 45 FIGURE 4.2.B: HISTOGRAM FOR.”T” (PART I.B) .................................................................................... 46 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART I.C) ............................................................................. 47 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART I.C) ................................................................................. 47 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART I.C) ............................................................................... 48 FIGURE 4.2.B: HISTOGRAM FOR.”T” (PART I.C) .................................................................................... 49 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART II) ............................................................................... 50 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART II) ................................................................................... 51 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART II) ................................................................................. 52 FIGURE 4.2.B: HISTOGRAM FOR.”T” (PART II) ...................................................................................... 52 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART II.D) ........................................................................... 53 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART II.D) ................................................................................ 54 FIGURE 4.2.1: QUANTILE PLOT FOR "T”(PART II.D) .............................................................................. 55 FIGURE 4.2.B: HISTOGRAM FOR.”T”(PART II.D) .................................................................................... 56 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART II.E) ............................................................................ 57 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART II.E) ................................................................................ 57 FIGURE 4.2.1: QUANTILE PLOT FOR “T”(PART II.E) ............................................................................... 58 FIGURE 4.2.B: HISTOGRAM FOR. “T”(PART II.E) ................................................................................... 59 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART II.F) ............................................................................ 60 TABLE 4.1: FREQUENCY TABULATION FOR P2O5 (PART II.F) ................................................................ 60 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART II.F)................................................................................. 61 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART II.F) .............................................................................. 62 TABLE 4.1: FREQUENCY TABULATION FOR “T” (PART II.F) ................................................................... 62 FIGURE 4.2.B: HISTOGRAM FOR. “T” (PART II.F) ................................................................................... 62 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART II.G) ........................................................................... 63 TABLE 4.1: FREQUENCY TABULATION FOR P2O5 (PART II.G) ............................................................... 64 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART II.G) ................................................................................ 64 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART II.G) ............................................................................. 65 TABLE 4.1: FREQUENCY TABULATION FOR “T” (PART II.G) .................................................................. 65 FIGURE 4.2.B: HISTOGRAM FOR. “T” (PART II.G) .................................................................................. 66 FIGURE 4.2.1: QUANTILE PLOT FOR P2O5 (PART II.H) ........................................................................... 67 viii List of Figures TABLE 4.1: FREQUENCY TABULATION FOR P2O5 (PART II.H) ............................................................... 67 FIGURE 4.2.B: HISTOGRAM FOR. P2O5 (PART II.H) ................................................................................ 67 FIGURE 4.2.1: QUANTILE PLOT FOR “T” (PART II.H) ............................................................................. 68 TABLE 4.1: FREQUENCY TABULATION FOR “T” (PART II.H) .................................................................. 69 FIGURE 4.2.B: HISTOGRAM FOR. “T” (PART II.H) .................................................................................. 69 FIGURE 5.1: A CAPTURE FROM THE "O.R.E. SOFTWARE" SHOWING THE VALUES OF THE SAMPLING POINTS (PART I) ................................................................................................................................ 75 FIGURE 5.2: A CAPTURE FROM O.R.E SOFTWARE SHOWING THE THICKNESS OF THE BOREHOLES (PART I) 75 FIGURE 5.3: CONTOUR MAPS FOR CARBON, ASH AND SULPHUR OF THE (PART I) USING THE TRIANGULAR METHOD A) PLOTS USING SURFER 7 B) PLOTS USING O.R.E. SOFTWARE ................. 81 FIGURE 5.6: CONTOUR MAPS FOR CARBON, ASH AND SULPHUR OF THE (PART II), USING THE TRIANGULAR METHOD A) PLOTS USING SURFER 7 B) PLOTS USING O.R.E. SOFTWARE ................. 82 FIGURE 5.7: OUTPUTS FROM VARIOWIN SHOWING THE VARIOGRAMS OF CARBON ........................... 83 FIGURE 5.8: CONTOUR MAPS AND 3D REPRESENTION FOR THE THICKNESS, ELEVATION AND OVERBURDEN FOR (PART I), CALCULATED BASED ON (OK) ............................................................. 84 FIGURE 5.9: CONTOUR MAPS AND 3D REPRESENTATION FOR THE CARBON, ASH AND SULPHUR FOR (PART I), CALCULATED BASED ON (OK) ............................................................................................. 85 FIGURE 6.1: SURFACE MINING PATTERN SHOWING EXTRACTION AND DEVELOPMENT (DIGISTAR, 2004). 88 FIGURE 6 2: MAIN OPERATIONS IN SURFACE AND UNDERGROUND MINING METHODS (DIGISTAR, 2004) 89 FIGURE 6 3: EXTRACTION OF ORE USING SURFACE MINING, (TAKEN FROM ELNASRMINING.COM). ... 90 FIGURE 6.4: TYPE OF TRENCHES, (AFTER, EL-ABDE RASSOUL, 1978). .................................................... 93 FIGURE 6.5: SHAPE OF TRENCHES. ......................................................................................................... 93 FIGURE 6.6: A PICTURE SHOWING THE BENCHES AND TRENCHES. (REFERENCE) ................................. 94 FIGURE 6.7: PERCUSSIVE DRILLS FOR REMOVING THE ORE AT EL MAHAMID. ...................................... 96 FIGURE 6.8: DRILLING OPERATION AT THE STUDY AREA (ELNASRMINING). ......................................... 97 FIGURE 6.9: REMOVING ORE (AFTER RANDALL, 1998). ......................................................................... 99 FIGURE 6.10: LOADING OF PHOSPHATE AT THE EXTRACTION AREA OF MAHAMIED, PICTURE TAKEN IN 2004. 100 FIGURE 6.11: AN EXAMPLE OF THE TRUCKS USED AT EL MAHAMID. ............................................... 101 FIGURE 6.12: DUMPING OF THE OVERBURDEN AT EL MAHAMID PHOSPHATE MINE. ..................... 101 FIGURE 6.1: A DIAGRAM FOR THE PROPOSED MINING INFORMATION SYSTEM (MIS) ....................... 103 FIGURE III.1: TRIANGULATION NET OF ZONE "D" AT EL MAHAMID AREA II. ................................... 117 FIGURE III.2: TRIANGULATION NET OF ZONE "E" AT EL MAHAMID AREA II. .................................... 117 FIGURE III.4: TRIANGULATION NET OF ZONE "G" AT EL MAHAMID AREA II. ................................... 118 FIGURE III.5: TRIANGULATION NET OF ZONE "H" AT EL MAHAMID AREA II. ................................... 119 ix List of Tables List of Tables TABLE I-1: CONT. ...................................................................................................................................... 110 TABLE I.1: CONT. ...................................................................................................................................... 111 x List of Abbreviations List of Abbreviations AR Apparent Electric Resistivity. GL Gamma Logging. SP Potentials of Self-Polarization. ML Micro Logging. LCL Lateral Current Logging. IMP/min Impulses/min. Cr2Vs The Variegated Shales sub-Formation. Cr2Ph The Phosphorite sub-Formation. Cr2Ph1 The Lower Productive Carbonate-Phosphate Member. vod Velocity of Detonation. ANFO Ammonium Nitrate and Fuel Oil. OK Ordinary Kriging SD Standard Deviation SK Simple Kriging xi List of Ssymbols List of Symboles B Max. Height of burden. K Const. depending on rock characteristics. d Borehole diameter. P Detonation pressure. T Ultimate tensile strength of rock. S Spacing between boreholes. H Length of borehole ρ Density of explosives. γ Volumetric weight of the material. α Slope angle of slip plane. H Vertical face height. C Force of cohesion. Hv Maximum height of the vertical face. φ Angle of repose. Hdmax Maximum digging of the excavation. a Width of the broken down of material formed. β Slope angle of the face. k Loosening factor of the face material. Ratio of length of least resistance line of first raw of blast holes to height. Ratio of distance between rows of blast holes to length of line of least resistance. Rd Digging radius. RL Loading radius. Chapter 1 Chapter 1.1 Introduction and Objectives 1 Introduction and Objectives Introduction Phosphate mining in Egypt started on 1940 when the first Phosphate mine was inaugurated in Safaga, Qusseir, and Hamrawein. In 1988, the exploit reserves in Egypt were 3325 million ton, which presented 6.22 % from the phosphate in Arab world Phosphorus is the eleventh most abundant element in the lithosphere. Owing to its relative reactivity, it generally is associated with calcium (Ca), sodium (Na), fluorine (F), chloride (Cl), metals such as iron (Fe), aluminium (Al), magnesium (Mg), heavy metals, for example cadmium (Cd), radionucleids like uranium (U) etc. Phosphate ores can be used in many industrial fields such as: 2 Chapter 1 Introduction and Objectives 1. The manufacture of the elemental phosphorous. 2. Phosphoric acid and its salts. 3. For making Ferro-phosphorous. 4. Metallurgical industries. 5. Phosphate ores are used in few cases for uranium extraction. 6. Fertilizer industry. 7. Photography. 8. Cosmetics. 9. Ceramics. 10. Insecticides. 11. Medicine. 1.1.1 Classification of Phosphate Rocks 1.1.1.1 Classification according to its grade: Poor grade P2O5 ranges from (15-22%). Medium grade P2O5 ranges from (22-27%). Rich grade P2O5 grater than (28-38%). 1.1.1.2 Classification according to its gangue minerals: Siliceous Ores: These contain Qz, Chalcedony and different forms of silica. Clayey Ores: These mainly contain clays and hydrous iron and aluminum silicates or oxides as gangue materials. Calcareous Ores: These contain calcite and dolomite as the major impurities with small amounts of silica. 1.1.2 Production Costs and Phosphate Availability A number of analysis on production costs for different producing mines and potential mines and deposits have been made. The most significant factors altering the cost situation for recovery and processing of phosphate rock and 3 Chapter 1 Introduction and Objectives thus the profitability would be; accessibility of the ore, degree of beneficiation required, capital investment, operating costs and, availability and cost of other resources.(Phosphorus & potassium,1998). Some calculations shown in Figure (1.1) are important for the estimates of the amount of commercially exploitable phosphate deposits. There, calculations were made in 1985; nevertheless the analysis is still relevant. Figure 1.1 1.2 Phosphate rock production cost (Website, 2004). Objectives The main objective of this graduation project is to use the previous mining courses and recent knowledge to re-estimate the ore reserves at Mahamied Phosphate Mine, Esna, Egypt. Evaluating the ore reserves has been done using the triangular method the methodology using Excel it has been taken into consideration several factors that might affect the accuracy of estimating the reserves using the manual method, among these factors, the screening and statistical analysis of the raw data before calculations. 4 Chapter 1 Introduction and Objectives Another objective of this graduation project is to use the available data and information from El Mahamid Mine to add a new record to a big database for the Egyptian mines. 1.3 Research Approach The Egyptian Geological Survey has provided the data used throughout this work. These data are given in Appendix I at the end of this dissertation. About 193 sampling boreholes with there X, and Y coordinates as well as P2O5 at part I and part II of study area. The work in this research can be divided into three main steps, see Figure (1.2). Understanding the data by running an intensive statistical analysis over the given data, such as screening the data to show the mean, modem, median, minimum, maximum, range, standard deviation, skew, histograms, normality, …etc. Determining the ore reserves, all thickness and average assay and use it to determining the tonnage and then calculate the total ore reserves. The calculation has been done using Excel and based on the triangular method. Preparing the data, the thickness and P2O5 to Mining Information System using Database for Egyptian Mines and use El Mahamid Phosphate mine as a new record to be added to the database this will be a part of a big project for the Egyptian mines in the near future. 1.4 Dissertation Organisation The dissertation lies in seven Chapters and two appendices in addition to a Compact Disc (CD) for the results and information. Chapter one gives an idea about the selected mining area and its historical background and the objectives of the work followed by the approach applied to achieve the objectives. Chapter two presents a literature review of the geological and geophysical studies of El 5 Chapter 1 Introduction and Objectives Mahamid area, its location, formations, and structural geology. Chapter three introduces the concepts and principles of the methods and techniques that used throughout this work, mainly the triangular method, variorums, and Kriging techniques. Chapter four starts with over viewing the available data at the study area and proceeds to the statistical analysis of all the variables. and ended with the possible correct sampling data that used through out the project for ore reserve estimation and calculating the average thickness and average assay of phosphate ore at El Mahamid area Chapter five illustrates the results obtained from implementing the different methods and techniques for ore reserve estimation and contouring the different variables, analysis and discussion of the results. Chapter six addresses the possible information and data can be to feed MIS that would involve in the future all the Egyptian mines also highlights the parameters and mining method. Finally, Chapter seven has reserved for the conclusions and recommendations. The dissertation presents in 116 Pages, 89 Figures and 37 Tables. The students have used 5 Softwares’ programs and several computer facilities (Internet, scanners, printers, and editing facilities) at the computer laboratory, Mining and Metallurgical Engineering Department, Faculty of Engineering, Assiut University. 6 Chapter 1 Introduction and Objectives Figure 1.1: A diagram explains the objectives of the project 7 Chapter 2 Chapter 2.1 Geological and Geophysical Studies 2 Geological and Geophysical Studies Introduction The aim of this chapter is to review the geological and geophysical studies related to the extraction of the phosphate ores in general, and thus focus on the case of El-Mahamied phosphate ores, Esna, Egypt in particular. This Chapter is divided into two main parts, the first is the background about the geological studies and the second will cover the appropriate geophysical methods or techniques that are used for exploration of phosphate deposits. 8 Chapter 2 Geological and Geophysical Studies 22 Geological Studies 221 Occurrence and origin of the world phosphate rock There are two main types of phosphate rock deposits, igneous and sedimentary, which have widely differing mineralogical, textural and chemical characteristics. Marine sedimentary phosphate beds, such as those of USA, are marine chemical deposits in large enclosed basins. This type also yields the important North African production. Apatite deposits are concentration of Apatite in begmatites, veins, and magmatic segregation’s of igneous rocks. They are little worked today except in Russia and Sweden. Over 30 countries are currently producing phosphate rock for use in domestic markets and/or international trade. The world’s top 12 producing countries account for nearly 95% of the world’s total phosphate production. The three major producing countries, i.e. the Morocco, China and USA, currently produce approximately two thirds of global phosphate production. Of these three major producers, Moroccan reserves account for around 50% of the world total. Morocco is also in the most advantageous situation as its potential reserves and geological in situ resources have been estimated to be approximately 60% of total world resources. The USA and China have between them around 20% of global resources. Current World phosphate rock production capacity is estimated at around 165195 million tons/year, or approximately 50 or more million tons /year P2O5. High – grade phosphate rock is available from many sources, such as Togo, Senegal, and Morocco. (Phosphorus & Potassium, 1998). 9 Chapter 2 Geological and Geophysical Studies Table (2.1) shows the amount of phosphate rock reserves in the most important countries in the world. Table 2.1 % of total (1996) United States China Morocco Russia South Africa Tunisia Jordan Iraq Brazil Peru All other Countries Global phosphate reserves, (After USGS, 1996). Production % Reserves Million ton 34 16 16 6 2 5 4 3 14 4 - 10 2 - 25 46 – 53 3 9 - 22 1 2-3 1 1-3 1 Potential Reserves Million ton 7 - 13 2 – 10 63 7 - 10 3 - 22 1 1–3 3 1-2 - Geological Reserves Million ton 25 9 50 9 3 1-2 1-2 2-3 1 1-2 Table (2.2) shows the production of phosphate in the Arab World. (B.Sc 1988) Table 2.2: No Arab country Phosphate in Arab World Exploit reserves 1 Morocco 40000 % 75.5 2 3 4 5 6 7 8 9 10 Egypt Spanish Sahara Iraq Jordan K.S.A Syria Algeria Palestine Tunisia 3325 3000 1760 1062 912 800 642 630 885 6.22 0.66 3.3 2.0 1.7 1.6 1.2 1.2 1.6 From the above table it is noticed that Morocco has the largest reserve in the Arab World. 10 Chapter 2 Geological and Geophysical Studies 2. 2. 2 Chemical and Physical Properties of Phosphate According to Pettijohn rocks containing more than (19.5%) P2O5 (about 50% Apatite) are defined as phosphorites; if they contain more than (7.8%) P2O5 (about 20%Apatite), they are described as phosphatic. 2 .2 .2 .1 Colors Phosphate rock is an earthy substance varying from a hard rock to a granular, loosely consolidated mass. Its color may be brown, gray, bluish gray, white or dark gray. 2 .2 .2.2 Hardness It varies in apparent hardness from (2-5). The Mineralogical Composition Of Phosphate Ores is shown in Table (2. 3). Table 2. 3: .No 1 2 3 4 5 6 2. 2.3 Minerals Dahllite Cllophane Fluor Apatite Chlor Apatite Hydroxy Apatite Apatite Mineralogical composition. Mineralogical Composition 9CaO.3P2O5.CaCo3.H2O 9CaO.3P2O5.CaCo3.H2O + H2O 9CaO.3P2O5.CaF2 9CaO.3P2O5.CaCl2 9CaO.3P2O5.Ca(OH)2 9CaO.3P2O5.Ca Phosphate in Egypt Phosphate ores, the principal mineral product of Egypt, are widely distributed in four main localities, namely, The Eastern Desert, Sinai, the Nile valley and the Western desert. The old phosphate mines at Safaga, Qusseir and Hamrawein where actually working since 1940.(B.Sc project 1988). The most important group of localities lies in the Qusseir-Safaga phosphatemining region in the Eastern Desert along the Red-Sea coast. The chemical compositions of these phosphorites are the Calcium and \ or Magnesium carbonates and Silica. 11 Chapter 2 Geological and Geophysical Studies The second group of localities includes those of Dakhla-Kharge region and Abu Tartur plateau. In Kharga, the P2O5 content of the phosphorite beds varies widely from less than 10% to a max. of 28% . In Dakhla, the P2O5 varies from (13-30%). The third group of localities lies in the Nile valley and includes the districts of Sibaiya and Idfo. The composition of the phosphorites varies according to the nature of its cementing material, e.g., the carbonate variety contains the following minerals: phosphate mineral (52.0), calcite (38.3), dolomite (1.4), quartz (4.2), clay (2.0), gypsum (1.2), limonite (1.0). The fourth group of localities of phosphate rock, which comprises minor deposits, occurs in the Gulf of Suez and central Sinai area. This includes Gabal el-Zeit, in The Eastern Desert, as well as wadi Gharandal and Gabal Tanka on the Eastern coast of the Gulf of Suez in Sinai. Figure (2.1) shows the belt of the phosphate in Egypt: Figure (2.1) The belt of the phosphate 12 Chapter 2 2.2.4 Geological and Geophysical Studies Nile Valley Phosphate The Nile valley phosphorite deposit is a part of the vast upper cretaceous marine phosphorite basin, which covered a considerable part of the Egyptian territory, and extended father into Jordan, Palestine, Syria and Iraq. The thickest accumulation of the Egyptian phosphoites occur along the base of the sequence at Abu Tartur (Kharga Oaasis), near the top of the sequence in the base and top of the sequence on the Red sea coast. These phosphorites are commonly composed of multiple accumulations of thinner individual beds. The phosphate-bearing sediments in the Nile valley region belong to the Duwi formation and having a total thickness of 25-40 m. 2.2.4.1 The Location and the topography El Mahamid deposit occupies a vast area of a bout 250 km2. Along the left and right banks of the Nile, to the south of the Qena and Luxor, between the towns of Esna and Idfu. The bounding coordinates latitudes (250 15/and 250 5/ N) and longitudes (330 32/ and 330 00/ E) .the area of the deposit is separated by the Nile Valley into the western Mahamid on the left bank and the eastern Mahamid on the right bank. 2.2.4.2 Stratigraphy and position of the phosphorites in the succession The Cenomanian stage The Cenomanian-Santonian-Campanion stages The Campanian stage The Danian stage The Paleocene The Lower Eocene 2.2.4.3 Geological setting El Mahamid deposit is mainly confined to the upper cretaceous marine sediments distributed in both the eastern and western areas. The overlying Paleocene sediments form the topographic highs, which limit the eastern area from the north and North-West. Stratigraphically, the 13 Chapter 2 Geological and Geophysical Studies upper cretaceous sediments are represented by rocks of the Campanian and Maestrichtian stages and are subdivided into two formations, which are, from bottom to top, the Duwi and Dakhla formations. The Duwi formation (companion) In the area of the deposit, this formation is litho logically subdivided into two sub-formations namely: The variegated shales sub-formation (Cr2 VS). The phosphorite sub-formation (Cr2 Ph). The important sub-formation is the second one (Cr2 Ph) it is measure from (20 to 32 m) in thickness and is subdivided into three members: Lower productive carbonate-phosphorite member (from 2-3 to 10-12 m). Middle phosphorite-clayey member (from 6-12 m). Upper phosphorite-clayey member (from 7-10 m). The lower productive carbonate-phosphorite member (Cr2 Ph1), which includes commercials phosphorite beds, is the main object of the investigations carried out in the area. 2) The Dakhla formation (Maestrichtion) The Dakhla clays, in general, do not contain neither phosphorite intercalation nor poor phosphatic marls and limestone. 2.2.4.4 The main features of the productive carbonate-phosphorite Phosphate El Mahamid included two features, are given below: Western Mahamid. Eastern Mahamid. 1) Eastern Mahamid The productive member in the Eastern Mahamid area is rather variable. Accordingly, the different prospected areas will be dealt with separately: The Sharawna area. The Oweiniya area. The Hagariya and Qurayat areas. 14 Chapter 2 Geological and Geophysical Studies Mussattah Yassin. 1) Sharawna area; in this area the productive member lies a relatively great depth from the surface. The features of this area are: Over the greater part of the area, the average p2o5 content (20-22%). And the average thickness of the bed is (0.65-0.70 m). The lower and upper phosphorite beds with thickness (1.0-1.2 m). The upper phosphorite bed with an average content (18-19%P2O5), and poor oyster phosphorites with (10-12%P2O5) and with thickness of (0.8-0.95 m). 2) The Oweiniya area, this area is the continuation of the Sharawna area, the features of this area are: The lower phosphorite bed attains an average thickness of (0.5-0.6 m). With content of (8-15 % P2O5). The carbonate- bearing ores, the average thickness of these carbonate rocks is range from (3.0-3.5 m) sometimes it reaches 5 m. Both the upper and lower phosphorite beds are characterized by facial nonpersistence. A Poor phosphatic oyster limestone bed, up to 4.5 m thick. 3) The Hagariya and Qurayat areas, the features of these areas are; The lower phosphorite bed with average content of (24-26 %P2O5) and its average thickness is (0.6 m) at Hagariya and (0.8 m) at Qurayat. The carbonate rocks are represented by poor phosphatic marls ranging in thickness from (0.5-0.6 m) at Qurayat, and from (0.8-1.0 m) at Hagariya. The upper phosphorite bed of the Hagariya area, its thickness ranges between (0.2-1.5 m). 15 Chapter 2 Geological and Geophysical Studies The section of the productive member is terminated by poor phosphatic marls and oyster limestones. 4) Mussattah Yassin area, the features of this area are: The lower phosphorite bed, with average content ranging between (17-18% and 23%). Its average thickness is (0.65-0.7m). The poor phosphatic oyster limestones from abed (2.0 to 4.0m) thick. The upper phosphorite bed, with average content of (16-19%p2o5). Its thickness does not usually exceed (0.45 m). The section of the productive member is terminated on top by a bed of poor phosphatic oyster limestone. Figure (2.2) shows the location of El Mahamid area; 16 Chapter 2 Geological and Geophysical Studies El Mahamid Figure 2.2 The location map of El Mahamid . 17 Chapter 2 2.3 Geological and Geophysical Studies Geophysical Investigation Geophysical methods have been applied to the investigation of drill holes for some forty-five years. Using initially the same electrode techniques as in surface exploration. The various instruments and techniques, specifically designed to suit the different environment in drill holes, are used in direct exploration, identification of geologic formation and formation fluids, and correlation between holes. Geophysical methods which have been applied in well logging include resistivity, self-potential induction, induced-polarization and occasionally other electrical methods, detection of gamma-rays and neutrons in radioactivity methods, acoustic logging, and measurement of magnetic and thermal properties. (Applied Geophysics 1974). The aim of logging operations was to determine: Thickness Structure Depth of occurrence of the phosphorite- bearing beds The work was started in October 1966 and had been continued till the middle of December 1967.During this time 228 bore hole were logged (in this number 118 in the area of western Mahamid, 110 in the eastern Mahamid) which amount to about 65% of the total number of the drilled bore holes (The total amount of bore holes are 350 In this study we work with 201 B.H. which presented 57 % from the total number of the area) (Dr. Rushdi Said, 1968 ). The following logging methods were tried: AR (apparent electric resistivity) GL (gamma logging) SP (potentials of self-polarization) ML (micro logging) This work resulted in recognition of the preliminary characteristics of the section by its physical properties: 18 Chapter 2 Geological and Geophysical Studies Apparent electric resistivity Natural gamma activity Natural electro –chemical activity The above work aimed to obtain: Data concerning phosphorites Summarize data on detect ability of each of the method Study practical possibilities of these methods The geological setting of the deposit It was stated that the depth of the bore holes ranges from (8-35m) and logging intervals vary from (4-25m) 2.3.1 Importance of some logging methods 2.3.1.1 The GL method Allows to detect with assurance phosphate- bearing beds as no other rocks with increased intensity of natural gamma – radiation occur in the section. Accuracy in definition of the bed structure will be increased if to interpret simultaneously the diagrams of GL and LCL (Figure (2.3)). 1-Cable-.K.T.SH- 2 2-The body of GL Borehole apparatus, it is also used as screen electrode A1,A2 OFL 3-Free wire of the cable 4-Rubber insulator 5-Lead electrode. A0 RE – Equivalent resistance of GL apparatus scheme Figure 2.3: A diagram of GL & LCL. 2-The Lateral Current Logging (LCL) curves 19 Chapter 2 Geological and Geophysical Studies a) Allows to distinguish in the phosphorite bed barren interbeds b) Understand their contacts, so a joint use of the GL & LCL methods enables to solve satisfactory the tasks of logging. 3-The method of AR Electrochemical activity and ML were not used in a further work. 2.3.2 Radioactivity logging Gamma Logging (GL): Gamma logging was used for detecting the phosphorite beds and the other rock types. 2.3.3 Interpretation of gamma logging measurements Different intensity levels of gamma radiation were recorded inside every bore hole which corresponds to different concentration of radioactive elements in the rocks, within the geological section measured, the a mount of radiation characterized a certain type of rocks. Thus, depending on the concentration of the radioactive elements. There are many factors that may affect the intensity of gamma radiation; the cementing materials; solidification of phosphorites; grain size; cavities; and casing pipes in bore holes and mud fluids. All the measurements of gamma logging are expressed only in imp/min (impulses/minute). It represents a cylindrical metallic capacity, hermetically sealed, with the hole in the center of the axis. The diameter of the hole is equal to that of the welldevice. The capacity was completely filled with crushed phophorite. Gamma logging diagrams were recorded in two scales: 1-1:100 searching and the speed of recording was 500-700 m/h 2-1:50 detailed one and the speed of recording not more than 300 m/h 20 Chapter 2 Geological and Geophysical Studies 2.3.3.1 Methods of interpretation Experimental operation by the GL method was carried out at the model B.H. aiming at checking the methods of interpretation applied. The diagrams obtained were interpreted and compared with the real section of the model. In all cases discrepancy in thickness did not exceed 5 cm. (see Figures (2.4), (2.5). Figure2.4. Figure 2.5. 2.3.4 Conclusions As it was mentioned above in the area under investigations all the phosphorites are characterized by the increased radioactivity and apparent resistivity. These physical properties of the phosphorites are favorable for their detection in the section with the help of; 21 Chapter 2 Geological and Geophysical Studies Gamma logging (GL) Lateral current logging (LCL) The arithmetical mean error in determination of thickness by means of logging was calculated to be (plus or minus 0.09 m or 11% from the 0.76 m). A remarkable dependence was noted between the intensity of natural gamma radiation and P2O5content in the productive beds. This served as the basis for searching of quantitative characteristic of such dependence. I (gamma) = f (P2O5%). Where; I (gamma) is intensity of natural gamma activity according to the GL data. P2O5 is content in percent by the chemical analysis data. Efficiency of logging in prospecting of the phosphorite deposits can be quantitatively estimated .The results of the control drilling and pitting showed that the thickness of the phosphorite horizons, according to the logging data, were determined with average increase equal to 20% over the whole area under studies. The cost of the logging team does not surpass 3% from the total expenses on geological and prospecting works all this evidence indicates convincingly geological and economical efficiency of logging all stages of prospecting for phosphorites. From the above work we can say that we use both of GL & LCL methods for the investigation in El Mahamid area, the actual amount of bore holes used were 201B.H. In the next chapter we will illustrate the statically analysis of the data and calculation of average thickness, average grade of P2O5 in the area with 22 Chapter 2 Geological and Geophysical Studies different methods In addition to Wadies running off the scraps, there are other more major ones running parallel to the strike or in faulted areas, and the access road makes use of two such Wadies, the Masagid and the Muzeira. These larger Wadies often have deep alluvium, sometimes with readily apparent terrace levels, probably a result of the very different climatic conditions from late Pliocene to early Pleistocene times. 23 List of Ssymbols Chapter 3.1 3 Ore Reserve Estimation Methods and Techniques Introduction The purpose of this Chapter is to demonstrate the principles, concepts and mathematical functions for the methods and techniques that are using for ore reserves estimation. It is proposed to examine two conventional methods (Polygon method and Triangular Method) and one of the geostatistics techniques (Ordinary Kriging). 3.2 Conventional Methods 3.2.1 Triangular Method The triangular method is similar to the polygonal method. It calculates the volume of a triangular-shaped prism formed between three adjacent drill holes Chapter 3 Ore Reserve Estimation Methods and Techniques (Figure 3.2). Like the polygonal method, bench levels are specified. Grade determinations for the prisms are determined differently than the polygon model. In the triangular model, the grade is determined by averaging the value of the three values at the corners of each triangle. 3 2 1 5 4 8 7 6 Borehole Grade% Triangle 1 2 3 4 5 6 7 8 1-2-4 1-4-6 2-3-5 2-4-5 3-5-8 4-5-7 4-6-7 5-7-8 0.12 0.21 0.17 0.50 0.33 0.05 0.26 0.15 Figure 3.2: Average Grade% 0.277 0.223 .0.237 0.346 0.217 0.363 0.270 0.247 Area m² 14.5 21.6 21.1 26.2 14.9 28.2 29.7 22.3 Results Total Area = 178.5 Total Area * Grade=49.9 Average Grade = 0.280 Triangular model showing drill hole locations at corners of triangles, and average value for the holes. The grade for each triangular prism-shaped area is found by averaging the three values at the corners. A) For each triangle 1) Average thickness ( h Av. ) = h1 h2 h3 …….…………………………(3.1) 3 2) Average assay ( AAv. ) = A1h1 A2 h2 A3 h3 …………………...…..(3.2) h1 h2 h3 3) Area (a) = p p L1 p L2 p L3 …………..…..(3.3) = a1h1 a2 h2 a3 h3 .......... an hn ……..….(3.4) a1 a2 a3 .......... an B) For whole area 1) Average thickness 25 Chapter 3 Ore Reserve Estimation Methods and Techniques 2) Average assay = a1hAv.1 AAv.1 a2 hAv.2 AAv.2 a3 hAv.3 AAv.3 .......... an hAv.n AAv.n ………....(3.5) a1hAv.1 a2 hAv.2 a3 hAv.3 .......... an hAv.n 3) Volume Area * Averagethickness ……………….(3.6) 4) Tonnage Volume .……………………………………(3.7) T .F Where: 3.3 h: A: a: T.F: Thickness of borehole, m Assay of metal, % Area of triangle, m2 Tonnage Factor, t/m3 L: p: Length of triangle side Half periphery of triangle = X 1 X s Y1 Ys = (L1+L2+L3 )/2 2 2 Geostatistics Techniques Geostatistics is the statistics of spatially or temporally correlated data . The technique has been used to be a practical approach to the problems of ore reserve estimation and mine planning. It has been also used for other applications concerned with petroleum and gas resources estimation. One of the characteristics that distinguish earth sciences data from most other data is that the data belongs to same location in space. Spatial features of the data set such as the location of extreme values, the overall trend, or the degree of continuity are of considerable interest (Isaaks and Srivastava, 1989). These features, in other words the variables Z(x), are functions describing natural phenomena that have geographic distributions, such as the elevation of terrain, the depth of groundwater table, or the ore grade within an ore body. In Practice, the application of geostatistics techniques is carried out in two fundamental steps: 1. Construction of the variograms 2. Conducting one of the suitable Kriging technique 26 Chapter 3 3.3.1 Ore Reserve Estimation Methods and Techniques Variogram Modelling A variogram is graph illustrating the average variability between samples and the distance between samples. The variogram can be described as variation in values among samples some distance apart as a measure of their spatial correlation. The mathematical formulation of variogram function is as follow: 2 N 1 z( xi ) z( xi h ) .……………………………………(3.8) (h) 2 N ( h ) i 1 Where Z(Xi) and Z(Xi+h) are two samples at Xi and Xi+h locations separated by h distance. The simplest method of comparing two sample values is to calculate the difference between two samples. When comparing a large number of sample pairs, the following will be found. Some difference will be positive and some will be negative. By squaring the difference, all become positive. Differences are measured between samples at similar distances apart are squared and averaged. One the results of these samples mean-squared difference measurements difference measurements are calculated, they can be displayed as simple X-Y scatter plot. Distance between samples is plotted on the X-axis and is labeled with an h; and, average squared differences between samples are plotted on the Y-axis and are labeled with the Greek letter for Gamma (γ). This graph is called a variogram by geostatisticians. After the graph is constructed, a line is drawn connecting the posted data. This variogram or semivariogram is commonly referred to as the experimental variogram. (Rashad 2002) Semivariogram is another term commonly used by geostatisticians. 27 Chapter 3 Ore Reserve Estimation Methods and Techniques Semivariogram plot distance (h) verses one-half the average squared differences (γ/2) rather than distance verses average squared differences as with the variogram. Semivariograms use the one-half factor so that plotted values are equivalent to the statistical variance. Most geostatistical practitioners calculate semivariogram, but refer to the displayed results as variograms. The shape of the variogram does not change when 2 divide the Gammas. The final step in analyzing the variogram is to compare the experimental variograms to models, which can be characterized by mathematical functions. This comparison about statistical spatial data variability can be made. The process of construction and modeling variogram is called variography. Figure 3.3, shows the main parameters calculated from the variograms, which Variogram (γ) are defined in Table 3.1. Figure 3.3: Variogram parameters 28 Chapter 3 Ore Reserve Estimation Methods and Techniques Table 3.1: Nugget Effect Definition of variogram parameters Quantifies the sampling and assaying errors and the short scale variability (i.e. spatial variation occurring at distance closer than the sample spacing). Scale (C) Is the vertical scale for the structured component of the variogram Each component of a variogram model has its own scale. Sill Is the total vertical scale of the variogram (Nugget Effect + Sum of all component scales) Linear, Logarithmic, and power variogram models not have a sill. Length Is the horizontal range of the variogram (Some variogram models do not have a length parameter; e.g. the linear model has a slope instead). Variance Is the mean squared deviation of each value from the mean value Variance is indicated by the dashed horizontal line in the diagram shown above. Pairs Represents the average value for the group of pairs separated by a specified distance (lag width) the number adjacent to the square symbols indicates the number pairs within each lag distance. Model Curve Shows the shape of the variogram model. Experiment Curve Displays the groups of variogram pairs on a plot of separation distance versus the estimated variogram. In order to be able to define characteristic quantities for the semivariogram, a model is often assumed. The basic variogram models, which are simple and isotropic, can be divided into two types. Those that reach a plateau and those 29 Chapter 3 Ore Reserve Estimation Methods and Techniques that does not. The most common variogram models are presented in Figure 3.4. The models occurring most often in literature are the spherical, the exponential, and the Gaussian (Isaaks and Srivastava, 1989). Spherical model: is probably the most commonly transition model. It is equation is given by: C 0 C[3h / 2a (h 3 / 2a 3 )] ha ........... …………………………….(3.9) ha C 0 C ( h) Where: C0 C C0 + C a is the random component of variation, i.e. the nugget effect variance. is the structural component of the variance. is the total variation or sill. is the range of influence. Exponential model: is another commonly used transition model. Its equation is given by: (h) C0 C[1 exp( 3h / a)] ………………...……………………………….(3.10) Gaussian model: is a transition model that is often used to model extremely continuous phenomena. Its equations is: (h) C 0 C[1 exp( 3h 2 / a 2 )] …………………………………………..….(3.11) Power model: linear model is not a transition model since it does not reach a sill, but increases linearly with h. In its standardised form it is written simply as: (h) C 0 C h …………………………………………………………...….(3.12) a Where: a is the slop. A variogram model should not be needlessly complex. Ideally, each variogram structure should have a physical interpretation. The more complicated the variogram model, the longer it takes to construct each Kriging matrix; hence, the longer the Kriging or simulation program will take. 30 Chapter 3 Ore Reserve Estimation Methods and Techniques h) h) Sill C C0 range a h Spherical model Exponential model h) h) h h Linear model Figure 3.4: 3.3.2 h Gaussian model Common variogram models, (after, Ahmed 2001) Kriging The Kriging technique is named after the South African geostatistician D. J. Krig. It is a technique for determining the best linear unbiased estimator with minimal estimation variance. It can be used on a point as well as on a block A Block is simulated by numerous point that are then integrated (Wellmer, 1998). Kriging was developed for the very specific application of predicting gold reserves in mines in South Africa from borehole information. It owes a great deal to the contribution of Matheron and his co-workers at the Ecoles des Mines (Mackay and O’Connell, 1991). Swan and Sandilands (1995) studied the difference between Kriging techniques and the other estimation methods and found that Kriging is a different and spatial way of making estimates of spatially distributed values from point value. The following are the key elements involved: Several Kriging techniques have found in literature. According to different requirements of different problems, one refers to simple Kriging when the mean is known and constant; universal Kriging and intrinsic Kriging that allow 31 Chapter 3 Ore Reserve Estimation Methods and Techniques fluctuations in the mean; log-normal Kriging when processing the logarithms of the original data; or other types of Kriging techniques described in literature. The following section describes the equations of the Kriging system. 3.3.2.1 Equations for the Kriging system without and with a known mean The Kriging matrix K contains the variance (e.g.σ11) and covariance (e.g.σ12) of all the points Xi (I=1, 2, ……, n) around the reference point P that are included the weighted σij is the covariance between the values Xi and Xj, or (Xi ,Xj) Cov(Xi, Xj), σii are the covariance’s of a point with respect to itself (where h = 0),and thuth are identical with the variance. 11 21 K n1 1 12 ........................... 1n 22 ........................... 2 n : : n 2 ........................... nn 1 1 1 1 ……………………………...….(3.13) 1 0 This is the Kriging matrix for case (a) (Kriging without a mean).The final row and column are missing from the matrix for case (b) (Kriging with known mean) Since σik = σki the matrix is symmetrical and, for example, σ12 = σ21 regardless of whether point 1 is viewed from point 2 or the other way round, the covariance between point 1 and 2 must be the same. The spacing between the two points is the same, and it is this dimension that determined the covariance, which can be derived from the variogram. The weighting factors λi describe a vector, λ . In addition, the LaGrange multiplier μ is introduced for the case (a) of Kriging without a mean. This parameter does not occur in case (b) (Kriging with a known mean). 32 Chapter 3 Ore Reserve Estimation Methods and Techniques 1 2 : …………………………...….…………………………...….………...….(3.14) n The third dimension in Eq. (3.16) see below is the vector D . This vector contains the covariance’s of the reference point P to all the other points that are being taken into consideration: p ,1 p , 2 D : …………………...….…………………………...….………...….(3.15) p ,n 1 This is also the vector for the case (a) (Kriging with an unknown mean). The final value 1 dose not occurs in case (b) (Kriging with a known mean). The following relationship between the Kriging matrix and the two vectors is then true: k D ...….………...….………...….………...….………...….………..(3. 16) Consider, for example, the reference point P and two additional points 1 and 2, then the system (3. 16) above for case (a) (Kriging without a mean) is: 11 12 21 22 1 1 1 1 p ,1 1 2 p , 2 ……...….………...….………...….……….……...(3.17) 0 1 For case (b) (kriging with a known mean), the system (3.16) above, for the reference point P and two additional points1 and 2 is: 11 12 1 p ,1 …...….………...….………...….……….……...............(3.18) 21 22 2 p , 2 33 Chapter 3 Ore Reserve Estimation Methods and Techniques The computation of this matrix system is as follows: each value in a row of the matrix is multiplied by the corresponding value for the vector, and then they (row X column) are summed together. In case (a) (Kriging without a mean) this yield the following system of equations: 11 1 12 2 p ,1 ...….………...….…….….……….……..................(3.19) 21 1 22 2 p , 2 ………...….………..….……….……...............….(3.20) 1 1 1 2 o 1……............………………………….……………...….(3.21) This is system of three equations with the three unknowns 1 , 2 and . In case (b) (Kriging with a known mean), the system is as follows: 11 1 12 2 p ,1 21 1 22 2 p , 2 …………………………….……………………....….(3.22) The unknown μ is missing from this system, and therefore it is a simpler system with only two equations. 3.3.2.2 Advantages of Kriging technique The technique has the following useful attributes: 1. it is an exact interpolator, it returns the observed values at measurement points. 2. it is a best linear unbiased estimator. 3. the Kriging equations do not involve the measured values. 4. measurements which represent averages over some specified area 5. measurement errors can be accounted for (Mackay and O’Connell, 1991). 34 Sampling Data and Statistical Analysis Chapter 4.1 4 Sampling Data and Statistical Analysis Introduction The data used throughout this research are collected from 19 boreholes at the (PART I) and 29 boreholes at the (PART II) of Mahamied Phosphate Mine. For each sampling borehole X, Y, Z, thickness of overburden, and thickness of the seam were measured. Most of the borehole samples have a complete analysis for the following one main variable: P2O5. The aim of this Chapter is to screen the data and test the main statistical parameters, such as, measure of location, measure of shape and measure of spread. Each set of variables has been tested separately and a summary of the overall data is given at this end of the Chapter. Chapter 4 Sampling Data and Preliminary Statistical Analysis A complete record of the raw data for both (PART I) and (PART II) is given in Appendix I including the chemical analysis of the sampling boreholes. 4.2 Summary Statistics for Area I 4.2.1 Summary Statistics for whole area 4.2.1.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 70 = 23.1889 = 21.1595 = 4.59995 = 8.19 = 29.84 = -4.05057 = 2.54084 This table shows summary statistics for P2O5. It includes measures of central tendency, measures of variability, and measures of shape. Of particular interest here are the standardized skewness and standardized kurtosis, which can be used to determine whether the sample comes from a normal distribution. Values of these statistics outside the range of -2 to +2 indicate significant departures from normality, which would tend to invalidate any statistical test regarding the standard deviation. In this case, the standardized skewness value is not within the range expected for data from a normal distribution. The standardized kurtosis value is within the range expected for data from a normal distribution Percentiles for P2O5 8.19% = 1.0 13.65% = 5.0 16.825% = 10.0 21.1% = 25.0 24.465% = 50.0 25.9% = 75.0 28.16% = 90.0 29.09% = 95.0 29.84% = 99.0 This above values shows sample percentiles for P2O5. The percentiles are values below which specific percentages of the data are found. 36 Chapter 4 Sampling Data and Preliminary Statistical Analysis Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 8 12 16 20 24 28 32 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART I) Frequency Tabulation for P2O5 Frequency tabulation for P2O5 (PART I) Table 4.1: -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 5.0 2.5 0 0.0000 0 0.0000 2 5.0 10.0 7.5 1 0.0143 1 0.0143 3 10.0 15.0 12.5 3 0.0429 4 0.0571 4 15.0 20.0 17.5 10 0.1429 14 0.2000 5 20.0 25.0 22.5 25 0.3571 39 0.5571 6 25.0 30.0 27.5 31 0.4429 70 1.0000 7 30.0 35.0 32.5 0 0.0000 70 1.0000 8 35.0 40.0 37.5 0 0.0000 70 1.0000 above 40.0 0 0.0000 70 1.0000 -------------------------------------------------------------------------------Mean = 23.1889 Standard deviation = 4.59995 Histogram for P2O5 frequency The StatAdvisor 40 --------------This option performs a frequency tabulation by dividing the range of P2O5 into equal width intervals and counting the number of data 30 values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the 20 intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 10 0 0 10 20 30 40 P2O5 Figure 4.2.b: Histogram for P2O5 (PART I) 37 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4.2.1.2 Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 70 = 0.683571 = 0.115342 = 0.339621 = 0.15 = 1.55 = 2.21918 = -0.0326775 Percentiles for “t” 1.0% = 0.15 5.0% = 0.25 10.0% = 0.275 25.0% = 0.4 50.0% = 0.65 75.0% = 0.9 90.0% = 1.2 95.0% = 1.4 99.0% = 1.55 Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.4 0.8 1.2 1.6 t Figure 4.2.1: Quantile plot for “t” (PART I) 38 Chapter 4 Sampling Data and Preliminary Statistical Analysis tabulation for “t” (PART I) Table 4.1:Frequency Frequency Tabulation for t -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.225 0.1125 3 0.0429 3 0.0429 2 0.225 0.45 0.3375 19 0.2714 22 0.3143 3 0.45 0.675 0.5625 15 0.2143 37 0.5286 4 0.675 0.9 0.7875 19 0.2714 56 0.8000 5 0.9 1.125 1.0125 6 0.0857 62 0.8857 6 1.125 1.35 1.2375 3 0.0429 65 0.9286 7 1.35 1.575 1.4625 5 0.0714 70 1.0000 8 1.575 1.8 1.6875 0 0.0000 70 1.0000 above 1.8 0 0.0000 70 1.0000 -------------------------------------------------------------------------------Mean = 0.683571 Standard deviation = 0.339621 Histogram for t frequency The StatAdvisor --------------20 performs a frequency tabulation by dividing the range This option of t into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in 16 each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by 12alternate mouse button and selecting Pane Options. You pressing the can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 8 4 0 0 0.3 0.6 0.9 1.2 1.5 1.8 t Figure 4.2.b: Histogram for “t” (PART I) 4.2.2 Summary Statistics for Part I. a 4.2.2.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 26 = 23.8912 = 20.1703 = 4.49114 = 10.93 = 29.61 = -2.95294 = 1.90069 39 Chapter 4 Sampling Data and Preliminary Statistical Analysis Percentiles for P2O5 1.0% = 10.93 5.0% = 15.17 10.0% = 15.82 25.0% = 22.75 50.0% = 25.27 75.0% = 26.78 90.0% = 28.16 95.0% = 28.59 99.0% = 29.61 Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 10 14 18 22 26 30 P2O5 Figure 4.2.1: Table 4.1: Quantile plot for P2O5 (PART I. a) Frequency tabulation for P2O5 (PART I. a) Frequency Tabulation for P2O5 -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 9.0 0 0.0000 0 0.0000 1 9.0 13.0 11.0 1 0.0385 1 0.0385 2 13.0 17.0 15.0 2 0.0769 3 0.1154 3 17.0 21.0 19.0 3 0.1154 6 0.2308 4 21.0 25.0 23.0 6 0.2308 12 0.4615 5 25.0 29.0 27.0 13 0.5000 25 0.9615 6 29.0 33.0 31.0 1 0.0385 26 1.0000 above 33.0 0 0.0000 26 1.0000 -------------------------------------------------------------------------------Mean = 23.8912 Standard deviation = 4.49114 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of P2O5 into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 40 Chapter 4 Sampling Data and Preliminary Statistical Analysis Histogram for P2O5 frequency 15 12 9 6 3 0 9 13 17 21 25 29 33 P2O5 Figure 4.2.b: Histogram for P2O5 (PART I. a) 4 2 2 2 Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 26 = 0.623077 = 0.0568462 = 0.238424 = 0.2 = 1.4 = 2.19328 = 3.61473 Percentiles for “t” 1.0% = 0.2 5.0% = 0.3 10.0% = 0.3 25.0% = 0.45 50.0% = 0.65 75.0% = 0.75 90.0% = 0.8 95.0% = 0.9 99.0% = 1.4 41 Chapter 4 Sampling Data and Preliminary Statistical Analysis Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.3 0.6 0.9 1.2 1.5 t Figure 4.2.1: Quantile plot for “t” (PART I. a) Frequency Tabulation Table 4.1: for tFrequency tabulation for “t” (PART I. a) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.25 0.125 1 0.0385 1 0.0385 2 0.25 0.5 0.375 7 0.2692 8 0.3077 3 0.5 0.75 0.625 13 0.5000 21 0.8077 4 0.75 1.0 0.875 4 0.1538 25 0.9615 5 1.0 1.25 1.125 0 0.0000 25 0.9615 6 1.25 1.5 1.375 1 0.0385 26 1.0000 above 1.5 0 0.0000 26 1.0000 -------------------------------------------------------------------------------Mean = 0.623077 Standard deviation = 0.238424 Histogram for t frequency 15 The StatAdvisor --------------This option 12 performs a frequency tabulation by dividing the range of t into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in 9 while the relative frequencies show the proportions in each interval, each interval. You can change the definition of the intervals by pressing the 6alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 3 0 0 0.3 0.6 0.9 1.2 1.5 t Figure 4.2.b: Histogram for “t” (PART I. a) 42 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4.2.3 Summary Statistics for Part I. b 4.2.3.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 32 = 23.9041 = 16.0579 = 4.00723 = 10.67 = 29.47 = -2.96259 = 2.80511 Percentiles for P2O5 10.67 = %1.0 17.33 = %5.0 19.23 = %10.0 21.49 = %25.0 25.3 = %50.0 26.28 = %75.0 28.16 = %90.0 29.04 = %95.0 29.47 = %99.0 Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 10 14 18 22 26 30 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART I.b) 43 Chapter 4 Sampling Data and Preliminary Statistical Analysis Frequency Tabulation P2O5 Table 4.1: for Frequency tabulation for P2O5 (PART I.b) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 9.0 0 0.0000 0 0.0000 1 9.0 12.4286 10.7143 1 0.0313 1 0.0313 2 12.4286 15.8571 14.1429 0 0.0000 1 0.0313 3 15.8571 19.2857 17.5714 3 0.0938 4 0.1250 4 19.2857 22.7143 21.0 7 0.2188 11 0.3438 5 22.7143 26.1429 24.4286 13 0.4063 24 0.7500 6 26.1429 29.5714 27.8571 8 0.2500 32 1.0000 7 29.5714 33.0 31.2857 0 0.0000 32 1.0000 above 33.0 0 0.0000 32 1.0000 -------------------------------------------------------------------------------Mean = 23.9041 Standard deviation = 4.00723 Histogram for P2O5 15 frequency The StatAdvisor --------------This option 12 performs a frequency tabulation by dividing the range of P2O5 into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data 9 values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by 6pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 3 0 9 13 17 21 25 29 33 P2O5 Figure 4.2.b: Histogram for. P2O5 (PART I.b) 4.2.3.2.Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 32 = 0.767188 = 0.129131 = 0.359347 = 0.15 = 1.55 = 0.529676 = -0.367043 44 Chapter 4 Sampling Data and Preliminary Statistical Analysis Percentiles for “t” 0.15 = %1.0 0.2 = %5.0 0.25 = %10.0 0.5 = %25.0 0.775 = %50.0 0.975 = %75.0 1.25 = %90.0 1.4 = %95.0 1.55 = %99.0 Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.4 0.8 1.2 1.6 t Figure 4.2.1: Quantile plot for “t” (PART I.b) Frequency Tabulation Table 4.1: for tFrequency tabulation for “t” (PART I.b) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.257143 0.128571 4 0.1250 4 0.1250 2 0.257143 0.514286 0.385714 5 0.1563 9 0.2813 3 0.514286 0.771429 0.642857 7 0.2188 16 0.5000 4 0.771429 1.02857 0.9 11 0.3438 27 0.8438 5 1.02857 1.28571 1.15714 2 0.0625 29 0.9063 6 1.28571 1.54286 1.41429 2 0.0625 31 0.9688 7 1.54286 1.8 1.67143 1 0.0313 32 1.0000 above 1.8 0 0.0000 32 1.0000 -------------------------------------------------------------------------------Mean = 0.767188 Standard deviation = 0.359347 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of t into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 45 Chapter 4 Sampling Data and Preliminary Statistical Analysis Histogram for t frequency 12 10 8 6 4 2 0 0 0.3 0.6 0.9 1.2 1.5 1.8 t Figure 4.2.b: Histogram for.”t” (PART I.b) 4.2.4 Summary Statistics for Part I.c 4.2.4.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 26 = 22.1931 = 21.8602 = 4.67549 = 8.19 = 29.84 = -2.3425 = 2.26453 Percentiles for P2O5 1.0% = 8.19 5.0% = 13.65 10.0% = 16.32 25.0% = 19.47 50.0% = 22.96 75.0% = 25.35 90.0% = 27.0 95.0% = 29.09 99.0% = 29.84 46 Chapter 4 Sampling Data and Preliminary Statistical Analysis Quantile Plot for p2o5 proportion 1 0.8 0.6 0.4 0.2 0 8 12 16 20 24 28 32 p2o5 Figure 4.2.1: Quantile plot for P2O5 (PART I.c) Frequency Tabulation Table 4.1: for p2o5 Frequency tabulation for P2O5 (PART I.c) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 6.66667 3.33333 0 0.0000 0 0.0000 2 6.66667 13.3333 10.0 1 0.0385 1 0.0385 3 13.3333 20.0 16.6667 6 0.2308 7 0.2692 4 20.0 26.6667 23.3333 16 0.6154 23 0.8846 5 26.6667 33.3333 30.0 3 0.1154 26 1.0000 6 33.3333 40.0 36.6667 0 0.0000 26 1.0000 above 40.0 0 0.0000 26 1.0000 -------------------------------------------------------------------------------Mean = 22.1931 Standard deviation = 4.67549 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of p2o5 into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data 16 values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane 12 Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. frequency Histogram for p2o5 8 4 0 0 10 20 30 40 p2o5 Figure 4.2.b: Histogram for. P2O5 (PART I.c) 47 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4 2.4 2 Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 26 = 0.611538 = 0.134662 = 0.366963 = 0.2 = 1.5 = 2.06124 = 0.260786 Percentiles for “t” 0.2 = %1.0 0.25 = %5.0 0.25 = %10.0 0.3 = %25.0 0.5 = %50.0 0.85 = %75.0 1.2 = %90.0 1.4 = %95.0 1.5 = %99.0 Quantile Plot for T proportion 1 0.8 0.6 0.4 0.2 0 0 0.3 0.6 0.9 1.2 1.5 T Figure 4.2.1: Quantile plot for “t” (PART I.c) 48 Chapter 4 Sampling Data and Preliminary Statistical Analysis Frequency Tabulation Table 4.1: for TFrequency tabulation for “t” (PART I.c) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.266667 0.133333 5 0.1923 5 0.1923 2 0.266667 0.533333 0.4 9 0.3462 14 0.5385 3 0.533333 0.8 0.666667 5 0.1923 19 0.7308 4 0.8 1.06667 0.933333 4 0.1538 23 0.8846 5 1.06667 1.33333 1.2 1 0.0385 24 0.9231 6 1.33333 1.6 1.46667 2 0.0769 26 1.0000 above 1.6 0 0.0000 26 1.0000 -------------------------------------------------------------------------------Mean = 0.611538 Standard deviation = 0.366963 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of T into equal width intervals and counting the number of data values in 10 each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by 8 pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting 6 Frequency Histogram from the list of Graphical Options. frequency Histogram for T 4 2 0 0 0.4 0.8 1.2 1.6 T Figure 4.2.b: 4.3 Histogram for.”t” (PART I.c) Summary Statistics for Area II 4.3.1 Summary Statistics for whole area 4.3.1.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 123 = 22.8336 = 16.1922 = 4.02395 = 11.28 = 31.1 = -1.21595 = -0.39346 49 Chapter 4 Sampling Data and Preliminary Statistical Analysis Percentiles for P2O5 12.89 = %1.0 16.0 = %5.0 17.09 = %10.0 20.55 = %25.0 23.12 = %50.0 25.32 = %75.0 27.71 = %90.0 29.35 = %95.0 30.35 = %99.0 Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 11 15 19 23 27 31 35 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART II) Frequency Tabulation Table 4.1: for P2O5 Frequency tabulation for P2O5 (PART II) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 10.0 0 0.0000 0 0.0000 1 10.0 13.0 11.5 2 0.0163 2 0.0163 2 13.0 16.0 14.5 5 0.0407 7 0.0569 3 16.0 19.0 17.5 16 0.1301 23 0.1870 4 19.0 22.0 20.5 25 0.2033 48 0.3902 5 22.0 25.0 23.5 40 0.3252 88 0.7154 6 25.0 28.0 26.5 23 0.1870 111 0.9024 7 28.0 31.0 29.5 11 0.0894 122 0.9919 8 31.0 34.0 32.5 1 0.0081 123 1.0000 above 34.0 0 0.0000 123 1.0000 -------------------------------------------------------------------------------Mean = 22.8336 Standard deviation = 4.02395 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of P2O5 into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 50 Chapter 4 Sampling Data and Preliminary Statistical Analysis Histogram for P2O5 frequency 40 30 20 10 0 10 14 18 22 26 30 34 P2O5 Figure 4.2.b: Histogram for. P2O5 (PART II) 4.3.1.2. Summary Statistics for "t" Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 123 = 0.602033 = 0.109482 = 0.33088 = 0.1 = 2.05 = 7.27373 = 7.49626 Percentiles for “t” 0.15 = %1.0 0.2 = %5.0 0.3 = %10.0 0.4 = %25.0 0.55 = %50.0 0.7 = %75.0 1.05 = %90.0 1.3 = %95.0 1.65 = %99.0 51 Chapter 4 Sampling Data and Preliminary Statistical Analysis Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.4 0.8 1.2 1.6 2 2.4 t Figure 4.2.1: Quantile plot for “t” (PART II) Frequency Tabulation Table 4.1: for t Frequency tabulation for “t” (PART II) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.3 0.15 19 0.1545 19 0.1545 2 0.3 0.6 0.45 64 0.5203 83 0.6748 3 0.6 0.9 0.75 22 0.1789 105 0.8537 4 0.9 1.2 1.05 9 0.0732 114 0.9268 5 1.2 1.5 1.35 7 0.0569 121 0.9837 6 1.5 1.8 1.65 1 0.0081 122 0.9919 7 1.8 2.1 1.95 1 0.0081 123 1.0000 8 2.1 2.4 2.25 0 0.0000 123 1.0000 above 2.4 0 0.0000 123 1.0000 -------------------------------------------------------------------------------Mean = 0.602033 Standard deviation = 0.33088 Histogram for t frequency The StatAdvisor 80 --------------This option performs a frequency tabulation by dividing the range of t into equal 60 width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. 40 You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 20 0 0 0.5 1 1.5 2 2.5 t Figure 4.2.b: Histogram for.”t” (PART II) 52 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4.3.2 Summary Statistics for Part II.d 4.3.2.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 30 = 25.1037 = 13.3617 = 3.65536 = 18.17 = 31.1 = -1.1176 = -0.517068 Percentiles for P2O5 1.0% = 18.17 5.0% = 18.35 10.0% = 18.75 25.0% = 23.63 50.0% = 25.67 75.0% = 27.55 90.0% = 29.765 95.0% = 30.35 99.0% = 31.1 Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 18 21 24 27 30 33 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART II.d) 53 Chapter 4 Sampling Data and Preliminary Statistical Analysis Frequency Tabulation for P2O5 Frequency Table 4.1: tabulation for P2O5 (PART II.d) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 17.0 0 0.0000 0 0.0000 1 17.0 19.5 18.25 4 0.1333 4 0.1333 2 19.5 22.0 20.75 2 0.0667 6 0.2000 3 22.0 24.5 23.25 4 0.1333 10 0.3333 4 24.5 27.0 25.75 11 0.3667 21 0.7000 5 27.0 29.5 28.25 6 0.2000 27 0.9000 6 29.5 32.0 30.75 3 0.1000 30 1.0000 above 32.0 0 0.0000 30 1.0000 -------------------------------------------------------------------------------Mean = 25.1037 Standard deviation = 3.65536 Histogram for P2O5 frequency The StatAdvisor 10 --------------This option performs a frequency tabulation by dividing the range 8 of P2O5 into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data 6 values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane 4 Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 2 0 17 20 23 26 29 32 P2O5 Figure 4.2.b: Histogram for. P2O5 (PART II.d) 4.3.2.2 Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 27 = 0.762963 = 0.182806 = 0.427558 = 0.15 = 2.05 = 2.3748 = 1.91188 54 Chapter 4 Sampling Data and Preliminary Statistical Analysis Percentiles for "t" 0.15% = 1.0 0.2% = 5.0 0.25% = 10.0 0.5% = 25.0 0.7% = 50.0 0.95% = 75.0 1.4% = 90.0 1.4% = 95.0 2.05% = 99.0 Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.4 0.8 1.2 1.6 2 2.4 t Quantile plot for "t”(PART II.d) Figure 4.2.1: Table 4.1: Frequency tabulation for “t” (PART II.d) Frequency Tabulation for t -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.4 0.2 4 0.1481 4 0.1481 2 0.4 0.8 0.6 14 0.5185 18 0.6667 3 0.8 1.2 1.0 5 0.1852 23 0.8519 4 1.2 1.6 1.4 3 0.1111 26 0.9630 5 1.6 2.0 1.8 0 0.0000 26 0.9630 6 2.0 2.4 2.2 1 0.0370 27 1.0000 above 2.4 0 0.0000 27 1.0000 -------------------------------------------------------------------------------Mean = 0.762963 Standard deviation = 0.427558 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of t into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 55 Chapter 4 Sampling Data and Preliminary Statistical Analysis Histogram for t frequency 15 12 9 6 3 0 0 0.5 1 1.5 2 2.5 t Figure 4.2.b: Histogram for.”t”(PART II.d) 4.3.3 Summary Statistics for Part II.e. 4.3.3.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 35 = 21.65 = 11.2193 = 3.34952 = 15.43 = 27.71 = -0.381436 = -0.87217 Percentiles for P2O5 15.43% = 1.0 16.34% = 5.0 16.66% = 10.0 18.17% = 25.0 21.87% = 50.0 24.11% = 75.0 25.21% = 90.0 27.58% = 95.0 27.71% = 99.0 56 Chapter 4 Sampling Data and Preliminary Statistical Analysis Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 15 18 21 24 27 30 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART II.e) Frequency Tabulation for P2O5Frequency Table 4.1: tabulation for P2O5 (PART II.e) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 14.0 0 0.0000 0 0.0000 1 14.0 16.1429 15.0714 1 0.0286 1 0.0286 2 16.1429 18.2857 17.2143 8 0.2286 9 0.2571 3 18.2857 20.4286 19.3571 1 0.0286 10 0.2857 4 20.4286 22.5714 21.5 10 0.2857 20 0.5714 5 22.5714 24.7143 23.6429 9 0.2571 29 0.8286 6 24.7143 26.8571 25.7857 3 0.0857 32 0.9143 7 26.8571 29.0 27.9286 3 0.0857 35 1.0000 above 29.0 0 0.0000 35 1.0000 -------------------------------------------------------------------------------Mean = 21.65 Standard deviation = 3.34952 Histogram for P2O5 10 frequency The StatAdvisor --------------8 This option performs a frequency tabulation by dividing the range of P2O5 into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data 6 values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the 4 intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency 2 Histogram from the list of Graphical Options. 0 14 17 20 23 26 29 P2O5 Figure 4.2.b: Histogram for. P2O5 (PART II.e) 57 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4.3.3.2 Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 32 = 0.546875 = 0.0441835 = 0.210199 = 0.2 = 1.25 = 3.15585 = 3.60273 Percentiles for "t" 0.2 = %1.0 0.25 = %5.0 0.35 = %10.0 0.425 = %25.0 0.55 = %50.0 0.65 = %75.0 0.8 = %90.0 0.95 = %95.0 1.25 = %99.0 Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.3 0.6 0.9 1.2 1.5 t Figure 4.2.1: Quantile plot for “t”(PART II.e) 58 Chapter 4 Sampling Data and Preliminary Statistical Analysis Frequency Tabulation for t Table 4.1: Frequency tabulation for “t”(PART II.e) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.214286 0.107143 1 0.0313 1 0.0313 2 0.214286 0.428571 0.321429 7 0.2188 8 0.2500 3 0.428571 0.642857 0.535714 15 0.4688 23 0.7188 4 0.642857 0.857143 0.75 6 0.1875 29 0.9063 5 0.857143 1.07143 0.964286 2 0.0625 31 0.9688 6 1.07143 1.28571 1.17857 1 0.0313 32 1.0000 7 1.28571 1.5 1.39286 0 0.0000 32 1.0000 above 1.5 0 0.0000 32 1.0000 -------------------------------------------------------------------------------Mean = 0.546875 Standard deviation = 0.210199 Histogram for t frequency 15 The StatAdvisor --------------This12 option performs a frequency tabulation by dividing the range of t into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in 9 each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing6 the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 3 0 0 0.3 0.6 0.9 1.2 1.5 t Figure 4.2.b: Histogram for. “t”(PART II.e) 4.3.4 Summary Statistics for Part II.f. 4.3.4.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 32 = 21.7206 = 25.9008 = 5.08929 = 11.28 = 30.2 = -0.380872 = -0.981406 59 Chapter 4 Sampling Data and Preliminary Statistical Analysis Percentiles for P2O5 11.28% = 1.0 12.89% = 5.0 15.73% = 10.0 17.125% = 25.0 21.965% = 50.0 25.49% = 75.0 27.71% = 90.0 30.06% = 95.0 30.2% = 99.0 Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 11 15 19 23 27 31 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART II.f) Frequency Tabulation for P2O5 Table 4.1: Frequency tabulation for P2O5 (PART II.f) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 10.0 0 0.0000 0 0.0000 1 10.0 13.4286 11.7143 2 0.0625 2 0.0625 2 13.4286 16.8571 15.1429 5 0.1563 7 0.2188 3 16.8571 20.2857 18.5714 5 0.1563 12 0.3750 4 20.2857 23.7143 22.0 7 0.2188 19 0.5938 5 23.7143 27.1429 25.4286 7 0.2188 26 0.8125 6 27.1429 30.5714 28.8571 6 0.1875 32 1.0000 7 30.5714 34.0 32.2857 0 0.0000 32 1.0000 above 34.0 0 0.0000 32 1.0000 -------------------------------------------------------------------------------Mean = 21.7206 Standard deviation = 5.08929 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of P2O5 into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 60 Chapter 4 Sampling Data and Preliminary Statistical Analysis Histogram for P2O5 frequency 8 6 4 2 0 10 14 18 22 26 30 34 P2O5 Figure 4.2.b: Histogram for. P2O5 (PART II.f) 4.3.4.2 Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 32 = 0.546875 = 0.0441835 = 0.210199 = 0.2 = 1.25 = 3.15585 = 3.60273 Percentiles for t 0.2 = %1.0 0.25 = %5.0 0.35 = %10.0 0.425 = %25.0 0.55 = %50.0 0.65 = %75.0 0.8 = %90.0 0.95 = %95.0 1.25 = %99.0 61 Chapter 4 Sampling Data and Preliminary Statistical Analysis Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.3 0.6 0.9 1.2 1.5 t Figure 4.2.1: Quantile plot for “t” (PART II.f) Frequency Tabulation Table 4.1: for t Frequency tabulation for “t” (PART II.f) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.214286 0.107143 1 0.0313 1 0.0313 2 0.214286 0.428571 0.321429 7 0.2188 8 0.2500 3 0.428571 0.642857 0.535714 15 0.4688 23 0.7188 4 0.642857 0.857143 0.75 6 0.1875 29 0.9063 5 0.857143 1.07143 0.964286 2 0.0625 31 0.9688 6 1.07143 1.28571 1.17857 1 0.0313 32 1.0000 7 1.28571 1.5 1.39286 0 0.0000 32 1.0000 above 1.5 0 0.0000 32 1.0000 -------------------------------------------------------------------------------Mean = 0.546875 Standard deviation = 0.210199 Histogram for t frequency The StatAdvisor 15 --------------This option performs a frequency tabulation by dividing the range of t into equal 12 width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in 9 each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You 6 can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 3 0 0 0.3 0.6 0.9 1.2 1.5 t Figure 4.2.b: Histogram for. “t” (PART II.f) 62 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4.3.5 Summary Statistics for Part II.g. 4.3.5.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 38 = 22.935 = 12.4164 = 3.52369 = 15.85 = 29.91 = -0.205003 = -0.449807 Percentiles for P2O5 15.85 = %1.0 16.0 = %5.0 17.91 = %10.0 20.79 = %25.0 23.185 = %50.0 25.04 = %75.0 28.25 = %90.0 29.35 = %95.0 29.91 = %99.0 Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 15 18 21 24 27 30 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART II.g) 63 Chapter 4 Sampling Data and Preliminary Statistical Analysis Frequency Tabulation for P2O5 Table 4.1: Frequency tabulation for P2O5 (PART II.g) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 15.0 0 0.0000 0 0.0000 1 15.0 17.2857 16.1429 2 0.0526 2 0.0526 2 17.2857 19.5714 18.4286 4 0.1053 6 0.1579 3 19.5714 21.8571 20.7143 8 0.2105 14 0.3684 4 21.8571 24.1429 23.0 12 0.3158 26 0.6842 5 24.1429 26.4286 25.2857 6 0.1579 32 0.8421 6 26.4286 28.7143 27.5714 4 0.1053 36 0.9474 7 28.7143 31.0 29.8571 2 0.0526 38 1.0000 above 31.0 0 0.0000 38 1.0000 -------------------------------------------------------------------------------Mean = 22.935 Standard deviation = 3.52369 Histogram for P2O5 frequency The StatAdvisor 12 --------------This option 10 performs a frequency tabulation by dividing the range of P2O5 into equal width intervals and counting the number of data values in each8 interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in6 each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You 4can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 2 0 15 19 23 27 31 P2O5 Figure 4.2.b: Histogram for. P2O5 (PART II.g) 4.3.5.2 Summary Statistics for “t” Count = 38 Average = 0.618421 Variance = 0.0854569 Standard deviation = 0.29233 Minimum = 0.3 Maximum = 1.65 Stnd. skewness = 4.54245 Stnd. kurtosis = 4.83634 64 Chapter 4 Sampling Data and Preliminary Statistical Analysis Percentiles for "t" 0.3% = 1.0 0.3% = 5.0 0.35% = 10.0 0.45% = 25.0 0.55% = 50.0 0.78% = 75.0 1.0% = 90.0 1.4% = 95.0 1.65% = 99.0 Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.3 0.6 0.9 1.2 1.5 1.8 t Quantile plot for “t” (PART II.g) Figure 4.2.1: Frequency Tabulation for t Table 4.1: Frequency tabulation for “t” (PART II.g) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.257143 0.128571 0 0.0000 0 0.0000 2 0.257143 0.514286 0.385714 18 0.4737 18 0.4737 3 0.514286 0.771429 0.642857 10 0.2632 28 0.7368 4 0.771429 1.02857 0.9 7 0.1842 35 0.9211 5 1.02857 1.28571 1.15714 1 0.0263 36 0.9474 6 1.28571 1.54286 1.41429 1 0.0263 37 0.9737 7 1.54286 1.8 1.67143 1 0.0263 38 1.0000 above 1.8 0 0.0000 38 1.0000 -------------------------------------------------------------------------------Mean = 0.618421 Standard deviation = 0.29233 The StatAdvisor --------------This option performs a frequency tabulation by dividing the range of t into equal width intervals and counting the number of data values in each interval. The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram from the list of Graphical Options. 65 Chapter 4 Sampling Data and Preliminary Statistical Analysis Histogram for t 18 frequency 15 12 9 6 3 0 0 0.3 0.6 0.9 1.2 1.5 1.8 t Figure 4.2.b: Histogram for. “t” (PART II.g) 4.3.6 Summary Statistics for Part II-h. 4.3.6.1 Summary Statistics for P2O5 Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 19 = 23.1942 = 8.37586 = 2.89411 = 18.17 = 28.75 = 0.122484 = -0.449142 Percentiles for P2O5 1.0% = 18.17 5.0% = 18.17 10.0% = 18.75 25.0% = 21.09 50.0% = 23.08 75.0% = 24.96 90.0% = 27.53 95.0% = 28.75 99.0% = 28.75 66 Chapter 4 Sampling Data and Preliminary Statistical Analysis Quantile Plot for P2O5 proportion 1 0.8 0.6 0.4 0.2 0 18 20 22 24 26 28 30 P2O5 Figure 4.2.1: Quantile plot for P2O5 (PART II.h) Frequency Tabulation forFrequency P2O5 Table 4.1: tabulation for P2O5 (PART II.h) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 17.0 0 0.0000 0 0.0000 1 17.0 19.5 18.25 3 0.1579 3 0.1579 2 19.5 22.0 20.75 3 0.1579 6 0.3158 3 22.0 24.5 23.25 5 0.2632 11 0.5789 4 24.5 27.0 25.75 6 0.3158 17 0.8947 5 27.0 29.5 28.25 2 0.1053 19 1.0000 6 29.5 32.0 30.75 0 0.0000 19 1.0000 above 32.0 0 0.0000 19 1.0000 -------------------------------------------------------------------------------Mean = 23.1942 Standard deviation = 2.89411 Histogram for P2O5 frequency 6 The StatAdvisor --------------5 performs a frequency tabulation by dividing the range This option of P2O5 into equal width intervals and counting the number of data 4 interval. The frequencies show the number of data values in each values in each interval, while the relative frequencies show the proportions3in each interval. You can change the definition of the intervals by pressing the alternate mouse button and selecting Pane 2 can see the results of the tabulation graphically by Options. You selecting Frequency Histogram from the list of Graphical Options. 1 0 17 20 23 26 29 32 P2O5 Figure 4.2.b: Histogram for. P2O5 (PART II.h) 67 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4.3.6.2 Summary Statistics for “t” Count Average Variance Standard deviation Minimum Maximum Stnd. skewness Stnd. kurtosis = 19 = 0.663158 = 0.151345 = 0.389031 = 0.2 = 1.5 = 1.16173 = -0.369185 Percentiles for “t” 1.0% = 0.2 5.0% = 0.2 10.0% = 0.2 25.0% = 0.3 50.0% = 0.55 75.0% = 0.95 90.0% = 1.3 95.0% = 1.5 99.0% = 1.5 Quantile Plot for t proportion 1 0.8 0.6 0.4 0.2 0 0 0.3 0.6 0.9 1.2 1.5 t Figure 4.2.1: Quantile plot for “t” (PART II.h) 68 Chapter 4 Sampling Data and Preliminary Statistical Analysis Frequency Tabulation for t Table 4.1: Frequency tabulation for “t” (PART II.h) -------------------------------------------------------------------------------Lower Upper Relative Cumulative Cum. Rel. Class Limit Limit Midpoint Frequency Frequency Frequency Frequency -------------------------------------------------------------------------------at or below 0.0 0 0.0000 0 0.0000 1 0.0 0.266667 0.133333 4 0.2105 4 0.2105 2 0.266667 0.533333 0.4 4 0.2105 8 0.4211 3 0.533333 0.8 0.666667 5 0.2632 13 0.6842 4 0.8 1.06667 0.933333 3 0.1579 16 0.8421 5 1.06667 1.33333 1.2 2 0.1053 18 0.9474 6 1.33333 1.6 1.46667 1 0.0526 19 1.0000 above 1.6 0 0.0000 19 1.0000 -------------------------------------------------------------------------------Mean = 0.663158 Standard deviation = 0.389031 Histogram for t frequency The StatAdvisor --------------5 This option performs a frequency tabulation by dividing the range of t into equal width intervals and counting the number of data values in each interval.4 The frequencies show the number of data values in each interval, while the relative frequencies show the proportions in each interval. You can change the definition of the intervals by 3 pressing the alternate mouse button and selecting Pane Options. You can see the results of the tabulation graphically by selecting Frequency Histogram 2 from the list of Graphical Options. 1 0 0 0.4 0.8 1.2 1.6 t Figure 4.2.b: Histogram for. “t” (PART II.h) 69 Chapter 4 Sampling Data and Preliminary Statistical Analysis 4.4 Summery of the Statistical Analysis and Discussion 4.4.1 Analysis for the Overall Data Table 4.15: Variable Mean Variance Ash Carbon Hydrogen Moisture Nitrogen Oxygen Sulphur 9.38053 68.7679 5.84211 4.27895 1.38684 8.27316 2.00947 16.6142 18.6876 0.106718 0.651721 0.611634 3.37975 0.55285 Table 4.16: Summary statistics for the (PART I) Standard Deviation 4.07605 4.32292 0.32667 0.807292 0.78207 1.83841 0.743539 4.4.2 Mean Variance 4.67 57.7 5.17 2.8 0.8 3.35 0.96 Standard Kurtosis 0.945177 0.784183 0.049751 -0.349306 11.0293 4.0223 -0.903897 Summary statistics for the (PART II) Standard Deviation 7.85586 8.6074 2.93384 Ash 69.5872 5.49326 2.34377 Carbon Hydrogen 5.78103 0.0744239 0.272807 1.28901 Moisture 4.31103 1.66156 Nitrogen 1.22655 0.0204163 0.142885 8.66586 1.93602 1.39141 Oxygen 2.5831 0.676529 0.822514 Sulphur Variable Standard Skew 19.4 1.99284 75.58 -1.2759 6.49 -0.33116 5.8 -0.32108 4.34 5.94596 9.74 -4.01834 3.25 0.346857 Min. Max. Standard Skew 3.2 16.95 1.9997 63.85 74 -0.39216 5.33 6.6 1.7339 2.8 9.5 5.12851 0.95 1.43 -0.84904 2.68 10.63 -6.3754 1.39 4.85 2.32822 Min. Max. Standard Kurtosis 2.13463 0.025317 1.75027 9.5931 -0.744281 13.3982 1.03893 Comments on the Results Two boreholes have been excluded from the first round of data surveying those were: (BH.Sand and BH.Conc.). The reason behind this decision was the expected difficulties in area calculations and misleading results due to very short distance between the boreholes. Statistical analysis of the different variables has showing that the following boreholes (M3, M5, M5a and M13) at the (PART I) do have missing data. In fact, the available data was provided without core thickness at these boreholes. In the case of the (PART II) boreholes: (K1, K2, and M13) had the same condition, i.e. provided with missing data. The standardised Skewness and standardized Korusis parameters for Oxygen and Nitrogen variables for the (PART I), are out of the accepted range (-2 to +2). 70 Chapter 4 Sampling Data and Preliminary Statistical Analysis Also, these parameters for Oxygen and Moisture variables, from the (PART II), are out of the accepted range, See Table 4.15 and Table 4.16. 71 Chapte 5.1 5 Results and Analysis Introduction Based on the statistical analysis for the chemical variables associated with the borehole sampling at Mahamied area, and referring to the results in Chapter 4. The actual sampling points that are suitable for estimation and analysis are 42 samples. Section 5.2 tabulates these data as X,Y and Z coordinates and thickness of both the overburden and Phosphate seam. Also the analysis of the Oxygen variable whether from (PART I) or (PART II) has showed a non-linear distribution, and it has been decided to exclude it from the further analysis. This Chapter presents the results obtained from the Software for both (PART I) and (PART II) for the following parameters: Average thickness, Total area, Tonnage, and demonstrates the distribution of the following variables: Ash, Carbon, and Sulphur. Results for the other variables (Hydrogen, Nitrogen, Moisture) are shown in Appendix II. Section 5.3 shows the results obtained using Triangular method, while section 5.4 illustrates the results of Ordinary Kriging. All the results are introduced in the form of tables and contour maps. Validation 5.2 of No. 1 2 Software is explained in Section 5.5. Original Sampling Data for Mahamied Phosphate Mine Table 5.1: 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 the Original sampling data from Mahamied mine, (PART I) Borehole X, m B1 140743.94 B10 138349.56 B12 138527.33 B16 138708.00 B2 139813.30 B3 139983.69 B3a 139618.31 B6a 139021.33 B7 139041.57 B9 138836.72 K1 139305.70 K2 139117.69 K3 138850.46 M1 138666.38 M10 137575.07 M11 136163.96 M12 135412.44 M14 134147.79 M15 137040.16 M16 136210.51 M17 133542.73 M18 136522.42 M19 135724.05 M2 138119.31 M21 136639.62 M21a 137216.33 M21b 137536.94 M22 135792.38 M23 135195.31 M25 136111.08 M4 138323.28 Y, m 1176265.65 1176831.04 1177846.81 1174969.00 1175667.11 1175452.57 1175046.93 1176764.27 1175830.13 1177310.10 1173481.83 1174305.66 1173920.16 1173177.70 1173191.28 1173193.10 1172620.16 1172143.41 1173614.17 1173795.41 1172798.53 1174346.31 1174410.09 1172768.20 1175814.20 1175545.04 1174998.73 1175129.77 1175081.10 1176277.45 1173686.01 Z, m 376.20 311.50 289.08 474.00 336.59 348.70 357.10 309.17 408.19 300.40 485.90 423.80 490.90 443.80 454.53 351.70 466.01 466.00 376.00 337.21 439.15 351.97 322.60 438.40 316.30 346.40 396.10 317.80 311.70 299.60 468.10 T11, m 130.10 360.20 474.25 253.35 088.29 052.73 051.37 302.63 256.00 382.05 116.80 000.00 185.26 049.65 151.10 139.10 256.75 262.43 154.60 186.33 340.24 262.48 292.63 046.50 383.35 324.60 300.17 399.15 417.79 464.78 185.30 T22, m 0.10 0.05 0.20 0.80 0.80 0.67 0.65 0.17 0.08 0.06 0.75 0.15 0.84 0.70 0.65 0.50 0.55 0.75 0.72 0.60 0.65 0.54 0.55 0.85 0.10 0.35 0.35 0.45 0.52 0.35 0.70 T1: Thickness of the Overburden T2: Thickness of the Phosphate Seam 73 Chapter 5 No. 32 33 Results and Analysis Borehole X, m M6 136512.28 M7 135146.48 Y, m 1172454.84 1171910.39 Table 5.1: No. 34 35 36 37 38 39 40 41 Borehole M8 M8a M9 S2 S3 S3a WW4 B15 X, m 134599.37 134377.35 138003.98 139462.10 140947.88 141560.55 139987.41 138288.45 Z, m 469.90 438.78 T11, m T22, m 139.25 0.70 153.26 0.84 Cont. Y, m 1171453.44 1171815.84 1173373.99 1175234.84 1176356.39 1176094.34 1176267.43 1175839.96 Z, m 433.90 436.80 461.47 346.80 371.10 479.90 328.71 346.40 T1, m 109.70 173.45 148.30 085.32 077.50 069.15 140.50 269.70 T2, m 0.67 0.85 0.70 0.63 0.00 0.05 0.20 0.20 74 Chapter 5 Results and Analysis Table 5.2: Original sampling data from Mahamied mine, (PART II) Figure 5.1: A capture from the "O.R.E. Software" showing the values of the sampling points (PART I) Figure 5.2: A capture from O.R.E Software showing the thickness of the boreholes (PART I) 5.3 Results of Triangular Method The following steps are showing a numerical example showing how would the average thickness from one triangle is calculated. B15 M21b B16 1. Calculating the lengths of the triangle sides based on the coordinates Side (M21b – B16) = √ (∆x) ² + (∆y) ² = √(1174998.73-1174969)² + (137536.94 -138708)² = 1171.437 m 75 Chapter 5 Results and Analysis Side (M21b – B15) = 1128.023 m Side (B15 – B16) = 966.744 m 2. Calculating the circumference of the triangle Periphery =1171.437+1128.023 + 966.744 =3266.204 m 3. Calculating the area of the triangle Area = √p(p- L1)(p- L2)(p- L3) = 503736.598 m2 Where: p = Half periphery of triangle L = Length of triangle side 4. Calculate the average thickness for the triangle = (∑ Thickness / 3) = (1.84+1+1.32)/3 = 1.387 5. Calculating the volume under each triangle are = Area * Average thickness = 1.387 * 503736.598 = 698514.749 m3 5.3.1 Upper Phosphate Seam Table 5.3: No. 1 2 3 4 5 6 7 8 9 10 11 3 4 Results of calculating the ore reserves from the (PART I) using O.R.E Software. Triangle B1-B3-WW4 B1-B3-S3a B1-S3-WW4 B1-S3-S3a B10-B12-B9 B10-B12-M25 B10-B6a-B9 B10-B6a-B15 B10-M25-B15 B12-B9-S3 B12-S3-S3a Area, m2 0308236.33 0397103.84 0034505.27 0054518.08 0204840.01 1087684.57 0177172.91 0334929.06 1092341.44 0419006.17 0139415.25 AV. T1, m 107.78 083.99 116.03 092.25 405.50 433.08 348.29 310.84 364.89 311.27 206.97 Volume13, m3 033220684.05 033354075.47 004003761.81 005029292.55 083062623.45 471050806.94 061708141.55 104110466.42 398588107.99 130422654.89 028854308.94 AV. T2, Volume24, m m3 0.32 0099663.08 0.27 0108541.72 0.10 0003450.53 0.05 0002725.90 0.10 0021166.80 0.20 0217536.91 0.09 0016536.14 0.14 0046890.07 0.20 0218468.29 0.09 0036313.87 0.08 0011617.94 Volume1: Volume of the Overburden Volume2: Volume of the Ore 76 Chapter 5 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 Results and Analysis B16-B3a-K2 B16-B3a-S2 B16-B7-S2 B16-B7-B15 B16-K2-M4 B16-M21b-B15 B16-M21b-M4 B2-B3-S2 B2-B3-WW4 B2-B7-S2 B2-B7-WW4 B3-B3a-S2 B3-B3a-K2 B3-K1-K2 B3-K1-S3a B6a-B7-WW4 B6a-B7-B15 B6a-B9-WW4 B9-S3-WW4 K1-K2-K3 K1-K3-M1 K1-M1-M2 K2-K3-M4 K3-M1-M4 0317886.09 0091614.90 0280350.94 0325906.61 0390414.17 0503736.60 0756948.00 0074500.47 0069821.04 0195424.18 0245834.18 0066011.79 0033886.87 0464533.67 1336233.72 0446198.97 0351660.28 0217796.91 0551909.32 0146314.97 0209342.64 0047710.57 0070327.99 0174153.87 101.57 130.01 198.22 259.68 146.22 274.41 246.27 075.45 093.84 143.20 161.60 063.14 034.70 056.51 079.56 233.04 276.11 275.06 200.02 100.69 117.24 070.98 123.52 140.07 Table 5.3: No. 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 Triangle M1-M2-M9 M1-M4-M9 M10-M15-M4 M10-M15-M6 M10-M2-M9 M10-M2-M6 M10-M4-M9 M11-M12-M6 M11-M12-M19 M11-M15-M16 M11-M15-M6 M11-M16-M19 M12-M14-M7 M12-M14-M17 M12-M17-M23 M12-M19-M23 Area, m2 0189318.59 0134678.72 0290523.28 0421686.19 0140450.67 0425222.65 0037744.60 0377191.81 0583317.18 0254071.61 0396765.26 0160806.54 0385407.10 0558479.93 2281257.33 0577750.51 AV. T1, m 081.48 127.75 163.67 148.32 115.30 112.28 161.57 178.37 229.49 160.01 144.32 206.02 224.15 286.47 338.26 322.39 032288749.63 011911158.36 055572098.25 084632514.67 057085058.40 138228680.75 186416106.50 005620811.87 006552006.59 027985393.35 039725984.51 004167984.43 001175874.32 026250797.38 106310754.53 103983694.09 097096919.58 059907217.24 110391062.22 014731966.91 024542633.12 003386655.33 008686913.66 024393731.93 0.53 0.69 0.50 0.36 0.55 0.45 0.62 0.70 0.56 0.50 0.36 0.65 0.49 0.52 0.49 0.15 0.15 0.14 0.09 0.58 0.76 0.77 0.56 0.75 0169539.25 0063519.66 0141109.97 0117326.38 0214727.79 0226681.47 0466784.60 0052150.33 0038867.05 0098363.50 0088500.31 0042907.66 0016604.57 0243105.95 0654754.52 0066929.85 0052749.04 0031217.56 0047832.14 0084862.68 0159798.21 0036578.10 0039618.10 0130034.89 Cont. Volume1, m3 015426309.38 017205206.80 047548976.11 062543090.34 016193961.86 047745416.48 006098268.82 067278445.49 133867404.05 040653997.80 057259839.37 033129363.02 086387716.83 159989607.58 771658102.64 186260986.00 AV. T2, Volume2, m m3 0.75 0141988.94 0.70 0094275.11 0.69 0200461.06 0.69 0290963.47 0.73 0102997.16 0.73 0311829.94 0.68 0025792.14 0.58 0220028.56 0.53 0311102.50 0.61 0154136.78 0.64 0253929.77 0.55 0088443.60 0.71 0274923.73 0.65 0363011.96 0.57 1307920.87 0.54 0311985.27 77 Chapter 5 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 Results and Analysis M12-M6-M7 M14-M17-M8 M14-M7-M8a M14-M7-M8 M14-M8-M8a M15-M16-M18 M15-M18-M21b M15-M21b-M4 M16-M18-M19 M18-M19-M22 M18-M21-M22 M18-M21-M21b M19-M22-M23 M2-M6-M8 M21-M21a-M25 M21-M21a-M21b M21-M22-M25 M21a-M21b-B15 M21a-M25-B15 M22-M23-M25 M6-M7-M8 M7-M8-M8a 0412300.97 0060817.08 0136824.41 0291919.48 0005232.73 0256792.38 0540277.30 0870433.98 0229857.83 0289464.50 0581719.96 0706370.07 0213186.86 0504925.18 0062449.54 0114383.53 0377116.28 0340132.09 0555595.87 0334867.08 0163114.14 0149862.35 183.09 237.46 196.38 175.13 181.86 201.14 239.08 213.36 247.15 318.09 348.33 315.33 369.86 098.48 390.91 336.04 415.76 298.16 353.03 427.24 134.07 145.47 075486810.63 014441420.93 026869576.86 051123859.21 000951623.61 051650362.68 129171298.24 185712891.67 056808595.60 092074799.36 202628575.92 222742028.55 078848580.77 049726715.03 024412149.90 038437440.16 156789865.03 101412649.94 196140157.86 143068613.10 021868712.11 021800476.27 Number of triangles Total area Volume Average thickness of (PART I) Reserves Average thickness of overburden Volume of overburden 0.70 0.69 0.81 0.75 0.76 0.62 0.54 0.59 0.56 0.51 0.36 0.33 0.51 0.74 0.27 0.27 0.30 0.30 0.30 0.44 0.74 0.79 0287236.34 0041963.79 0111283.85 0219912.68 0003959.43 0159211.27 0289948.82 0513556.05 0129486.58 0148591.78 0211358.25 0233102.12 0108014.68 0373644.64 0016653.21 0030502.27 0113134.88 0102039.63 0166678.76 0147341.52 0120160.75 0117891.72 73 26030587.2m2 12166938.7m3 0.467m 17381340.9 ton 241.096m 6275863588m3 Beside the above results, the estimation of the thickness of the overburden or the thickness of the Phosphate seam at any un-sampled point within the selected triangulation net can be estimated using the O.R.E. Software. The following are examples of some random points Point X, m Y, m 1 134718.38 113346.81 T1 (PART I) (Overburden), m 328.7 T2 (PART I), m 0.576 78 Chapter 5 Results and Analysis 2 3 4 5 6 7 138091.27 137536.94 137040.16 137870.93 140125.16 136294.60 1174516.28 1174998.73 1173614.17 1176465.45 1175906.13 1175007.82 247.78 300.17 154.60 358.91 099.70 342.49 0.58 0.65 0.72 0.15 0.39 0.39 Point 3 refers to borehole M21b and point 4 refers to borehole M15 Table 5.5: No. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 Results of average assay calculations of the (PART I) using O.R.E. Software Triangular B16-B2-B15 B16-B2-K1 B16-K1-K3 B16-K1-M4 B16-K3-M4 B16-M4-B15 K1-K3-M4 K1-M2-M4 M10-M15-M4 M10-M15-M6 M10-M2-M9 M10-M2-M4 M10-M2-M6 M10-M4-M9 M14-M17-M8 M14-M17-M7 M14-M7-M8a M14-M7-M8 M14-M8-M8a M15-M16-M6 M15-M16-M19 M15-M19-M6 M15-M19-B15 M15-M4-B15 M16-M19-M6 M17-M19-M7 M17-M7-M8 M19-M6-M7 Carbon, Ash, Hydrogen, Moisture, Sulphur, A*Vol. A*Vol. A*Vol. A*Vol. A*Vol. 261295.5 030070.8 022328.1 016950.1 006118.8 551596.7 075157.2 046301.0 035552.8 015586.5 107782.5 019605.6 009125.0 007516.2 004308.8 337219.5 052911.2 028261.6 021937.1 010686.2 152716.4 023183.6 012939.1 010549.2 005243.9 167967.8 023580.6 014344.8 011033.4 004621.5 085766.8 013834.2 007064.6 005822.6 003246.2 245581.2 034419.4 020408.8 016744.0 008235.2 134785.4 023556.3 011624.6 008581.6 002588.0 194495.7 035470.4 016990.9 012652.7 004327.1 070014.2 009460.1 005899.9 005303.2 001743.7 147712.6 018293.2 012372.2 010717.8 003943.9 213291.7 027847.1 018080.5 015758.0 006301.1 017744.0 002297.6 001465.2 001256.6 000354.0 030400.4 002433.3 002635.8 001389.1 000710.7 141028.6 011268.0 011874.7 006974.3 002595.0 082282.6 005653.8 006910.2 004267.7 001791.3 162784.6 011394.6 013819.9 008003.3 003448.7 002887.0 000195.8 000248.9 000140.5 000076.7 238484.6 042834.8 020882.0 013648.9 007387.4 083285.8 020354.3 007439.4 005423.0 003105.8 408975.1 095135.2 036536.3 028261.8 013125.1 593204.9 166928.2 054412.9 041805.3 018894.8 499677.5 092076.5 043816.9 028972.2 010407.7 094302.1 017366.8 008071.7 006711.9 004106.8 1065490.4 149726.2 089360.9 069657.7 030906.9 321407.3 025349.9 026896.5 017194.0 008047.2 742853.7 109220.7 062301.1 052294.9 023373.8 79 Chapter 5 No. 29 30 31 32 Results and Analysis Triangular M2-M4-M9 M2-M6-M8 M6-M7-M8 M7-M8-M8a Total Volume, m3 Average Assay Carbon, A*Vol. 059238.1 260984.7 087346.9 086813.1 7646425 67.90% Ash, Hydrogen, Moisture, Sulphur, A*Vol. A*Vol. A*Vol. A*Vol. 007167.3 004955.7 004179.2 001552.6 027531.9 022414.8 016918.4 008877.8 007478.8 007309.6 005080.9 002384.3 005846.9 007249.0 004830.2 002425.6 1186941 10.54% 654282 5.81% 495497 4.40% 220722 1.96% 80 Chapter 5 Results and Analysis thickness contour map of area I 805500 805000 804500 Y, m 804000 803500 803000 802500 802000 801500 801000 277000 278000 279000 280000 X, m Figure 5.3: Contour maps for Carbon, Ash and Sulphur of the (PART I) using the Triangular method a) Plots using SURFER 7 b) Plots using O.R.E. Software 81 Chapter 5 5.3.2 Results and Analysis Main Phosphate Seam 1176000 Y 1175000 1174000 1173000 1172000 135000 136000 137000 138000 139000 140000 141000 X a) Carbon% b) Carbon% a) Ash% b) Ash% a) Sulphur% b) Sulphur% Figure 5.6: Contour maps for Carbon, Ash and Sulphur of the (PART II), using the Triangular method a) Plots using SURFER 7 b) Plots using O.R.E. Software 82 Chapter 5 5.4 Results and Analysis Results of Ordinary Kriging Technique Variowin 2.21 Software has been used to generate the variograms of all the studied variables. Figure 5.7 Show and example using Carebon samples from the (PART II). Figure 5.7: Outputs from Variowin showing the variograms of Carbon 83 Chapter 5 5.4.1 Results and Analysis Upper Phosphate Seam 1177000 1176000 Y 1175000 1174000 1173000 1172000 134000 135000 136000 137000 138000 139000 140000 141000 X Thickness, m 1177000 1176000 Y 1175000 1174000 1173000 1172000 134000 135000 136000 137000 138000 139000 140000 141000 X Elevation, m 1177000 1176000 Y 1175000 1174000 1173000 1172000 134000 135000 136000 137000 138000 139000 140000 141000 X Overburden, m Figure 5.8: Contour maps and 3D represention for the Thickness, Elevation and Overburden for (PART I), calculated based on (OK) 84 Chapter 5 Results and Analysis 1175000 Y 1174000 1173000 1172000 134000 135000 136000 137000 138000 139000 X Carbon % 1175000 Y 1174000 1173000 1172000 134000 135000 136000 137000 138000 139000 X Ash % 1175000 Y 1174000 1173000 1172000 134000 135000 136000 137000 138000 139000 X Sulphur % Figure 5.9: Contour maps and 3D representation for the Carbon, Ash and Sulphur for (PART I), calculated based on (OK) 85 Chapter 5 Results and Analysis Main Phosphate Seam 5.5 Validation of the Results In order to examine the reliability of the developed Software, The results of ore reserve estimation of the (PART II) are compared with the last report about the same area and provided by The Ministry of Industry and Mining Projects, Egypt, (1996). Proved Ore Reserves of the (PART II) = 27 million tons (Report) Calculated ore reserves using O.R.E Software = 26.62 million tons. This close difference does not mean that the calculations done using the developed software is correct rather than it just a hint of the correct way. However, It is believed that the difference came from the high precision of the method used in the O.R.E Software. Using the correct coordinates of the sampling points will give more exact determination of the lengths than measuring the lengths from the existing maps (low accuracy especially with the small map scale). Another way to check the quality of the developed Software is comparing the visual results with one of the known Software’s (SURFER 7.0). Figures 5.3 and 5.6 showed how close is the two results. 86 Chapter 6.1 6 Some Useful Information to MIS Introduction Like, other mining information, surface mining information and data, such as, height of bench, type and shape of trench, drilling, blasting, machines, mining methods, etc., need an efficient system to combine, access, manipulate, and update, the information in a format that is easily accessible and readily communicated to the authorities, researcher and investors. The task in this chapter is to provide as much as possible useful information to aid in building the MIS (Mining Information System), developed by B.Sc. students at Mining and Metallurgical Engineering Department, Assiut University. (El Mokadum and et al., 2003) Chapter 6 Mining Information System (MIS) At this point, the simple calculations of surface mining parameters were calculated and made available in a digital format, so one can easily use them as part of the MIS. The following sections are explaining how the information has gathered. 6.2 Surface Mining Method 6.2.1 General Essential factors for surface mine operation, Figure (6.1): 1. Choice of the site of mine taking into consideration the nearest presence of the ore than solving the transportation system. 2. Development system and mining method. 3. Removal of the overburden according to the development scheme and mining method also extraction of ore. 4. Loading and transportation to the place of storing. Figure 6.1: Surface mining pattern showing extraction and development (Digistar, 2004). 6.2.2 Advantages of surface mining 1. 2. 3. 4. 5. 6. 7. Cost of extraction for one ton in surface less than underground. No need for support and natural ventilation. Economic flexibility of operation. Drainage of water is easy than underground. Sufficient light. Used large power and high machines. Greater productivity of labour at low cost. 88 Chapter 6 Mining Information System (MIS) 6.2.3 Disadvantages 1. Dependence up on climatic condition. 2. Considerable original out lay the purchase of equipment and excavator of spoil. 3. Required large area for mining. 6.2.4 Factors favouring surface mining: 1. 2. 3. 4. 5. 6. 6.3 Higher productivity. Greater out put per mine. Greater consideration of all operation and of men and machine. Lower operation cost per ton. Lower capital cost per annual mine tonnage. Greater geological certainty. Surface or Underground Mining Methods? One of the most important steps in mining development is to decide the most appropriate mining method for ore extraction. This vital step always follows the ore reserve estimation. Normally upon calculating the volumes of the overburden and reserves, several approaches have to be examined to decide Surface or Underground, Figure (6.2) shows the main factors in both methods. Figure 6 2: Main operations in Surface and Underground mining methods (Digistar, 2004) 89 Chapter 6 6.3.1 Mining Information System (MIS) Calculation of Stripping Ratio The stripping ratio can be calculated using one of the following formulae. 1. Stripping Ratio = Volume of overburden removed Volume of mineral recovered (6.1) 2. Stripping Ratio = Volume of overburden removed Weight of mineral recovered (6.2) 3. Stripping Ratio = Thickness of overburden removed Thickness of mineral recovered (6.3) At El Mahamid area, the only available information is the volume of both the overburden and the ore recovered, so equation (6.1) is used to determine the stripping ratio as follows: Volume of over burden removed = 12,000,000 m3 given by the Company. Volume of mineral removed = 193637780.3 m3 Calculated in Chapter 4. Stripping Ratio = 12000000/193637780.33 = 0.62 Since the stripping ratio is less than one, so for the given situation surface mining method is preferable, Figure (6.3), shows the preparation of the area at East Mahamid for extraction using surface mine technology. Note that the thickness of the overburden is very small. . Figure 6 3: Extraction of ore using surface mining, (taken from ElNasrmining.com). 90 Chapter 6 6.4 Mining Information System (MIS) Height of bench Height of bench can be calculated according to three considerations: 1) Stability of face slope. 2) The safety of the work place. 3) Efficiency of the work place. 6.4.1 Height of bench due to stability of the face slope H Where: H C α γ 4C sin 2 (6.4) Vertical face height, m. Force of cohesion, t/m2. Slope angle of slip plane. Volumetric weight of the material, t/m3 6.4.1.1 The Maximum height of the vertical face Hv 6.4.1.2 4C (6.5) ,m The limiting height of a vertical face Hv 2C. cos (1 sin ) (6.6) Where: Φ = Angle of repose. 6.4.2 Height of bench due to safety of working place H v ≤ H d max (6.7) Where: Hdmax = Maximum digging of the excavation in meters. 6.4.3 Height of bench calculated from the efficiency of work place sin .sin H V 0.7a (1 ) sin ( ) 0.5 (6.8) 91 Chapter 6 Mining Information System (MIS) Where: a Β K Rd Rl α k γ 6.5 Width of the broken down of material formed = 0.8 (Rd+Rl). Slope angle of broken down material. Slope angle of the face. Loosening factor of the face material. Ratio of length of least resistance line of first raw of blast holes to face height. Ratio of distance between rows of blast holes to length of line of least resistance. Digging radius = 13.40 m Loading radius = 12.10 m 0.55 - 0.70 0.75 - 0.85 35 1.5 1.82 t/m3 Development schemes and mine trenches Development and design of surface mining systems and trenches is generally carried out for: External, and/or Internal. In both cases, the classification of development schemes is mainly: Separate trench. Group trench. Twin trenches. 6.5.1 Type of trenches 1) The capital trench. 2) The sectional trench. 3) The special trench. Figure (6.4) shows different types of trenches 92 Chapter 6 Mining Information System (MIS) Capital trench Figure 6.4: 6.5.2 Sectional trench Special trench Type of trenches, (After, El-Abde Rassoul, 1978). Shape of trenches: Figure (6.5) shows the different shapes of the trenches. Those are: 1) 2) 3) 4) 5) 6) Straight. Loop. Curved. Dead lock. Spiral. Combination. Figure 6.5: Shape of Trenches. Some of these shapes can be seen in Figure (6.6) 93 Chapter 6 Mining Information System (MIS) Figure 6.6: 6.6 A picture showing the benches and trenches. (Reference) Calculation of height of bench The height of bench at El Mahamid phosphate mine has been calculated based on the stability of face slope, using equation (6.4). H 4 * 74 86.5 m 1.82 * sin (2 * 70) The maximum height of the vertical face, can be calculated from equation (6.5) Hv 4 * 74 162 .63 m 1.82 The limiting height of the vertical face is determined from equation (6.6) as: Hv 2 * 74 * cos (45) 196.32 m 1.82 (1 sin( 45)) Height of bench due to safety of working place is calculated using equation (6.7) as: H v ≤ 1.5*14 = 21 m Height of bench calculated from the efficiency of work place: Substitute at equation (5). 94 Chapter 6 Mining Information System (MIS) H v 0.7 * 20.4 * Where: a k β α ή ή Rd Rl Hdmax C α φ 6.7 sin 35 * sin 85 15.36 m 1.5 * 0.55 1 0.75 sin 85 35 0.8 (13.8 + 12.1) = 20.4 m 1.5 85 35 0.55 0.75 13.4 m. 12.1 m. 15 m. 74 ton/m2 70 45 Drilling Applying mechanical, thermal, and physico chemical, electric spark and other methods can break up rock. The purpose of drilling is to create large or small diameter holes in the natural rock massive. The drilling of borehole is labor consuming and costly process especially when drilling is done rather difficulty breaking rocks. 6.7.1 Method of borehole drilling The two methods; rotary and percussion are still the basis of all conventional drilling techniques. 6.7.1.1 Rotary blast hole diameter: In rotary drilling, the disintegrations of the rock occur as a result of a concurrent action on bit of a load (pressure) and of a torque. Under the effect of the pressure, the bit penetrates the rock, while under that of the torque it shears it. Rotary drilling can be employed in very soft material 95 Chapter 6 Mining Information System (MIS) when drag bit are used, and in medium to very hard rock when rolling cutter are used. Most rotary blast holes are shallow, from (30 to 60) ft, and are in the (6 to 9) in rang, although the rotary method is capable of drilling (3 to17) in holes. Rotary drills used in open pit blast hole drilling consist of a power source, a drill string composed of a single or connected series of hollow drill pipe, and a drill bit. 6.7.1.2 Percussive blast hole drilling for surface mining Percussive drills are most commonly used to drill small diameter holes in hard rock and large diameter holes where heavy rotary rigs cannot be used or are not available percussive drilling is employed for holes from (2 to 12) inch in diameter to depth of 100 feet with surface drills. Figure (6.7) shows how El Nasr mining company is using this method at El Mahamid phosphate mine. Figure 6.7: Percussive drills for removing the ore at El Mahamid. However, the Rotary drilling, (Figure 6.8), has several advantages, among them: Rotary drilling is preferable in many sedimentary rocks. Rotary drilling is an alternative in hard rock provided that the drill is adequate size and large holes are acceptable. 96 Chapter 6 Mining Information System (MIS) Rotary drilling gives a wide range of hole size and may be used to greater depths. Rotary drilling in bad ground may be the sole economic method. Figure 6.8: 6.8 Drilling operation at the study area (ElNasrMining). Blasting Explosives can define as: Solid or liquid substance or mixture of substances which on the application of suitable stimulus to a small portion of the mass is converted in a very short interval of time into other more stable substances, largely or entirely gaseous, with the development of very high temperature and pressure” (Abdel Erassoul, 1978). The factors affecting the selection of the explosives are: 1) Explosives cost and properties. 2) Rock properties. 3) Working condition. 6.8.1 Calculation of burden and spacing for 4 inch. borehole diameter: First method (Pearce formula) B K *d * P T (6.9) Where: B Max. height of burden in inches. K Constant depending on rock characteristics: = 0.7 for strong rock. = 1.0 for weak rock. d = Borehole diameter. P = Detonation pressure, gm/cm2 97 Chapter 6 Mining Information System (MIS) T = Ultimate tensile strength of rock, gm/cm2 4.18 *107 * vod P 1 0.8 2 vod gm/cm2 (6.10) Density of explosives, gm/cm3 Velocity of detonation, ft/ sec. 0.84 gm/cm3 For ANFO. For 4 inch borehole diameter vod = 11800 ft/ sec, and substitute at equation (6.10): 4.18 *10 7 * 0.84 * 11800 P 29240 .4 gm / cm 2 1 0.8 * 0.84 2 For Phosphate; substitute in equation (6.9): B 0.9 * 4 * 29240 .4 3.64 m 18.473 S = 1.25 B (6.11) S = 1.25 * 3.64 = 4.55 m S = Spacing between borehole. 6.8.2 Calculation of burden and spacing for 2 inch borehole diameter: For 2 inch boreholes diameter vod = 9200 ft/sec, and substitute at equation (6.10). 4.18 *10 7 * 0.84 * 9200 P 20410 .8 kg / cm 2 1 0.8 * 0.84 2 For Phosphate, Substitute at equation (6.9): B 0 .9 * 4 * 20410 .8 3.04 m 18.473 S = 1.25 B S = 1.25 * 3.04 = 3.8 m. 98 Chapter 6 6.9 Mining Information System (MIS) Loading and Unloading Bench level intervals are to a large measure determined by the type of shovel or loader used, and these are selected on the basis of the character of the ore and the manner in which it breaks upon blasting and supports itself on the working face (Randall, 1998). Figure (6.9) illustrates by sketches loading ore cars. Figure 6.9: Removing ore (After Randall, 1998). 99 Chapter 6 Mining Information System (MIS) The loading and loading processes of the phosphate ores at Mahamid as well as the overburden is carried out at the study area using different equipment such as the trucks showing in Figure (6.10). Figure 6.10: Loading of phosphate at the extraction area of Mahamied, Picture taken in 2004. 6.10 Equipment The following equipment is used at El Mahamid phosphate mine: 6.10.1 Trucks Ore trucks are very large hauling trucks used to carry between 50-250 tons of ore each load, see Figure (6.11). Usually those trucks are powerful enough to climb steep inclines. The main purpose of using them is to move the broken rock to a waste pile or mill depending on ore grade. 100 Chapter 6 Mining Information System (MIS) Figure 6.11: An Example of the trucks used at El Mahamid. 6.10.2 Drag Line Specifications Drag line type 380 W, is a very important apparatus at East Sebaiya mines, which use in the metallurgical industries, by removing over burden by open cast mine. Figure (6.12) shows a picture taken at the study area. The specification and capacity of the dragline is highly requested for the MIS. Figure 6.12: Dumping of the overburden at El Mahamid phosphate mine. 101 Chapter 6 Mining Information System (MIS) 102 Chapter 6 Mining Information System (MIS) Figure 6.1: A Diagram for the proposed Mining Information System (MIS) 103 Chapter 7.1 7 Conclusions and Recommendations Conclusions The phosphate ore reserves at Eastern El Mahamid, Esna, Egypt, have been estimated using 340 sampling points. The Triangular method is used as the basic of the mathematical calculations of the average thickness, average assay and estimation of the total volume and tonnage of the ore. The large number of the boreholes require an accurate and fast way of calculations with minimum risk of errors in calculations The students has chosen EXCEL software to carry out most of the calculations, and another 3 Software’s for displaying the output data in the form of contour maps and 3D representation of the variables under study The main points reached at the end of this project are: Chapter 7 Conclusions and Recommendations A review of the geological and geophysical studies at the study area and introducing new geological maps for the ore concentrate and types of phosphate. Estimating the tonnage of ore reserve at acquired area provided that sufficient sampling boreholes are available. Calculating the area and average thickness or Assay within any portion of the entire area. Determine the lengths between any two sampling points using their X and Y coordinates. Mapping the locations of the boreholes at the area. Link the output data with Surfer Software for contouring the surfaces and conducting a 3D representation of the thickness and P2O5 at the study area. An intensive study has been made over all the available data about the study area in the Internet and introduced in a fore suitable for the MIS. In one sentence; the average thickness of the phosphate ore at the study area is estimated as 0.61 meter and the ore reserves as 44 million tons with average P2O5 = 23%. The dissertation has also introduced some useful information about the mining operations at the study area that can be used for the database of the Egyptian Mines (MIS), where the available information of Mahamied Phosphate Mine has used as the second input record, followed El Maghara coal mine. 7.2 Recommendations The introduced methodology is based on the Triangular method for ore reserve estimation, using Excel software,. However, it is recommended to test it on one or more of the following methods and techniques for more accurate calculations such as: Kriging techniques (OK, SK, UK) or Multiquadric technique. 105 Chapter 7 Conclusions and Recommendations The calculations and gathered information about the area need more work to maximize the benefit of using the MIS. Other data and information require a field study and a good cooperation from the company. A questionnaire has to be designed and send to the other Egyptian authorizations and mining companies to prepare and provide the required information so that a complete database can be created (Mining Information System for Egyptian Mines). 106 References References Atef et al, 1999 “A Study in the Structural and Building Materials in Red Sea Governorate“, Mining & Metallurgical Engineering Department, Faculty of Engineering, Assiut University. 128 P. Ahmed El-Otify et al, 1997 “A Study on the Structural and Building Materials in Kharga Oasis”, Mining & Metallurgical Engineering Department, Faculty of Engineering, Assiut University. 132 P. Moataz El-Nashar et al, 1997 “A Geostatistic Studies of Baharia Oasis Iron Ore”, Mining & Metallurgical Engineering Department, Faculty of Engineering, Assiut University. 54 P. Carls Pavetto, “Surface Mine Blasting”, Mining Information Services Maclean Hunter Publishing Company, 29 North Wacker Drive Chicago. 317 P. Randall D. Peterson, P.E. and David A. Hettinger, 1998 “Softwall Mining: New Technology for Phosphatic Clays and Other Deposits in Soft, Shallow Conditions”, The Society for Mining Metallurgy and Exploration Annual Convention, Orlando, Florida. Mikhailov, L. A. et al, 1970 “Stratigraphy of the Phosphate-Bearing Cretaceous and Paleogene Sediments of the Nile Valley between Idfu and Qena”, Studies on Some Mineral Deposits of Egypt, by O. Moharram et al, Geol. Survey. Egypt, Article7. 109134 P. Rushdi Said, 1968 “Report on the Results of Geological Exploration at The ElMahamid Phosphorite Deposit Carried out in 1966-1968”, Egyptian General Organization For Geological Research and Mining. 154-173 P. Abdel-Rassoul, E, I., 1978. “Studies on the Relations between the Properties of Surface Mine Faces and Blasting Results” MSc Thesis, Mining Engineering Mining & Metallurgical Engineering Dept, Faculty of Engineering, Assiut University. 157 P. 107 References W. M. Telford et al, 1974 "Applied Geophysics", Cambridge University. 860 P. Abo El-Hagag E. El-Sabry et al, 1990 “Gold Mineralization of The Hangaliy Area at Eastern Desert”, Mining & Metallurgical Engineering Department, Faculty of Engineering, Assiut University. 61 P. Eugene P. Pfleider et al, 1968 "Surface Mining", The American Institute of Mining, Metallurgical, and Petroleum Engineers, Inc. New York. 1048 P. "Phosphate Rock and its Characteristics" The Article Originally Appeared in the Journal Phosphorus & Potassium, Issue No: 217, (September-October, 1998), Electronic Version on: http://www.nhm.ac.uk/mineralogy/phos/p&k217/steen.htm. Ahmed, S. S. (2001). “Three-dimensional Characterisation of Groundwater Parameters around Mines and Landfill Sites”. PH.D., Thesis, Royal School of Mines, Imperial College of Science, Technology & Medicine, London, UK. Issak, E. H. and Srivastava, R. M. (1989). “An Introduction to Applied Geostatistics”. Oxford Univ. Press, New York, 561 p. Nakhla, F. M. (1990). “Geology and Characteristics of Developed Main Phosphate Seam in Mahamied Phosphatefield, North Sinai, Egypt”. Proceedings of 7th Symposium, Phaner. Develop. Egypt. PP. 65-92. Rashad, M. Z. (1999). A Brief Course in Application of Computer Methods in Mining Industry. A course for 2nd year mining. Mining & Met. Eng. Dept., Faculty of Engineering, Assiut University, Egypt. Rashad, M. Z. (2003). “Principles of Mining Geostatistics”. Lecture Notes, 4th Year Mining Engineering, Mining and Metallurgical Engineering Department, Assuit University. Weller, J. M. (1960). “Stratigraphic Principles & Practice”. Web Sites: http://www.uk-rocks.net. http://www.elnasrmining.com. http://Sanangelo.Tamu.Edu/Agronomy/Mg/Phospht.htm. www.softwallequipment.com Software’s: Microsoft Office 2000 (Word, Excel and Power Point), (2000). ORACLE® Database. Release 9.0.0, ORACLE Corp, (2001). SGWIN, Statistical Graphics under Windows, (1998). SURFUR 7. Release 7.0, Golden® Software, Inc., (1993-1999). VARIOWIN, Release 2.21, Yvan Pannatier el al, (1993-1998). 108 Appendix I.1 I Original Data X, Y Coordinates,"t"and P2O5 of Sampling Points at Mahamid Table I-1 summarizes the original data of area I at El Mahamid district. X, Y,"t" and P2O5 of the ore deposit at the different borehole locations are given in meters Table I-1: Co-ordinates of old drilled boreholes at Mahamid phosphate mine, Esna. B.H No. X (m) Y (m) K-15 K-16 K-17 K-18 K-19 K-20 K-21 K-22 K-23 K-24 L-13 801515 801980 802290 802743 803110 803610 803819 804290 804549 805153 800651 277460 277430 277423 277590 277460 277480 277495 277517 277460 277107 277790 t (m) P2O5% 0.25 0.35 0.25 0.40 0.15 1.00 1.40 0.75 0.40 0.30 0.35 21.56 21.75 21.10 20.83 10.67 29.47 28.59 25.29 25.66 26.66 8.19 Appendix II Other Results of Data Analysis Table I-1: Cont. B.H No. X (m) Y (m) L-14 L-15 L-16 L-17 L-19 L-20 L-21 L-22 L-23 L-25 M-13 M-14 M-15 M-16 M-17 M-18 M-19 M-20 M-21 M-23 M-24 M-25 N-13 N-14 N-15 N-16 N-17 N-18 N-19 N-20 N-21 N-22 N-23 N-25 O-14 O-15 O-16 O-17 O-18 O-19 O-20 O-21 O-22 O-23 O-26 P-17 P-18 P-21 P-25 Q-21 R-18 801160 801526 801858 802297 803020 803560 803805 804275 804748 805338 800709 801115 801519 801876 802320 802665 803010 803805 803805 804667 805025 805341 800782 801128 801501 801558 802258 802657 803013 803475 803820 804238 804657 804506 801027 801489 801889 802243 802668 802992 803401 803870 804225 804568 805783 802240 802649 803775 805410 803750 802647 277810 277820 277845 277757 277860 277882 277873 277858 277920 277902 278190 278163 278218 278205 278220 278218 278225 278250 278252 278250 278252 278315 278609 278570 278540 278588 278602 278621 278627 278650 278655 278641 278716 278702 278935 278870 279040 279010 278960 279036 279030 279060 279071 279048 279071 279337 279337 279463 279451 279801 280090 t (m) P2O5% 0.50 1.20 0.8 0.25 0.92 1.20 0.50 0.70 0.65 0.40 0.35 0.45 1.50 0.90 0.70 0.50 0.90 1.00 0.90 0.65 0.40 0.20 0.30 0.95 0.60 0.95 0.65 0.80 0.90 0.75 0.60 0.55 0.80 0.80 0.40 1.4 0.25 0.30 0.80 1.55 1.40 0.80 0.65 0.75 0.30 0.70 1.25 0.45 0.30 0.75 1.00 18.50 24.55 25.45 19.47 25.90 26.87 26.58 24.57 24.13 18.86 16.32 22.39 23.41 29.09 25.66 19.23 25.66 25.65 25.45 22.75 15.82 15.17 19.40 25.45 22.54 24.38 23.77 23.93 25.66 19.04 27.07 20.93 25.45 24.69 27.00 13.65 23.38 18.12 22.16 21.37 27.94 25.98 26.78 27.49 10.93 25.35 17.33 25.25 20.45 24.21 25.05 110 Appendix II Other Results of Data Analysis Table I.1: Cont. B.H No. X (m) Y (m) I-22 J-15 J-16 J-17 J-20 J-21 J-22 J-23 804260 801525 801914 802240 803495 803565 804230 804480 276869 277073 277050 277020 277090 277115 277120 277115 t (m) P2O5% 0.60 0.85 0.50 0.20 0.90 0.65 0.60 0.65 23.14 29.84 24.90 21.80 21.61 28.16 29.61 28.16 111 Appendix II Appendix II.1 Other Results of Data Analysis II Other Results of Data Analysis X, Y Coordinates,"t" and P2O5 of Sampling Points Table II-1 summarizes the original data of area II at El Mahamid district. X, Y,"t" and P2O5 of the ore deposit at the different borehole locations are given in meters. Table II-1: X Y, Co-ordinates, thickness and Assay at drilled boreholes at Mahamid phosphate mine. B.H. No. X (m) Y (m) t (m) P2O5 A-17 A-19 A-20 A-25 A-26 A-27 A-28 B-17 B-19 B-20 B-21 B-22 802330 803150 803490 805410 805790 806200 806598 802380 803070 803475 803850 804250 273540 273537 273560 273548 273557 273548 273560 273927 273940 273927 273927 273957 0.25 0.80 0.50 1.05 0.35 0.30 0.40 0.20 0.20 1.15 0.55 0.60 21.09 22.10 22.26 20.83 16.80 16.43 20.55 20.74 19.49 22.27 24.69 24.73 112 Appendix II Other Results of Data Analysis Table II.1: Cont. B.H. No. X (m) Y (m) t (m) P2O5% B-24 B-25 B-26 B-27 B-28 C-17 C-19 C-20 C-21 C-22 C-23 C-24 C-25 C-26 C-27 C-28 D-17 D-18 D-19 D-20 D-21 D-22 D-23 D-24 D-25 D-26 D-27 D-28 D-29 E-21 E-22 E-23 E-25 E-26 E-27 E-28 E-29 E-30 F-17 F-18 F-19 F-20 F-21 F-22 F-23 F-24 F-25 F-26 F-27 F-28 F-29 F-30 804995 805410 805796 806215 806590 802330 803040 803420 803805 804230 804601 804990 805398 805780 806190 806570 802330 802630 803010 803400 803775 804192 804580 804970 805375 805760 806150 806450 806940 803770 804169 804550 805387 805720 806140 806540 806905 807320 802130 802590 802980 803350 803740 804150 804550 804930 805325 805710 806110 806501 806901 807280 273975 273957 273950 273935 273950 274330 274338 274330 274329 274329 274330 274352 274352 274352 274352 274348 274719 274720 274728 274724 274723 274730 274756 274740 274740 274735 274723 274728 274756 275130 275145 275145 275151 275163 275150 275153 275175 275090 275527 275550 275557 275560 275555 275557 275555 275560 275560 275560 275550 275560 275570 275598 0.60 0.50 0.35 0.3 0.45 0.30 0.90 1.50 1.3 0.45 0.60 0.55 0.60 0.50 0.30 0.20 0.20 0.50 0.55 0.65 0.95 1.05 0.6 1.4 0.45 0.4 0.80 0.50 1.25 0.5 0.45 0.85 0.65 0.35 0.40 0.80 0.55 0.35 0.70 0.30 1.30 0.75 0.60 0.80 1.00 0.67 0.78 0.40 0.30 0.55 0.45 0.45 24.11 21.87 17.77 17.99 23.85 24.96 23.08 24.58 23.36 21.82 16.66 22.68 23.08 27.58 27.31 22.12 25.72 26.54 18.75 27.53 28.75 18.17 17.86 24.98 23.24 23.72 21.09 27.71 20.80 24.81 26.58 23.70 23.91 25.78 23.55 22.87 17.09 11.28 27.55 20.54 26.52 30.35 24.81 28.36 25.12 20.79 23.82 25.04 17.91 20.14 17.16 12.89 113 Appendix II Other Results of Data Analysis Table II.1: Cont. B.H. No. X (m) Y (m) t (m) P2O5% G-17 G-18 G-19 G-20 G-21 G-22 G-23 G-24 G-25 G-26 G-27 G-28 G-29 G-30 G-31 G-32 G-33 H-17 H-19 H-20 H-24 H-25 H-26 H-27 H-28 H-29 H-30 H-31 H-32 H-33 H-34 I-25 I-26 I-28 I-29 I-30 I-31 I-32 I-33 I-34 I-35 J24 J25 J34 B'24 B'25 B'26 B'27 B'28 C'23 C'24 C'25 802192 802580 802980 803340 803710 804148 804565 804905 805320 805700 806098 806498 806890 807270 807660 808145 808479 802190 802910 803330 805160 805301 805670 806075 806460 806860 807250 807640 808125 808520 808909 805260 805630 806440 806850 807237 807630 808101 808515 808827 809251 805130 805301 808870 805010 805410 805796 806190 806610 804660 805040 805450 275900 275920 275930 275933 275945 275908 275803 275950 275945 275940 275940 275950 275970 275990 276020 2760580 276085 276170 276348 276190 276360 276353 276353 276250 276360 276390 276437 276456 276475 276510 276540 276775 276691 276676 276790 276828 276840 276859 276890 276965 276885 277115 276960 277110 273180 273160 273150 273201 273290 272755 272740 272755 1.40 0.15 0.60 0.45 1.10 0.95 1.65 0.70 0.40 0.45 0.35 0.45 0.35 0.65 0.65 0.40 0.25 2.05 0.70 0.25 0.50 0.45 0.45 0.55 0.55 0.55 0.65 0.65 0.55 0.35 0.45 0.45 0.60 0.60 0.40 0.65 0.60 0.95 0.90 0.45 0.35 0.35 0.35 0.55 0.25 0.60 0.30 0.10 0.35 0.20 0.75 0.60 29.21. 30.32 24.81 31.10 27.61 25.62 23.98 29.91 24.39 19.65 21.18 15.85 15.73 20.79 16.26 24.37 21.81 25.62 18.35 20.41 23.13 21.80 18.35 20.81 16.00 22.13 15.48 18.17 25.95 30.20 25.63 28.25 23.97 19.64 30.06 21.24 25.25 25.32 28.74 27.70 25.35 23.02 29.35 27.48 16.34 .21.55 25.21 23.12 21.46 24.3 19.01 21.62 114 Appendix II Other Results of Data Analysis Table II.1: Cont. B.H. No. X (m) Y (m) t (m) P2O5% D'23 D'24 D'25 804880 805080 805468 272530 272348 272370 0.30 0.50 0.40 15.43 24.19 22.57 115 Appendix III Appendix Results of Area II III Results of Area II III.1 Calculated tonnage and average assay at area II As it has been mentioned before the study area II was divided into 5 zones, named, (d,e,f,g, and h). Calculation of the average thickness, average assay and total tonnage at each zone has been carried out using the same steps explained in Chapter 4. Figures (III.1 through III.5) show the distribution of the boreholes at each of the 5 zones respectively, while Figure (III.6) shows the over all area II. 116 Appendix III Results of Area II 276600 276400 276200 276000 1 16 275800 X, m 2 1 15 275400 18 275200 20 19 5 6 12 11 7 13 14 17 275600 4 3 9 10 22 8 25 21 23 26 24 3 27 3 34 275000 35 274800 32 31 36 29 33 37 28 30 3 3 274600 802000 802500 803000 803500 804000 804500 Y, m Figure III.1: Triangulation net of zone "d" at El Mahamid area II. 275000 274000 X, m 3 7 4 5 6 8 23 223 21 20 18 19 17 3 3 3 3 3 3 27 28 25 29 26 39 24 40 38 3 41 43 44 42 47 3 45 46 48 49 1 274500 273500 273000 272500 272000 804000 2 804500 805000 805500 9 10 3 11 3 16 15 3 30 31 12 3 3 14 3 13 32 33 35 37 36 34 806000 806500 807000 Y, m Figure III.2: Triangulation net of zone "e" at El Mahamid area II. 117 Appendix III Results of Area II 277500 277000 1 276500 X, m 276000 275500 275000 274500 7 9 10 16 3 5 6 11 12 13 4 31 35 33 29 34 32 28 36 37 38 39 43 42 41 40 44 2 8 25 24 26 23 22 27 15 17 18 21 19 14 20 30 45 274000 273500 806000 806500 Figure III.3: 807000 807500 Y, m 808000 808500 809000 809500 Triangulation net of zone "f" at El Mahamid area II. 277500 6 277000 X, m 276500 276000 30 30 31 30 275500 51 275000 274500 804000 5 7 56 55 8 4 9 13 54 3 10 12 2 11 53 1 28 27 26 25 24 23 22 34 37 39 33 38 32 35 36 48 46 47 52 50 49 804500 805000 805500 14 15 21 40 45 17 16 20 41 18 19 42 44 806000 43 806500 807000 Y, m Figure III.4: Triangulation net of zone "g" at El Mahamid area II. 118 Appendix III Results of Area II 274800 274600 3 10 9 5 1 4 X, m 274400 274200 7 14 2 6 13 16 19 17 20 11 274000 273800 21 12 15 8 22 23 18 273600 273400 802000 802500 803000 803500 804000 804500 Y, m Figure III.5: Triangulation net of zone "h" at El Mahamid area II. 278000 277000 X,m 276000 275000 274000 273000 272000 801000 802000 803000 804000 805000 806000 807000 808000 809000 810000 Y, m Figure III.6: Triangulation net of area II at Eastern El Mahamid. 119 Appendix III Results of Area II Table III.1: Summary of Zone II of, El Mahamid area. Zone 1 2 3 4 5 No.of Tri. 37 49 45 56 23 No.of B.H. 27 36 32 38 21 Area, m2 2784153 4261362 3785742 4504577 2061931 17397765 Av. Thick 0.733 0.495 0.551 0.624 0.700 Av. P2O5 25.56 21.7 20.82 23.37 23.28 Tonnage 3715573 3836305 3799033 5115320 2626814 19093045 Result of part II No. of triangles No. of B.H. Area Volume Av.Thick. Av.Assay Tonnage 210 123 17323592 10444529.965 0.603 22.946 19009044.536 120