The Evolution of Filters for Astronomical Applications: A Manufacturer’s View Robert W. Sprague, Thomas A. Mooney, John R. Potter, Kevin R. Downing, Michael J. Tatarek and Ali Smajkiewicz Materion Barr Precision Optics & Thin Film Coating Westford, MA U.S.A. Overview ■ Who/what is Materion? ■ Why do we pursue a small fastidious market? ■ What has changed in this market from our perspective over the last twenty years? ■ How the change has influenced our technological development? Materion Barr Precision Optics &Thin Film Coatings Fabricator of Thin Film Coatings Buellton, CA Westford, MA Windsor, CT ■ 700+ people ■ 100+ deposition systems ■ ALL Physical Vapor Deposition (PVD) ■ 1 to 1,000,000s of parts ■ Optical filters from 180 nm to 60 µm ■ Non-optical Thin Film Structures Shanghai, PRC Buellton, CA Formerly Thin Film Technology (TFT) ■ Precision thin film coating ■ Magnetron sputter, IAD and Evaporation ■ Specialty thin film coatings ■ Aerospace and medical applications ■ Infrared filters Windsor, CT Formerly Technimet ■ Engineered films ■ Barrier coatings ■ Roll-to-roll coating Up to 54” wide Medical applications ■ Precision slitting Wai Gai Qiao Free Trade Zone Shanghai Formerly EIS Optics ■ Optical coatings ■ Magnetron sputter, evaporation, IAD ■ Opto-mechanical assemblies ■ Patterned filters ■ Wafer level packaging ■ Large volume commercial applications ■ Projection display light engines Westford and Tyngsboro , MA Formerly Barr Associates ■ Evaporation, IAD, magnetron and Ion Beam Sputtering (IBS) ■ Founded in 1971 by Edward Barr ■ 110,000 ft² (11,800m²) ■ Wavelength from 150 nm to beyond 60 um ■ Provide optical filter solutions for virtually all key markets and applications ■ Purchased by Brush Wellman in 2009 ■ Name changed to Materion in 2011 ■ Location at which the work in this presentation was performed Astronomers Are Always Looking To Improve On Previous Results… Each instrument is unique. Astronomers use all manner of optical filters. Wide Band Bessel set and its derivatives Narrow Band Hydrogen line filters Beam Splitters Order separation for spectrographs Notch Laser Guide star Ground-based Professional Astronomers Have Unique Challenges and Advantages Looking Through The Atmosphere Turbulence limits effective aperture Atmospheric absorption limits spectral regions Light Pollution Larger Primary Mirror MORE LIGHT See Fainter Objects See Farther Back In Time Shorter Exposure Better resolution Size Evolution Telescopes, Instruments, Filters Palomar, 1949, 5 meter Keck , 1993, 10 meter E-ELT, 2015, 40 meter Typical Instrument Astronomer Filter Size 50 mm MOSFIRE EAGLE 250 mm 500 to 750 mm Technologies Enabling Large Scopes Spin Casting Up To 8.4 Meters Steward Observatory Mirror Lab Light Weight Honeycomb Mirrors Segmented Primaries Thirty Meter Telescope (TMT) will have 492 segments Diffraction-limited observations provide gains in sensitivity that scale as D4 (D is the primary-mirror diameter) “TMT will provide a sensitivity gain of a factor more than 100 as compared to current 8 m telescopes.” (SCIENCE-BASED REQUIREMENTS DOCUMENT TMT.PSC.DRD.05.001.CCR18) Adaptive Optics Compensate for atmospheric turbulence Solid State Detectors Mosaics of large area CCDs We Have Adapted All Aspects Of The Manufacturing Process ■ Material Fluorides and Sulphides to Oxides ■ Methods Evaporation to IAD, Sputtering ■ Deposition Systems ■ Substrate Preparation ■ Test Equipment ■ Facilities Material Change ■ Prior to 1980’s Filters were produced with evaporation, mostly resistively heated Many materials were hygroscopic, filters had to be encapsulated for long life and stable operation Difficult to create with a very good transmitted wave front Oxide materials Lower absorption in the blue and UV Highly porous and thus susceptible to drift In the 80’s, “energetic” processes were developed Ion assisted deposition, magnetron sputtering, Dual Ion Beam Sputtering, ion plating and others Produced filters with very high packing density, no measurable humidity drift What makes a filter “Big” ■ Driven by : Uniformity of spectral characteristics Narrow filters (bw ~.02% in visible) - big is 70 mm Broad band (bw a few % or more) - 700 mm is big Sensitivity of design Stability of the deposition process 14 H beta Narrow Band Filter ■ Diameter: 70 mm +/- 0.2 mm ■ Clear aperture: 65 mm minimum diameter ■ CWL = 486.136 +/- 0.03 nm ■ FWHM <= 0.05 nm (0.01%) ■ Peak T% > 45% (Goal > 50%) ■ Transmission variation < 5% over clear aperture ■ TWF < 0.25 waves P-V @ 430 nm over 65 mm CA min (see note) ■ Operating temp: 18-20ºC ■ AOI = 0 degrees, collimated beam ■ Out-of-band blocking OD4 from 340-640 nm Our Measurements Blocking 8 7 6 OPTICAL DENSITY 5 4 3 2 1 0 340 355 370 385 400 415 430 445 460 475 490 505 520 535 550 565 580 595 610 625 640 WAVELENGTH (NM) Our Measurements Transmission uniformity Customers Measurement Transmission Customers Measurement uniformity map Black color in this map corresponds to a central wavelength of 486.115 nm (and below) White color to a central wavelength of 486.155 nm (or above) Gray scale is linear, the extreme values (black/white) of the gray scale have not been incurred in the map) Black ring demarks the clear aperture Study the Sun Spots ■ High resolution video image ■ View the video at: http://www.nso.edu/press/H-Beta Broad Band Filter Growth 1997-2004 75 mm for SDSS Delivered 1997 150 mm for WIYN Delivered 2004 Broad Band Filter Growth 2004-2008 570 mm for Pan-STARRS Delivered 2008 Pan-STARRS was at the limit of our capabilities. Broad Band Filter Sets Sloan Digital Sky Survey Bessel- Johnson Filters Made from color filter glass Absorption based Angle insensitive Size limited by CFG manufacture Interference Based Angle sensitive Bandwidths and position broadly tunable Size limited by deposition system Pan-STARRS Filters Comparison of Pan-STARRS filter set measured at Barr Associates and in use. Barr’s measurements are the lower curves. http://svn.pan-starrs.ifa.hawaii.edu/trac/ipp/wiki/PS1_Photometric_System Next Steps ■ Large filters require large deposition systems ■ Precision filters larger than 560 mm could not be made ■ Acquired a new chamber based on experience and modeling System delivered in January 2013 First filter shipped in March 2013 Subaru Hyper Suprime Camera Filters All Dielectric Filter Fully Blocked for Si 7 6 ABS 5 4 3 2 1 0 300 400 500 600 700 800 Wavelength (nm) %T LAO_130321 %T 100 90 80 70 60 50 40 30 20 10 0 300 400 500 600 700 800 Wavelength (nm) 900 1000 1100 900 1000 1100 Uniformity of Green Filter 0.40% Defiation from target ceter wavelength 0.35% 0.30% 0.25% 0.20% 0.15% 0.10% 0.05% 0.00% 0 50 100 150 Distance from Center (mm) 200 250 300 Rugates Development supported by Air Force (1997-2004) Based on sinusoidal refractive index variation Bandwidth is proportional to amplitude of index variation Reflectance per cycle is proportional to index contrast Rejection is by reflection, so more rejections mean more cycles Spatial period of structure determines wavelength of reflection Ideally has no harmonics Works very well for applications requiring narrow rejection bands in broad transmission spectra Beam splitters for Guide Stars Light pollution rejection Rugate Cost Drivers ■ Relative Bandwidth (FWHM/CWL) Reflection per cycle is determined by index contrast ■ Rejection requirement (OD) ■ Wavelength Longer wavelength means longer cycles ■ Cost ~ Wavelength * OD/RBW Rugate Filters can be Made at any Wavelength from Visible through SWIR Three band rugate on Sapphire 100% Transmission (%) 90% MODEL Measured Uncoated 80% 70% 60% 50% 40% 30% 20% 10% 0% 300 800 1300 1800 2300 2800 3300 3800 4300 4800 5300 5800 6300 Wavelength (nm) Bandwidths can be Large or Small Range of Rugates produced at Barr Associates 100% 90% BW ~ 2% BW~ 106% 80% 70% Transmission 60% 50% 40% 30% 20% 10% 0% 400 900 1400 1900 Wavelength (nm) 2400 2900 Single Notch at 45 degrees AOI 100 90 80 70 45° Random verage Polarization Calcualted T @45 (S+P)/2 50 40 30 1 20 0.9 10 0 400 450 500 550 600 650 Waveelngth (nm) 700 750 800 850 900 Fraction of High Index m aterial Transmission 60 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 0 2000 4000 6000 8000 Thickness (nm) 10000 12000 14000 What do they want ? Remove the ‘Meinel bands’ of the hydroxyl radical (OH) in an ionospheric layer at 90 km. See what is in between 1 nm band width 81 rejection bands OD 3 1 0.9 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 1050 1100 1150 1200 1250 1300 1350 1400 1450 1 nm band width 81 rejection bands OD 3 1.3 mm of coating 0.95 0.9 0.85 0.8 0.75 0.7 0.65 Per Cent High Index 0.6 0.55 0.5 0.45 0.4 0.35 0.3 0.25 0.2 0.15 0.1 0.05 0 0 28464 77307 132083 192221 252983 313156 374798 434070 494531 555129 615473 675936 736427 Metric Thickness (nm) 802684 866573 927176 1015695.8125 1110747 1182702 1254702 Conclusion The only way to know your limitations is to exceed them! ■ Astronomers require you keep pushing the envelope of what is possible because they demand the highest performance ■ The methods then developed can be applied to other projects