“I hereby declare that I have read this thesis and in my opinion this thesis is sufficient in terms of the scope and quality for the award of the degree of Master of Science (Physics).” Signature :……….……………….. Name of Supervisor : Assoc. Prof. Dr. Noriah Bidin Date :…21 / 11 / 2005……………… DEVELOPMENT OF A WATER COOLING SYSTEM FOR Nd:YAG LASER CHAMBER NOR AZIAWATI BINTI AZAHARI A thesis submitted in fulfilment of the requirements for the award of the degree of Master of Science (Physics) Faculty of Science Universiti Teknologi Malaysia NOVEMBER 2005 I declare that this thesis entitled “Development of A Water Cooling System for Nd:YAG Laser Chamber” is the result of my own research except as cited in the references. The thesis has not been accepted for any degree and is not concurrently submitted in candidature of any other degree. Signature :……………………… Author’s name : NOR AZIAWATI BINTI AZAHARI Date :…21 / 11 / 2005……………………. Dedication to my beloved father and mother (Azahari Yusoff and Azizah Yaman),sisters, brother and all my friends. Thanks for everything ………… ACKNOWLEDGEMENT First and foremost I wish to give all the praise to Almighty God for giving me the strength and time to complete this research. With His blessings may this work be beneficial for the whole of humanity. I’m deeply indebted to my supervisor, Associate. Professor Dr. Noriah Bidin, for her help, guidance and encouragement throughout this work. She has thought me her professionalism and the profound art of research which inevitably is reflected in this thesis. For all these, and for innumerable friendly discussions we have had, I am very grateful. Thanks also go to my co-supervisor, Dr Johari Adnan for his advice, guidance and motivation. Without their continue support and interest, this thesis would not have been the same as presented here. My sincere appreciations extend to all my colleagues and friends at Laser Technology Laboratory for their co-operation and assistance. I would also like to acknowledge the support of my parents, sisters and brother for their kindly good encouragement in the course of my study. Finally, I am also indebted to Universiti Teknologi Malaysia for the financial support in my Master study and Government of Malaysia, Ministry of Science, Technology and Innovation for granting this project through IRPA vote, 74531. Without this financial support, this project would not be possible. ABSTRACT In solid state lasers, only a small fraction of electrical input power is converted to laser radiation. The remainder of the input power is converted to heat. Therefore, solid state lasers require cooling for the pump source and active medium. In the case of flashlamp pumping usage, a cooling system in the chamber is desirable. Without adequate cooling, the laser seals, pumping cavity, lamps and the rod itself would be damaged by overheating. Thus, the aim of this project is to develop a water cooling system such that the lowest practical operating temperature is produced, and to monitor temperatures of the laser chamber during the pumping process. In order to achieve these objectives, a refrigerated water cooling system was developed which included an internal and external water cooling system. Measurements of various parameters of this water cooling system were made in order to determine its appropriateness in solid state laser chamber. A laser chamber was set-up, which comprised of a Nd:YAG laser rod, flashlamp, chamber heat sink and stainless steel blocks. An aluminium laser house was designed inclusive with electrical and water piping system. After assembling the whole system, the circulation of water in the cooling system was tested. This is to ensure no leakage occurred during the pumping process. The flow rate of water during circulation is 9.83 ± 0.01 liter / min. The minimum temperature of the cooling system that could be achieved was 18.00 ± 0.05 oC. The temperature distribution during pumping process was monitored at different points on the laser chamber. The information obtained leads to the calculation of heat dissipation from the laser chamber which operated with and without chilled distilled water. The comparison results shows that 20% improvement in heat liberated from flashlamp, whereas, 90% and 86% improvement in heat absorption in chamber heat sink and stainless steel blocks respectively. This indicated that the cooling system provided in the laser chamber was very effective in carrying out the excess heat from pumping process. ABSTRAK Dalam laser pepejal, hanya pecahan kecil kuasa masukan elektrik ditukarkan kepada pancaran laser. Lebihan daripada kuasa masukan ditukar kepada haba. Oleh itu, laser pepejal perlu penyejukan pada sumber pengepaman dan medium aktif. Dalam kes yang melibatkan penggunaan lampu kilat, sistem penyejukan dalam kebuk diperlukan. Tanpa penyejukan secukupnya, pelekat-pelekat dalam laser, rongga pengepaman, lampu dan rod laser sendiri akan rosak disebabkan oleh pemanasan berlebihan. Oleh itu, tujuan projek ini adalah untuk membina sistem penyejukan air supaya suhu proses terendah yang praktikal dihasilkan, dan juga untuk memantau suhu kebuk laser semasa proses pengepaman. Untuk mencapai objektif ini, sistem penyejukan air telah dibangunkan yang terdiri daripada sistem penyejukan dalaman dan luaran. Pengukuran pelbagai parameter sistem penyejukan air ini telah dilakukan dengan tujuan untuk menentukan kesesuaiannya dalam kebuk laser pepejal. Kebuk laser yang terdiri daripada rod laser Nd:YAG, lampu kilat, kebuk penebat haba dan blok keluli tahan karat telah dibina. Rumah laser aluminium juga dibangunkan yang lengkap dengan sistem saluran elektrik dan air. Selepas menggabungkan seluruh sistem, edaran air dalam sistem penyejukan diuji. Ini dilakukan untuk memastikan tiada kebocoran semasa proses pengepaman. Kadar aliran air semasa edaran diperolehi sebagai 9.83 ± 0.01 liter/ min. Suhu minimum sistem penyejukan yang dapat dicapai adalah 18.00 ± 0.05 oC. Taburan suhu semasa proses pengepaman dipantau di titik berlainan pada kebuk laser. Maklumat yang diperoleh digunakan untuk pengiraan haba dikeluarkan daripada kebuk laser dimana dikendalikan dengan dan tanpa penyejukan air suling. Keputusan yang diperolehi hasil perbandingan menunjukkan lebihan haba yang dibebaskan oleh lampu kilat dalam sistem yang disejukkan adalah 20%, sementara haba yang diserap oleh kebuk penebat haba dan keluli tahan karat masing-masing didapati bertambah sebanyak 90% dan 86% . Ini menunjukkan sistem penyejukan yang dibekalkan pada kebuk laser amat efektif untuk membawa keluar lebihan haba semasa proses pengepaman. TABLE OF CONTENTS CHAPTER 1 TITLE PAGE DECLARATION ii ACKNOWLEDGEMENT iv ABSTRACT v ABSTRAK vi CONTENT vii LIST OF TABLES xi LIST OF FIGURES xii LIST OF SYMBOLS xv INTRODUCTION 1.1 Overview 1 1.2 Thermal Loading of Lamp-pumped 3 Nd:YAG Lasers 2 1.3 Previous Research 4 1.4 Problem Statement 5 1.5 Research Objective 5 1.6 Research Scope 6 1.7 Thesis Outline 6 LITERATURE REVIEW 2.1 Introduction 8 2.2 Solid State Laser 8 2.3 Basic Construction of Solid State Lasers 10 2.4 The Nd:YAG Laser 12 2.4.1 Principle of Operation 13 2.5 Energy Transfer in Solid State Lasers 15 2.6 Thermo-optics Effects 16 2.7 Fundamental of Heat Transfer 17 2.8 Modes of Heat Transfer 18 2.8.1 Conduction 18 2.8.2 Convection 19 2.8.3 Radiation 19 2.9 Cooling Techniques in Solid State Lasers 20 2.9.1 Liquid Cooling 20 2.9.1.1 Water Cooler with a Liquid to Air 22 Heat Exchanger 2.9.1.2 Water Cooler with a 23 Liquid to Liquid Heat Exchanger 2.9.1.3 Water Cooler with a Refrigeration 24 Unit 2.10 3 2.9.2 Air or Gas Cooling 25 2.9.3 Conductive Cooling 26 Summary 27 DEVELOPMENT OF A WATER COOLING SYSTEM 3.1 Introduction 28 3.2 Water Cooling System 28 3.2.1 External Coolant 29 3.2.2 Internal Coolant 34 4 3.3 Laser Chamber 36 3.4 Lab Recorder 36 3.5 Monitoring Laser Chamber 38 CHARACTERIZATION OF THE WATER COOLING SYSTEM 4.1 Introduction 40 4.2 Water Temperature 40 4.2.1 Temperature of External Coolant 41 4.2.2 Temperature of Internal Coolant 43 4.3 4.4 5 Water Quality 46 4.3.1 The pH Level 47 4.3.2 Conductivity and Resistivity of Water 49 Summary 53 DEVELOPMENT OF A LASER CHAMBER 5.1 Introduction 54 5.2 Laser Chamber 55 5.2.1 Nd:YAG Laser rod 56 5.2.2 Flash lamp 56 5.2.3 Flow Tube 57 5.2.4 Stainless Steel Block 58 5.2.5 Chamber Heat Sink 60 5.2.6 Base Plate 62 5.2.7 Technical accessories 64 5.3 Assembly of the Laser Chamber 64 5.4 The Laser House 68 6 5.5 Piping 71 5.6 Testing the Circulation System 72 5.7 Water Flow 74 5.8 Summary 76 TEMPERATURE MONITORING DURING PUMPING PROCESS 6.1 Introduction 77 6.2 Heat Loss 78 6.3 The Temperature Distribution of Laser Chamber 80 6.3.1 80 The Temperature Distribution of the Laser Chamber with chilled water 6.3.2 The Temperature Distribution of the 84 Laser Chamber without water cooling 7 6.4 Heat at Different Part of the Laser Chamber 87 6.5 Summary 89 CONCLUSION AND SUGGESTIONS 7.1 Conclusion 91 7.2 Problems and Suggestions 93 REFERENCES 96 APPENDIX A 101 PUBLICATIONS 103 LIST OF TABLES TABLE NO. TITLE PAGE 4.1 Temperature measurement of external coolant upon times 42 4.2 Temperature measurement of internal coolant times domain 44 4.3 pH of distilled water at various temperatures 47 4.4 Conductivity of distilled water at various temperatures 50 4.5 Resistivity of distilled water as the reciprocal of conductivity 51 at various temperatures 5.1 Physical properties of pump used by internal cooling system 75 6.1 Physical properties of laser chamber 79 6.3 Temperature at different parts of laser chamber with 81 chilled water operation 6.4 Temperature of laser chamber at different part without 85 chilled water 6.5 The results of energy absorbed at different parts in laser chamber during pumping process 89 LIST OF FIGURES FIGURE NO. TITLE PAGE 2.1 A generic solid state laser 10 2.2 Typical Pumping Cavities ;(a) Single ellipse, 11 (b) Double ellipse, (c) Circular Cylinder, (d) Close-warp 2.3 Energy level system of Nd:YAG laser 13 2.4 The flowchart of energy transfer in solid state lasers 16 2.5 Schematic of a water cooler containing a water to water 23 heat exchanger 2.6 Schematic of a water cooler employing a refrigeration unit 24 2.7 Laser head of a small air-cooled Nd:YAG laser 25 2.8 Typical geometry of a conductively cooled laser rod 26 3.1 The schematic diagram of whole cooling system 29 3.2 The circulation in external coolant 30 3.3 The schematic diagram of external coolant 32 3.4 Photograph of compressor based refrigeration system 33 components 3.5 Photograph of whole system of external coolant 33 3.6 The schematic diagram of internal coolant 35 3.7 The schematic diagram for Lab Recorder calibration 37 3.8 Experimental set-up for temperature measurement of 39 pumping system 4.1 The temperature of external coolant with respect to time 43 4.2 The temperature of internal coolant at various times 45 4.3 Graph pH versus temperature for distilled water 48 4.4 Graph resistivity versus temperature of distilled water 52 5.1 The photograph of Nd:YAG laser rod 56 5.2 The photograph of flashlamp 57 5.3 The photograph of flow tube 57 5.4 Engineering drawing of block 1. (Dimensions are in 58 millimeters (mm)) 5.5 Engineering drawing of block 2. (Dimensions are in 59 millimeters (mm)) 5.6 The photograph of stainless steel blocks 1 and 2 60 5.7 Dimension of top view of the chamber heat sink. (Dimensions 60 are in millimeters (mm)) 5.8 The photograph of chamber heat sink 61 5.9 Dimension of side view of the chamber heat sink. (Dimensions 61 are in millimeters (mm)) 5.10 Dimension of front view of the chamber heat sink. (Dimensions 62 are in millimeters (mm)) 5.11 Dimension of top view of base plate. (Dimensions are 63 in millimeters (mm)) 5.12 Dimension of side view of base plate. (Dimensions are 63 in millimeters (mm)) 5.13 The photograph of base plate 63 5.14 The photograph of O ring, block clamps and other screw 64 used to ensemble laser chamber 5.15 The schematic diagram of complete pumping chamber 66 from side view 5.16 The schematic diagram of pumping chamber without 66 chamber heat sink from side view 5.17 The photograph of pumping chamber (From side view) 67 5.18 The photograph of pumping chamber without 67 chamber heat sink (From top view) 5.19 Technical drawing of front cover of laser house from (a) front view , (b) side view. (Dimensions are in 68 millimeters (mm)) 5.20 Technical drawing of housing from (a) front view (b) top view 69 (c) side view. (Dimensions are in millimeters (mm)) 5.21 The photograph of laser (a) from top view without laser trail, 70 (b) from top view with laser trail and (c) from side view including the laser chamber 5.22 Dimension of side view of L pipe. (Dimensions are in 71 millimeters (mm)) 5.23 The photograph of L pipe 71 5.24 Schematic diagram showing circulation of cooling system 72 from coolant to the laser head 5.25 The flow path of distilled water in laser chamber 73 during circulation (top view) 5.26 The detail of circulation system in laser chamber 74 (focused in ellipsoid space) 6.1 Temperature profile at laser chamber when operated 83 with chilled water 6.2 Temperature profile without chilled water 87 LIST OF SYMBOLS Qo - Heat before Q - Heat after t2 - Time maximum t1 - Time minimum ∆θ - Temperature change cp - Specific heat m - Mass θ - Temperature R - Water flow rate v - Volume t - Time Pabsorbed - Power absorbed Pi - Power input %Pabsorbed - Percentage of power absorbed CHAPTER 1 INTRODUCTION 1.1 Overview The first decade of solid-state laser technology has seen the development of an enormous number of lasing materials and a large variety of interesting design concepts. However, in recent years the technology has matured to a point where solid state lasers have reached a plateau in their development. To a major extent, the growth in importance of solid state lasers for industrial and military applications and as a general research tool are due to the improvement in reliability and maintainability of these systems. A wealth of applications for solid state lasers has emerged in materials processing, holography, range finding, target illumination and designation, satellite and lunar ranging, thermonuclear fusion, plasma experiments, and in general for scientific work requiring high power densities (Koechner, 1976). A solid state laser system contains, for its lasing element, a ruby, Nd-YAG, Nd-glass or the like. Solid state lasing elements are fabricated into solid cylinders of various lengths and diameters. The rods are optically transparent and the ends are cut flat and parallel to each other. The end surfaces are polished very highly and coated with a reflective material. These laser elements are optically pumped (illuminated) by a high intensity flashlamp or krypton-arc or tungsten halogen lamp. Some of these lasers operate in the pulsed mode and others operate in both pulsed and continuous wave modes. They are cooled either by air or tap water circulating through the laser head, which includes flashlamp (Muncheryan, 1983). In all solid state laser elements, the excitation to emission occurs in the dopant, for example the dopant is neodymium ions in the YAG lasers. The energy of radiation from the flashlamp is at least equal or greater than the energy of the photons produced in the respective dopant. The excited atoms are raised to a higher than normal quantum state (energy state) from which they return to the ground state in steps, emitting photons of wavelengths characteristics of the dopant. The greater the energy applied to the dopant from the optical pump the greater is the intensity of the emitted radiation; this stimulating energy does not alter the frequency of the radiation from the particular dopant. Because the photons in the lasing cavity are produced by equal-energy photons, any two photons in the cavity are of the same phase, frequency, amplitude and direction. When the energy from the optical pump is not sufficient to excite the dopant atoms to radiation, the energy in transition may dissipate in the form of heat or photons. This condition elevates the temperature of the laser rod; the elevated temperature in the rod tends to reduce the photon emission. So that, to prevent from overheating, the lasing rod is cooled either by circulation of air or distilled water through the laser head (Muncheryan, 1983). Since Nd:YAG laser is the most powerful laser in this category, our study will be directed to a system containing a Nd:YAG laser rod in the laser head. Thus, it is important that during the planning stages of a laser system, careful measurement includes water temperature, quality and flow rate must be made to provide a suitable cooling system (Muncheryan, 1979). 1.2 Thermal Loading of lamp-pumped Nd:YAG Lasers Consider a typical continuous wave (cw) Nd:YAG laser with an output power of 300 watts and input power of 12 kilowatts. Assuming a quantum efficiency of 50% (low) this means that 600 watts are absorbed in the laser. Thus 11,400 watts are not absorbed in the laser. The majority of this power is optical power from the lamps outside the pump bands of the laser. This excess power is absorbed by the cavity and by the lamps, thus dramatically increases the temperature of the laser. Roughly 10% to 20% of the electrical power will be dissipated as heat through the electrodes and 30% to 50% as heat through the envelope. In addition to causing mechanical overheating problem (seals and so on), thermal gradient will cause thermal focusing in the laser rod (Kuhn, 1998). Typically the lamps, the cavity, and the Nd:YAG rod are cooled by water. The usual pattern is to first take the incoming cold water and confine it to the region of the laser rod with a flow tube. This will remove the heat deposited in the rod that is not converted into laser light. Next, the water is allowed to flow through the major part of the laser cavity to remove the heat deposited in the reflectors and in the cavity walls. Finally, the water can be confined to the region around the lamps with a flow tube. This removes the heat absorbed in the quartz envelope. Many variations on this theme are possible depending on the total power dissipation in the laser. For example, in extremely high average power lasers, a water cooling loop is provided through the electrodes to avoid destroying them. In very low power lasers, water cooling may only be provided over the lamps. In some extremely low power lasers, it may even be possible to use air cooling (Kuhn, 1998). 1.3 Previous Research Advanced Nd laser application which requires increasingly higher average output power necessitate operating near the stress-fracture limit, i.e., a regime in which output power is limited by the possibility of material fracture arising from thermally induced stresses in the laser medium (Eggleston et al., 1984; Emmett et al., 1984). Mangir and Rockwell (1986) have found large variations in the heat generation accompanying flashlamp pumping of various types of Nd-doped phosphate glass and Yittrium Aluminium Garnet (YAG). According to Chen et al., (1990) thermal effects in flashlamp-pumped Nd:YAG lasers arise from the fact that nearly ten percent of the flashlamp energy is converted to heat in the laser medium, while about three percent is stored in the inversion as useful gain at the time of lasing. This heating is due to the sizeable quantum defect between the pump spectrum and the lasing wavelength, and quenching mechanisms. A new mode of laser operation is proposed by Bowman (1999) which should result in little or no heat generations within solid state laser materials. The technique utilizes balanced spontaneous and stimulated emission within the laser medium. The result would be a radiation balanced laser device in which no excess heat is generated because of the average quantum defect of the radiation process is adjusted to zero. If such a laser device can be realized, much higher average powers systems should be possible without many of the thermal and beam quality issues that limit conventional solid state laser. From year 2000 onwards, the research on thermal heating in solid state laser was more focused on diode pumped solid state laser which was found to have many advantages over lamp-pumped solid state laser. The advantages include high system efficiency and component lifetime and also reduction of thermal load of the solid state laser material (Koechner, 1988). Usievich et.al, (2001) present a paper that discloses an analytical method which delivers the exact temperature distribution in a circularly cylindrical symmetrical, longitudinally, and transversely nonuniform heat source distribution and circularly symmetrical cooling means. The analytical expressions obtained for the temperature distribution open the way to a better understanding of thermal phenomena and represent a fast tool for solid state laser design and optimization. 1.4 Problem Statement When laser rod was pumped by flashlamp, the temperatures of the rod will increase and the rod will expand. Such expansion will result in the change of length of the laser cavity and may cause overheating on laser equipment. To prevent the laser rod from experiencing drastic changes, it needs to be controlled by developing a cooling system and monitoring the laser chamber temperatures during the pumping process. 1.5 Research Objective The main objectives of this research are listed as follows: 1. To develop a cooling system. 2. To develop a laser chamber. 3. To measure the circulation of cooling system over the laser head. 4. To analyze dissipation of heat at different points on laser chamber during pumping process. 1.6 Research Scope In this study, a water cooling system and laser chamber for high power Nd:YAG solid state laser are developed. The input power of the flashlamp used for pumping is 1.6 kW. The measured parameters of water cooling system are including water temperature, quality and flow rate. A laser chamber is set-up which comprised of a laser rod, flashlamp, heat sink and stainless steel blocks. A laser house is built inclusive of electric and water piping system. The water cooling system is installed in the laser chamber and the circulation is tested. The laser rod is pumped with flashlamp and the temperatures at different points which include the flashlamp, stainless steel block and chamber heat sink of the laser chamber are measured within an hour. 1.7 Thesis Outline This thesis consists of seven chapters. The first chapter reviews some of previous research related to thermal heating in solid state laser. This chapter also contains the objectives of the research under taken. Chapter II covers the literature review related to the research work. This includes the fundamental of solid state laser, thermal effect in solid state laser, the fundamental of heat transfer and description of several types of cooling techniques used in solid state lasers. Chapter III describes the preparation of materials, development of water cooling system and facilities involved in the research; and also describe the technique used to measure temperature. In chapter IV the measurement of various parameters of a water cooling system is discussed. Two parameters are tested which include water temperature and water quality in order to ensure the cooling system is appropriate for chilling of the laser rod. The development of a laser chamber is explained in chapter V. This involves the development of the component in the laser chamber, the design of the laser house inclusive of an electric and water piping system and testing of the circulation of water cooling system in the laser chamber. Pumping of the laser rod is discussed in chapter VI. The temperature was monitored at different part of the laser chamber. The amount of heat dissipation was estimated based on the temperature information. The measurement was carried out with and without chilling of the distilled water. Finally, some conclusions of the project are drawn in chapter VII. These include summary of the project and discussion of the problems encountered during the work of the project; and finally last but not least, works to be carried out in the near future are suggested. CHAPTER 2 LITERATURE REVIEW 2.1 Introduction In solid-state lasers only a small fraction of electrical input is converted to laser radiation, the remainder of the input power is converted to heat. Solid state lasers require cooling of the pump source, active medium and in case of flashlamp pumping, cooling of the pump enclosure. In this chapter the fundamental of a solid state laser, thermal effect in solid state lasers, fundamental of heat transfer and several types of cooling techniques used in solid state lasers are treated. 2.2 Solid State Laser A solid state laser is one in which the atoms that emit light are fixed within a crystal or glassy material (Hecht, 1992). The first demonstration of laser action by Maiman was achieved in 1960 using ruby (Cr3+Al2O3). In 1960, Johnson and Nassau demonstrated the first solid state neodymium laser, in which the neodymium ion was a dopant in calcium tungstate (CaWO4). Elias Snitzer demonstrated the first neodymiumglass laser at American Optical Centre in the same year. In 1963, the best choice of neodymium host for most commercial applications- yttrium aluminium garnet (YAG), was demonstrated as a laser material by Geutic, Marcos and Van Ultert (Koechner and Bass, 2003). Compared to other lasers, the solid state lasers have several advantages. The solid state lasers can operate in continuous wave (cw), pulsed, Q-switched and modelocked modes to obtain high average power, high pulse repetition rate, high pulse energy and high peak power. The average power of 4 kW has commercially been achieved with modular construction YAG lasers. The peak power of 1013-1014 W has also been obtained (Kuhn, 1998). More than 100 solid state materials can produce laser beams. Most of these beams range in the visible and near infrared regions of the electro-magnetic spectrum. The UV wavelength has also been achieved by harmonic generators due to the advert of new non-linear materials and high beam quality obtained from diode pumped lasers. Significant progress has been made in the development of the tunable solid state lasers (Gan, 1995). Laser beams produced by some solid state lasers can be developed with optical fibre, which makes lasers more flexible and applicable in dangerous or difficult to access processing environments. Solid state lasers are also more compact and have lower maintenance compared to high power CO2 lasers and excimer lasers (Sintec, 2000). Solid state lasers are widely used for various applications, for examples in pure science, medicine, diagnostics and entertainment. It is expected, based on the trend observed in the past, that in general the use of various types of lasers will increase and dominate many fields. In particular, it is expected that by improving the reliability of the existing lasers or by introducing solutions needed, the market size of solid state lasers may increase significantly (Kalisky, 1999). 2.3 Basic Construction of Solid State Lasers A typical solid state laser usually consists of a laser rod (gain medium), a pumping cavity, two mirrors and a power supply as shown in Figure 2.1. The gain medium is placed in a reflective pumping cavity. Inside the cavity is an elliptical space with the rod (gain medium) at one focus of the ellipse and a flashlamp at the other focus. Light from an external source, pulsed flashlamp, a bright continuous arc lamp or another laser enters the laser rod and excites the light emitting atoms. Ideally all the light emitted by the lamp are coupled into the rod by the cavity. The optical resonator consists of two mirrors mounted separately from the lasing medium. The cavity mirrors form a resonant cavity around the inverted population in the laser rod, providing the feedback needed to generate a laser beam that emerges through the output mirror (Hecht, 1992). The cooling system is necessary since most of the light energy from the lamp is lost as heat (LEOT, 2001). Reflective cavity – focuses pump light onto laser rod Rear mirror Laser rod Pump light Lamp light source Output mirror Laser beam Lamp Power Supply Figure 2.1: A generic solid state laser [Hecht, 1992] One of the most important elements in solid state lasers is a pumping cavity. Besides providing good coupling between the pumping source and the absorbing material, it is also responsible for the pump density distribution in the laser element which influences the uniformity, divergence and optical distortion of the output beam (Koechner, 1976). Figure 2.2 shows some of the typical pumping cavities. (a) (b) (c) (d) Lamp Rod Figure 2.2: Typical Pumping Cavities ;(a) Single ellipse, (b) Double ellipse, (c) Circular Cylinder, (d) Close-warp [Sintec, 2000] Among the pumping cavities, the elliptical cavities have been most extensively used in the development of solid state lasers (Sintec, 2000). In this configuration, a linear lamp and a laser rod, possibly with different radii, are placed at the foci of an elliptical cylinder, as shown in Fig.2.2(a). This geometry usually results in the most efficient cavity. This cavity has further advantage that it minimizes the weight and size of laser head. Since the energy delivered to a discharge lamp is limited, scheme to focus the energy from many lamps onto a single crystal are attractive. Fig. 2.2(b) shows two partial elliptical cylinders having one common axis at which crystal is placed. Fig 2.2(c) and 2.2(d) show example of closed-coupled non focusing pump cavities. The lamp and rod are placed as close together as possible, and reflector closely surrounds the lamp and rod. The reflector can be circular or oval in cross section. Fig 2.2(d) type is often used in laboratory setups of low-repetition rate pulsed lasers. The efficiency of the closely wrapped cavity is found to be about as good as when an elliptical cylinder is used. The advantage of these pump cavity is fabrication simplicity (Sintec, 2000). The laser material is shaped into a cylindrical rod whose ends is round and polished to be plane parallel. When the rod is placed between two mirrors facing each other, and is strongly irradiated by an intense light source around it, a laser radiation is emitted. The rod ends are usually anti-reflection coated for the Nd:YAG wavelength of 1064 nm. The rod ends are held in place and sealed by O-rings in the ends of the rod holders to protect them from the pump light (Sintec, 2000). 2.4 The Nd:YAG Laser The primary commercial example of a conventional solid state laser is Nd:YAG. Nd:YAG lasing at 1.064 µm can be frequency doubled to 532 nm, tripled to 355 nm and quadrupled to 266 nm. Continuous wave Nd:YAG lasers are available in power levels up to several hundred watts and pulsed Nd:YAG lasers are available with pulse energies up to a few several joules per pulse (Kuhn, 1998). YAG has a combination of desirable properties as a host medium for Nd3+ ions: it has relatively high thermal conductivity, which allows it to disperse the waste heat from the optical pumping process; it has high mechanical strength, and can be grown as crystals of large size with good quality. The Nd3+ ions substitute within the YAG lattice in a single site so the emission and absorption lines are homogeneously broadened. Typical Nd3+ doping densities range up to 1% (Davis, 1996). 2.4.1 Principle of Operation Lasing is dependent on the rapid transitions from the lower lasing level to the ground state by radiationless transition. When the rod temperature is low, these transitions will occur at high rate. Hence, lasing efficiency depends mainly on cooling efficiency. Higher output powers can be achieved by having lower operating temperature. This explains why cooling systems are generally operated at temperature just above the threshold of this effect (Sintec, 2000). Figure 2.3: Energy level system of Nd:YAG laser [Wilson et.al, 1987] Figure 2.3 shows the energy levels involved in the Nd:YAG laser action. The number of 0, 1, 2 and 3 in Figure 2.3 represent the energy level E0, E1, E2, and E3 It is essentially a four levels system, with the lasing transition taking place between the 4F3/2 (E2) and 4I11/2 states (E1). The terminal state E1 is sufficiently far above the ground state to be practically empty at room temperature. The initial and final states are split into 2 and 6 crystal field level respectively, so that several lasing wavelengths are possible. The most powerful of these occurs at 1.064 µm and this is usually the one used (Wilson et al,1987). If (E1 – E0) is large compared with the thermal energy, kT, at the temperature of operation, then the populations of the levels E1, E2, and E3 are all effectively zero before pumping commences. Thus a population inversion can readily be achieved between levels E1 and E2, again the level E3 may be broad for effective pumping. Pumping excites atoms from the ground state into level E3, whence they decay rapidly into the metastable level E2, so that N2 increases rapidly to give inversion population inversion between E2 and E1. If the lifetime of the transition from level E1 to level E0 is short, then the population inversion can be maintained easily with modest pumping. Nd:YAG laser pumping requirements are modest, and for pulsed operation it can be met with a fairly simple flashlamp and reflecting cavity. To avoid overheating and subsequent damage of the laser rod, cooling air may be blown through the cavity. Continuous wave (cw) operation is also possible; the most popular pumping source being the quartz-halogen lamp. The most effective pumping bands lie between 700 nm and 900 nm in wavelength, which are reasonably close to the peak output of the lamps which occur at about 1 µm. Even so only a few percent of the total radiation emitted is usefully absorbed in the laser material. Consequently the overall power efficiency (it also applies to pulsed lasers) is fairly low. CW outputs of up to several hundred watts are possible, which implies that large amounts of waste heat will be produced, necessitating water cooling of the laser rod (Wilson et al,1987). 2.5 Energy Transfer Processes in Solid State Lasers Figure 2.4 shows the flow chart of simplified way the energy balance in a laser system. The electrical input power supplied to the lamp is either dissipated as heat by the lamp envelope and electrodes or emitted as radiation. A portion of the radiation will be absorbed by the metal surfaces of the pump cavity. The radiation reflected from the walls will be either absorbed by the lasing medium or will return to lamp. The light which is absorbed by the lamp will add energy to the radiation process in the same way as the electrical does, and the returned light will be radiated with the same efficiency as the power supplied electrically. One consequence of the reabsorption is that a lamp, when enclosed in the pumping cavity, is operated under a higher thermal loading resulting in shorter lamp life than when operated in the open for the same electrical input power. Since most laser cavities are liquid cooled, a distinction is made by the radiation actually absorbed by the surrounding cooling liquids and flow tube. The pump power absorbed by the laser rod causes stimulated emission and fluorescence at the laser wavelength and other main emission bands. The remainder is dissipated as heat by the laser material (Koechner, 1988). External Power Lamp input Heat loss by lamp Loss from source & transfer Light Light absorbed by pumping cavity Light absorbed by coolant and flowtube Light absorbed by lamp Light absorbed by laser rod Heat loss by rod Energy loss by fluorescence Stimulated emission Laser beam Optical losses Figure 2.4: The flowchart of energy transfer in solid state lasers [Koechner, 1988] 2.6 Thermo-optics Effects The optical pumping process in a solid state laser material is associated with the generation of heat for a number of reasons: (a) the energy difference of photons between the pump band and the upper laser level is lost as heat to the host lattice; similarly, the energy difference between the lower laser level and the ground state is thermalized. The difference between the pump and laser photon energies, termed quantum defect heating, is the major source of heating in solid-state lasers. (b) In addition, nonradiative relaxation from the upper level to the ground state, due to concentration quenching, and nonradiative relaxation from the pump band to the ground state will generate heat in the active medium. (c) In flashlamp-pumped systems, the broad spectral distribution of the pump source causes a certain amount of background absorption by the laser host material, particularly in the ultraviolet and infrared regions of the lamp spectrum. Absorption of lamp radiation by impurity atoms and color centers can further increase heating. The temperature gradients set-up in the gain material as a result of heating can lead to stress fracture, which represents the ultimate limit in average power obtainable from a laser material. Below the stress fracture limit, thermal lensing and birefringence adversely affect output beam quality. Also, due to thermal lensing, the operating point of the resonator within the stability diagram becomes a function of input power. Therefore the output beam quality and mode structure are power dependent because the thermal lens can only be compensated for one input power level (Koechner et.al, 2003). Efficient heat removal and the reduction of the thermal effects that are caused by the temperature gradients across the active area of the laser medium usually dominate design considerations for high average power systems. 2.7 Fundamental of Heat Transfer Since pumping process involves heat transfer, it would be better to discuss the fundamental of thermodynamics including the first and second law. The first law of thermodynamics involves the conservation of energy. It states that energy can be neither created nor destroyed; it can only change forms (Cengel et al., 1998). Transferring heat energy is subject to the second law of thermodynamics. The second law (for a closed system) states that for a spontaneous process there is a net increase in entropy that is a measure of the disorder that exists in a system (Martin, 1999). The first and second laws of thermodynamics govern the various modes of heat transfer: conduction, convection and radiation. 2.8 Modes of Heat Transfer Heat transfer is traditionally divided into three elementary forms: conduction, convection and radiation. Each of this represents a way in which energy flows from a hotter body to a cooler body. The rate at which heat flow maybe represented by the . symbol Q . In general, the amount of energy which flows as heat during the interval between t1 and t2 is given by (Espinola, 1994) t2 . Q = ∫ Q dt t1 (2.1) In most cases, we will be studying constant heat flow, so . Q = Q(t 2 − t1 ) (2.2) 2.8.1 Conduction In conduction, heat flows from a regions of higher temperature to a region of lower temperature. This occurs within solid, liquid, or gaseous mediums or between different mediums that make direct physical contact with each other (Kreith, 1973). The transfer of the energy of motion between adjacent molecules conducts the heat. In a gas, 'hotter' molecules, have greater energy and motions, and impart energy to adjacent molecules at lower energy levels. This type of transfer occurs to some extent in all solids, gases or liquids in which a temperature gradient exists. In conduction, energy can also be transferred by "free" electrons, which is important in metallic solids (Geankopolis, 1993). Examples of conduction are heat transfer through the surfaces of cold plates or through the walls of refrigerator. In this particular project, stainless steel blocks, would absorb excess heat during pumping process, by conduction. 2.8.2 Convection In convection, the combined action of heat conduction, energy storage, and mixing motion serve to transport energy. Convection is most important as the mechanism of energy transfer between a solid surface and a liquid or a gas (Kreith, 1973). In forced-convection heat transfer, a pump, fan, or other mechanism forces a fluid to flow past a solid surface. In natural or free convection, warmer or cooler fluid next to the solid surface causes a circulation because of density differences resulting from the temperature differences in the fluid (Geankopolis, 1993). An example of free convection is the loss of heat into ambient air via the fins of a heat exchanger. If a fan is used to circulate the air over the heat exchanger fins, this becomes an example of forced convection. In the experiment carried out, circulation of water cooling system either in external or internal is also in category of forced convection system. 2.8.3 Radiation In radiation, heat flows from a higher temperature body to a lower temperature body when the bodies are separated in space, even across a vacuum (Kreith, 1973). The same laws that govern the transfer of light also govern the transfer of heat. Solids and liquids tend to absorb the radiation being transferred through it, hence radiation is important mainly in transfer through space or gases (Geankopolis, 1993). Examples of radiation include the transfer of heat from the sun to the earth, and from a quartz flashlamp to a cool object (laser rod) that requires warming. 2.9 Cooling Techniques in Solid State Lasers Cooling can be defined as a process of removing heat from an enclosed space or material and maintaining that space or material at a temperature lower than its surrounding. As heat is removed, a space or material becomes colder. The more heat is removed, the colder the object becomes (Air Conditioning and Refrigeration Inst, 1997). Most laboratory and industrial lamp pumped which require high power lasers, usually used liquid cooling to cool the laser head. Purely convective air cooling suffices for very low power lamp lasers, which are used where portability is a paramount concern. Some low power low-repetition rate lamp pumped lasers also use forced air cooling (Hecht, 1992). Cooling techniques that usually applied to solid state laser are liquid cooling, air or gas cooling and convective cooling (Koechner, 1976). 2.9.1 Liquid Cooling The primary purpose of the liquid used in the cooling system is to remove the heat generated in the laser rod, pump source and laser cavity. Sometimes the coolant serves additional functions, such as index matching between laser rod and coolant, thereby reducing internal reflections for depumping modes, or as a filter to remove undesirable pump radiation. The coolant is forced under pressure to flow over the rod and lamp surfaces. These elements are located either inside flow tube or in cooling chambers machined out of the main body of a laser head. The temperature difference between the part to be cooled and the liquid is a function of the velocity and the cooling properties of the flowing fluid. At low velocities, the flow is laminar and most of the temperature drop is due to pure conduction across a stationary boundary layer at the liquid interface. For higher velocities, the flow becomes turbulent, leading to a more efficient heat transfer process with a subsequent lower temperature drop. Turbulent flow requires a greater pressure differential for the same volume flow, but the necessary differential usually is still small compared to the total pressure difference associated with the complete cooling system (Koechner, 1976). Water is preferably used as a coolant for solid state lasers. From purely heat transfer considerations, water is by far the best fluid. As compared to the other coolants it has the highest specific heat and thermal conductivity and the lowest viscosity. Water has the additional advantage over all other coolants that it is chemically stable under intensive ultraviolet radiation (Teppo, 1975). With the exception of lasers cooled directly by tap water, a closed-loop cooling system is employed which consists in its most basic form of at least a liquid pump, a heat exchanger and a reservoir. Commercially available coolers contain, in addition to these components, a particle filter, a demineralizer, gauges and sensors for monitoring flow temperature and pressure. If common tap water is used, periodic cleaning is necessary to remove deposition of organic and mineral deposits. In closed-loop systems, if demineralization and filtering are employed, the need to clean surfaces exposed to the cooling fluid is essentially eliminated (Koechner, 1976). The heat exchanger removes heat from the closed-loop system by thermal coupling to an outside heat sink. This can be established in several ways: (1) Water cooler with a liquid to air heat exchanger (2) Water cooler with a liquid to liquid heat exchanger (3) Water cooler with a refrigeration unit 2.9.1.1 Water Cooler with a Liquid-to-Air Heat Exchanger Liquid-to-air heat exchangers transfer heat from hydraulic fluid to ambient air. Working much like an automobile radiator, they allow air to be passed over finned tubes containing the hot liquid. The finned tubes can be made of aluminum, copper, steel, or stainless steel, and are brazed or roller expanded to the header tank. Air is moved through the core by forced or induced-draft fans. Air-cooled exchangers are most commonly used where water is costly or unavailable in sufficient quantities to dissipate the required heat, or where a portable heat exchanger is required. In some instances, they have been used to help supply plant heating requirements during winter months. Typically, liquid-to-air exchangers are larger, heavier, and noisier than liquid-toliquid units. In return, they operate without necessity for water and they are portable. They require ambient air temperature at least 10 to 15 °C below the required oil output temperature for efficient operation. The only requirement for long life is that the fins must be protected from clogging and dirty environments; a single mesh (window screen) overlay avoids fin clogging and provides for easy cleaning (Kren et.al, 2000). 2.9.1.2 Water Cooler with a Liquid-to-Liquid Heat Exchanger In a liquid-to-liquid heat exchanger the heat generated within the closed loop is exhausted to external water. Figure 2.5 shows the plumbing diagram of a typical cooler with a liquid-to-liquid heat exchanger. The water flows from the reservoir to a centrifugal pump, through a heat exchanger into the laser head, and back again in the reservoir. This sequence of components minimizes the static pressure in the laser head. The temperature of the closed-loop water is regulated by a control valve in the external supply line. The valve probe is located in the reservoir. As the temperature at the reservoir increases, the valve is opened, thereby allowing more external cooling water flow through the heat exchanger. The system contains an in-line honeycomb filter to remove particulate matter and a bypass demineralizer which will maintain low electrical conductivity in the water and minimize corrosion. The return line is monitored by a low-flow interlock and an over-temperature switch. If flow falls below a preset value or the discharge temperature exceeds a certain limit, the interlock turns off the power supply. The system also contains gauges to display temperature in the return line and the discharge pressure (Koechner, 1976). Figure 2.5: Schematic of a water cooler containing a water to water heat exchanger [Koechner, 1976] 2.9.1.3 Water Cooler with a Refrigeration Unit In both types of cooler that mention earlier, the temperature of the closed loop can be regulated only over a relatively narrow temperature range. Furthermore, the temperature of the cooling loop is always above ambient air temperature or the temperature of the external cooling water. Figure 2.6 shows a diagram of a cooler which maintains the cooling water at a precise, reproducible temperature which is independent of the ambient air or water temperature. This cooler contains a thermostatically controlled refrigeration stage between the heat exchanger and a water cooled condenser by means of a compressor. Any changes in the heat dissipation of the load, or temperature variations in the external lines, are compensated by a hot gas bypass valves which regulates the amount of refrigeration. Smaller units contain air cooled condensers, thus eliminating the need for an external water source (Koechner, 1976). Figure 2.6: Schematic of a water cooler employing a refrigeration unit [Koechner, 1976] 2.9.2 Air or Gas Cooling In a low average power lasers, especially portable systems, forced air is sometimes used to cool the laser rod and flashlamp. Air flow is generated by employing miniature axial or centrifugal blowers or fans which have been designed for air cooling of electronic equipment. The air flow required for cooling the laser head is calculated from the dissipated heat and the maximum temperature difference along the air stream. Figure 2.7 shows an example of an air-cooled Nd:YAG laser. A vane axial fan located upstream generates an air flow which passes through the pump cavity and over the rod and flashlamp. Besides convection cooling, the laser rod is also cooled by conduction into a copper heat sink which it is mounted (Rundle, 1975). Figure 2.7: Laser head of a small air-cooled Nd:YAG laser [Korad KYM, 1975] A cooling system which has been employed very successfully in small military laser systems is based on the use of compressed dry nitrogen as the coolant medium to transfer the heat generated in the laser cavity to the ambient air. The compressed nitrogen is circulated through the laser pumping cavity by means of an axial flow blower. Nitrogen exhausted from the cavity is then ducted through fins of a heat exchanger, where it gives up the energy picked up in the laser cavity. The cooled nitrogen is then ducted back through the cavity again to complete the nitrogen cooling loop. A fan provides the required air flow through the heat exchanger (Teppo,1975). 2.9.3 Conductive Cooling In a variety of commercial and military systems the laser rod is mounted directly to a heat sink, as shown schematically in Figure 2.8. Good conduction cooling of the laser element requires intimate thermal conduct between the laser rod and the heat sink. The laser rod can be mechanically clamped, soldered or bonded to the heat sink. If the laser rod is mechanically clamped to a heat sink, a temperature gradient across the rodclamp interface will develop (Koechner, 1976). Pump reflector Flashlamp Ruby, radius r θ Gallium surface Pedestal Figure 2.8: Typical geometry of a conductively cooled laser rod [Koechner, 1976] In a space-borne Nd:YAG laser system the rod was soldered to a mounting structure of pure niobium, having a thermal coefficient of expansion which closely matches that of Nd:YAG. The mounting surface for the rod is a groove to provide intimate contact with the rod over 900 of its periphery. The rod was soldered to the heat sink with indium solder after the contact surfaces were gold-plated. The heat was removed from the rod mounting structure by a heat pipe. A fin-type radiator at the condensor end of the heat pipe radiated the heat into space (Foster and Kirk, 1971). In another technique, a small Nd:YAG is bonded to a copper heat sink by means of a silver-filled epoxy adhesive. In this case, ultraviolet-free flashlamps must be employed to avoid decomposition of the epoxy. The temperature distribution in a conductively cooled rod has been calculated with the assumption that is uniformly produced by absorption of radiation and no losses occur except by conduction through the contact surface of the heat sink (Kaplan, 1964). 2.10 Summary In this research, the technique used to cool the laser rod and flashlamp in laser chamber was liquid cooling. This is due to the high heat dissipation (the power input level of flashlamp used was 1.6 KW), which would be radiated into the laboratory or operating environment of the laser. Water is an effective and reliable means of cooling high power laser systems. The development of the water cooling system in this research will be describes more in the next chapter. CHAPTER 3 DEVELOPMENT OF A WATER COOLING SYSTEM 3.1 Introduction In this chapter, the development of water cooling system and laser chamber is described. In general, a water cooling system is used to circulate cooled distilled water through a flashlamp and laser rod contained in the laser chamber. Temperature of laser chamber then is monitored during laser pumping process. 3.2 Water Cooling System This section describes the development of cooling system in the project. The type of coolants chosen in the study is the liquid cooling. Liquid cooling offers several advantages as a removal mechanism. First, in applications where power densities exceed the limits of air-cooling, liquid cooling is the only practical heat removal mechanism. Second, liquid cooling offers a high-performance cooling solution and results in a compact design. Further, liquid cooling also offers better control over changes in the heat load and higher reliability (Kelkar, 2002). It also provides critical temperature monitoring of chamber components and is cleaner than air cooling (American Laser Technique, 2001). In the development, the water cooling system was divided into two parts that are external and internal cooler. The type of cooling cycle process involves is a closed loop system. This system used similar concept as applied in an ordinary refrigerator. The system provides a constant supply of chilled and pressurized water. The schematic diagram of whole cooling system including external system and internal system is shown in Figure 3.1. Laser chamber Internal Cooler External Cooler Figure 3.1: The schematic diagram of whole cooling system 3.2.1 External Cooler An external cooler is used to cool the distilled water in the internal cooler. It uses tap water which circulates through a pair of cooling coils mounted inside the tank. This particular cooler is located outside the lab to reduce vibration created by the compressor and other related components and also for easy maintenance. The process involved is a refrigeration cycle and it works continuously. This type of process can maintain the cooling water at a precise, reproducible temperature, which is independent of the ambient air, or water temperature (Koechner, 1976). Refrigerant moves from the compressor to the condenser, then through a metering device consisting of oil receiver tank, filter drier and expansion valve, eventually to an evaporator (cooling coil), and the cycle then repeats. The circulation cycle in external cooler is shown in Figure 3.2. Compressor Condenser Metering Device (oil receiver tank, filter drier and expansion valve) Cooling coil (Evaporator) Figure 3.2: The circulation in external cooler The refrigeration cycle process used to cool a tap water in external cooler begins with the compressor. The compressor compresses the refrigerant and receives low pressure gas from the evaporator and converts it to high pressure gas. As the gas is compressed, the temperature rises. The hot refrigerant gas then flows to the condenser. The condenser is a heat exchanger that uses a colder fluid, an ambient air, to cool the refrigerant. As refrigerant flows through this heat exchanger, it condenses to a hot liquid. Liquid refrigerant exits the condenser and flows to the system's expansion valve. The expansion valve is used to create a pressure drop. The temperature and boiling point of liquids decrease as the pressure decreases. Some refrigerant liquid vaporizes and the temperature of the liquid-gas mixture drops. The cool refrigerant then flows to the evaporator. The refrigerant enters the evaporator as a low temperature gasliquid mixture. By designing, the temperature of the heat source is always higher than the refrigerant's boiling point. In the evaporator, the refrigerant vaporizes as it absorbs heat from the heat source. The refrigerant's temperature remains constant as it vaporizes. The refrigerant then exits the evaporator as a gas, enters the compressor and the cycle starts again. The thermostat responds to the temperature of water. From this process, a tap water in external cooler is cooled continuously. A cooled tap water then was flow to internal cooler through a water pipe that connected between two systems. This cooled tap water is circulated through cooling coil that mounted in internal cooler reservoir to cool distilled water inside. The schematic diagram of whole external cooler is shown in Figure 3.3. Photograph of the components used to develop the external cooler is shown in Figure 3.4. The whole external cooler system is shown in Figure 3.5. Oil receiver tank Condenser Expansion valve Filter drier Water tank Compressor Cooling coil To Internal coolant controller box Thermostat Refrigerant lines Water lines Figure 3.3: The schematic diagram of external cooler Oil Receiver Tank Condenser (Fan Coil Unit) Controller Box Compressor (R-22) Filter drier Expansion Valve Figure 3.4: A photograph of compressor based refrigeration system components Water tank nlet utlet Outle Compressor based refrigeration Figure 3.5: A photograph of whole system of external cooler 3.2.2 Internal Cooler This internal cooler is used to circulate the distilled water into the laser chamber equipment. It is located inside the lab and at a lower position from the laser chamber equipment. The stainless steel reservoir is used to keep the distilled water that is pumped to laser chamber. It dimension is 42 x 6 x 8 cm. The cooling coil which is located inside the reservoir is used as a medium to flow a cooled tap water from an external cooler to cool the distilled water in the reservoir. The internal cooler uses distilled water to cool both the flashlamp and the laser rod in the chamber. Tap water meets the needs of most liquid-cooling applications. However, distilled water has chemical and electrical properties that make it the optimal choice for cooling when the liquid circuit contains micro-channels or when sensitive electronics are involved. As the name implies, distilled water has an extremely low concentration of ions, which imparts important performance attributes. Firstly it eliminates mineral deposits that block the coolant flow. This will degrade cooling efficiency and system operating performance. Secondly it eliminates the risk of electrical arcing due to static charge build up from the circulating coolant. The arc can damage sensitive control electronics in the equipment being cooled. The lack of ions in distilled water eliminates both of these problems (LYTRON Application Note, 2002). The temperature of distilled water in reservoir was monitored by a pocket digital thermometer, which was put inside it. The type of thermometer used was pocket digital thermometer 310 from TPI Inc. It can measure temperature either in Fahrenheit and Celsius. The range of temperature measurement is from –50 0C up to 150 0C. This is appropriate since the distilled water required to be cooled is in the range of 15-25 0C only. The coolant is pumped by a pump from the reservoir up to the laser head via plastic tubes. The length of the plastic tube is almost 3 m. An internal cooler normally is placed a distance away from the laser head, and must be in the lower position to prevent overflow when the laser head is not in operation. The coolant was circulated through laser rod and flashlamp located in laser chamber, then return to the reservoir. The schematic diagram of the whole internal cooler system is shown in Figure 3.6. Laser head Temperature sensor Cooling coil To external coolant Reservoir Water pump Water line Figure 3.6: The schematic diagram of internal cooler 3.3 Laser Chamber All solid state laser systems require a pump chamber. The laser pump chamber is the heart of the laser system. It is where electrical energy is converted to coherent light at the laser rod's specified wavelength. The laser chamber is designed to be assembled with water cooling compartment. Neodymium-doped, yttrium aluminium garnet (Nd:YAG) laser rod is used in an optical configuration to produce high power, low divergence beam. The optical head contains a 75 mm x 4 mm diameter oscillator rod with a single flashlamp enclosed within a heat sink reflector. This features a glazed ceramic reflector (chamber heat sink), to provide diffuse coupling of the pulsed pump light- and is flooded with circulating distilled water to cool the flashlamp and the laser rod. The detail of the development of laser chamber will be described in chapter five. 3.4 Lab Recorder (LR) In this project, a Lab recorder (LR) was used to monitor the temperature of the laser head during pumping process. The LR was interfaced to a Personal Computer (PC). The Lab Recorder model LR4200E from YOKOGAWA was used in this experiment. Any DC voltage, thermocouple or RTD input could be selected for each channel. RS-232C interfaces bi-directional communication was used in which it allowed data output and panel setting through computer. Communication input was analog-recorded, enabling raw measured data and communication input data to be recorded simultaneously. LR PC software was used to read measurement data directly from the Lab Recorder. The software sets and controls the LR recorder. It periodically acquires data measured by an LR recorder to a personal computer, and saves it to a hard disk. It is also capable of displaying waveforms and digital values in real time while data logging is taking place (LR PC Software Manual,1997). To calibrate the Lab Recorder, the thermometer and the twisted end of thermocouple (type T) when connected to Lab Recorder were immersed in the water as shown in Figure 3.7. The water was heated with Gallenkemp Regulator Hotplate. The data were taken from the thermometer with 5 0C increment starting from 0 0C to 95 0C. At the same time temperature reading from the thermocouple was taken. The result of the calibration is shown in Appendix A. Thermometer Thermocouple ‘T’ Retort stand Personal Computer (PC) Beaker LR Water Hot plate Figure 3.7: The schematic diagram for Lab Recorder calibration 3.5 Monitoring Laser Chamber The temperature measurement during the pumping process was measured using thermocouple type ‘T’ which was interfaced to a Personal Computer (PC) via a Lab Recorder (LR). The measurement was taken three times a day. The duration of the experiment was about one hour. An average was calculated by dividing the total by three. Two conditions were considered. First condition, the temperature was taken during pumping process with water coolant circulated. Second condition, is without circulating water coolant. The data were measured at three different parts of pumping chamber, which include a stainless steel block, a chamber heat sink and a flashlamp. During pumping process, laser chamber is the part of laser which received the most excess heat. Flashlamp is a source for optical pumping. The white light radiated from the flashlamp is used to excite a laser rod. However not all the energies are used. In fact only some small portion responsible to absorb and excited population on the laser rod. The rest of the heat, dissipated to various compartments in the laser chamber. This includes especially the laser rod and flashlamp holder, which made from metal (which easy to conduct heat), stainless steel. Beside the holder, the laser rod and the flashlamp are enclosed in a heat sink, which was made from ceramic (insulator). However, this heat sink also absorbs excess heat. Thus these two components, that are laser holder and the heat sink, are responsible for absorbing most of the excess heat. Consequently these two parts are monitored. The quantities of heat received by the laser chamber were determined by measuring the temperature at those particular points. The total heat given by the flashlamp was monitored by measuring the temperature at the cathode and anode. A thermocouple type T was employed as a temperature sensor. The sensor was interfaced to a personal computer via a Lab Recorder (LR). The thermocouple was connected to the specific point like, stainless steel block, heat sink and electrode, due to the reason mention previously. The pumping process was running for one hour. It start from room temperature up to the constant reading obtained from temperature measurements. The pumping process was operated at two conditions. The first condition involves with the laser chamber which was chilled. In the second condition, the water is still running but has not been cooled. The temperature was taken three times at each different location on the laser chamber as mentioned before, and the average was calculated. The schematic diagram of the experimental set-up for temperature measurement is shown in Figure 3.8. Personal Computer (PC) Thermocouple type ‘T’ Lab Recorder (LR) Pumping Chamber Power Supply Cooling System Figure 3.8: Experimental set-up for temperature measurement of pumping system CHAPTER 4 CHARACTERIZATION OF THE WATER COOLING SYSTEM 4.1 Introduction Conditions of cooling water can have significant effect on the operating performance of equipment. In lasers, water conditions can affect beam pointing, power stability, warm-up characteristics and plasma tube lifetime (Rabiah, 1998). Careful selection, design and monitoring of multiple cooling water systems will minimize any long-term problems that might other wise occur. It is unwise to assume that available water is adequate for equipment cooling needs without first understanding the critical variable involved. These variables include water temperature and water quality. In this chapter, the developed cooling system was characterized to ensure it can provide a good system to cool a Nd:YAG laser chamber. 4.2 Water Temperature Water temperature stability is important since temperature fluctuations may cause thermal stresses on the equipment which could cause shortage of life, poor beam pointing on lasers, poor power stability and equipment damage (Rabiah, 1998). In this study, temperatures of the water cooling system in the external and internal systems were measured. Initially the temperature measurement was taken at the time the system was switched on up to the point where the minimum of cooling temperature was achieved. The temperature of internal coolant was taken simultaneously with the data of temperature from external coolant. 4.2.1 Temperature of External Coolant The temperature of external coolant was tested by using thermometer based on mercury. The temperature was measured from the time the system was on, to a point when the minimum of cooling temperature that is 18.0 ± 0.5 0C, was achieved. The reading was taken for three sequential days. The obtained data are listed in Table 4.1. These data are used to plot graph of temperature against time such as shown in Figure 4.1. Table 4.1: Temperature variation of external coolant with time Temperature ( θ ± 0.5oC ) Time (min) (± 0.01s) Day 1 Day 2 Day 3 Average 15.0 25.0 24.0 26.0 25.0 30.0 24.0 24.0 24.0 24.0 45.0 26.0 23.0 23.0 24.0 60.0 24.0 23.0 25.0 23.0 75.0 23.0 22.0 24.0 23.0 90.0 22.0 21.0 23.0 22.0 105.0 22.0 21.0 23.0 22.0 120.0 21.0 21.0 22.0 21.3 135.0 21.0 20.0 21.0 21.0 150.0 21.0 20.0 21.0 20.6 165.0 21.0 20.0 20.0 20.3 180.0 20.0 19.0 20.0 19.7 195.0 20.0 18.0 19.0 19.0 210.0 20.0 18.0 19.0 19.0 225.0 19.0 19.0 19.0 18.0 240.0 19.0 17.0 18.0 18.0 255.0 19.0 17.0 18.0 18.0 270.0 18.0 18.0 18.0 18.0 285.0 18.0 18.0 18.0 18.0 300.0 18.0 18.0 18.0 18.0 27 Temperature(0C) 25 23 21 19 17 15 0 50 100 150 200 250 300 350 Time(min) Figure 4.1: Variation in the temperature of external coolant with respect to time The graph of Figure 4.1 shows that the temperature of the external coolant exponentially decreasing upon time. The minimum temperature was achieved after four hours operating. This means that, the cooling system must be operated four hour earlier before operating a laser system. This duration is considered to be quite a long period of waiting. This is possibly due to the utilization of a bigger size of the water tank or reservoir. The problem may be overcome by using a smaller tank. 4.2.2 Temperature of Internal Coolant The temperature of internal coolant was taken at the same time with the temperature from external coolant. The data were also taken for three days and the average value was calculated. The obtainable data from this experiment are listed in Table 4.2. The data are used to plot graph of temperature versus time such as shown in Figure 4.2:- Table 4.2: Temperature variation of internal coolant with time Temperature (θ ± 0.05oC) Time (min) (± 0.01s) Day 1 Day 2 Day 3 Average 15.0 25.30 25.20 25.10 25.20 30.0 25.00 24.50 24.90 24.80 45.0 24.50 22.20 23.50 23.40 60.0 24.00 22.20 23.40 23.20 75.0 23.20 22.00 23.20 22.80 90.0 23.00 21.80 22.40 22.40 105.0 22.80 21.40 21.80 22.00 120.0 22.40 21.20 21.80 21.80 135.0 22.20 21.00 21.00 21.40 150.0 22.00 20.80 20.20 21.00 165.0 21.80 20.40 20.20 20.80 180.0 21.40 20.20 19.60 20.40 195.0 20.40 20.00 20.20 20.00 210.0 20.00 19.80 19.60 19.80 225.0 19.80 19.40 19.00 19.40 240.0 19.40 19.20 19.00 19.20 255.0 19.00 19.00 19.00 19.00 270.0 18.80 18.60 18.70 18.70 285.0 18.60 18.40 18.50 18.50 300.0 18.20 18.00 17.80 18.00 27 Temperature(0C) 25 23 21 19 17 15 0 50 100 150 200 250 300 350 Time(min) Figure 4.2: Variation in the temperature of internal coolant with respect to time The curve obtained from the graph in Figure 4.2, shows that the temperature inversely proportional with respect to the time. The minimum temperature was achieved at the same value with external coolant that is 18.00 ± 0.05 oC. It shows that the configuration of the graph is almost similar between the two systems. Both water cooling systems are found to have an exponentially decrease cooling temperature profile. However the curvature of the graph is different between the two systems. The temperature for internal coolant is found to have a more drastic and smoother profile. The difference arises possibly due to the different type of water and size of tank used in both systems. The internal system used distilled water, which is much more clean compared to tap water used in external system which is known to contain more impurities and other chemical agents like chlorine. In addition the temperature reading of internal cooling system is taken using a digital thermometer. So that, the measurement is considered more accurate. In term of tank sizes, the internal one has a smaller size and made from metal whereas the external tank has bigger size and made from fibre glass. Furthermore, the external coolant is exposed with different kind of atmosphere environment. The daily temperature outside the lab is not consistent. Weather changes, for example rainy or hot summer days, can contribute to temperature changes for external system. These conditions are in marked contrast to the internal coolant system which has more stable temperatures. 4.3 Water Quality Poor water quality can cause a wide variety of equipment failures, mineral build-up or corrosion of the inner tubes. The constituents of the processed cooling water that are of most concern are pH levels and resistivity. The pH of distilled water for the water cooling system was measured using pH meter CyberScan pH500 from EUTOCH Instruments made in Singapore, and water conductivity was measured using a conductivity meter YSI 30 from YSI Incorporated USA. These two variables were used to determine the water quality. Both parameters were taken with respect to temperatures in the range of 10-60 0C which are considered as an appropriate temperature range during laser pumping process. The measurement for water quality is only considered for the distilled water used in internal coolant because this is the water that will circulate through the laser chamber which contains a laser rod and a flashlamp. 4.3.1 The pH Level In this experiment, the pH of the distilled water used in internal coolant was measured as the water temperature changes. The data collected are listed in Table 4.3. The data are used to plot a graph pH level versus water temperature. The graph is shown in Figure 4.3. Table 4.3: pH of distilled water at various temperatures Water pH Level (± 0.005) Temperature (θ ± 0.5 oC) Experiment 1 Experiment 2 Experiment 3 Average 10.0 6.540 6.560 6.5500 6.550 15.0 6.650 6.680 6.690 6.673 20.0 6.780 6.800 6.740 6.773 25.0 6.780 6.800 6.760 6.780 30.0 6.840 6.860 6.780 6.827 35.0 6.880 6.880 6.840 6.867 40.0 6.880 6.890 6.860 6.877 45.0 6.890 6.890 6.880 6.887 50.0 6.880 7.000 6.890 6.923 55.0 6.890 7.000 6.940 6.943 60.0 6.880 6.870 6.890 6.880 8 7.5 pH 7 6.5 6 5.5 5 0 10 20 30 40 50 60 0 Water Temperature ( C) Figure 4.3: Graph pH versus temperature for distilled water Figure 4.3 shows that the pH level for the distilled water stays almost constant with change in temperature. It is worth noting that, a pH level between 6.0 to 8.0 is considered as a stable pH value for cooling process (Coherent, 2003). Water systems that are either acidic (pH values of less than 7.0), or basic (pH values of greater than 7.0), can lead to electrochemical corrosion depending upon the metals that are present in the cooling system (Rabiah, 1998). In this case, the pH level for distilled water was found within 6.550 ± 0.005 to 6.943 ± 0.005 corresponding to the temperatures in the range of 10 oC to 60 oC. The pH level obtained from the internal system is almost near 7, means that, the water is quite clean and safe to circulate through laser rod and flashlamp in laser chamber. Meanwhile to avoid the failures of component inside laser chamber, frequent checks of the water coolant are necessary to ensure the pH level of the distilled water used. 4.3.2 Conductivity and Resistivity of Water Conductivity and resistivity are parameters to measure the ability of a fluid to conduct electrical current. Conductivity is simply the reciprocal of resistivity: conductivity microsiemen (µS) = 1/ resistivity, megaohm meter (MΩm). In practice, conductivity units are typically used when referring to water ranging from drinking water to sea water, while resistivity units are reserved for ultra pure water such as deionized or reverse-osmosis water (Paparone, 2004). Resistivity is a measure of the concentration of dissolved minerals and metals in solution. Using the equation conductivity (µS) = 1/ resistivity (MΩm), the resistivity of distilled water was determined. In this particular experiment, the conductivity of distilled water was measured at different water temperature. The collected data of the measurement are listed in Table 4.4. The data were used to calculate a resistivity of data for distilled water as listed in Table 4.5. This calculated resistivity is used to plot a graph as shown in Figure 4.4. Table 4.4: Conductivity of distilled water at various temperatures Conductivity of distilled water ( ± 0.05 µS) Temperature (θ ± 0.5oC) Experiment 1 Experiment 2 Experiment 3 Average 10.0 8.30 9.00 8.80 8.70 15.0 8.10 8.80 8.60 8.50 20.0 7.80 8.60 8.40 8.27 25.0 7.80 8.20 8.00 8.00 30.0 7.60 8.50 7.60 7.90 35.0 7.40 8.40 7.40 7.73 40.0 7.40 8.20 7.40 7.73 45.0 7.50 8.20 7.40 7.70 50.0 7.40 8.20 7.40 7.67 55.0 7.40 8.00 7.40 7.60 60.0 7.40 8.00 7.40 7.60 Table 4.5: Resistivity of distilled water as the reciprocal of conductivity at various temperatures Resistivity Temperature Conductivity ( 1/ Conductivity) (θ ± 0.5oC) ( ± 0.05 µS) (± 0.01 MΩm) 10.0 8.70 0.11 15.0 8.50 0.12 20.0 8.27 0.12 25.0 8.00 0.13 30.0 7.90 0.13 35.0 7.73 0.13 40.0 7.73 0.13 45.0 7.70 0.13 50.0 7.67 0.13 55.0 7.60 0.13 60.0 7.60 0.13 0.15 0.145 Resistivity(M Ωm) 0.14 0.135 0.13 0.125 0.12 0.115 0.11 0.105 0.1 0 10 20 30 40 50 60 0 Temperature( C) Figure 4.4: Graph resistivity versus temperature of distilled water It is found from Figure 4.4 that, the resistivity of the distilled water increases drastically in the range of 10 to 20 0C. Thereafter, it remains constant even when the temperature is continuously increased to 60 0C. The resistivity for distilled water obtained is in the range of 0.11 ± 0.01 to 0.13 ± 0.01 MΩm. The suitable range of resistivity level for a process of cooling is in between 50 kΩm to 2 MΩm (Coherent, 2003). Water with very low resistivity corresponds to high concentration of dissolved salts. This condition can result in the formation of deposits on the envelope of the plasma tube, which gradually will result in the formation of an insulating layer of scale between the tube and cooling water. This can lead to poor cooling and possible tube failure due to cracking of the flow tube (Coherent Laser, 2003). However, the resistivity of the distilled water used in this cooling system is considered quite high ( 0.11 – 0.13 ) ± 0.01 MΩm. Hence the conditions of poor cooling system and the failure of flow tube are potentially low. 4.5 Summary A water cooling system for Nd:YAG was successfully developed. The characteristics of water cooling system are: first it has a minimum temperature of 18.00 ± 0.05 oC, second the pH level of distilled water is in the range of (6.550 – 6.943) ± 0.005 which is in the stable range and third it possesses distilled water with quite low resistivity in the range of (0.11-0.13 ) ± 0.01 MΩm. CHAPTER 5 DEVELOPMENT OF A LASER CHAMBER 5.1 Introduction All solid state laser systems require a pump chamber. The pump chamber is the heart of the laser system. It is where electrical energy is converted to coherent light at the specified wavelength of laser rod. In this research, the laser chamber is designed and installed with water cooling system. Basically a laser pump chamber is made up of: • An alumina diffuse reflector • A parallel cooling path • High UV absorbing flow tubes • O-rings • A Lamp • A Laser rod In a typical pulsed solid-state laser, pump energy is delivered to the solid state medium via a flashlamp, which is essentially a very bright strobe light. Usually, the flashlamp and the solid state medium are rod-shaped and of equal diameters, and are positioned at the two focus of a reflective elliptical cavity (called a resonator or pump chamber), thus ensuring that all photons emitted from the flashlamp will find their way to the rod for maximum efficiency. Photons created by stimulated emission "resonate" between the highly reflective (HR) mirror and the output coupler (OC), or partially reflective mirror, and on to the delivery device (Shore, 2000). 5.2 Laser Chamber Solid state laser is controlled by reflectivity of laser pump cavity. As far as laser is concerned, important role of cavity (usually called light-focusing cavity) must reflect irradiation of pump light source back towards laser-producing material source. In this research, it features a glazed ceramic reflector (chamber heat sink), to provide diffuse coupling of the pulsed pump light- and is flooded with circulating distilled water to cool the flashlamp and the laser rod. The design of pumping chamber consists of a Nd:YAG laser rod, flashlamp, flow tube, two stainless steel blocks, chamber heat sink, base plate and all stainless steel screws and clamps. All components in the laser chamber were designed according to the size of laser rod and flashlamp that had been manufactured by KENTEK Laser Corp. 5.2.1 Nd:YAG laser rod Neodymium-doped, yttrium aluminium garnet (Nd:YAG) laser rods are used in an optical configuration to produce high power, low divergence beam. Neodymium-doped yttrium aluminum garnet (Nd:YAG) possesses a combination of properties uniquely favorable for laser operation. The YAG host is hard, of good optical quality and has a high thermal conductivity. The dimension of laser rod used was 75 mm x 4 mm with 1% of impurities of Nd and 1064 nm anti-reflected (AR) coating on both ends. It is manufactured by KENTEK Laser Corp. The photograph of the Nd:YAG laser rod utilized in this particular equipment is shown in Figure 5.1. Figure 5.1: The photograph of Nd:YAG laser rod 5.2.2 Flashlamp Source of powerful light is in the form of a linear lamp and used to excite photon emission in a solid-state laser. It dimension was 66 mm arc, with 137.2 mm glass and 4 mm x 6 mm envelope. It has 4.7 mm x 9.9 mm connectors Xenon and manufactured by KENTEK Laser Corp. The photograph of flashlamp used to pump the laser rod is shown in Figure 5.2. Figure 5.2: The photograph of flashlamp 5.2.3 Flow tube Material used was samarium quartz and with process flame polished ends. The material was chosen because of its robustness with the temperature changes due to heating from flashlamp and cooling from chiller inside the pumping chamber during pumping process. The dimension of the flow tube is 70 mm x 10 mm. It functions is used to enclose a laser rod, enriched reflection, confine and smoothing the flow of coolant water, and the most important is to absorb ultraviolet (UV) light produced from the xenon flash lamp. The photograph of the flow tube utilized in this experiment is given in Figure 5.3. Figure 5.3: The photograph of flow tube 5.2.4 Stainless steel block Two blocks made from stainless steel were designed. The stainless steel was chosen as a material because it resistance to corrosion and staining, low maintenance, relative inexpense, and familiar luster make it an ideal material. They are used for holding chamber heat sink, laser rod and flash lamp. Block 1 was designed with two holes to hold laser rod and flash lamp. While block 2 was made with two holes at the side and another two holes at the bottom. Two holes at the bottom were specifically made for cooling purposes. The chilled water supplied from internal cooling system via L pipe was attached with the block. This is to ensure that the chilled water can circulate through laser rod and flashlamp. The dimension and drawing of these two blocks are shown in Figure 5.4 and Figure 5.5 respectively. Figure 5.4: Engineering drawing of block 1. (Dimensions are in millimeters (mm)) Figure 5.5: Engineering drawing of block 2. (Dimensions are in millimeters (mm)) The sizes of both blocks were quite large. The main objective was to ensure a laser rod and flash lamp remained in stable position. It is also to prevent from expansion of laser rod due to overheating during the pumping process. Both blocks 1 and 2 are shown in Figure 5.6. Figure 5.6: The photograph of stainless steel blocks 1 and 2 5.2.5 Chamber heat sink Chamber heat sink was needed to provide diffuse coupling of pulsed pump light. It was made from ceramic (alumina). The configuration of 45oside view of laser chamber was made for easy to clamp the chamber heat sink with the holder. The dimension and schematic drawing of this chamber are shown in Figure 5.7, 5.9 and 5.10 while the photograph is shown in Figure 5.8. Figure 5.7: Dimension of top view of the chamber heat sink. (Dimensions are in millimeters (mm)) Figure 5.8: The photograph of chamber heat sink Figure 5.9: Dimension of side view of the chamber heat sink. (Dimensions are in millimeters (mm)) Figure 5.10: Dimension of front view of the chamber heat sink. (Dimensions are in millimeters (mm)) 5.2.6 Base plate It was used to hold the clamped pumping chamber in steady place. It is consist of two holes which are needed to put ‘L’ shape pipe for a coolant to flow through the flashlamp and laser rod. The technical drawing of these base plates is shown in Figure 5.11 and 5.12 respectively and the photograph is shown in Figure 5.13. Figure 5.11: Dimension of top view of base plate. (Dimensions are in millimeters (mm)) Figure 5.12: Dimension of side view of base plate. (Dimensions are in millimeters (mm)) Figure 5.13: The photograph of base plate 5.2.7 Technical Accessories Other related components such as O ring, block clamp and related screws are used to assemble all components in the laser chamber. An O ring was utilized to seal laser rod, flowtube and flashlamp in order to prevent water leaking during circulation process of chilled water in the laser chamber. The photograph of assembling components is depicted in Figure 5.14. Figure 5.14: The photograph of O ring, block clamps and other screw used to assemble laser chamber 5.3 Assembly of the Laser Chamber The assembling of the pumping chamber began by attaching heat sink chamber into two stainless steel blocks. The blocks were then screwed on the base plate. The end of a flow tube inside the chamber heat sink was ensured tightened in between the two blocks. A flashlamp was then slid into the pumping chamber. The polarity (positive and negative side) of the lamp was identified by ensuring that it was placed correctly. A great care must be taken not to touch the quartz body of the lamp. It is easily contaminated and can cause early failure. Two screws and the flashlamp clamp plate were seal with the ‘O’ ring at each end of the lamp to prevent leakage of water coolant during circulation. The laser rod is fixed to the rod tube with a watertight silicone rubber seal. The rod was placed in the pumping chamber, by pushing an ‘O’ ring of the correct size over the plain cylindrical end tubes. The rod must be carefully inserted into the pumping chamber until the ‘O’ ring rests against the end block. The other ‘O’ ring, clamp plate and screws were fitted at the other end and alternately screwed with tighten a little by a little at a time. It was to avoid placing any bending forces on the rod, until all screws are completely tight. The chamber clamps were screwed between two blocks for completely attaching chamber heat sink with each block. The schematic diagrams of the whole pumping chamber are shown in Figure 5.15 and Figure 5.16. The photograph of the laser chamber is shown in Figure 5.17 and Figure 5.18. Flashlamp clamp Chamber Heat Sink Stainless steel block 2 Stainless steel block 1 Flash lamp Chamber clamp Base plate Figure 5.15: The schematic diagram of complete pumping chamber from side view Nd:YAG Laser rod Stainless steel block 2 Rod tube Flashlamp clamp Flow Tube Stainless steel block 1 Flash lamp Laser rod clamp Base plate Figure 5.16: The schematic diagram of pumping chamber without chamber heat sink from side view Flashlamp clamp Chamber Heat Sink Stainless steel block Base plate Figure 5.17: The photograph of pumping chamber (Side view) Stainless steel block Flashlamp clamp Flash lamp Nd:YAG rod Rod clamp Flow tube Base plate Figure 5.18: The photograph of pumping chamber without chamber heat sink (Top view) 5.4 The Laser House A house was designed in order to place a laser chamber in a stable condition and to provide other facilities such as pumping and electrical facilities. The material used for the house was stainless steel. The technical drawing of the house with its specific dimensions is shown in Figure 5.19 – 5.20. The photograph of the whole house including the sliding mounting and the laser chamber is depicted in Figure 5.21. 10 40 30 Ø 10 70 70 115 Ø 130 60 30 60 240 (a) (b) Figure 5.19: Technical drawing of front cover of laser house from (a) front view, (b) side view. (Dimensions are in millimeters (mm)) 50 110 20 20 10 10 25 35 10 70 10 240 (a) 600 110 160 130 700 (b) 45 35 70 10 700 (c) Figure 5.20: Technical drawing of housing from (a) front view (b) top view (c) side view. (Dimensions are in millimeters (mm)) (a) (b) (c) Figure 5.21: The photograph of laser house (a) from top view without laser trail, (b) from top view with laser trail and (c) from side view with the laser chamber 5.5 Piping The L pipe is used as a connector to provide cooled distilled water from internal cooling system circulated into the laser chamber. It was attached to base plate to one of stainless steel block. It is made from stainless steel. The technical drawing and photograph of this L pipe is shown in Figure 5.22. The photograph of the L shaped pipe is manifested in Figure 5.23. 200 55 19 75 19 16 Figure 5.22: Dimension of side view of L pipe. (Dimensions are in millimeters (mm)) Figure 5.23: The photograph of L pipe 5.6 Testing the Circulation System The cooling system was tested to ensure that the circulation of the distilled water through the flashlamp and the laser rod in the laser chamber was smooth and contained no leakage. A flow rate was measured in order to ensure a smooth circulation. Figure 5.24 shows a schematic diagram of all components involved in this circulation system. It begins with an external cooling system which supplies a chilled water. The coolant flows through a pair of cooling coil in an internal cooling system to cool the distilled water. The distilled water then flows through a rubber hose that connects the internal cooling system to the L pipe, which then goes into the laser house. The L pipe was attached under the base plate to enter into the stainless steel block 2. The cooled distilled water then circulates through the laser chamber, during pumping process. Laser chamber Laser house Internal cooling system External cooling system Water line Water flow in L pipe inside laser house Figure 5.24: Schematic diagram showing circulation of cooling system from coolant to the laser head A schematic diagram of the circulation of the distilled water in the laser chamber is shown in Figure 5.24 (top view) and Figure 5.25 (side view). A cooled distilled water flows through the laser rod and then through the flashlamp. This will remove the heat deposited in the rod that is not converted into light, so that it can prevent overheating in the laser chamber. Inlet hole Block 1 Block 2 Flow tube Outlet hole Laser rod Flashlamp Chamber heat sink Water flow Figure 5.25.: The flow path of distilled water in laser chamber during circulation (top view) Laser rod Chamber heat sink Flow tube Flashlamp Ellipsoid space in the heat sink. chamber Water flow Inlet Outlet L pipe Figure 5.26: The detail of the circulation system in laser chamber (concentrated in ellipsoid space) 5.7 The Water Flow The flow rate of the coolant to the laser head must be kept possibly constant. The rate at which heat is conducted from the laser depends on the flow rate. Changes in the flow rate cause temperature changes in the laser head, which may result in problems such as drift in the laser output power and output beam direction (beam pointing). Long term flow rate stability can be measured using a flow rate transducer or by manual recording of data over time the laser is used. This should be done in a critical situation when there is a suspected problem with the flow rate stability (Coherent Laser, 2003). The water flow rate was determined by measuring the volume of water collected in an interval of time, using beaker and stop watch. The water flow rate R, is determined by dividing volume by time taken (Lytron, 2002) R= v t (5.1) where v is volume (liter/l) and t is time (min). If a flow meter is not available, a graduated container and a timer can be used to determine the fluid flow rate by measuring the amount of fluid that has passed through the system and dividing by the amount of time that has elapsed (Lytron, 2002). A constant flow rate is essential when measuring the flow in this manner. The density of the fluid should be used to convert the volumetric flow rate to mass flow rate. In this experiment the volume of water taken is fixed to 2260.0 ± 0.5 ml, the data is taken for five times with an average time taken of 13.80 ± 0.01 s. Using equation (5.1), the flow rate of water entering the laser chamber is 9.83 ± 0.01 l/min. The distilled water was circulated by using MARCH pump. The detail specification of the pumped is listed in Table 5.1. The water coolant was circulated through the laser rod, flashlamp and return back to the reservoir. Table 5.1: Physical properties of pump used by internal cooling system Physical Properties Value Angular speed 3000 rpm Power 49.7 W Radius of the motor 42.6 mm Manufactured MARCH, MFG, Inc. 5.8 Summary A laser pumping chamber for Nd:YAG was successfully developed. The system includes a Nd:YAG laser rod, a linear flashlamp, a flow tube, a chamber heat sink, two stainless steel blocks and a base plate. The pumping chamber was provided with the water cooling system developed earlier. A circulation of distilled water through the laser chamber was tested to ensure no leakage occurred during circulation. A flow rate was calculated to be as 9.83 ± 0.01 liter / min during the pumping process. CHAPTER 6 TEMPERATURE MONITORING DURING PUMPING PROCESS 6.0 Introduction An appreciable amount of heat normally dissipates during a pumping process. This may cause degradation of the laser performance and could damage other components. Henceforth, it is desirable to cool the chamber during a pumping process. The aim is to estimate the percentage of heat dissipated in different part of the laser chamber during a pumping process, with and without cooling the distilled water. Since the heating of the laser media severely limits its performance, this measurement may have significant practical design consequences (Mangir and Rockwell, 1986). Therefore, it is essential to quantify the heat generated accompanying flashlamp pumping of Nd:YAG. In this chapter, the calculation of the heat loss during pumping process is presented. 6.1 Heat Loss The heats Q gained (or lost) at three different parts in laser chamber were obtained by using the relation (Nelkon and Parker, 1980): Q = mcp∆θ (6.1) where Q is the heat gained (J), m is the mass of object (g), cp is the specific heat (J/goC) and ∆θ is the temperature change (oC). The power absorbed was calculated by dividing heat with the exposure duration time, t Pabsorbed = Q t (6.2) While the percentage of the power absorbed in different part of the laser chamber was calculated using equation: % Pabsorbed = Pabsorbed × 100% Pi (6.3) where Pabsorbed is the power absorbed (W) and Pi is the power input (W). During pumping process the heat is produced by a flashlamp. The ends of flashlamp were connected to two electrodes made from cooper. The whole flashlamp tube was held by stainless steel block and enclosed by heat sink. The heat sink is made from ceramic and polished to shine to stand as a reflector. The physical properties of all components in the laser chamber are listed in Table 6.1. The flashlamp used in this experiment was supplied with 16kW input power (Lumonics, 1991). Table 6.1: Physical Properties of the Laser Chamber elements [Cengel and Boles, (1998), Applied Ceramics Inc, (2003)] and their respective temperature change with and without chilled water cooling. Physical properties Items Temperature Mass (± 0.005 g) Specific heat, cp o (± 0.001 J/g C) Temperature change, change, o θmax- θmin (± 0.05 C) θmax- θmin (± 0.05 oC) with chilled without chilled water water Flashlamp 6.440 0.386 59.80 66.10 Heat sink 683.380 0.879 2.40 24.00 Stainless 852.010 0.460 2.50 17.70 steel block 6.2 The Temperature Distribution of the Laser Chamber In this project, the temperature distribution during pumping process was carried out. Therefore the energy absorbed in the laser chamber could be estimated. The temperature data was measured using the thermocouple type ‘T’ which was interfaced to Personal Computer (PC) via a Lab Recorder (LR). The thermocouple was attached to three parts of the laser chamber that were stainless steel block, ceramic chamber heat sink and flashlamp. Two conditions were considered during the measurement, which were performed with and without a water cooling system. In the first case, the study was carried out by chilled distilled water which was circulated through the flashlamp and flow tube. In the second condition, the water is still circulated in the laser chamber, but not being chilled. The system was operated for an hour. 6.2.1 The Temperature Distribution of the Laser Chamber With Chilled Water Temperature at different parts of the laser chamber while being cooled by chilled distilled water is listed in Table 6.3. Table 6.3: Temperature at different parts of laser chamber with chilled water operation Time (± 0.01 s) 0.0 60.0 120.0 180.0 240.0 300.0 360.0 420.0 480.0 540.0 600.0 660.0 720.0 780.0 840.0 900.0 960.0 1020.0 1080.0 1140.0 1200.0 1260.0 1320.0 1380.0 1440.0 1500.0 1560.0 1620.0 1680.0 1740.0 1800.0 1860.0 1920.0 1980.0 2040.0 2100.0 2160.0 Temperature, θ (± 0.05 oC) Stainless steel Flashlamp Chamber heat block sink 27.10 27.90 28.80 29.30 29.70 30.10 30.20 30.40 30.40 30.40 30.40 30.40 30.40 30.30 30.30 30.20 30.20 30.20 30.10 30.10 30.10 30.10 30.00 30.00 30.00 30.00 29.90 29.90 29.90 29.90 29.90 29.90 29.90 29.80 29.90 29.80 29.80 33.80 56.50 68.40 74.50 79.40 82.90 84.90 87.60 88.90 89.80 90.50 91.10 91.50 92.00 92.30 92.50 92.70 92.80 93.00 93.00 93.20 93.20 93.20 93.20 93.20 93.10 93.30 93.30 93.30 93.30 93.40 93.00 93.50 93.40 93.50 93.50 93.50 25.70 26.10 26.60 27.00 27.50 27.90 28.20 28.40 28.50 28.60 28.70 28.70 28.70 28.80 28.90 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.80 28.70 28.70 28.70 28.70 28.60 28.60 28.60 28.60 Time (± 0.01 s) 2220.0 2280.0 2340.0 2400.0 2460.0 2520.0 2580.0 2640.0 2700.0 2760.0 2820.0 2880.0 2940.0 3000.0 3060.0 3120.0 3180.0 3240.0 3300.0 3360.0 34200. 3480.0 3540.0 3600.0 Temperature, θ 0(± 0.05 oC)0 Stainless steel Flashlamp Chamber heat block sink 29.80 29.80 29.80 29.80 29.70 29.70 29.70 29.70 29.70 29.70 29.70 29.60 29.70 29.70 29.60 29.60 29.60 29.60 29.50 29.50 29.50 29.50 29.50 29.50 93.50 93.50 93.50 93.50 93.30 94.50 93.50 93.80 93.90 93.50 93.50 93.70 93.80 93.50 93.90 93.80 93.80 93.50 93.90 93.50 93.40 93.60 93.70 93.60 28.60 28.60 28.60 28.60 28.50 28.50 28.50 28.50 28.50 28.40 28.40 28.40 28.40 28.40 28.30 28.30 28.30 28.30 28.30 28.30 28.20 28.20 28.20 28.20 The result of temperature monitoring of the laser chamber by chilling the water coolant is shown in Figure 6.1. The graph illustrates the temperature profile of the flash lamp, chamber heat sink and stainless steel block. It is obvious that, the temperature of the flashlamp increases drastically within the first 14 minutes; and remains constant as the time proceeds. The maximum temperature obtained from the flashlamp is 93.6 ± 0.05 oC. The temperature profile for the flashlamp is much higher compared to the other two tested components. This is due to the measurement of temperature was taken directly onto the electrode, outside the laser chamber. Hence the heat does not dissipated in the chilled water. However, the other two tested parts received the heat transfer indirectly where some of the heat was dissipated through the circulated chilled water. 100 90 O Temperature( C) 80 70 60 50 40 30 20 10 0 0 1000 2000 3000 4000 Time(s) Chamber heat sink flashlamp stainless steel block Figure 6.1: Temperature profile at laser chamber when operated with chilled water. The stainless steel block for example is uninsulated. The block is a metal; it can easily conduct the heat away. On the other hand chamber heat sink is made from ceramic; and thus an insulator. Less heat transfers during the circulation of chilled water because most of the heat has been carried away by the chilled and running water. Thus, only the left over heat was transferred to the heat sink and the stainless steel block. As a result, the temperature profiles for both components almost similar and relatively much lower as compared to the flashlamp temperature. The temperature profiles for both cases slightly increase in the initial stage, but subsequently remain constant throughout the one hour operation. 6.2.2 The Temperature Distribution of the Laser Chamber Without Water Cooling The result obtained from the second experiment without chilled the water is shown in Figure 6.4. Such studied was carried in an attempt to predict what would happen to the laser chamber, in case the cooling system is not operational. It is to ensure whether it is safe to run the laser system, if the coolant is not functional. In this investigation, the water was let to run, but the chilled water was switched off. The temperatures are still detected at the same points on laser chamber which include the flashlamp, stainless steel block and chamber heat sink. Table 6.4: Temperature of laser chamber at different part without chilled water Time (± 0.01 s) 0.0 60. 120.0 180.0 240.0 300.0 360.0 420.0 480. 540.0 600.0 660.0 720.0 780.0 840.0 900.0 960.0 1020.0 1080.0 1140.0 1200.0 1260.0 1320.0 1380.0 1440.0 1500.0 1560.0 1620.0 1680.0 1740.0 1800.0 1860.0 1920.0 1980.0 2040.0 2100.0 2160.0 2280.0 Temperature, θ (± 0.05 oC) Stainless steel Flashlamp Chamber heat block sink 26.90 28.20 29.20 29.90 30.40 31.00 31.70 32.30 32.70 33.40 33.90 34.30 34.70 35.40 35.70 36.30 36.80 37.20 37.80 38.10 38.60 39.10 39.40 39.90 40.20 40.60 41.20 41.50 41.90 42.20 42.60 43.00 43.40 43.60 44.00 44.50 44.70 44.90 36.10 58.50 68.50 77.00 78.70 79.60 82.30 83.90 85.80 87.10 87.80 89.20 89.70 90.00 90.30 90.40 90.30 90.70 90.90 91.30 91.90 92.30 92.60 92.90 93.50 93.90 94.20 93.50 94.90 95.20 95.80 95.90 96.00 96.20 96.50 96.80 96.90 97.50 24.50 24.90 25.80 26.40 27.20 27.60 28.30 28.70 29.30 29.70 30.10 30.80 31.10 31.60 32.10 32.50 32.90 33.40 33.80 34.10 34.60 34.90 35.40 35.80 36.20 36.50 36.90 37.40 37.70 38.10 38.40 38.70 39.10 39.50 39.80 40.30 40.60 40.80 Time (± 0.01 s) 2340.0 2400.0 2460.0 2520.0 2580.0 2640.0 2700.0 2760.0 2820.0 2880.0 2940.0 3000.0 3060.0 3120.0 3180.0 3240.0 3300.0 3360.0 3420.0 3480.0 35400. 3600.0 Temperature, θ (± 0.05 oC) Chamber heat Flashlamp Stainless steel sink block 45.20 45.50 45.90 46.30 46.60 46.90 47.30 47.60 47.90 48.20 48.50 48.80 49.40 49.40 49.60 50.10 50.40 50.70 50.90 50.90 50.90 50.90 97.70 97.90 97.90 98.10 98.40 98.60 99.00 99.60 99.60 99.70 100.10 100.20 100.90 100.70 101.20 101.20 101.40 101.40 101.60 101.70 102.10 102.20 41.20 41.60 41.90 42.10 42.30 42.60 43.10 43.30 43.70 43.90 44.30 44.40 44.70 44.20 43.70 43.40 43.20 42.90 42.70 42.50 42.50 42.20 120 O Temperature( C) 100 80 60 40 20 0 0 1000 2000 3000 4000 Time(s) Chamber heat sink flashlamp stainless steel block Figure 6.2: Temperature Profile Without Chilled Water. The features of the results are still similar with the first experiment. The heat from the flashlamp of course becomes much higher. In fact the highest temperature obtained was 102.2 ± 0.05 oC. Different results were obtained for both the block and the heat sink. The temperature profiles are found to have almost linear relationship. This is reasonable because more heat is transferred to both components, since the water is not chilled. 6.3 Heat at different Part of the Laser Chamber The temperature data obtained can be used to calculate the heat loss from the flashlamp, and the heat absorbed by the stainless steel block and the heat sink. Using Equation (6.2), the power loss by the flashlamp was calculated to be 0.04 ± 1.75 x 10-4 W in the case where the laser chamber was circulated by chilled water. While 0.02 % power have been absorbed by the stainless steel block which is used to stabilize the laser head. 0.03 % power has been absorbed by the heat sink. The power loss by the flashlamp from the second experiment without the chilled water was 0.05 ± 0.19 x 10-3 W . 0.25 % energy has been absorbed by heat sink and 0.12 % by stainless steel block. The detailed of calculated results of heat and power absorbed by the flashlamp, heat sink and stainless steel block are shown in Table 6.5. Calculation of percentage improvement between two experiments was made in order to shown the efficiency of water cooling system applied. The calculation was made using equation; % Im provement = Pabsorbed ( withoutchilledwater ) − Pabsorbed ( withchilledwater ) × 100 Pabsorbed ( withoutchilledwater ) The result shows that the flashlamp had 20% improvement during pumping process with circulation of chilled water rather than without using chilled water. While the stainless steel and chamber heat sink had showed higher percentage of improvement which was 90% and 86% respectively. This indicates that the water cooling system that provided in the system was effectively dissipating all the excess heat from the pumping process. However, when the results obtained with and without the chilled water were compared, the excess heat was found to be ten times higher in the heat sink and almost seven times in the stainless steel block, but relatively very small change occurred in the flashlamp. Nevertheless, it was advisable to cool the water coolant for the sake of safety and long life expectancy of the laser crystal and the flashlamp tube. Table 6.5: The Result of Energy Absorbed by Different Part in the Laser Chamber during the Pumping Process. Component Flashlamp Heat sink With chilled water Heat , Q (J) Power absorbed, Pabsorbed(W) Percentage Power Absorbed (%) Without chilled water Heat , Q (J) 148.65 ± 0.63 0.04 ± 1.75 x 10-4 2.50 x 10-3 164.31 ± 0.68 1441.66 ± 31.65 0.40 ± 0.88 x 10-3 0.03 14416.58 ± 46.13 Power absorbed, Pabsorbed(W) Percentage Power Absorbed (%) Percentage of improvement (%) 0.05 ± 0.19 x 10-3 4.00 ± 1.28 x 10-2 3.13 x 10-3 20 0.25 90 Stainless steel block 979.81± 21.73 0.27 ± 6.05 x 103 0.02 6937.07± 34.68 1.93 ± 9.65 x 10-3 0.12 86 6.4 Summary The high percentage of improvement liberated from flashlamp, chamber heat sink and stainless steel blocks indicated that the cooling system provided in the laser chamber was very effective in carrying out the excess heat from pumping process. Without chilled water, the absorption in the heat sink was found to be ten times higher and seven times higher in the stainless steel block, in comparison to the situation with chilled water coolant. CHAPTER 7 CONCLUSION AND SUGGESTIONS 7.1 Conclusion The objectives of this research have been successfully achieved. The temperature distribution of the laser chamber during the pumping process has been studied. The water cooling system and laser chamber for a solid state laser have been successfully developed. A water cooling system is used to circulate cooled distilled water through a flashlamp and laser rod contained in the laser chamber. This water cooling system was divided into two parts; external and internal cooler. An external cooler is used to cool the distilled water in the internal cooler. Tap water was used in the external cooler to circulate through a pair of cooling coils mounted inside the tank. This external cooler was put outside the lab to reduce vibration created by the compressor and other related components and also enhance maintenance purposes. While an internal cooler was used to circulate the distilled water into the laser chamber equipment. It is located inside the lab. Several critical parameters which include water temperature, water quality and resistivity were measured. These measurements were made to ensure the water cooling system was appropriate for cooling a Nd:YAG laser system. The minimum temperature that could be achieved for this water cooling system is 18.00 ± 0.05 0C. The pH level of distilled water used was measured in the range of (6.550-6.943) ± 0.005 which was considered as the stable level. The distilled water also posses quite high resistivity in the range of (0.11-0.13) ± 0.01 MΩm. A laser pumping chamber for Nd:YAG was successfully developed. It is here where electrical energy is converted to coherent light at the laser rod's specified wavelength. The system include Nd:YAG laser rod, a linear flashlamp, a flow tube, a chamber heat sink, two stainless steel blocks and a base plate. All components are properly assembled to form a laser chamber. Piping and electrical power lines are also included in this design. Piping provides path for the distilled water to flow. Circulation of distilled water throughout the laser chamber was tested to ensure no leaking occurred during the pumping process. The flow rate of the distilled water in this circulation was found to be 9.83 ± 0.01 liter/ min. The laser rod in the laser chamber was pumped using a flashlamp. The measurement of temperature distribution during a pumping process was carried out. The thermocouple was attached to three parts of the laser chamber consisting of stainless steel block, ceramic chamber heat sink and flashlamp. The measurements were done under two conditions. In the first condition, the distilled water was cooled by the external cooler while in the second condition, the distilled water was not cooled. The heat liberated in the laser chamber was calculated. The result obtained shows that the flashlamp had 20% improvement during pumping process with circulation of chilled water rather than without using chilled water. On the other hand the stainless steel and chamber heat sink had shown higher percentage of improvement which was 90% and 86%, respectively. Without chilling distilled water, the absorption in the heat sink was found to be ten times higher and seven times higher in stainless steel block, in comparison the situation with chilled water. This indicates that the cooling process with chilled water successfully prevents the excess heat generated during the pumping process from heating the rest of the components. This also means that the cooling system is very efficient and effective in transferring the excess heat away from the laser chamber during the pumping process. 7.2 Problem and Suggestions In this study, the measurement of critical variables for water cooling system only includes water temperature, water flow and water quality. For future works it would be advantageous that the laser system is incorporated with an interlocking system that would shut the laser off when the water temperature gets too high thus preventing the laser from operating when the water temperature is too high. The rate of water coolant that flows from the cooling system to the laser head should be kept as constant as possible. Therefore, a digital flow rate transducer is required to monitor the flow rate continuously. Typically, a temperature control system is necessary in solid state laser to enhance laser stability. As mentioned earlier, this research only covers the initial stage of preparing the water cooling system and development of a laser chamber. In additional, we have also developed a preliminary works on temperature control system such as shown in Figure 7.1. However because of the time constraint and involvement of extensive electronic circuits design, the work could not be carried out. This could be performed in the future. Basically the idea of our recent works is to ensure that the temperature remain in the specific window, by controlling the speed of the water pump which used to circulate distilled water through the laser head. A microcontroller based control circuit using PIC16F870 is desired to be developed in order to control the laser chamber and water temperature, water flow rate and speed of water pump. An assembly language program needs to be written and programmed into the microcontroller. This system is constructed by interfacing with Personal Computer running Linux via RS-232 serial communication. The digital flow transducer will be used to detect the water flow rate continuously and display data measurement in Personal Computer (PC). The temperature is detected by the thermocouple and displayed on the PC. By using this system, a totally smart laser can be designed. Flow Transducer Solid state Laser Head Water cooling system Switch Mode Power Supply (SMPS) PIC Microcontroller Thermocouple Water pump Switch Water lines Circuit lines PC Figure 7.1: The schematic diagram of the suggested design programmable temperature controller in solid state laser head using microcontroller PIC16F870 The development of laser chamber and the measurement of variables for the water cooling system had been done in this study which will be beneficial for future researchers. The suggested idea and the information provided will lead to better understanding. 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Lab Recorder Personal Computer APPENDIX A Data observed from calibration of Lab Recorder is listed in Table 1. The graph is shown in Figure 1. Table 1: Calibration data for Lab Recorder Thermometer measurement ± 0.5 (oC ) 0.0 5.0 10.0 15.0 20.0 25.0 30.0 35.0 40.0 45.0 50.0 55.0 60.0 65.0 70.0 75.0 80.0 85.0 90.0 95.0 Lab Recorder measurement, θ (0C) ± 0.05 Average θ1 θ2 θ3 0.20 5.20 10.50 16.00 20.80 25.80 31.00 35.90 41.00 45.60 50.90 56.10 60.80 65.80 70.20 75.50 81.00 85.80 90.80 95.80 0.30 5.40 10.50 15.60 20.60 25.40 30.80 35.80 40.80 45.70 50.90 55.90 60.40 65.40 70.20 75.90 81.00 85.90 90.90 95.60 0.10 5.20 10.80 15.30 20.80 25.40 30.40 36.40 40.80 45.30 50.40 55.60 61.20 65.20 70.10 75.80 80.90 86.00 90.60 95.60 0.20 5.30 10.60 15.60 20.70 25.50 30.70 36.00 40.90 45.50 50.70 55.90 60.80 65.50 70.20 75.70 81.00 85.90 90.80 95.70 Lab Recorder measurement vs thermometer measurement Lab Recorder measurement (0C) 120 100 y = 1.0034x + 0.4971 80 60 40 20 0 0 20 40 60 80 0 Thermometer measurement ( C) Figure 1: Calibration curve for Lab Recorder 100 PUBLICATIONS 1. Nor Aziawati Azahari, Noriah Bidin, Calibration of A Water Cooling System for Nd:YAG Laser, Proceeding of Annual Fundamental Science Seminar (AFSS 2004), 14-15 June 2004, Skudai, Johor. 2. Nor Aziawati Azahari, Noriah Bidin, Estimation of A Wasted Heat During Nd:YAG Laser Pumping Process, Proceeding of Persidangan Fizik Kebangsaan (PERFIK 2004), 5-7 October 2004, Seri Kembangan, Selangor. 3. Nor Aziawati Azahari, Johari Adnan, Ahmad Hadi Ali, Mohd Fairuz Jani, Noriah Bidin, Development of A Programmable Switch Mode Power Supply (SMPS) for Controlling Water Pump in Solid State Laser Pumping System Using PIC16f870 Microcontroller, Proceeding of The XXI Regional Conference and Workshop on Solid State Science and Technology (RCWSST 2004), 10-13 October 2004, Kota Kinabalu, Sabah.