EVALUATION OF MARSHALL PROPERTIES OF ASPHALT MIXTURES WITH AGGREGATE GRADATIONS DESIGNED USING THE BAILEY METHOD ROSMAWATI BINTI MAMAT A project report submitted in partial fulfillment of the requirements for the award of the degree of Master of Engineering (Civil - Transportation and Highway) Faculty of Civil Engineering Universiti Teknologi Malaysia NOVEMBER 2008 iii Special dedication to my parents Mamat Bin Embok and Minah Binti Mohamad My brothers, Mohd Nizam, Mohd Nazri and Mohd Nazaruddin My sisters, Zanariah, Roslina, Nor Zuliana and Nur Hasimah Mohd Zahiruddin,Hammizi,Siti Hawa and Puziah Puteri Najwa Adlina and Putera Abdul Azim Faris Adli, Fitri Azri and Farhan Adha Mohamad Fahmi Bin Pathil that always inspire, love and stand besides me. My supervisor, my beloved friends, and all faculty members For all your love, care, support, and believe in me. Thank you so much. iii iv ACKNOWLEDGEMENT Praise and thanks to Allah for his blessings which has enabled to me to complete my master project. Firstly, I would like to express my sincere appreciation to my supervisor, Assoc. Prof. Dr. Mohd Rosli Hainin and my co-supervisor, Tuan Haji Che Ros Bin Ismail, who generously shared their insights and suggestions, guidance, for their critics, trust, encouragement, and attention. My special thanks go to Prof. Ir. Dr. Hasanan Bin Mohd Noor, Dr. Haryati Binti Yaacob and miss Nor Hidayah Binti Hassan for their critical judgments, advice and comments during the master project presentation. Special thanks are also extended to all technicians of Highway and Transportation Laboratory UTM, Mr. Suhaimi, Mr. Ahmad Adin, Mr. Abdul Rahman, Mr. Azman and Mr. Sahak for their time, help during the laboratory experimental work and valuable advice given in the whole duration of this project. Last but not least, I am grateful my fellow course mates, Nhat, Azreena, Samikhah, Fid, Azah, Tiong, Esarwi who given their utmost help, co-operation and encouragement in completing this project successfully. iv v ABSTRACT This study investigates the properties of asphalt concrete mixtures with aggregate gradations designed using Bailey method and compared with the JKR specification. Bailey method is a systematic approach in blending aggregates with difference gradation (fine aggregate and coarse aggregate) that provides aggregate interlocking as the backbone of the structure and a balanced continuous gradation to complete the mixtures. The Bailey gradation parameter separates the aggregate structure into three gradation namely coarse, medium and fine. This separation were quantified by the decrease in the volume of coarse aggregate in the structure when changing from coarse to fine gradation. The aggregates structures designed using Bailey method were applied in Marshall mix design method to obtain the Marshall properties based on Malaysian Standard and the gradation parameters were compared with the requirement from JKR specification. Two hot mix mixtures considered in this study were Asphalt Concrete Wearing (ACW 14) and Asphalt Concrete Wearing (ACW 10). The mixtures have nominal maximum aggregate sizes (NMAS) of 12.5 mm and 9.5 mm respectively and each sample was compacted using 75 blows per face. The compaction characteristics of the mixtures were analyzed using data from the Marshall Compactor. The value for both VTM and VMA from graph shows when the size of aggregate is smaller (fine aggregate), the percentage of voids in mineral aggregate is low, on the other hand the percentages of VMA and VTM is higher for coarse aggregate. v vi ABSTRAK Kajian ini dijalankan untuk mengkaji campuran konkrit berbitumen dengan pengadunan batu baur menggunakan kaedah Bailey dan membandingkan dengan spesifikasi JKR. Kaedah Bailey adalah secara sistematik campuran batu baur yang gradasi (batu baur halus dan batu baur kasar) yang menyediakan saling kunci batu baur sebagai tulang belakang kepada struktur dan gradasi berterusan yang seimbang bagi melengkapkan campuran. Parameter gradasi bagi kaedah Bailey mengasingkan struktur batu baur kepada tiga iaitu kasar, sederhana, dan halus. Pengasingan ini dibezakan melalui penurunan isipadu bagi batu baur kasar di dalam struktur apabila ia bergerak dari gradasi kasar kepada gradasi halus. Rekabentuk struktur batu baur menggunakan kaedah Bailey di gunakan dalam kaedah Marshall untuk mendapatkan ciri-ciri Marshall berdasarkan piawaian Malaysia dan parameter gradasi di bandingkan dengan spesifikasi JKR. Dua campuran panas telah digunakan dalam kajian ini iaitu konkrit berbitumen (ACW 14) dan konkrit berbitumen (ACW 10). Campuran ini mempunyai saiz nominal maksimum batu baur 12.5 mm dan 9.5 mm dan setiap sampel dipadatkan dengan 75 hentaman. Ciri-ciri pemadatan bagi campuran dianalisa menggunakan data dari pemadat Marshall. Nilai bagi kedua-dua VTM dan VMA daripada graf menunjukkan apabila saiz batu baur kecil (batu baur halus), peratus udara dalam mineral batu baur tersebut adalah rendah, manakala peratus bagi VMA dan VTM adalah tinggi untuk batu baur kasar. vi vii TABLE OF CONTENTS CHAPTER 1 2 TITLE PAGE DECLARATION ii DEDICATION iii ACKNOWLEDGEMENT iv ABSTRACT v ABSTRAK vi TABLE OF CONTENTS vii LIST OF TABLES xi LIST OF FIGURES xii LIST OF ABBREVIATIONS/SYMBOLS xiv LIST OF APPENDICES xvi INTRODUCTION 1 1.1 Background 1 1.2 Problem Statement 2 1.3 Objective of the Study 4 1.4 Scope of the Study 4 1.5 Significance of the Study 4 LITERATURE REVIEW 6 2.1 Introduction 6 2.2 Asphalt Cement Binder Role 7 2.2.1 Aggregate Roles 8 2.2.2 Aggregate Gradation 9 2.3 History of Bailey Method 11 vii viii 2.4 Mixture Design 12 2.4.1 Marshall Mix Design 2.5 Aggregate Packing 3 13 15 2.5.1 Coarse and Fine Aggregate 17 2.5.2 Bailey Method of Aggregate Blending and Evaluation 19 2.5.3 Combining Aggregate by Weight 20 2.5.4 Chosen Unit Weight of Coarse Aggregate 20 2.5.5 Analysis of the Design Blend 21 2.5.5.1 CA Ratio 21 2.5.5.2 Coarse Portion of Fine Aggregate 23 2.5.5.3 Fine Portion of Fine Aggregate 24 2.5.5.4 Summary of Ratios 24 METHODOLOGY 25 3.1 Introduction 25 3.2 Operational Framework 25 3.3 Materials 29 3.3.1 Aggregates 29 3.3.2 Bituminous Binder 30 3.4 Sieve Analysis 30 3.4.1 Dry Sieve Analysis 3.4.2 31 3.4.1.1 Apparatus 31 3.4.1.2 Procedures 31 Wash Sieve Analysis 32 3.4.2.1 Apparatus 33 3.4.2.2 Procedures 33 3.5 Aggregate Gradation 34 3.6 Determination of Specific Gravity for Aggregate 35 3.6.1 Specific Gravity for Coarse Aggregate 36 3.6.1.1 Apparatus 36 3.6.1.2 Procedures 36 3.6.2 Specific Gravity for Fine Aggregate 3.6.2.1 Apparatus 37 38 viii ix 3.6.2.2 Procedures 3.7 Aggregate Structure Design 3.7.1 Aggregate Blending 3.8 Marshall Mix Design 3.8.1 Marshall Mix Design Procedures 40 41 42 42 3.8.1.1 Apparatus 43 3.8.1.2 Procedures 44 3.8.2 Theoretical Maximum Density 46 3.8.2.1 Apparatus 47 3.8.2.2 Procedures 47 3.8.3 Flow and Stability Test 48 3.8.3.1 Apparatus 48 3.8.3.2 Procedures 49 3.9 Data Analysis 4 38 50 3.9.1 Bulk Specific Gravity 51 3.9.2 Void Fill with Bitumen 51 3.9.3 Void in Total Mix 51 3.9.4 Void in Mineral Aggregate 52 3.9.5 52 Determination of Optimum Bitumen Content RESULTS AND DISCUSSIONS 53 4.1 Introduction 53 4.2 Materials Preparation 53 4.2.1 Aggregate 54 4.2.1.1 Gradation Analysis 54 4.2.1.2 Washed Sieve Analysis 57 4.2.1.3 Specific Gravity 57 4.3 Marshall Sample 58 4.3.1 Sample Preparation 58 4.3.2 Determination of Optimum Bitumen Content 58 4.3.3 Theoretical Maximum Density 59 4.3.4 Results of Volumetric Properties 59 4.3.5 Analysis Volumetric Properties Based on R Square 61 ix x 5 CONCLUSIONS AND RECOMMENDATIONS 63 5.1 Conclusions 63 5.2 Recommendations 64 REFERENCES 65 APPENDICES A-H 68 x xi LIST OF TABLES TABLE NO. TITLE PAGE 2.1 Bailey Method Criteria for NMAS ½ inch 12 2.2 Recommended Ranges of Aggregate Ratios (NMPS,mm) 22 3.1 Gradation Limits for Asphaltic Concrete 35 3.2 Total number of samples 42 4.1 Combination Gradation Limit for ACW 10 55 4.2 Combination Gradation Limit for ACW 10 56 4.3 Mass of dust in washed sieve analysis 57 4.4 (a) Specific Gravity of materials for ACW10 57 4.4 (b) Specific Gravity of materials for ACW14 58 4.5 Optimum Bitumen Content for ACW10 and ACW14 59 4.6 (a) Marshall mix design results of the ACW10 mixes 60 4.6 (b) Marshall mix design results of the ACW14 mixes 60 xi xii LIST OF FIGURES FIGURE NO TITLE PAGE 2.1 Distresses in Flexible Pavements Rutting 7 2.2 Permanent Deformation in Asphalt Mixtures 8 2.3 Cubical Aggregate 9 2.4 Smooth-Rounded Aggregate 9 2.5 Typical Conventional Aggregate Gradation Curve 10 2.6 Structure of dense graded mix 18 2.7 Regions in the gradation Curve as Defined by the Bailey Method 19 3.1 Developing the Combined Aggregate Blend 27 3.2 Evaluate the Combined Blends (Aggregate Ratio) 27 3.3 Flow diagram for laboratory analysis process 28 3.4 Sieve Analysis Equipment 30 3.5 Mechanical Sieve Shaker 32 3.6 The aggregate was sieve in the mechanical sieve shaker 33 3.7 Wash Sieve Process 34 3.8 Fine Analysis Equipment 38 3.9 Procedures to determine SG for Fine Aggregate 40 3.10 Automatic Marshall Compacter 44 xii xiii 3.11 Marshall Procedures 45 3.12 Apparatus for TMD test 46 3.13 Water bath 48 3.14 Machine for flow and stability test 50 4.1 Combination of Gradation Limit for ACW 10 55 4.2 Combination of Gradation Limit for ACW 14 56 4.3 VTM vs Bit. Content for ACW 10 (R Square Result) 61 4.4 VTM vs Bit. Content for ACW 14 (R Square Result) 61 4.5 VMA vs Bit. Content for ACW 10 (R Square Result) 62 4.6 VMA vs Bit. Content for ACW 14 (R Square Result) 62 xiii xiv LIST OF ABBREVIATIONS/SYMBOLS AASHTO American Association of State Highway and Transportation Officials AC Asphalt Cement ACW 10 Asphalt Concrete Wearing with Nominal Maximum Aggregate Size of 10mm ACW 14 Asphalt Concrete Wearing with Nominal Maximum Aggregate Size of 14mm ASTM American Society for Testing and Materials CA Coarse Aggregate CA Ratio Coarse Aggregate Ratio DG Dense Graded FAc Ratio Fine Aggregate Coarse Ratio FAf Ratio Fine Aggregate Fine Ratio Gsb Combined bulk specific gravity of total aggregate Gmb Bulk specific gravity of compacted mix Gmm Theoretical maximum density HMA Hot Mix Asphalt JKR Jabatan Kerja Raya MRP Malaysia Rock Product NAPA National Asphalt Pavement Association NMAS Nominal Maximum Aggregate Size OBC Optimum Bitumen Content OPC Ordinary Portland Cement PCS Primary Control Sieve PG Performance Grade SCS Secondary Control Sieve xiv xv TCS Tertiary Control Sieve TMD Theoretical Maximum Density US United State UTM Universiti Teknologi Malaysia VFA Voids Filled with Asphalt VMA Voids in Mineral Aggregate VTM Voids in Total Mix xv xvi LIST OF APPENDICES APPENDIX TITLE PAGE A Aggregate size distribution and determination of filler 68 B Wash sieve analysis (ACW 14 and ACW 10) 74 C Specific gravity for coarse and fine aggregate (ACW 14 and ACW 10) 77 D Marshall Test Results (ACW 14 and ACW 10) 82 E Volumetric Properties (ACW 14 and ACW 10) 88 F Determination of OBC at 4% Air Voids (NAPA) 92 G H Theoretical maximum density (TMD) for ACW 14 and ACW 10 Gradation Limit for ACW 10 and ACW 14 94 100 xvi CHAPTER 1 INTRODUCTION 1.1 Background Hot mix asphalt (HMA) is the most common material used for paving applications around the world. It primarily consists of asphalt cement binder and mineral aggregates. It is defined as a combination of heated and dried mineral aggregates that are uniformly mixed and coated with a hot asphalt binder. When bound by asphalt binder, mineral aggregate acts as a stone framework that provides strength and toughness to the system. The behavior of HMA depends on the properties of the individual components and how they react with each other in the system. HMA is a composite material consisting of aggregate particles with different sizes, an asphalt binder that is much softer than the aggregate, and air voids (Alshamsi, 2006) The mixture design process consists of two main parts, the volumetric design portion and empirical mechanical testing to verify the design. In addition, the design method may include other requirements that the mixture must meet in order to satisfy the overall specification standard. Such requirements may include certain aggregate qualities like minimum percent of crushed aggregate, maximum amount of rounded sand materials and specific aggregate gradation requirements (Asphalt Institute, 2001). 2 Controlling the volumetric in HMA is not a new concept and in fact has been around for over a century. In 1903, Bitulithic Macadam, an early HMA design based on volumetric, was patented by Frederick J. Warren, founder of Warren Brothers Company in Boston, Massachusetts. Back then, Mr. Warren designed an experiment to determine the optimum size and gradation of aggregate particles needed to fill a container of known volume (Roberts et al., 1996). 1.2 Problem Statement Generally, in the conventional method the mixtures is accepted or rejected based on those criteria at an early stage in the design process without any validation of their expected performance. An example of such criteria is the percentage of voids in the mineral aggregate (VMA). VMA is the total void space between the aggregate particles in compacted asphalt concrete, including air voids and asphalt not absorbed by the aggregates. It were report by several researchers and highway agencies that there exist difficulties in meeting the minimum voids in VMA requirements (Kandhal, Foo and Mallick, 1998). Studies have also shown that the current defined VMA criteria were seen to be insufficient to correctly differentiate well performing mixtures from poor ones. In other words, the design process in the Marshall mix system does not properly address the expected performance of the designed mixtures in terms of major pavement distresses like permanent deformation and rutting through laboratory performance testing. So, the new method is looking for improvement on those specifications and requirements especially designing the aggregate gradations to improve mixture stability. In the current Marshall mix system, guidance is lacking in the selection of the design aggregate gradations and understanding the interaction of the aggregate structure with mixture design and performance (Asphalt Institute, 2001). Furthermore, the trial and error nature of the actual conventional process of formulating the gradation curve, and the use of weight instead of volume when blending aggregates, offer alternatives to evaluate more rational approaches to design 2 3 an aggregate structure based on principles of aggregate packing concepts (Vavrik et al., 2002) A key to a successful mixture design is the balance between the volumetric composition and the properties of the raw materials used (binder and aggregates). The interaction between these components coupled with the different types and magnitude of loadings the pavement were subjected to results in highly complex mixture responses that require more complete understanding of asphalt mixture behavior. The key step to achieve that is to understand how the mechanical performances of asphalt mixtures were affected by different mixture components and properties (Kandhal, Foo and Mallick, 1998). From the above discussion, there is clearly a need to address the issues of concern in the current Marshall mix design system by introducing more rational which is the new method for aggregate structure known as Bailey method. It is a systematic step to the current system for better design and evaluation of asphalt mixtures. The Bailey method of gradation evaluation focus on the aggregate properties that affect the way aggregates fit together (or pack) in a confined space or volume. To analyze the packing factors, the method defines four key principles that break down the overall combined aggregate blend into four distinct fractions. Each fraction is then analyzed for its contribution to the overall mix volumetric (Vavrik et al., 2001). By comparing the size of particles that fit into the voids between the largest aggregate pieces to the size of the largest aggregate pieces found in a fraction, ratios can be developed that is an indication of how well all the particles in the fraction fit together. Once a mix designer has been taught the principles of the Bailey method and how to apply them, and then begin to predict how changes in the factors that affect packing will change volumetric and compactability of a particular mixture (Vavrik et al., 2001). . 3 4 1.3 Objective of the Study The objective of this study is to evaluate Marshall properties of asphalt concrete mixtures with aggregate gradations designed using Bailey method. 1.4 Scope of the Study In order to archive the objective, the two types of mix designs of asphalt concrete (ACW) were prepared in accordance to the JKR Specification. They were ACW 10 and ACW 14. The aggregate structure (coarse, medium, and fine) was design using the Bailey method of aggregate gradation evaluation. aggregate structure has the highest volume of coarse particles. The coarse This volume decreases as the structure becomes finer. Asphalt cement 80-100 PEN was used in the designed mixture. This study focus in designing the aggregate gradations and performing Marshall mixture design to determine the design asphalt content that provides four percent air void that is currently being used by the Marshall system as an acceptable design parameter for dense graded mixtures (Lavin, 2003). The evaluation tests were conducted in order to determine the best performing aggregate skeleton for each aggregate type and size combination (Thompson, 2006). This evaluation includes determining compaction properties of the mixtures. 1.5 Significance of the Study From the results of this study, it can provide a better understanding in the relationship between aggregate gradation and mixture voids. The Bailey method procedure help to ensure aggregate interlock and good aggregate packing, giving resistance to permanent deformation, while maintaining volumetric properties that provided resistance to environmental stress (Thompson, 2006). Use of the Bailey 4 5 method will ensure coarse aggregate interlock and control of aggregate packing, allowing the designer to specify desired mixture properties. This will eliminate the normal trial and error process used in determining the design aggregate gradations and will help in the transition to contractor mix design. The evaluation tools in the Bailey method can also be used for quality control during the construction process. The proper changes to the production process can be made to meet the quality requirements in the field as a result of the understanding of the effects of aggregate gradations on the properties of the asphalt mixture (Aurilio, William and Lum, 2005). It were expected that, the results of this research will provide a better understanding of the relationship between aggregate gradations and the volumetric properties, ease of construction, and performance. 5 CHAPTER II LITERATURE REVIEW 2.1 Introduction HMA is the most popular bituminous mix. It primarily consists of asphalt cement binder and mineral aggregates. The binder acts as an adhesive agent that binds aggregate particles into a cohesive mass. When bound by asphalt cement binder, mineral aggregate acts as a stone framework that provided strength and toughness to the system. The behavior of HMA depends on the properties of the individual components and how they react with each other in the system (Baladi et al., 1998). Generally, HMA is being used to categorize any asphalt mixture that is mixed while hot. Both the asphalt binder and aggregate are heated to get a fluidity to coat the aggregate and to dry the aggregate, respectively. Different construction project will have different kind of mixture to suit to the site conditions. There are many methods of designing a HMA mix, which among them are the conventional method of Hveem and Marshall, and the newest method called Superpave (Garber and Hoel, 2002). This chapter discusses the overview of the history of Bailey method, Marshall mix design and the aggregate gradations design (coarse, medium and fine). The literature review was done to enhance the understanding in HMA mixture design using the Bailey method. It also reviews the previous researches related to the objective of the study. 7 2.2 Asphalt Cement Binder Role Asphalt cement is one of the two principal constituents of HMA pavement. It is a dark brown to black cementitious material that is either naturally occurring or is produced by the distillation of crude oil (Roberts et al., 1996). In the context of asphalt pavements, three asphalt cement binder characteristics were considered very important to the performance of the pavement in service. These are: temperature susceptibility, viscoelasticity, and aging (Roberts et al., 1996; Asphalt Institute, 2001). The properties of the asphalt cement binder are very dependent on its temperature. At high temperatures, asphalt cement binder becomes viscous and displays plastic response when subjected to loads higher than its viscosity at a particular temperature. This behavior under high temperature can be a contributing factor to one of the most common asphalt pavement distresses which is rutting as shown in Figure 2.1. Figure 2.1: Distresses in Flexible Pavements Rutting (Alshamsi, 2006) 7 8 2.2.1 Aggregate Roles Aggregates are the second principal material in HMA. They play an important role in the performance of asphalt mixtures. For HMA, they make up about 90 to 95 percent by weight and comprise 75 to 85 percent of the volume (Roberts et al., 1996; Asphalt Institute, 2001). Therefore, knowledge of aggregate properties is crucial to designing high quality HMA mixtures. An aggregate’s mineral composition largely determines its physical characteristics and how it behaves in an HMA pavement. Therefore, when selecting an aggregate source, knowledge of the quarry rock’s mineral properties can provide valuable information about the suitability of the resulting aggregate for HMA pavements (Cooper and Brown, 1991). Regardless of the source, aggregate are expected to provide a strong stone skeleton to resist the repeated traffic load applications. When a mass of aggregate is subjected to excessively high loads, a shear plane develops resulting in the aggregate particles sliding or shearing with respect of each others. This behavior produces what is called permanent deformation in asphalt pavement (Lavin, 2003). Along this shear plane, the applied shear stress exceeds the shear strength of the asphalt mixture (Figure 2.2). Figure 2.2: Permanent Deformation in Asphalt Mixtures (Alshamsi, 2006) 8 9 It is known that aggregate has relatively little cohesion (Ervin and Dukatz, 1989). The shear strength is mainly dependent on the internal friction provided by the aggregate. Here, the shape and texture of the aggregate play important role in providing the required interlock. Cubical, rough textured aggregate (Figure 2.3) provide more shear resistance than rounded, smooth-textured aggregate (Figure 2.4). The internal friction provides the ability of aggregate to interlock and create a strong mass that is able to resist the applied traffic load. Figure 2.3: Figure 2.4: 2.2.2 Cubical Aggregate (Alshamsi, 2006) Smooth-Rounded Aggregate (Alshamsi, 2006) Aggregate Gradation The largest portion of the mixture’s resistance to the applied traffic loads is provided by the aggregate structure. Aggregate is expected to provide a strong stone skeleton to resist repeated load applications. One of the key aggregate properties that are related to asphalt mixture performance is gradation. Aggregate gradation is the distribution of the different particle sizes in a mass of aggregate expressed as percent of the total weight (Roberts, Mohamad and Wang, 2002). Sieve analysis is the 9 10 process by which aggregate gradation is determined in the laboratory. Aggregate particles are passed through a series of sieves stacked with progressively smaller openings from top to bottom, and weighing the material retained on each sieve. Gradation of an aggregate is traditionally represented in graphical format by a gradation curve for which the ordinate is the total percent by weight passing a given sieve on an arithmetic scale, while the particle size plotted to a logarithmic scale as shown in Figure 2.5 (Roberts et al., 1996). For asphalt mixtures, it is generally accepted that a well-balanced, continuous gradation will provide the greatest permanent deformation resistance for any given type and quality of aggregates (Roberts et al., 1996; NAPA, 2002). Figure 2.5: Typical Conventional Aggregate Gradation Curve (Robert et al., 2006) Gradation is considered a key factor in the resistance of mixture to permanent deformation (Ervin, 1989; Hveem, 1946). The most important concept is that gradation will provide the greatest structural strength (resistance to rutting) for any given type and quality of aggregate. 10 11 2.3 History of Bailey Method The Bailey method was originally developed by Mr. Robert Bailey (retired) of the Illinois Department of Transportation. It is a systematic approach to blending aggregates that provides aggregate interlock as the backbone of the structure and a balanced continuous gradation of particles to complete the blend. Mr. Bailey developed these methods as a means to combat the rutting of asphalt mixes while maintaining the proper durability characteristics (Vavrik et al., 2002). He began to develop a series of analytical procedures to evaluate mixtures being proposed by contractors in the district where he was the Chief Materials Engineer. As he began to refine the procedure, he used this new analytical tool to predict mixture volumetric often to the amazement, and sometimes the frustration, of the contractor’s quality control personnel and to offer suggestions on how to make the necessary gradation changes to meet the volumetric requirements (Vavrik et al., 2002). The Bailey method for gradation selection considers the packing characteristics of aggregates. The parameters in the method are related directly to VMA, air voids, and compaction properties. The principles in Bailey method can be used from the asphalt mix design through the quality control process, but are not a mix design method (Vavrik et al., 2002). The aggregate blends initially selected for this research were based on the upper and lower limits of the three Bailey method criteria (Vavrik et al., 2002). Four sieves are evaluated under the Bailey method: the half sieve, the primary control, the secondary control and tertiary control. Table 2.1, shows the sieves are evaluated under Bailey method criteria. 11 12 Table 2.1: Bailey Method Criteria for NMAS ½ inch Ratio Lower Limit Upper Limit CA Ratio 0.50 0.65 FAc Ratio 0.35 0.50 FAf Ratio 0.35 0.50 The Bailey method uses three ratios of the various sieves above to control the final gradation. The ratios are as follows (Vavrik et al., 2001): CA Ratio = (% Passing Half Sieve - % Passing PCS) (100% - %Passing Half Sieve) (2.1) FAc Ratio = % Passing SCS % Passing PCS (2.2) FAf Ratio = % Passing TCS % Passing SCS (2.3) Where: CA Ratio = Coarse Aggregate Ratio FAc Ratio = Fine Aggregate Coarse Ratio FAf Ratio = Fine Aggregate Fine Ratio PCS = Primary Control Sieve SCS = Secondary Control Sieve TCS = Tertiary Control sieve 2.4 Mixture Design This section provides an overview of the mixture design methods that have been or being used by the asphalt industry. Generally, most of the mix design methods rely on experience and performance of mixes of known composition. Almost all mixture design methods include specimen fabrication and compaction in the mix design process to determine the mixture composition and volumetric properties. 12 13 Mixture designs were performed on all the aggregate structures that were formulated using the Bailey method of aggregate gradation and evaluation. The Marshall mixture design method were follow. All the mixtures were design for normal volume traffic. HMA is defined as a combination of heated and dried mineral aggregates that are uniformly mixed and coated with a hot asphalt binder. HMA can describe any asphalt mixture that is mixed while hot (Hanson, Mallick and Brown, 1994). 2.4.1 Marshall Mix design The Marshall method has been proven to produce quality HMA from which long-lasting pavements can be constructed. The basic concepts of the Marshall mix design method were originally developed by Bruce Marshall of the Mississippi Highway Department around 1939. The Marshall mix design system provides guidance in selecting the appropriate component materials for asphalt concrete mixtures. However, the selection of the design aggregate gradations is left to the experience of the mix designer (Asphalt Institute, 2001). It is important to understand the influence of the aggregate gradations on the volumetric properties, construction, and performance of the asphalt mixture to achieve the desired properties and performance. The Bailey method provides a systematic approach to blending aggregates to meet the Marshall volumetric criteria based on the concepts of aggregate interlock and aggregate packing. In addition, Bailey method provides tools for evaluating the effect of aggregate gradations on mixture properties, constructability, and performance. The results of this research will provide a better understanding of the relationship between aggregate gradations and the volumetric properties, ease of construction, and performance of typical mixtures (Vavrik et al., 2001). 13 14 For all HMA mixes, the mix design procedure involves a process of selecting and proportioning ingredients to obtain specific pavement performance properties is economical. The gradation mixture must have the following criteria (Asphalt Institute, 2001): (i) Enough asphalt binder to ensure a durable compacted pavement by thoroughly coating and bonding the aggregate. (ii) Enough workability to permit mixture placement and compaction without aggregate segregation. (iii) Enough mixture stability to withstand the repeated loading of traffic without distortion or displacement. (iv) Sufficient voids or air spaces in the compacted mixture to allow a slight additional amount of added compaction by the repeated loading of traffic. These air voids will prevent asphalt binder bleeding or a loss of mixture stability. The volume of air voids should not be so large to allow excessive oxidation or moisture damage of the mixture. (v) The proper selection of aggregates to provide skid resistance in high speed traffic applications. Marshall mix design incorporates several major steps. These are selection of materials, selection of aggregate gradation, selection of asphalt binder, and evaluation of mix design. As it is with all hot mix asphalt, the design compactions a level is 75 blows of compaction and were established. In the Marshall mix design method consists of five steps. The five steps is described as follow: i) Prepare a series of initial samples, each at different asphalt binder content. For ACW 14 instance, two to three samples each might be made at 4, 4.5, 5.0, 5.5, and 6.0 percent asphalt by dry weight for a total of 15 samples. For ACW 10 instance, two to three samples each might be made at 5.0, 5.5, 6.0, 6.5, and 7.0 percent asphalt by dry weight for a total of 15 samples. There should be at least two samples above and two below the estimated optimum asphalt content. (ii) Compact these trial mixes using the Marshall drop hammer which is 75 blows per face. This hammer is specific to the Marshall mix design method. 14 15 (iii) Test the samples in the Marshall testing machine for stability and flow. This testing machine is specific to the Marshall mix design method. Passing values of stability and flow depend upon the mix class being evaluated. (iv) Determine the density and other volumetric properties of the samples. (v) Select the optimum asphalt binder content. The asphalt binder content corresponding to 4 % air voids is selected as long as this binder content passes stability and flow requirements. The Marshall method specified procedure of heating, mixing and compacting the mixture of asphalt and aggregates, which is then subjected to a stability-flow test and a density-voids analysis (Garber and Hoel, 2002). 2.5 Aggregate Packing The importance of aggregate gradation and the need for understanding the interlocking mechanism of aggregates have been a topic of interest by several researchers. One of the earliest attempts to explain and quantify the packing of a mass of aggregates was carried out by Tons and Goetz, (1968). In their study, the packing volumes were introduced as the theoretical basis for understanding the bulk behavior and interlocking mechanisms of aggregates. The angularity and texture of an aggregate particle was unified by the term packing. The more angular the rock is, the higher its packing. The particle volume was defined as the volume which a single rock particle occupies in a mass of mono volume particles. Due to irregular shape of aggregate particles, aggregates usually touch one another at the peaks of the surface roughness. Therefore, the packing includes not only the solid mass and the surface capillaries but also the volume of the surface voids. In other words, the packing volume can be visualized as the volume enclosed by a dimensionless membrane stretching along the peaks of the surface roughness. For a mass of aggregate, this membrane divides voids into inter particle voids and particle surface voids (Tons 15 16 and Goetz, 1968). (Ishai and Tons, 1971) demonstrated experimentally that in bituminous mixtures, surface voids of large particles provide sufficient space not only for asphalt, but also for smaller particles. They explained conceptually using a container filled with one size, coarse, smooth particles. Under constant packing volume of the particles, any additional increase in the mass volume will be equal to a change on the volume of inter particle voids. Some of the particles may penetrate through and under the imaginary packing volume membrane of coarse particles. They defined this interaction between coarse and fine aggregates as the fines lost by rugosity. They further observed that less active fine particles will be located between the larger rough particles which will be packed closer together with thinner asphalt films between them exhibiting higher resistance to shear, tensile and compressive deformation (Kandhal and Cross, 1993). On the other hand, smooth textured particles will be simply pushed apart by the more active fines between them and show low strength. Aggregate particles cannot be packed together to fill a volume completely. There will always be space between the aggregate particles. The degree of packing depends on (Ishai and Tons, 1971): (i) Type and amount of compactive energy. Several type of compactive force can be used, including shearing. Higher density can be achieved by increasing the compactive effort (i.e, gyrations). (ii) Shape of the particles. Flat and elongated particles tend to resist packing in a dense configuration. Cubical particles tend to arrange in dense configurations. (iii) Surface texture of the particles. Particles with smooth textures will reorient more easily into denser configurations. Particles with rough surfaces will resist sliding against one another. (iv) Size distribution (gradation) of the particles. Single-sized particles will not pack as densely as a mixture of particle sizes. (v) Strength of the particles. Strength of the aggregate particles directly affects the amount of degradation that occurs in a compactor or under rollers. Softer aggregates typically degrade more than strong aggregates and allow denser aggregate packing to be achieved. 16 17 2.5.1 Coarse and Fine Aggregate The traditional definition of coarse aggregate is any particle that is retained by the 5 mm sieve. Fine aggregate is defined as any aggregate that passes the 5 mm sieve (sand, silt, and clay size material). In the Bailey method, the definition of coarse and fine is more specific in order to determine the packing and aggregate interlock provided by the combination of aggregates in various sized mixtures (Thompson, 2006). The Bailey method definitions are: (i) Coarse Aggregate - Large aggregate particles that when placed in a unit volume, create voids (ii) Fine Aggregate - Aggregate particles that can fill the voids, it can created by the coarse aggregate in the mixture. From these definitions, more than a single aggregate size is needed to define coarse or fine. The definition of coarse and fine depends on the nominal maximum Aggregate size (NMAS) of the mixture. In a dense graded blend of aggregate with a NMAS of 5 mm, the 5 mm particles come together to make voids. Those voids are large enough to be filled with 10 mm aggregate particles, making the 10 mm particles fine aggregate. In the Bailey method, the sieve which defines coarse and fine aggregate is known as the primary control sieve (PCS), and the PCS is based on the NMAS of the aggregate blend (Vavrik et al., 2001). The PCS is defined as the closet sized sieve to the result of the PCS formula in Equation 2.4. PCS = NMAS x 0.22 (2.4) Where: PCS = PCS for the overall blend NMAS = NMAS for the overall blend, which is one sieve larger than the first sieve that retains more than 10%. 17 18 2.5.2 Bailey Method of Aggregate Blending and Evaluation One of the methods that are attempting to rationalize the aggregate gradation procedure is the Bailey method of aggregate gradation evaluation (Vavrik et al., 2001; TRB Circular, 2002). The Bailey method is a comprehensive gradation evaluation procedure to provide aggregate interlock as the backbone for the aggregate skeleton (Vavrik et al., 2001; TRB Circular, 2002). In this method, the definition of coarse and fine aggregate is not based on the conventional No. 4 sieve (5 mm). Coarse aggregates are defined as the large aggregate particles that when placed in a unit volume, create voids. Fine aggregates are those particles that can fill the voids created by the coarse aggregates. The sieve that separates the coarse and fine aggregates is called the PCS. It is dependent on the nominal maximum particle size of the aggregate blend. The PCS is mathematically defined as 0.22 of the NMAS based on two and three dimensional analysis of the packing of different shaped particles (Figure 2.6). Furthermore, the aggregate blend below the PCS is divided into coarse and fine portions, and each portion is evaluated (Figure 2.7). The method provides a set of tools that allows the evaluation of aggregate blends (Alshamsi, 2006). Figure 2.6: Two Dimensional Aggregate Packing Model (Aurilio, William and Lum, 2006) 18 19 Figure 2.7: Regions in the gradation curve as defined by the Bailey method (Vavrik et al., 2001) Aggregate ratios, which are based on particle packing principles, and the relative proportions passing certain critical sieves, are used to analyze the particle packing of the overall aggregate structure. The coarse aggregate ratio (CA Ratio) is used to characterize the packing and size distribution of the coarse portion of the aggregate blend. The coarse portion of the fine aggregate is evaluated using the fine aggregate ratio of the coarse portion (FAc), and the fine portion of the fine aggregate is evaluated using the fine aggregate ratio of the fine portion (FAf). All these ratios are calculated using mathematical equations that relate the amount of aggregate passing specific critical sieve sizes. In Summary, the Bailey method involves the following approach (Vavrik et al., 2001): (i) Evaluates packing of coarse and fine aggregates individually; (ii) Contains a definition for coarse and fine aggregate; (iii) Evaluates the ratio of different size particles; and (iv) Evaluates the individual aggregates and the combined blend by aggregate. 19 20 2.5.3 Combining Aggregate by Weight All aggregate blends contain an amount and size of voids, which are a function of the packing characteristics of the blend. In combining aggregates we must first determine the amount and size of the voids created by the coarse aggregates and fill those voids with the appropriate amount of fine aggregate. Mix design methods generally are based on volumetric analysis, but for simplicity, aggregates are combined on a weight basis. Most mix design methods correct the percent passing by weight. 2.5.4 Chosen Unit Weight of Coarse Aggregate The designer needs to select the interlock of coarse aggregate desired in their mix design. Therefore, they choose a unit weight of coarse aggregate, which establishes the volume of coarse aggregate in the aggregate blend and the degree of aggregate interlock. In the Bailey method, coarse graded is defined as mixtures which have a coarse aggregate skeleton. Fine graded mixtures do not have enough coarse aggregate particles to form a skeleton, and therefore the load is carried predominantly by the fine aggregate. To select a chosen unit weight we need to decide if the mixture is to be coarse graded or fine graded (TRB Circular, 2002). In summary, the amount of additional consolidation, if any, beyond the selected chosen unit weight depends on several factors: (i) Aggregate strength, shape, and texture. (ii) The amount of fine aggregate that exists in each coarse aggregate. (iii) Combined blend characteristics. (iv) Type of compactive effort applied (Marshall, Gyratory, and etc.). (v) Amount of compactive effort applied (75 vs 125 gyrations, 50 vs 75 blows, etc). 20 21 2.5.5 Analysis of the Design Blend After the combined gradation by weight is determined, the aggregate packing is analyzed further. The combined blend is broken down into three distinct portions, and each portion is evaluated individually. The coarse portion of the combined blend is from the largest particle to the PCS. These particles are considered the coarse aggregates of the blend. The fine aggregate is broken down and evaluated as two portions. To determine where to split the fine aggregate, the same 0.22 factor use on the entire gradation is applied to the PCS to determine a secondary control sieve (SCS). The SCS then becomes the break between coarse and fine graded. The fine is further evaluated by determining the tertiary control sieve (TCS), which is determined by multiplying the SCS by the 0.22 factor (Vavrik et al., 2001). 2.5.5.1 CA Ratio The CA Ratio is used to evaluate packing of the coarse portion of the aggregate gradation and to analyze the resulting void structure. Understanding the packing of coarse aggregate requires the introduction of the half sieve. The half sieve is defined as one half the NMAS. Particles smaller than the half sieve are called ‘interceptors’. Interceptors are too large to fit in the voids created by the larger coarse aggregate particles and hence spread them apart. The balance of these particles can be used to adjust the mixture’s volumetric properties. By changing the quantity of interceptors it is possible to change the VMA in the mixture to produce a balanced coarse aggregate structure. With a balanced aggregate structure the mixture should be easy to compact in the field and should adequately perform under load (Vavrik et al., 2001; TRB Circular, 2002). The equation for the calculation of the coarse aggregate ratio is given in Equation below. CA Ratio = (% Passing Half Sieve - % Passing PCS) (100% - %Passing Half Sieve) 21 22 The packing of the coarse aggregate fraction, observed through the CA Ratio, is a primary factor in the constructability of the mixture. As the CA Ratio decreases, compaction of the fine aggregate fraction increases because there are fewer interceptors to limit compaction of the larger coarse aggregate particles. Therefore, a mixture with a low CA Ratio typically requires a stronger fine aggregate structure to meet the required volumetric properties (Vavrik et al., 2001). Also, a CA Ratio below the corresponding range suggested in Table 2.2 could indicate a blend that may be prone to segregation. It is generally accepted that gap-graded mixes, which tend to have CA Ratios below these suggested ranges, have a greater tendency to segregate than mixes that contain a more continuous gradation. Table 2.2: Recommended Ranges of Aggregate Ratios (NMPS,mm) CA Ratio Fac Ratio FAf Ratio 37.5 mm 0.80 - 0.95 0.35 - 0.50 0.35 - 0.50 25 mm 0.70 - 0.85 0.35 - 0.50 0.35 - 0.50 19 mm 0.60 - 0.75 0.35 - 0.50 0.35 - 0.50 12.5 mm 0.50 - 0.65 0.35 - 0.50 0.35 - 0.50 9.5 mm 0.40 - 0.55 0.35 - 0.50 0.35 - 0.50 4.75 mm 0.30 - 0.45 0.35 - 0.50 0.35 - 0.50 As the CA Ratio increases towards 1.0, VMA will increase. However, as this value approaches 1.0, the coarse aggregate fraction becomes ‘unbalanced’ because the interceptor size aggregates are attempting to control the coarse aggregate skeleton. Although this blend may not be as prone to segregation, it contains such a large quantity of interceptors that the coarse aggregate fraction causes the portion above the PCS to be less continuous. The resulting mixture can be difficult to compact in the field and have a tendency to move under the rollers because it does not want to ‘lock up’. Generally, mixes with high CA Ratios have an S-shaped gradation curve in this area of the 0.45-power grading chart. As the CA Ratio exceeds a value of 1.0, the interceptor-sized particles begin to dominate the formation of the coarse aggregate skeleton. The coarse portion of the coarse aggregate is then considered ‘pluggers’ as these aggregates do not control the aggregate skeleton, but rather float in a matrix of finer coarse aggregate particles (Vavrik et al., 2002). 22 23 2.5.5.2 Coarse Portion of Fine Aggregate All of the fine aggregate (below the PCS) can be viewed as a blend by itself that contains a coarse and a fine portion and can be evaluated in a manner similar to the overall blend. The coarse portion of the fine aggregate creates voids that will be filled with the fine portion of the fine aggregate. As with the coarse aggregate, it is desired to fill these voids with the appropriate volume of the fine portion of the fine aggregate without overfilling the voids (Vavrik et al., 2001; Vavrik et al., 2002). The equation that describes the FAc is given in Equation below. As this ratio increases, the fine aggregate (i.e., below the PCS) packs together tighter. This increase in packing is due to the increase in volume of the fine portion of fine aggregate. It is generally desirable to have this ratio less than 0.50, as higher values generally indicate an excessive amount of the fine portion of the fine aggregate is included in the mixture (Vavrik et al., 2001; TRB Circular, 2002). A FAc Ratio higher than 0.50, which is created by an excessive amount of excessively fine, should be avoided. This type of a blend normally shows a ‘hump’ in the sand portion of the gradation curve of a 0.45 gradation chart, which is generally accepted as an indication of a potentially tender mixture. FAc Ratio = % Passing SCS % Passing PCS If the FAc Ratio becomes lower than the range of values, the gradation is not uniform. These mixtures are generally gap-graded and have a in the 0.45-power grading chart, which can indicate instability and may lead to compaction problems. This ratio has a considerable impact on the VMA of a mixture due to the blending of sands and the creation of voids in the fine aggregate. The VMA in the mixture will increase with a decrease in this ratio (Vavrik et al., 2001). 2.5.5.3 Fine Portion of Fine Aggregate The fine portion of the fine aggregate fills the voids created by the coarse portion of the fine aggregate. This ratio shows how the fine portion of the fine aggregate packs together. One more sieve is needed to calculate the FAf, the TCS. 23 24 The TCS is defined as the closest sieve to 0.22 times the SCS. FAf Ratio = % Passing TCS % Passing SCS The FAf Ratio is used to evaluate the packing characteristics of the smallest portion of the aggregate blend. Similar to the FAc Ratio, the value of the FAf Ratio should be less than 0.50 for typical dense-graded mixtures. VMA in the mixture will increase with a decrease in this ratio (Vavrik et al., 2001). 2.5.5.4 Summary of Ratios CA ratio is describes how the coarse aggregate particles pack together and, consequently how these particles compact the fine aggregate portion of the aggregate blend that fills the voids created by the coarse aggregate. FAc Ratio describes how the coarse portion of the fine aggregate packs together and, consequently, how these particles compact the material that fills the voids it creates. FAf Ratio describes how the fine portion of the fine aggregate packs together. It also influences the voids that will remain in the overall fine aggregate portion of the blend because it represents the particles that fill the smallest voids created (Vavrik et al., 2001; TRB Circular, 2002). 24 CHAPTER III METHODOLOGY 3.1 Introduction The purpose of this study was to evaluate the laboratory performance of asphalt mixtures with aggregate gradations that were designed using Bailey method. This chapter provides detailed information on the materials used and their properties. It also highlights the laboratory procedures for the tests performed. The tests were carried out according to the required specifications. This study used the Marshall method as published by National Asphalt Pavement Association (NAPA) along with the Public Works Department of Malaysia’s (JKR) specifications for the different type of mixes. The types of mixes use were ACW10 and ACW14. The gradation limits of mixes were as specified by JKR. 3.2 Operational Framework The laboratory work consisted of two series of tests. The tests conducted for the first series were sieve analysis and determination of specific gravity for aggregate (coarse and fine). The aggregates obtained from the Malaysian Rock Product Quarry (MRP) were dried sieve to separate the aggregates into different sizes. Washed sieve analyses were done to determine the percentage of dust and silt-clay material in order to check the need for filler material that were referred to ASTM C 117. The 26 determinations of specific gravity for coarse and fine aggregates were done according to ASTM C 127 and C 128. Aggregate blending satisfying the JKR gradation limits were used. Bitumen of 80-100 PEN were used in this study. The second series involved was the Marshall mix design. 90 samples were prepared in order to determine the optimum bitumen content (OBC) for each mix design and 12 samples were prepared for Theoretical Maximum Density. The bulk specific gravity and density of compacted sample were done in accordance to ASTM D 2726. The stability and flow test were conducted for Marshall sample according to ASTM D 1559. To achieve the objectives of the study, a test plan has been designed as shown in Figure 3.1 and 3.2 below. Figure 3.1 shows the summary of combined aggregate blend and evaluation of combined blends using Bailey method. Figure 3.2 shows the procedure of the Marshall mixture. Before developing combined aggregate blend, several aspects need to be considered: these are mix type and NMAS, weight of coarse aggregate and the desired percentage of -0.075mm in the combined blend. After aggregate blending, evaluate the combined blend: Coarse Aggregate (CA), (CA Ratio, FAc Ratio and FAf Ratio. Dense graded mix and 80-100 PEN bitumen were used in Marshall mixes as recommended by JKR. The mix designs were conducted according to JKR and AASHTO standards to produce three mixture types (ACW10 and ACW14). The gradation limits for the mixes were prepared according to JKR/SPJ/rev2005. This test was carried out to evaluate the performance of asphalt mixtures. The general procedures for laboratory work are illustrated in Figure 3.3. 26 27 Determine the mix type and NMAS Choose the weight of coarse Aggregate: i) ii) Blend the individual coarse aggregate by weight Blend the individual fine aggregate by weight Choose the desired percentage of -0.075mm in the combined blend Figure 3.1: Developing the Combined Aggregate Blend The 1st Bailey principles - CA - The 2nd Bailey principles - CA Ratio - The 3rd Bailey principles - FA c Ratio - The 4th Bailey principles - FA f Ratio Figure 3.2: Evaluate the Combined Blends (Aggregate Ratio) 27 28 Aggregate From MRP Quarry Dry sieve analysis to distribute the aggregates into different sizes Wash sieve analysis to determine the percentage of dust and silt-clay Determination of specific gravity for coarse and fine aggregate Gradation design for ACW10 and ACW14 (Medium, Coarse and Fine) Combine aggregate blend (ACW10 and ACW14) with different gradation size Aggregate Blend Ratio Marshall Mix Design: (Sample Preparation) Theoretical Maximum Density Testing: Marshall Test (Stability and Flow) Analysis And Discussion Figure 3.3: Flow diagram for laboratory analysis process 28 29 3.3 Materials Asphalt mixture is a composite material that is largely made of two main components; aggregate and asphalt cement. This section describes the properties of the aggregates and the asphalt cement binders used. 3.3.1 Aggregates According to JKR/SPJ/rev2005, aggregate for asphaltic concrete shall be a mixture of coarse and fine aggregates. The coarse aggregate used were screened crushed hard rock and retained on 5mm sieve opening angular in shape, free from dust, clay, and other organic matter and deleterious substances. Fine aggregate normally consists of quarry dusts. Fine aggregate conformed to the requirements, sand equivalent of aggregate fraction passing the 5mm sieve shall be not less than 45%, fine aggregate angularity shall not be less than 45%, and the water absorption shall not be more than 2% (ASTM C 136). The specific gravity for coarse and fine aggregate was determined according to ASTM C 127 and C 128. Detailed laboratory evaluation procedures of individual stockpiles were conducted to determine the basic aggregate properties such as specific gravity, gradation, and other Marshall consensus properties. The laboratory tests conducted on each aggregate stockpile included: (i) washed sieve analysis (ASTM C 117) to determine as-received gradation. (ii) specific gravity and absorption ( ASTM C 127 for coarse aggregate andASTM C 128 for fine aggregate). The aggregates used in this study were obtained from Malaysia Rock Product (MRP) quarry, which locates at Ulu Choh, Johor, Malaysia. 29 30 3.3.2 Bituminous Binder An 80/100 PEN bitumen was used as binder in this study. The bitumen contents for all of the samples range between 4–6% for ACW 14 and 5-7% for ACW 10 with 0.5% increment according to JKR/SPJ/rev2005. 3.4 Sieve Analysis There are two methods for determining aggregate gradation, dry sieve analysis and washed-sieve analysis. These methods were used primarily to determine the grading of aggregates including both coarse and fine fractions ensuring the aggregate were well blended within the gradation limit as specified in JKR (2005). It is a process of separating dry aggregate into different sizes through a series of sieves of progressively smaller openings for determination of particle size distribution. Figure 3.4 shows the equipment for Sieve Analysis. Figure 3.4: Sieve Analysis Equipment 30 31 3.4.1 Dry Sieve Analysis Dry sieve analyses were performed on aggregates obtained from the quarry, MRP. These tests were done to separate the aggregate into different sizes. Dry sieve analysis was conducted in accordance with ASTM C 136 and AASHTO T 305. 3.4.1.1 Apparatus The apparatus that were used for dry sieve analysis included: (i) Sieves with various sizes starting from 20 mm to pan - Sieves were mounted on substantial frames that were constructed in a manner that prevent loss of material during sieving. Suitable sieve sizes were selected to furnish the information required by the specifications covering the materials to be tested; (ii) Mechanical Sieve Shaker was imparted a vertical and/or lateral motion to the sieve, caused the particles thereon to bounce and turn so as to present different orientations to the sieving surface; (iii) Oven, An oven of appropriate size capable of maintaining a uniform temperature of 110±5ºC (230±9ºF). 3.4.1.2 Procedures (i) The samples were dried to constant weight at a temperature of 110±5ºC (230±9ºF). (ii) The sieves were nested in order of decreasing size of opening, from top to bottom and the samples were placed on the top sieve. The sieves were stirred up by mechanical apparatus for a sufficient period. (iii) The quantity of material was limited on given sieve so that all particles have opportunity to reach sieve openings a number of times during the sieving operation. 31 32 (iv) The sieve processes were continued for a sufficient period. (v) In order to prevent the overloading of individual sieve, the portion of the sample finer than 5mm (No. 4) sieve were distributed among two or more sets of sieves. 3.4.2 Wash Sieve Analysis Wash sieve analysis were done to determine the amount of weight of dust and silt-clay material in the original sample and removes clay or dust on the aggregate by washing. It is also used to determine the total filler needed for the particular mix. Wash sieve analysis was in accordance with ASTM C 117 and AASHTO T 27. Figure 3.5 and 3.6 shows the equipment for dry sieve analysis. Figure 3.5: Mechanical Sieve Shaker 32 33 Figure 3.6: The aggregate was sieve in the mechanical sieve shaker 3.4.2.1 Apparatus The apparatus used for washed sieve analysis were: (i) Sieve size of 600 and 75μm; (ii) Container; (iii) An oven capable of maintaining a temperature of 110±5°C. 3.4.2.2 Procedures The procedures for washed sieve analysis are as follow: (i) The aggregate samples were weighed before being placed on the 600μm sieve, with the 75μm sieve at the bottom. (ii) The aggregate were thoroughly washed until no particles pass the 75μm sieve (Figure 3.7). 33 34 (iii) Carefully, the samples were poured into the container and were left to allow all the aggregate to sink before draining the water out of the container. (iv) The washed samples were dried in an oven at a temperature of 110±5°C for 24 hours. (v) The dried weight were recorded, B. (vi) The required filler were calculated as follows. Dust percentage = [(A – B) / A] x 100 Where: A = Weight of dry sample before wash, g B = Weight of dry sample after wash, g Figure 3.7: Wash Sieve Process 3.5 Aggregate Gradation Aggregate gradation greatly influences the performance of the pavement layers. As such the aggregate from the quarry stockpiles were sieved to obtain the combined gradation. Aggregate grading is carried out to determine the proportion of aggregate required from each stockpile to fit into the given specification. The percent passing of the aggregate through the selected sieves is determined by taking weights retained on individual sieves. The maximum particle size in a mixture is important to ensure good performance. If the maximum particle size is too small, 34 35 the mix may be unstable, if it is too large, workability and segregation may be problem. The aggregate grading was conducted to determine the percentage of aggregate required for every size according to JKR/SPJ/rev2005. The curve with subjected to the sample grade were produced from the graph percent passing percent sieve size to the power of 0.45 with upper and lower limit. Then the mass retained were calculated using the percent passing for every sample size. The gradation of the combined coarse aggregate, fine aggregate and mineral filler for ACW 10 and ACW 14 should conform to the appropriate envelopes as illustrates in Table 3.1. Table 3.1: Gradation Limits for Asphaltic Concrete Mix Type Wearing Course Wearing Course Mix Designation AC 10 AC 14 BS Sieve Size, mm Percentage Passing (by weight) 20.0 3.6 100 14.0 100 90 – 100 10.0 90 – 100 76 – 86 5.0 58 – 72 50 – 62 3.35 48 – 64 40 – 54 1.18 22 – 40 18 – 34 0.425 12 – 26 12 – 24 0.150 6 – 14 6 – 14 0.075 4–8 4–8 Determination of Specific Gravity for Aggregate The specific gravity of an aggregate provides a mean of expressing the weight-volume characteristics of material. Specific gravity for coarse and fine aggregates was determined separately. Coarse aggregate is the aggregates that are retained on the 5mm sieve while fine aggregates are those that passing 5mm sieve. 35 36 3.6.1 Specific Gravity for Coarse Aggregate The specific gravity tests of coarse aggregate were conducted to determine the value of bulk, SSD and apparent specific gravity. The equipment and procedures for determining the specific gravity and water absorption of coarse aggregates as outlined in ASTM C 127. 3.6.1.1 Apparatus (i) Balance that is accurate to 0.1g of the sample weight; (ii) Sample container - a wire basket of 3.35mm (No. 6); (iii) Water tank; and (iv) Sieves with of 5mm sieve. 3.6.1.2 Procedures The procedure for determining specific gravity for coarse aggregate was as follow: (i) The sample of aggregate is mixed and it is reduced to the approximate quantity needed, 1 kg. (ii) All the material passing a 5mm (No. 4) sieve by dry sieving is rejected and is washed to remove dust or coatings from the surface. (iii) The test sample is dried to constant weight at a temperature of 110±5ºC (230±9ºF). (iv) The sample is cooled in air at room temperature until the aggregate has cooled to a temperature that is comfortable to handle. (v) Subsequently the aggregate is immersed in water at room temperature for a period of 15 to 19 hours. (vi) The test sample is removed from the water and it is rolled in a large absorbent cloth until all visible films of water are removed. (vii) The larger particles are wiped individually. 36 37 (viii) The weight of test sample in the saturated surface-dry condition is recorded, B to the nearest 1.0g. (ix) After weighing, the saturated-dry surface test sample is place immediately in the sample container and its weight in water is determined, C. (x) The test sample is dried to constant weight at a temperature of 110±5ºC (230±9ºF). (xi) The sample is cooled in air at room temperature until the aggregate has cooled to a temperature that is comfortable to handle and it is weighed as A. (xii) Bulk specific gravity is calculated as follows: Gmb = A / (B-C) Where: A = Weight of oven-dry test sample in air, g B = Weight of saturated surfaced-dry test sample in air, g C = Weight of saturated test sample in water, g (xiii) Bulk specific gravity is calculated as follows: Gma = A / (A-C) 3.6.2 Specific Gravity for Fine Aggregate The specific gravity test for fine aggregate was conducted to determine the value of bulk, SSD and apparent specific gravity. The equipment (Figure 3.8) and procedures for determining the specific gravity and water absorption of fine aggregates were described below according to ASTM C 128. 37 38 3.6.2.1 Apparatus (i) Balance having the capacity of 1kg with the accuracy of 0.1g; (ii) Pycnometer - A container into which the fine aggregate test sample can be readily introduced and in which the volume content can be reproduced within ±0.1cm3. The volume of container filled to mark was at least 50% greater than the space required to accommodate the test sample; (iii) Mould in the form of a frustrum of a cone with dimensions as follow: 40±3mm inside diameter at the top, 90±3mm inside diameter at the bottom, and 75±3mm in height; and with the metal having a minimum thickness of 0.8mm; and (iv) Tamper weighing 340±15g and having a flat circular face 25±3mm in diameter. Figure 3.8: Fine Analysis Equipment 3.6.2.2 Procedures The procedure for determining the specific gravity of fine aggregate was as follow: (i) 500g weight of fine aggregates was placed in the container and 30g (6% of the sample) of water was mixed to get a saturated surface dry condition for 24 hours (Figure 3.9). 38 39 (ii) Partially the pycnometer was partially filled with water. (iii) Immediately the pycnometer was introduced with the approximately 500g of saturated surface dry fine aggregate prepared. (iv) The additional water was filled to approximately 90% of capacity. (v) The pycnometer was rolled, inverted and agitated to eliminate all the bubbles. (vi) The total weight of the pycnometer, specimen and water were determined, C to the nearest 0.1g. (vii) The fine aggregate was removed from the pycnometer and was dried to constant weight at a temperature of 110±5ºC (230±9ºF). (viii) The fine aggregate was cooled in air at room temperature. (ix) The weight was record to the nearest 0.1g, A. (x) The weight of the pycnometer filled with water, B was recorded. (xi) Bulk specific gravity was calculated as defined in AASHTO M 132 as follows: Gmb = A / (B+S-C) Where: A = Weight of oven-dry specimen in air, g B = Weight of pycnometer filled with water, g C = Weight of pycnometer with specimen and water, g S = Weight of saturated surface-dry specimen, g (xii) Apparent specific gravity was calculated as defined in AASHTO M 132 as follows: Gma = A / (B+A-C)] 39 40 Figure 3.9: Procedures to determine SG for Fine Aggregate 3.7 Aggregate Structure Design The objectives of this study was to design the aggregate structure using an analytical aggregate gradation method that will allow a rational blending of different sizes of aggregate to achieve an optimum aggregate structure for better mixture performance. The Bailey method for aggregate gradations evaluation was utilized for this purpose. Three aggregate structures was design for each aggregate type (coarse, medium, and fine). The structure was design to meet the recommended ranges of the Bailey method Parameters. 40 41 The aggregate in a dense graded asphalt mixture have the most significant contribution in the load bearing capacity of an asphalt mixture. The aggregate also determine the surface texture and skid resistance of the pavement (Kandhal and Mallick, 2000). The asphalt binder is used to cement the aggregate particles together. The gradation of the asphalt mixture is the one major variable that the designer can alter to give the properties desired. Aggregate gradation is the distribution of the aggregate particle sizes expressed as a percent of the total weight. The gradation of the aggregate expressed as a percent of the total volume has the most significance, but expressing the gradation as a percent by weight is easier to calculate and is standard practice throughout the world. The gradation is determine by sieve analysis and is expressed as a total percent passing each sieve size in descending order. Total percent passing each sieve is the current recognized method for describing aggregate gradation (Vavrik et al., 2002). A dense graded asphalt mixture generally contains a combined gradation of several aggregates, since a single aggregate generally will not provide all the desired properties for a dense graded mixture. The volume in the aggregate packing that allows for asphalt binder and air voids is known as the VMA of the asphalt mixture. Dense graded HMA is usually a blend of several aggregates (Cooper and Brown, 1991). In most cases no single aggregate gradation will give all the properties that are desired of the asphalt mixture (NAPA, 2002). Dense graded HMA is a proportion of both coarse and fine aggregates. 3.7.1 Aggregate Blending Aggregate blending involved the process of proportioning the aggregates to obtain the desired gradation that were well within the gradation limits. The gradation limits for the mixes that were prepared as specified by JKR/SPJ/rev2005. For this study, the mixes that were prepared are ACW10, ACW14, and ACB28. The mixes combined coarse aggregates and fine aggregates. A smooth curve within the appropriate gradation envelope is desired. 41 42 3.8 Marshall Mix Design The concept of Marshall method of designing paving mixtures was formulated by Bruce Marshall. The procedure of Marshall design was standardized by the American Society for Testing and Materials (Roberts et al., 1996). The main purpose of design was to eliminate the OBC for each mixes. Marshall Method used a standard test specimen of 102mm in diameter (4-inch) and 64mm in height (2.5inch). These were prepared using a specified procedure for heating, mixing and compacting the asphalt mixes. Marshall design was divided into two stages of laboratory works which were sample preparation and testing. The procedure for the Marshall design starts with the preparation of test samples. Six gradations were prepared for each combination of aggregates and bitumen content for ACW 10 at 5.0%, 5.5%, 6.0%, 6.5%, and 7.0% and for ACW 14 at 4.0%, 4.5%, 5.0%, 5.5% and 6.0%. The samples were prepared using Marshall hammer compactor of 75 blows per face. Total number of samples were prepared for this study, are described in the Table 3.2 below. Table 3.2: Total number of samples Mix Type 3.8.1 Number of Samples Marshall (Compacted Sample) 90 TMD (Loose Mix) 12 Total Samples 102 Marshall Mix Design Procedures The equipment and procedures for preparing the Marshall compacted sample were outlined in ASTM D 1559. 42 43 3.8.1.1 Apparatus (i) Pans, metal, flat bottom for heating aggregate; (ii) Pans, metal, round, approximately 4 liters capacity for mixing asphalt and aggregate; (iii) Oven and hot plate, electric for heating aggregate, asphalt and equipment as required; (iv) Scoop for batching aggregates; (v) Containers, gill types tins, beakers, pouring pots or sauce pans for heating asphalt; (vi) Thermometers, armored, glass, or dial type with metal stem, 10ºC to 23ºC for determining temperature of aggregates, asphalt and asphalt mixtures; (vii) Balance – To the nearest 0.1g; (viii) Mixing spoon, large or trowel, small; (ix) Spatula; (x) Compaction pedestal; (xi) Compaction mould, consisting of a base plate, forming mould and collar extension; (xii) Compaction Hammer, consisting of a flat circular tamping face 98.4mm in diameter and equipped with a 4.5kg weight constructed to obtain a specified 457mm height of drop (Figure 3.10); (xiii) Mould holder; (xiv) Oil grease for extruding compacted specimens from mould; (xv) Gloves; (xvi) Marking crayons for identifying test specimens; and (xvii) Filter paper. 43 44 Figure 3.10: Automatic Marshall Compactor 3.8.1.2 Procedures The procedures were: (i) Aggregates were dried in the oven at temperature of 160ºC to 170ºC for at least 12 hours before blending process. (ii) Bitumen was melted at minimum temperatures 170°C (maximum 170°C±5°C) at least for 2 hours. (iii) Mould was heated at 160°C to 170°C before use. Filtration paper was cut as mould size and put at the base of mould before it filled by mix sample. (iv) Then, required amount of bitumen was added into the aggregate and mixed for 2 to 3 minutes to yield a mix having a uniform distribution of asphalt throughout at 150°C to 170°C. (v) Oil grease was spread on the inner surface of the mould and the filter paper was put at base of mould. 44 45 (vi) The blended mixes were put inside the mould and flat using the spatula by penetrating it 15 times at perimeter mould and 10 times at the middle of the mixes. (vii) When the temperature reaches 150°C, the filter paper was put at the top of sample and the compaction was performed. (viii) The compaction was performed at 75 blows for both top and the bottom surface of the samples. Then samples were cooled or maintained at room temperature for 24 hours before extrusion. Figure 3.11 below shows the Marshall procedures. Figure 3.11: Marshall Procedures 45 46 3.8.2 Theoretical Maximum Density The theoretical maximum density (TMD) was used to determine the void in total mix (VTM) for the sample. The equipment and procedures for conducting TMD test were referred in ASTM D 2041-91 (Figure 3.12). There are two methods to determine the theoretical maximum density either using calculation or from theoretical maximum density test. In this study, the calculation method was used to obtain the theoretical maximum density value by using equation as follows: TMD = A / (A+B+C) Where: A = Mass of oven dry sample in air, gram B = Mass of vacuum container filled with water, gram C = Mass of vacuum container filled with water and sample (after vacuum), gram Figure 3.12: Apparatus for TMD test 46 47 3.8.2.1 Apparatus (i) Vacuum Container; (ii) Balance; (iii) Vacuum pump or water aspirator; (iv) Residual pressure manometer; (v) Manometer or vacuum gauge; (vi) Thermometers; (vii) Water bath; (viii) Bleeder valve; and (ix) Protective gloves. 3.8.2.2 Procedures (i) A weighed sample of oven dry paving mixture in the loose condition was placed in a tarred vacuum vessel. Sufficient water at a temperature of 25±4°C was added to completely submerge the sample. (ii) Vacuum was applied 15 minutes to gradually reduce the residual pressure in the vacuum vessel to 30 mm of Hg or less. (iii) At the end of the vacuum period, the vacuum was gradually released. (iv) The volume of the sample of paving mixture was obtained either by immersing the vacuum container with sample into a water bath and weighing or by filling the vacuum container level full of water and weighing in air. At the time of weighing the temperature was measured as well as the mass. (v) From the mass and volume measurements the specific gravity or density at 25°C was calculated. If the temperature employed was different from 25°C, an appropriate correction is applied. 47 48 3.8.3 Flow and Stability Test This test method covers the measurement of the resistance to plastic flow of cylindrical samples of bituminous mix loaded on the lateral surface by means of the Marshall apparatus. Marshal stability was generally the maximum load carried by a compacted sample tested at 60°C at a loading rate of 2 inches/minute. The flow was measured at the same time as the Marshall stability. The flow was equal to the vertical deformation of the sample. High flow values generally indicate a plastic mix that was experience permanent deformation under traffic, whereas low flow values may indicate a mix with higher than normal voids and insufficient asphalt for durability and one that may experience premature cracking due to mix brittleness during the life of the pavement. The flow and stability value of each test sample was determined in accordance with ASTM D 1559. 3.8.3.1 Apparatus (i) Marshall testing head consist of upper and lower segments; (ii) Flow meter; (iii) Thermometer with a range from 20°C to 70°C; (iv) Rubber gloves to remove specimens from water bath; (v) Compression machine; and (vi) Water bath (Figure 3.13). Figure 3.13: Water bath 48 49 3.8.3.2 Procedures (i) Specimen was immersed in the water bath with the temperature maintain at 60±1°C for 45 minutes. (ii) The guide rods and the test heads thoroughly were cleaned prior conducted the test. Besides, the guide rods were lubricated so that the upper test slid freely over them. The testing-head temperature was suggested to maintain at 21°C to 38°C. (iii) Specimen then was extracted from the water bath and was dried before placing it in the lower testing head. After that, the upper testing head placed on the specimen and the complete assembly then was located in position on the testing machine (Figure 3.14). (iv) The flow meter was placed in position over one of the guide rods and then the flow meter was adjusted to zero. While the test load was being applied, the flow meter sleeve needed to be held firmly against the testing heads upper segment. (v) The flow meter reading was recorded before the specimen was being loaded. (vi) The load at a constant rate of testing head movement of 50.8mm per minute was applied to the specimen until the maximum load reading was obtained and the load decreased as indicated by the dial. (vii) Afterward, the maximum load until it began to decrease was noted or being converted from the maximum micrometer dial reading. (viii) The last reading at the flow meter was recorded. The last value of flow meter was deducted to the earliest value, which indicated as a flow value in mm unit. (ix) The elapsed time started from specimen removal from water bath to maximum load being determined shall not exceed 30s. 49 50 Figure 3.14: Machine for flow and stability test 3.9 Data Analysis In the Marshall method each compacted sample was subjected the following analysis: (i) Bulk Specific Gravity; (ii) Void in Total Mix (VTM); (iii) Void Filled with Bitumen (VFB); (iv) Void in Mineral Aggregate (VMA); (v) Stability; and (vi) Flow. 50 51 3.9.1 Bulk Specific Gravity After compaction, the sample was removed from the mould and cooled at room temperature. Bulk specific density was determined using the following equation: Specific Gravity = A / (B-C) Where: A = Weight of dry sample in air B = Weight of saturated surface dry sample C = Weight sample in water 3.9.2 Void Filled with Bitumen Voids fill with bitumen (VFB) is the percentage of void volume filled with bitumen. The equation in determining the VFB is as follows: VFB = [1 – (Gmm*PA / Gmb)] x 100 Where: 3.9.3 Gmm = Theoretical Maximum Density PA = Aggregate Percentage Gmb = Aggregate Bulk Specific Gravity Void in Total Mix Void in total mix(VTM) for hot mix asphalt mixture was defined as void volume between the aggregates coated by bitumen. The equation in determining the VTM is as follows: VTM = [1 - (Gmb / Gmm)] x 100 Where: Gmb = Bulk Specific Gravity Gmm = Theoretical Maximum Density 51 52 3.9.4 Void in Mineral Aggregate Void in Mineral Aggregate (VMA) may be defined as the volume of intergranular void space between the aggregate particles of a compacted paving mixture that include air voids and the effective bitumen content (volume of bitumen not absorbed into the aggregate). It was expressed as a percent of the total volume of the specimen. This value can be obtained using the following formula: VMA = 100 – [Gmb x Ps / Gsb] Where: 3.9.5 Gmb = Bulk specific gravity of compacted mixture Gsb = Combined bulk specific gravity of the total aggregate Ps = Percent of aggregate in the mixture Determination of Optimum Bitumen Content The average values of bulk specific gravity, stability, flow, VFB, and VMA obtained were plotted separately against the bitumen content and smooth curve were drawn through the plotted values. The mean optimum bitumen content for ACW10 and ACW14 was determined by averaging four optimum bitumen contents as specified in JKR/SPJ/2007. Determination of OBC for ACW mixes: (i) Peak of curve taken from stability graph; (ii) Flow equals to 3mm from the flow graph; (iii) Peak of curve taken from the bulk specific gravity graph; and (iv) VTM equals to 4% from the VTM graph. The individual test values for stability, flow, stiffness, VTM and VFB at the optimum bitumen content then were determined from the plotted smooth curves and compare with the desired design criteria. If any of the values do not comply with the specification, the mix design procedures were repeated until all the design parameters were satisfied. 52 CHAPTER IV RESULTS AND DISCUSSIONS 4.1 Introduction This chapter includes the analysis of all the results and discussion of the result obtains from the analysis. The several tests were obtained to determine the Marshall properties for ACW14 (coarse, medium and fine) and ACW10 (coarse, medium and fine). That includes mixture design data and gradation analysis, results from the laboratory tests presented and discussed in the previous chapter, and the effect of the different mixture parameters on those test results. 4.2 Materials Preparation Mixtures designed were performed on all the aggregate gradations that were formulated using the Bailey method of aggregate gradation and evaluation. The ACW 14 and ACW 10 were divided to three gradations (coarse, medium and fine) were choosing in this study to get the Marshall properties with aggregate gradations design using the Bailey method. Penetrations 80/100 were used as bituminous binder in this study. The bitumen contents for all of the samples were ranged between 4– 6% for ACW 14 and 5-7% for ACW 10 with 0.5% increment according to JKR/SPJ/rev2005. The dense graded were choosing in this study to analyzed the different gradation (coarse, medium and fine) which follow the JKR specifications. 54 All the properties of the materials used were measured for further analysis purposes. Laboratory test were conducted to determine the Marshall properties of the mixes according to the specifications referred to JKR, ASTM and ASSTHO. Data from the test were analyzed and results were compared with Malaysian Standard (JKR specification). 4.2.1 Aggregate The aggregate used in this study based on the gradation from ACW 14 and ACW 10 which referred to JKR specification. The aggregates were supplied by MRP Quarry which located at Ulu Choh, Johor. A sample aggregate for each stockpile were blend together to determine the proportion specification for ACW 14 and ACW 10. As a result, the gradations of blended aggregate obtained (medium, coarse and fine) were use into design mix in order to determine the volumetric and Marshall properties of the mixes. 4.2.1.1 Gradation Analysis As mentioned earlier, the aggregate gradations designed using the Bailey methods were further evaluated by the power law gradation evaluation method. The methods look at distinct regions in the gradation curve and describe them using one that are related to the size distribution of the aggregates in those particular regions. The correlation between the parameters describing the fine portion of the aggregate gradation curve is, however, relatively weak. This is not unexpected since the FAC from the Bailey method describes the middle portion of the curve only while the parameters from the power law method considers the whole portion of the gradation curve from the divider sieve to the No.200 sieve (Vavrik et al., 2002). In other words, the fine parameters from the two methods describe different regions of the gradation curve and, thus are not expected to correlate well with each others. Table4.1, 4.2 and Figure 4.1, 4.2 shows the combination of gradation. 54 55 Table 4.1: Combination Gradation Limit for ACW 10 Sieve Sieve Size Lower Upper % Passing % Passing % Passing Size ^0.45 Limit Limit Medium Coarse Fine 14 3.279 100 100 100 100 100 10 2.818 90 100 95 97 91 5 2.063 58 72 65 60 68 3.35 1.723 48 64 56 49 60 1.18 1.077 22 40 31 24 36 0.425 0.680 12 26 19 15 23 0.15 0.426 6 14 10 9 12 0.075 0.312 4 8 6 6 6 ACW10 120 % Passing 100 80 60 40 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 0.45^Sieve Size Lower Limit % Passing Medium % Passing Fine Upper Limit % Passing Coarse Figure 4.1: Combination of Gradation Limit for ACW 10 55 56 Table 4.2: Gradation Limit for ACW 14 Sieve Sieve Size Lower Upper % Passing % Passing % Passing Size ^0.45 Limit Limit Medium Coarse Fine 20 3.850 100 100 100 100 100 14 3.279 90 100 95 98 92 10 2.818 76 86 81 85 79 5 2.063 50 62 56 51 54 3.35 1.723 40 54 47 40 48 1.18 1.077 18 34 26 20 31 0.425 0.680 12 24 18 13 20 0.15 0.426 6 14 10 9 12 0.075 0.312 4 8 6 6 6 ACW 14 % P a s s in g 120 100 80 60 40 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 0.45^Sieve Size Lower Limit % Passing Medium % Passing Fine Upper Limit % Passing Coarse Figure 4.2: Combination of Gradation Limit for ACW 14 56 57 4.2.1.2 Washed Sieve Analysis Washed sieve analyses were conducted to determine the filler content (material passing 75 µm) that needed in the mixture and the amount of filler which stick to the coarse aggregate according to ASTM C 117. Filler used in this research were dust and hydrated lime. The amounts of filler content needed in each mixes in this research are shown in Table 4.3. All the detail calculations in determining the filler content were attached in Appendix B. Table 4.3: Mass of dust in washed sieve analysis Sample Mass of Dust -1200 g Mass of Dust-TMD (1500 g) ACW10 Coarse 14.5 20.1 ACW10 Medium 17.9 22.4 ACW10 Fine 17.8 24.2 ACW14 Coarse 15.8 21.4 ACW14 Medium 18.05 22.5 ACW14 Fine 19.6 27.65 4.2.1.3 Specific Gravity Specific gravity and absorption of aggregates were determine and analyzed according to ASTM C 127 for coarse aggregates and ASTM C 128 for fine aggregates. Detail calculations of the specific gravity were attached in the Appendix C. The average specific gravity for each materials used in this research are summarized in Table 4.4(a) and Table 4.4(b). Table 4.4(a): Specific Gravity of materials for ACW10 Material Aggregate Coarse Specific Gravity 2.578 Aggregate Fine 2.574 57 58 Table 4.4(b): Specific Gravity of materials for ACW14 4.3 Material Aggregate Coarse Specific Gravity 2.576 Aggregate Fine 2.733 Marshall Sample The equipments and procedures for preparing the Marshall were referred to ASTM D 1559. Two types of mixtures were prepared which are ACW14 and ACW10, and both of mixtures divided by 3 gradations (fine, medium and coarse) 4.3.1 Sample Preparation Three types of mixtures were prepared by different gradation which is fine, medium and coarse. Three samples were prepared for each bitumen contents which have ranged between 5 – 7% for ACW10 and 4-6% for ACW14, all of this sample in order to obtain the OBC as shown in Appendix D. 4.3.2 Determination of Optimum Bitumen Content Marshall mixtures design method is to obtain the OBC from various asphalt content. OBC were determined using NAPA procedure where the design OBC were determine as the bitumen content required achieving 4% air void (VTM). OBC from Marshall mixture design method for ACW10 Medium was found to be 5.5%, Coarse at 5.1%, Fine at 5.1% and OBC for ACW14 for Medium at 4.4%, Coarse at 4.8% and Fine at 4.3%. The results of OBC of different gradation are summarized in Table 4.5. From the results, the value of OBC for ACW10 is higher than ACW14. It is because aggregate size for ACW 10 is smaller than ACW 14. When the OBC is 58 59 increase, the durability also increases. In term of stability and stiffness, the medium gradation (control mix) shows better result compare to coarse and fine, it is because the stability value increases with increasing asphalt content. VMA decrease to a minimum value and then it increase with increasing asphalt content. This results indicate that for the ACW10 mixes, it increase the durability because the content of bitumen for ACW10 is 5-7. All the graphs for determination of optimum bitumen content at 4% air void were shown in Appendix E. Table 4.5: Optimum Bitumen Content for ACW10 and ACW14 Optimum bitumen Content (OBC) Types Medium (M) Coarse (C) Fine (F) 5.5 4.4 5.1 4.8 5.1 4.3 ACW 10 ACW 14 4.3.3 Theoretical Maximum Density Theoretical Maximum Density test were conducted using the Rice Method at 5% and 6% bitumen content for ACW 14 and ACW 10 each mixes. The TMD tests were conducted twice to verify the results. Size of the sample were determined according to ASTM D 2041 based on the size of largest particle of aggregate in the mixes. The sample weights used in this study were 1500gram. The full results for TMD were shown in Appendix F. 4.3.4 Results of Volumetric Properties Volumetric properties of HMA consist of VMA, VTM and VFB. Based on the result obtained, relationship between volumetric properties (Stability, Stiffness, Flow, VTM and VFB) and Bitumen Content were evaluated. Then from the VTM graph the optimum bitumen content that most improve the HMA mixes were determined. Results indicate all the volumetric properties values obtained for 59 60 modified mixes were almost the same as conventional mix. The values of volumetric properties slightly increased and decreased inconsistently based on size of aggregate gradation but still within the specification range. The rest of the parameters were subjected to the OBC respectively and in compliance with JKR Specification. The results of volumetric properties of OBC are summarizing in Table 4.6(a) and 4.6(b). Table 4.6 (a): Marshall mix design results of the ACW10 mixes Volumetric properties OBC (%) Stability, S (kg) Flow, F (mm) Stiffness (kg/mm) VTM (%) VFB (%) VMA (%) Specification Medium Coarse Fine 5.5 5.1 5.1 13650 12500 13400 > 8000 1.4 2.1 2.1 2.0 – 4.0 mm 9700 5800 6000 > 2000 N/mm 4 4% 4% 3.0% - 5.0% 72 76% 75% 70% - 80% 16.7 15.2 15.1 - (JKR/SPJ/2007) Table 4.6 (b): Marshall mix design results of the ACW14 mixes Volumetric properties OBC (%) Stability, S (kg) Flow, F (mm) Stiffness (kg/mm) VTM (%) VFB (%) VMA (%) Specification Medium Coarse Fine 4.4 4.8 4.3 15250 11700 14400 > 8000 1.3 1.8 1.8 2.0 – 4.0 mm 11500 5700 8100 > 2000 N/mm 4% 4% 4% 3.0% - 5.0% 72% 73% 71% 70% - 80% 14.5 15.2 13.7 - (JKR/SPJ/2007) Adhering to the recommended Bailey ratios produced satisfactory results in terms of volumetric for coarse mixtures. Fine and Medium mixtures however had lower VMA than the current JKR Specification. The results are approved by Bailey definitions which are for large aggregate particles that when placed in a unit volumes create voids. 60 61 Analysis Volumetric Properties Based on R Square Coarse aggregate, which is predominantly a function of the coarse aggregate blend by volume, seems to have the strongest correlations with mixture volumetric. As the Coarse aggregate ratio increases, the smaller size particles in the coarse portion of the aggregate structure become dominant, creating an inverse effect on the main volumetric parameters VMA. As shown in Figure 4.3 strong correlation between VMA and Bitumen Content (R2 for Coarse = 0.9948) in which VMA is increase by having high bitumen content. For Figure 4.4 is the correlation between VMA and Bitumen Content for Coarse (R2 =0.9948). VTM vs Bitumen Content 7 6 VTM (%) 5 R2 = 0.9948 4 VTM (M) R2 = 0.9738 3 VTM ( C) VTM (F) 2 1 R 2 = 0.9418 0 4 5 6 7 8 Bit. Content (%) Figure 4.3: VTM vs Bit. Content for ACW 10 (R Square Result) VTM vs Bitumen Content 7 VTM (% ) 6 R2 = 0.991 5 R2 = 0.9948 4 VTM (M) VTM ( C ) 3 VTM (F) 2 1 R2 = 0.9941 0 3 4 5 6 7 Bit. Content (%) Figure 4.4: VTM vs Bit. Content for ACW 14 (R Square Result) 61 62 As shown in Figure 4.5, strong correlation between VMA and Bitumen Content (R2 for Coarse = 0.983) in which VMA is increase by having high bitumen content. For Figure 4.6 also same which is the correlation between VMA and Bitumen Content for Coarse (R2 = 0.8602) and Medium (R2 =0.8729) in which VMA increase by having high bitumen content. VMA vs Bitumen Content 18 17.5 VMA (%) 17 R2 = 0.7771 16.5 16 VMA (M) VMA ( C ) R2 = 0.983 15.5 VMA (F) 15 R 2 = 0.9037 14.5 14 4 5 6 7 8 Bit. Content (%) Figure 4.5: VMA vs Bit. Content for ACW 10 (R Square Result) VMA vs Bitumen Content 16 R2 = 0.8602 V M A (% ) 15.5 15 VMA (M) 14.5 VMA ( C ) R2 = 0.8729 VMA (F) 14 13.5 R2 = 0.7358 13 3 4 5 6 7 Bit. Content (%) Figure 4.6: VMA vs Bit. Content for ACW 14 (R Square Result) 62 CHAPTER V CONCLUSIONS AND RECOMMENDATIONS 5.1 Conclusions Based on this study, this report documents the findings of an extensive study on design and characterization of asphalt mixtures for use as road pavement material. Several aspects of asphalt mixtures were addressed using laboratory test equipment and technical literature from different information sources. From this limited study, result shows that the OBC for ACW10 is higher more than AWC14, it is because aggregate size for ACW10 is smaller than ACW14. The analysis shows that the results for this study still follow the JKR Specification but still need further study. The findings of this study are summarized as follows: (i) A simplified design approach was recommended in which asphalt mixtures are designed based on an analytical aggregate gradation method and fundamental performance tests that describe the behavior of asphalt mixtures based on sound engineering principles. (ii) The Bailey method provides a rational approach of aggregate blending and evaluation. (iii) Adhering to the currently recommended Bailey ratios, results in terms of volumetric shows that the coarse graded mixtures is more in line with the generally accepted levels of JKR specification. Fine and 64 medium mixtures however, had lower VMA than the current Marshall recommendations. (iv) CA ratio, a gradation parameter from the Bailey method which is predominantly a function of the coarse aggregate blend by volume, seems to have the strongest correlations with mixtures volumetric. The strongest correlation was the VMA. 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Bailey Method for Gradation Selection in Hot-Mix Asphalt Mixture Design, TRB, National Research Council, Washington, D.C.,p 1. 67 APPENDIX A AGGREGATE SIZE DISTRIBUTION AND DETERMINATION OF FILLER ACW 14 MEDIUM Sieve Size ^0.45 (mm) 20.0 14.0 10.0 5 3.35 1.180 0.425 0.150 0.075 3.850 3.279 2.818 2.063 1.723 1.077 0.680 0.426 0.312 Gradation Limit % Passing % Retained Lower Upper 100 100 90 100 76 86 50 62 40 54 18 34 12 24 6 14 4 8 100 95 81 56 47 26 18 10 6 5 14 25 9 21 8 8 4 Passing (g) 1200 1140 972 672 564 312 216 120 72 Pan (gram) Before After = = Before After = = Washed-sieve Analysis 1) Mass of blended aggregates (gram): Aggregate Dust (gram): 2) Mass of blended aggregates (gram): Mass Aggregate Dust (gram): Average Aggregate Dust (gram): Average Filler Content (gram) = Pan - Average Aggregate Dust Antistripping Agent (OPC) = 24 gram (2% * 1200) Weight of pan used (gram) = Average filler content – OPC Total Aggregate Weight (gram) = Filler + Total Agg. Retained Marshall Mass Mass Retained Retained on Each Sieve (g) (g) 0 0 60 60 228 168 528 300 636 108 888 252 984 96 1080 96 1128 48 72 Gram 1128.8 1110.6 18.2 1130.6 1112.7 17.9 18.05 53.95 24 29.95 1181.95 Mass Passing (g) 1500 1425 1215 840 705 390 270 150 90 Before After = = Before After = = TMD(1500) Mass Mass Retained Retained on each Sieve (g) (g) 0 0 75 75 285 210 660 375 795 135 1110 315 1230 120 1350 120 1410 60 90 1410 1387.3 22.7 1410 1387.7 22.3 22.5 67.5 30 37.5 1477.5 68 AGGREGATE SIZE DISTRIBUTION AND DETERMINATION OF FILLER ACW 10MEDIUM Sieve Size ^0.45 (mm) 14.0 10.0 5 3.35 1.180 0.425 0.150 0.075 3.279 2.818 2.063 1.723 1.077 0.680 0.426 0.312 Gradation Limit Lower 100 90 58 48 22 12 6 4 Upper 100 100 72 64 40 26 14 8 Washed-sieve Analysis 1) Mass of blended aggregates (gram): Aggregate Dust (gram): 2) Mass of blended aggregates (gram): % Passing % Retained 100 95 65 56 31 19 10 6 5 14 25 9 21 8 8 4 Mass Passing (g) 1200 1140 780 672 372 228 120 72 Pan (gram) Before After = = Before After = = Aggregate Dust (gram): Average Aggregate Dust (gram): Average Filler Content (gram) = Pan - Average Aggregate Dust Antistripping Agent (OPC) = 24 gram (2% * 1200) Weight of pan used (gram) = Average filler content – OPC Total Aggregate Weight (gram) = Filler + Total Agg. Retained Marshall Mass Retained (g) 0 60 420 528 828 972 1080 1128 72 1129.3 1111 18.3 1128.2 1110.7 17.5 17.9 54.1 24 30.1 1182.1 TMD(1500) Mass Mass Retained Mass Retained Mass on Each Sieve (g) 0 60 360 108 300 144 108 48 gram Passing (g) 1500 1425 975 840 465 285 150 90 Pan(gram) Retained (g) 0 75 525 660 1035 1215 1350 1410 90 Before After = = Before After = = 1410 1387.1 22.9 1410 1388.2 21.8 22.4 67.7 30 37.7 1477.7 on each Sieve (g) 0 75 450 135 375 180 135 60 gram 69 AGGREGATE SIZE DISTRIBUTION AND DETERMINATION OF FILLER ACW 14COARSE Sieve Size ^0.45 (mm) 20.0 14.0 10.0 5 3.35 1.180 0.425 0.150 0.075 3.850 3.279 2.818 2.063 1.723 1.077 0.680 0.426 0.312 Gradation Limit Lower 100 90 76 50 40 18 12 6 4 Upper 100 100 86 62 54 34 24 14 8 Washed-sieve Analysis 1) Mass of blended aggregates (gram): Aggregate Dust (gram): 2) Mass of blended aggregates (gram): % Passing % Retained 100 98 85 51 40 20 13 9 6 2 13 34 11 20 7 4 3 Mass Passing (g) 1200 1176 1020 612 480 240 156 108 72 Pan (gram) Before After = = Before After = = Aggregate Dust (gram): Average Aggregate Dust (gram): Average Filler Content (gram) = Pan - Average Aggregate Dust Antistripping Agent (OPC) = 24 gram (2% * 1200) Weight of pan used (gram) = Average filler content - OPC Total Aggregate Weight (gram) = Filler + Total Agg. Retained Marshall Mass Mass Retained Mass Passing (g) 1500 1470 1275 765 600 300 195 135 90 Retained (g) 0 24 180 588 720 960 1044 1092 1128 72 on Each Sieve (g) 0 24 156 408 132 240 84 48 36 gram 1129.3 1113.4 15.9 1128.6 1112.9 15.7 15.8 56.2 24 32.2 1184.2 Before After = = Before After = = TMD(1500) Mass Mass Retained Retained (g) 0 30 225 735 900 1200 1305 1365 1410 90 on each Sieve (g) 0 30 195 510 165 300 105 60 45 1410.7 1390.3 20.4 1410.2 1387.8 22.4 21.4 68.6 30 38.6 1478.6 70 AGGREGATE SIZE DISTRIBUTION AND DETERMINATION OF FILLER ACW 10COARSE Sieve Size ^0.45 (mm) 14.0 10.0 5 3.35 1.180 0.425 0.150 0.075 3.279 2.818 2.063 1.723 1.077 0.680 0.426 0.312 Gradation Limit Lower 100 90 58 48 22 12 6 4 Upper 100 100 72 64 40 26 14 8 Washed-sieve Analysis 1) Mass of blended aggregates (gram): Aggregate Dust (gram): 2) Mass of blended aggregates (gram): % Passing % Retained 100 97 60 49 24 15 9 6 0 3 37 11 25 9 6 3 Mass Passing (g) 1200 1164 720 588 288 180 108 72 Pan (gram) Marshall Mass Mass Retained Retained on Each Sieve (g) (g) 0 0 36 36 480 444 612 132 912 300 1020 108 1092 72 1128 36 72 gram Mass Passing (g) 1500 1455 900 735 360 225 135 90 Pan(gram) TMD(1500) Mass Mass Retained Retained (g) on each Sieve (g) 0 0 45 45 600 555 765 165 1140 375 1275 135 1365 90 1410 45 90 gram Before After = = 1128 1112.5 15.5 Before After = = 1410 1390.2 19.8 Before After = = 1128.2 1114.7 13.5 14.5 57.5 Before After = = 1410 1389.2 20.8 20.3 69.7 Aggregate Dust (gram): Average Aggregate Dust (gram): Average Filler Content (gram) = Pan - Average Aggregate Dust Antistripping Agent (OPC) = 24 gram (2% * 1200) Weight of pan used (gram) = Average filler content - OPC Total Aggregate Weight (gram) = Filler + Total Agg. Retained 24 33.5 1185.5 30 39.7 1479.7 71 AGGREGATE SIZE DISTRIBUTION AND DETERMINATION OF FILLER ACW 14FINE Sieve Size ^0.45 (mm) 20.0 14.0 10.0 5 3.35 1.180 0.425 0.150 0.075 3.850 3.279 2.818 2.063 1.723 1.077 0.680 0.426 0.312 Gradation Limit % % Passing Retained Lower Upper 100 100 90 100 76 86 50 62 40 54 18 34 12 24 6 14 4 8 Washed-sieve Analysis 1) Mass of blended aggregates (gram): Aggregate Dust (gram): 2) Mass of blended aggregates (gram): 100 92 79 54 48 31 20 12 6 8 13 25 6 17 11 8 6 Mass Passing (g) 1200 1104 948 648 576 372 240 144 72 Pan (gram) Before After = = Before After = = Aggregate Dust (gram): Average Aggregate Dust (gram): Average Filler Content (gram) = Pan - Average Aggregate Dust Antistripping Agent (OPC) = 24 gram (2% * 1200) Weight of pan used (gram) = Average filler content – OPC Total Aggregate Weight (gram) = Filler + Total Agg. Retained Marshall Mass Mass Retained Retained on Each Sieve (g) (g) 0 0 96 96 252 156 552 300 624 72 828 204 960 132 1056 96 1128 72 72 gram 1128 1108.1 19.9 1128 1108.7 19.3 19.6 52.4 24 28.4 1180.4 Mass Passing (g) 1500 1380 1185 810 720 465 300 180 90 Before After = = Before After = = TMD(1500) Mass Mass Retained Retained (g) on each Sieve (g) 0 0 120 120 315 195 690 375 780 90 1035 255 1200 165 1320 120 1410 90 90 1410 1381.0 29.0 1410 1383.7 26.3 27.7 62.4 30 32.4 1472.4 72 AGGREGATE SIZE DISTRIBUTION AND DETERMINATION OF FILLER ACW 10FINE Sieve Size ^0.45 (mm) 14.0 10.0 5 3.35 1.180 0.425 0.150 0.075 3.279 2.818 2.063 1.723 1.077 0.680 0.426 0.312 Gradation Limit % % Passing Retained Lower Upper 100 100 90 100 58 72 48 64 22 40 12 26 6 14 4 8 Washed-sieve Analysis 1) Mass of blended aggregates (gram): Aggregate Dust (gram): 2) Mass of blended aggregates (gram): 100 91 68 60 36 23 12 6 0 9 23 8 24 13 11 6 Mass Passing (g) 1200 1092 816 720 432 276 144 72 Pan (gram) Before After = = Before After = = Aggregate Dust (gram): Average Aggregate Dust (gram): Average Filler Content (gram) = Pan - Average Aggregate Dust Antistripping Agent (OPC) = 24 gram (2% * 1200) Weight of pan used (gram) = Average filler content – OPC Total Aggregate Weight (gram) = Filler + Total Agg. Retained Marshall Mass Mass Retained Retained on Each Sieve (g) (g) 0 0 108 108 384 276 480 96 768 288 924 156 1056 132 1128 72 72 gram 1128 1110.3 17.7 1128 1110.1 17.9 17.8 54.2 24 30.2 1182.2 Mass Passing (g) 1500 1365 1020 900 540 345 180 90 Pan(gram) Before After = = Before After = = TMD(1500) Mass Mass Retained Retained (g) on each Sieve (g) 0 0 135 135 480 345 600 120 960 360 1155 195 1320 165 1410 90 90 gram 1410 1385.5 24.5 1410 1386.1 23.9 24.2 65.8 30 35.8 1475.8 73 APPENDIX B WASH SIEVE ANALYSIS (ACW 14-MEDIUM MIX) Mix Marshall TMD Sample 1 2 1 2 Mass before washing, (g) 1128.8 1130.6 1410 1410 Mass after washing, (g) 1110.6 1112.7 1387.3 1387.7 Mass of Dust, (g) 18.2 17.9 22.7 22.3 Average, (g) 18.05 22.5 WASH SIEVE ANALYSIS (ACW 10-MEDIUM MIX) Mix Marshall TMD Sample 1 2 1 2 Mass before washing, (g) 1129.3 1128.2 1410 1410 Mass after washing, (g) 1111 1110.7 1387.1 1388.2 Mass of Dust, (g) 18.3 17.5 22.9 21.8 Average, (g) 17.9 22.4 74 WASH SIEVE ANALYSIS (ACW 14-COARSE MIX) Mix Marshall TMD Sample 1 2 1 2 Mass before washing, (g) 1129.3 1128.6 1410.7 1410.2 Mass after washing, (g) 1113.4 1112.9 1390.3 1387.8 Mass of Dust, (g) 15.9 15.7 20.4 22.4 Average, (g) 15.8 21.4 WASH SIEVE ANALYSIS (ACW 10-COARSE MIX) Mix Marshall TMD Sample 1 2 1 2 Mass before washing, (g) 1128 1128.2 1410 1410 Mass after washing, (g) 1112.5 1114.7 1390.2 1389.2 Mass of Dust, (g) 15.5 13.5 19.8 20.8 Average, (g) 14.5 20.3 75 WASH SIEVE ANALYSIS (ACW 14-FINE MIX) Mix Marshall TMD Sample 1 2 1 2 Mass before washing, (g) 1128 1128 1410 1410 Mass after washing, (g) 1108.1 1108.7 1381.0 1383.7 Mass of Dust, (g) 19.9 19.3 29.0 26.3 Average, (g) 19.6 27.65 WASH SIEVE ANALYSIS (ACW 10-FINE MIX) Mix Marshall TMD Sample 1 2 1 2 Mass before washing, (g) 1128 1128 1410 1410 Mass after washing, (g) 1110.3 1110.1 1385.5 1386.1 Mass of Dust, (g) 17.7 17.9 24.5 23.9 Average, (g) 17.8 24.2 76 APPENDIX C SPECIFIC GRAVITY FOR COARSE AGGREGATE (MRP – ACW 14) Coarse Aggregate In Water Saturated Surface Dry (SSD) Ovendry Ovendry SG Bulk, Gsb = SSD − InWater SSD SG SSD, Gssd = SSD − InWater Ovendry Sg Apparent, Gsa = Ovendry − InWater SSD − Ovendry Absorbtion, % = Ovendry Sample 1 616 1000.9 992.2 Sample 2 615.4 1000.1 990.6 Average 2.578 2.575 2.576 2.600 2.600 2.600 2.637 2.640 2.639 0.877 0.959 0.918 AGGREGATE GRADATION FOR COARSE AGGREGATE (MRP – ACW 14) Coarse (gram) 1000 Sieve Size (mm) % Retained Mass Retained (g) 14 5 113.6 10 14 318.2 5 25 568.2 77 SPECIFIC GRAVITY FOR COARSE AGGREGATE (MRP – ACW 10) Coarse Aggregate In Water Saturated Surface Dry (SSD) Ovendry Ovendry SG Bulk, Gsb = SSD − InWater SSD SG SSD, Gssd = SSD − InWater Ovendry Sg Apparent, Gsa = Ovendry − InWater SSD − Ovendry Absorbtion, % = Ovendry Sample 1 617.2 1001.7 992.2 Sample 2 616.1 1001.6 993 Average 2.580 2.576 2.578 2.605 2.598 2.602 2.646 2.635 2.640 0.957 0.866 0.912 AGGREGATE GRADATION FOR COARSE AGGREGATE (MRP – ACW 10) Coarse (gram) 1000 Sieve Size (mm) % Retained Mass Retained (g) 10 5 142.9 5 30 857.1 78 SPECIFIC GRAVITY FOR FINE AGGREGATE (MRP – ACW 14) Fine Aggregate-500g Picnometer Picnometer + Water (600ml) Picnometer + Water (600ml) + Sample Saturated Surface Dry (SSD) Ovendry B C S A Sample 1 280.4 854.9 1181.2 500.3 493.3 Sample 2 280.4 863.4 1177.7 500.4 489.8 Sample 1 Sample 2 Average SG Bulk, Gsb = A B+S–C 2.835 0.032 2.632 2.739 2.733 SG Bulk, Gssd = S B+S–C 2.875 0.027 2.689 2.763 2.782 SG Apparent, Gsa = = 2.954 0.027 1.419 0.310 2.791 2.814 2.164 2.872 Absorption, % A A+B–C S–A A SG BlendedBulk = 100 % Coarse 2.662 + SGbulk Coarse SG BlendedApparent = % Fine SGbulk Fine 100 % Coarse SGapp Coarse 1.792 2.765 + % Fine SGapp Fine 79 SPECIFIC GRAVITY FOR FINE AGGREGATE (MRP – ACW 10) Fine Aggregate-500g Picnometer Picnometer + Water (600ml) Picnometer + Water (600ml) + Sample Saturated Surface Dry (SSD) Ovendry SG Bulk, Gsb = A B+S–C SG Bulk, Gssd = S B+S–C SG Apparent, Gsa = Absorption, % = A A+B–C S–A A SG BlendedBulk = B C S A Sample 1 2.357 0.032 2.391 0.027 2.441 0.027 1.461 0.310 100 % Coarse = + SGapp Coarse Sample 2 2.792 2.739 2.831 2.763 2.907 2.814 1.420 Average 2.574 2.611 2.674 1.440 % Fine SGbulk Fine 100 % Coarse Sample 2 280.4 858.3 1181.7 500.0 493 2.576 SGbulk Coarse SG BlendedApparent Sample 1 280.4 875.9 1166.8 500 492.8 2.662 + % Fine SGapp Fine 80 AGGREGATE GRADATION FOR FINE AGGREGATE (MRP-ACW 14) Fine (gram) 700 Sieve Size (mm) 3.35 % Retained 9 Mass Retained (g) 180 1.18 21 420 0.425 8 160 0.15 8 160 0.075 4 80 AGGREGATE GRADATION FOR FINE AGGREGATE (MRP-ACW 10) Fine (gram) 700 Sieve Size (mm) 3.35 % Retained 9 Mass Retained (g) 153 1.18 25 424 0.425 12 203 0.15 9 153 0.075 4 68 81 APPENDIX D: MARSHALL TEST RESULT (ACW 10-MEDIUM) % BIT % BIT. SPEC. SPEC. NO. NO. a b WEIGHT (gram) SSD c BULK SPEC. GRAV. IN IN VOL. MAX. AIR WATER cc. BULK THEOR. BIT AGG. VOIDS d e f g h i j % Bit. by wt. VOLUME - % TOTAL d bxg (100-b)g c-e f SGbit SGag VOIDS (%) FILLED TOTAL AGG. (BIT) MIX k l m n 100-i-j 100-j 100(i/l) 100-(100g/h) STABILITY (kg) FLOW MEAS. CORR. (mm) p q r o Corr. STIFFNESS s q Factor Pxo r of mix. 5.0 1204.0 1202.8 671.2 532.8 2.258 0.96 14213 13645 1.09 1228.9 1227.2 685.8 543.1 2.260 0.93 14267 13268 1.42 1223.9 1222.5 683.7 540.2 2.263 0.93 14267 13268 1.78 13394 1.43 2.260 AVG 5.5 17.2 63.9 6.2 690.2 541.0 2.273 0.93 15512 14426 1.56 1226.1 688.0 539.4 2.273 0.93 15763 14659 1.21 1226.4 1222.1 686.4 540.0 2.263 0.93 15763 14659 1.48 14582 1.42 2.393 12.1 82.8 5.1 17.2 70.3 5.2 1231.7 1230.9 705.0 526.7 2.337 0.96 14819 14226 0.97 1229.5 1228.6 696.7 532.8 2.306 0.96 14505 13925 1.66 1234.0 1233.3 701.7 532.3 2.317 0.96 15085 14481 1.41 14211 1.35 1237.5 1236.7 704.0 533.5 2.318 0.96 14471 13892 1.41 1252.1 1251.7 721.0 531.1 2.357 0.96 14520 13939 1.41 1236.3 1235.8 704.9 531.4 2.326 0.96 15462 14843 1.22 14225 1.35 1241.9 1241.7 710.1 531.8 2.335 0.96 14766 14176 1.35 1247.3 1246.9 715.1 532.2 2.343 0.96 15109 14504 1.40 1244.6 1244.0 712.7 531.9 2.339 0.96 15379 14764 1.39 14481 1.38 2.320 2.333 AVG AVG 6.2 1229.7 AVG 7.0 82.8 1227.4 2.270 6.5 11.0 1231.2 AVG 6.0 2.410 2.339 2.376 2.360 2.343 13.5 14.7 15.9 84.1 84.2 83.9 2.4 1.1 0.2 15.9 15.8 16.1 85.2 93.1 98.8 2.4 1.1 0.2 9366.3 10292.9 10552.6 10562.9 10493.7 82 MARSHALL TEST RESULT (ACW 14-MEDIUM)) % BIT % BIT. SPEC. SPEC. NO. NO. a b WEIGHT (gram) SSD c BULK SPEC. GRAV. VOLUME - % TOTAL IN IN VOL. AIR WATER cc. BULK THEOR. BIT AGG. VOIDS d e f g h i j % Bit. by wt. VOIDS (%) MAX. d bxg (100-b)g c-e f SGbit SGag 530.4 529.3 531.2 2.295 2.311 2.301 2.302 2.322 2.323 2.334 2.326 2.359 2.352 2.350 2.353 2.365 2.371 2.378 2.371 2.333 2.371 2.375 2.360 STABILITY (kg) FILLED TOTAL AGG. (BIT) MIX k l m n 100-i-j 100-j 100(i/l) 100-(100g/h) o FLOW MEAS. CORR. (mm) p q r Corr. STIFFNESS s Q Factor Pxo R of mix. 4.0 1219.5 1224.9 1224.2 1217.3 1223.3 1222.3 689.1 695.6 693.0 AVG 4.5 1230.9 1232.6 1230.6 1229.4 1231.7 1229.7 701.5 702.3 703.8 529.4 530.3 526.8 5.0 1237.8 1243.6 1238.1 1237.0 1242.2 1237.4 713.4 715.4 711.5 524.4 528.2 526.6 5.5 1247.1 1238.1 1246.2 1246.3 1237.8 1245.7 720.1 716.1 722.3 527.0 522.0 523.9 AVG AVG AVG 6.0 AVG 1248.0 1246.2 1248.2 1247.4 1245.9 1247.5 713.4 720.7 723.0 534.6 525.5 525.2 0.96 0.96 0.96 2.450 2.432 2.415 2.398 8.9 10.2 11.4 12.7 85.0 85.5 86.0 86.2 6.0 4.4 2.5 1.1 15.0 14.5 14.0 13.8 59.8 70.0 81.8 91.9 6.0 0.96 0.96 0.96 15693 16676 16032 0.96 0.96 0.96 15334 15139 15661 0.96 1.00 0.96 14021 14878 14369 4.3 2.5 1.1 0.96 0.96 0.96 2.381 13.7 85.3 0.9 14.7 93.8 14858 15465 15979 0.9 11535 13513 13802 14264 14846 15340 14817 15065 16009 15390 15488 14721 14533 15035 14763 13460 14878 13794 14044 11074 12972 13250 12432 2.24 1.38 1.59 1.74 1.35 1.06 1.31 1.24 1.14 1.55 1.49 1.39 1.85 1.61 1.38 1.61 2.30 1.85 1.41 1.85 8531.8 12490.4 10595.4 8705.1 6707.9 83 MARSHALL TEST RESULT (ACW 14-COARSE) % BIT % BIT. SPEC. SPEC. NO. NO. a b WEIGHT (gram) SSD c BULK SPEC. GRAV. VOLUME - % TOTAL IN IN VOL. AIR WATER cc. BULK THEOR. BIT AGG. VOIDS d e f g h i j % Bit. by wt. VOIDS (%) MAX. d bxg (100-b)g c-e f SGbit SGag 540.9 537.2 541.4 2.273 2.289 2.277 2.280 2.303 2.300 2.297 2.300 2.308 2.319 2.329 2.319 2.338 2.350 2.338 2.342 2.343 2.346 2.348 2.345 STABILITY (kg) FILLED TOTAL AGG. (BIT) MIX k l m n 100-i-j 100-j 100(i/l) 100-(100g/h) o FLOW MEAS. CORR. (mm) p q r Corr. STIFFNESS s Q Factor pxo R of mix. 4.0 1237.5 1234.0 1240.4 1229.3 1229.6 1232.8 696.6 696.8 699.0 AVG 4.5 1237.8 1239.8 1235.4 1235.5 1235.7 1232.5 701.4 702.6 698.8 536.4 537.2 536.6 5.0 1240.3 1241.7 1241.6 1239.2 1240.6 1240.5 703.5 706.7 709.0 536.8 535.0 532.6 5.5 1244.5 1245.9 1247.5 1244.1 1245.5 1247.1 712.3 715.9 714.1 532.2 530.0 533.4 AVG AVG AVG 6.0 AVG 1248.2 1250.6 1247.4 1247.5 1250.2 1247.0 715.7 717.7 716.2 532.5 532.9 531.2 0.89 0.89 0.89 2.449 2.432 2.415 2.398 8.9 10.0 11.3 12.5 84.2 84.5 84.8 85.2 6.9 5.4 4.0 2.3 15.8 15.5 15.2 14.8 56.0 64.9 73.9 84.2 6.9 0.89 0.89 0.89 13102 13459 13020 0.89 0.96 0.96 12475 12016 12570 0.96 0.96 0.96 12407 12674 11898 5.4 4.0 2.3 0.96 0.96 0.96 2.381 13.7 84.8 1.5 15.2 90.1 12095 13566 13153 1.5 11967 11498 11958 10764 12074 11706 11515 11661 11978 11587 11742 11103 11535 12067 11568 11911 12167 11422 11833 11488 11039 11479 11335 1.77 1.65 1.66 1.69 1.87 1.84 1.92 1.88 2.15 2.30 2.10 2.18 2.20 2.33 2.58 2.37 2.79 2.95 3.10 2.95 6800.0 6256.9 5298.4 4992.9 3846.9 84 MARSHALL TEST RESULT (ACW 10-COARSE) % BIT % BIT. SPEC. SPEC. NO. NO. a b WEIGHT (gram) SSD c BULK SPEC. GRAV. VOLUME - % TOTAL IN IN VOL. AIR WATER cc. BULK THEOR. BIT AGG. VOIDS d e f g h i j % Bit. by wt. VOIDS (%) MAX. d bxg (100-b)g c-e f SGbit SGag 540.6 537.9 536.7 2.328 2.343 2.312 2.328 2.350 2.329 2.335 2.338 2.344 2.353 2.353 2.350 2.351 2.328 2.359 2.346 2.330 2.356 2.347 2.344 STABILITY (kg) FILLED TOTAL AGG. (BIT) MIX k l m n 100-i-j 100-j 100(i/l) 100-(100g/h) o FLOW MEAS. CORR. (mm) p q r Corr. STIFFNESS s Q Factor pxo R of mix. 5.0 1260.4 1261.1 1242.0 1258.6 1260.5 1241.1 719.8 723.2 705.3 AVG 5.5 1273.9 1248.4 1249.5 1273.4 1247.7 1249.0 732.1 712.7 714.5 541.8 535.7 535.0 6.0 1252.5 1252.6 1246.2 1252.1 1252.2 1245.8 718.4 720.4 716.7 534.1 532.2 529.5 6.5 1263.5 1261.5 1262.9 1258.8 1258.4 1258.3 728.1 721.0 729.5 535.4 540.5 533.4 AVG AVG AVG 7.0 AVG 1281.9 1290.6 1282.1 1281.0 1290.2 1281.4 732.1 743.0 736.1 549.8 547.6 546.0 0.89 0.89 0.89 2.422 2.405 2.388 2.371 11.3 12.5 13.7 14.8 84.8 84.7 84.7 84.1 3.9 2.8 1.6 1.1 15.2 15.3 15.3 15.9 74.4 81.7 89.5 93.2 3.9 0.89 0.89 0.96 14653 13213 13386 0.96 0.96 0.96 13134 12795 12852 0.96 1.00 1.00 12315 11829 12330 2.8 1.6 1.0 0.89 0.89 0.89 2.355 15.9 83.6 0.5 16.4 97.1 14065 13702 13958 0.5 11734 12228 11462 12518 12194 12423 12378 13041 11760 12850 12550 12609 12283 12338 12410 11822 11829 12330 11994 10443 10883 10201 10509 1.87 2.30 2.04 2.07 1.92 2.48 2.33 2.24 2.40 2.73 2.87 2.67 2.68 2.55 2.65 2.63 3.26 3.19 3.40 3.28 5979.9 5594.5 4653.8 4566.1 3200.8 85 MARSHALL TEST RESULT (ACW 14-FINE) % BIT % BIT. SPEC. SPEC. NO. NO. A b WEIGHT (gram) SSD c BULK SPEC. GRAV. VOLUME - % TOTAL IN IN VOL. AIR WATER cc. BULK THEOR. BIT AGG. VOIDS d e f g h i j % Bit. by wt. VOIDS (%) MAX. d bxg (100-b)g c-e f SGbit SGag 522.1 527.6 525.0 2.337 2.337 2.337 2.337 2.348 2.354 2.350 2.351 2.371 2.367 2.369 2.369 2.382 2.380 2.381 2.381 2.376 2.380 2.379 2.378 STABILITY (kg) FILLED TOTAL AGG. (BIT) MIX k l m n 100-i-j 100-j 100(i/l) 100-(100g/h) o FLOW MEAS. CORR. (mm) p q r Corr. STIFFNESS s Q Factor pxo R of mix. 4.0 1223,2 1234.2 1228.5 1220.1 1233.2 1226.7 701.1 706.6 703.5 AVG 4.5 1230.1 1233.8 1234.4 1228.3 1232.3 1232.5 707.0 710.3 710.0 523.1 523.5 524.4 5.0 1238.4 1238.3 1238.7 1237.5 1236.8 1237.9 716.4 715.8 716.1 522.0 522.5 522.6 5.5 1246.3 1242.4 1244.3 1245.6 1241.8 1243.7 723.3 720.7 721.9 523.0 521.7 522.4 AVG AVG AVG 6.0 AVG 1247.8 1245.9 1246.9 1247.0 1245.5 1246.6 723.0 722.5 722.8 524.8 523.4 524.1 1.00 0.96 0.96 2.453 2.436 2.418 2.401 9.1 10.3 11.5 12.7 86.2 86.2 86.5 86.4 4.7 3.5 2.0 0.8 13.8 13.8 13.5 13.6 65.7 74.7 84.9 93.7 4.7 0.96 0.96 0.96 15512 15763 15763 1.00 1.00 1.00 14819 14505 15085 0.96 1.00 1.00 14471 14520 15462 3.5 2.0 0.8 0.96 0.96 0.96 2.384 13.9 85.9 0.3 14.1 98.1 14213 14267 14267 0.2 14766 15109 15379 14213 13696 13696 13869 14891 15132 15132 15052 14819 14505 15085 14803 13892 14520 15462 14624 14176 14504 14764 14481 1.84 1.76 1.68 1.76 1.93 1.53 1.62 1.69 1.81 2.12 2.02 1.98 2.08 2.23 2.12 2.69 2.62 3.09 2.59 2.77 7879.9 8888.9 7463.7 5436.6 5234.2 86 MARSHALL TEST RESULT (ACW 10-FINE) % BIT % BIT. SPEC. SPEC. NO. NO. A b WEIGHT (gram) SSD c BULK SPEC. GRAV. VOLUME - % TOTAL IN IN VOL. AIR WATER cc. BULK THEOR. BIT AGG. VOIDS d e f g h i j % Bit. by wt. VOIDS (%) MAX. d bxg (100-b)g c-e f SGbit SGag 533.5 530.8 533.0 2.310 2.321 2.318 2.316 2.346 2.344 2.345 2.345 2.353 2.349 2.349 2.350 2.354 2.329 2.323 2.336 2.344 2.339 2.340 2.341 STABILITY (kg) FILLED TOTAL AGG. (BIT) MIX k l m n 100-i-j 100-j 100(i/l) 100-(100g/h) o FLOW MEAS. CORR. (mm) p q r Corr. STIFFNESS s Q Factor pxo R of mix. 5.0 1243.4 1232.5 1242.8 1242.8 1231.2 1242.0 709.9 701.7 709.8 AVG 5.5 1246.2 1249.0 1244.2 1245.7 1248.1 1243.3 715.2 716.5 714.0 531.0 532.5 530.2 6.0 1222.6 1252.4 1249.5 1221.9 1251.8 1249.1 703.2 719.4 717.7 519.4 533.0 531.8 6.5 1252.0 1258.9 1261.4 1255.8 1250.8 1250.5 718.6 721.9 723.1 533.4 537.0 538.3 AVG AVG AVG 7.0 AVG 1256.4 1257.6 1258.1 1252.4 1258.3 1260.8 722.0 719.6 719.2 534.4 538.0 538.9 0.96 0.96 0.96 2.411 2.394 2.377 2.361 11.2 12.5 13.7 14.7 84.8 85.4 85.2 84.2 3.9 2.1 1.2 1.1 15.2 14.6 14.8 15.8 74.1 85.9 92.2 93.2 3.9 0.96 0.96 0.96 14007 14304 14434 1.00 0.96 0.96 12996 13289 12827 0.96 0.89 0.89 11186 11436 11306 2.1 1.1 1.1 0.96 0.96 0.96 2.344 15.9 83.9 0.2 16.1 98.9 12143 15289 13842 0.1 12451 12894 12456 11658 14677 13289 13208 13447 13732 13857 13679 12996 12757 12314 12689 10739 10178 10062 10326 11953 12378 11958 12096 2.19 1.77 2.25 2.07 2.17 2.06 2.85 2.36 2.58 2.60 2.59 2.59 4.09 3.92 3.66 3.89 3.28 3.18 3.21 3.22 6380.6 5796.1 4899.3 2654.6 3752.8 87 APPENDIX E: VOLUMETRIC PROPERTIES OF ACW 14 Flow vs Bitumen Content Density vs Bitumen Content 3 2.400 Density 2.360 Density (M) 2.340 Densit ( C) 2.320 Density(F) 2.300 Flow (mm) 2.380 2.5 Flow (M) 2 Flow( C ) Flow (F) 1.5 2.280 1 2.260 3 4 5 6 3 7 4 Stability vs Bitumen Content 14000 Stability (M) 13000 Stability ( C ) 12000 Stability (F) 11000 10000 5 Bit. Content (%) 6 7 Stiffness (N) Stability (N) 15000 4 6 7 Stiffness vs Bitumen Content 16000 3 5 Bitumen Content (%) Bitumen Content (%) 13000 12000 11000 10000 9000 8000 7000 6000 5000 4000 Stiffness (M) Stiffness ( C ) Stiffness (F) 3 4 5 6 7 Bit Content (%) 88 VMA vs Bitumen Content 7 16 6 15.5 5 VMA (% ) VTM (M) 4 VTM ( C ) 3 VTM (F) 2 15 VMA (M) 14.5 VMA ( C ) VMA (F) 14 13.5 1 0 13 3 4 5 6 3 7 4 5 6 7 Bit. Content (%) Bit. Content (%) VFB vs Bitumen Content 100 90 VFB (%) VTM (% ) VTM vs Bitumen Content VFB (M) 80 VFB ( C ) 70 VFB (F) 60 50 3 4 5 6 7 Bit. Content (%) 89 VOLUMETRIC PROPERTIES OF ACW 10 Flow vs Bitumen Content 4 2.420 2.400 2.380 2.360 2.340 2.320 2.300 2.280 2.260 2.240 3.5 Density(M) Density (C ) Density(F) Flow (mm) Density Density vs Bitumen Content 3 Flow (M) 2.5 Flow( C ) Flow (F) 2 1.5 1 4 5 6 7 4 8 5 Stability vs Bitumen Content Stability (M) 13000 Stability ( C ) 12000 Stability (F) 11000 10000 Bit. Content (%) 7 8 Stiffness (N) Stability (N) 14000 6 8 Stiffness vs Bitumen Content 15000 5 7 Bitumen Content (%) Bitumen Content (%) 4 6 11000 10000 9000 8000 7000 6000 5000 4000 3000 2000 Stiffness (M) Stiffness ( C ) Stiffness (F) 4 5 6 7 8 Bit. Content (%) 90 VMA vs Bitumen Content 18 6 17.5 5 17 16.5 VTM (M) 4 VTM ( C) 3 VTM (F) 2 VMA (%) 7 VMA (M) 16 VMA ( C ) 15.5 VMA (F) 15 14.5 1 14 0 4 5 6 7 4 8 5 6 7 8 Bit. Content (%) Bit. Content (%) VFB vs Bitumen Content VFB (%) VTM (%) VTM vs Bitumen Content 100 95 90 85 80 75 70 65 60 VFB (M) VFB ( C ) VFB (F) 4 5 6 7 8 Bit. Content (%) 91 APPENDIX F: DETERMINATION OF OBC AT 4% AIR VOID (NAPA) FOR ACW 10 VTM vs Bitumen Content(ACW10-FINE) VTM vs Bitumen Content(ACW10-COARSE) 6 5 5 VTM Power (VTM) 2 VTM 4 3 VTM 3 Power (VTM) 2 1 1 0 0 4 5 6 7 4 8 5 6 7 8 Bitumen Content (%) Bitumen Content (%) VTM vs Bitumen Content(ACW10-MEDIUM) 7 6 5 VTM VTM 4 4 VTM 3 Power (VTM) 2 1 0 4 5 6 7 8 Bitumen Content (%) 92 DETERMINATION OF OBC AT 4% AIR VOID (NAPA) FOR ACW 14 VTM vs Bitumen Content(ACW14-FINE) 5 8 7 6 5 4 3 2 1 0 VTM Pow er (VTM) VTM 4 3 VTM 2 Pow er (VTM) 1 0 3 4 5 6 7 3 4 Bitum en Content (%) 5 6 7 Bitumen Content (%) VTM vs Bitumen Content(ACW14-MEDIUM) VTM VTM VTM vs Bitumen Content(ACW14-COARSE) 7 6 5 4 3 2 1 0 VTM Pow er (VTM) 3 4 5 6 7 Bitum en Content (%) 93 APPENDIX G THEORETICAL MAXIMUM DENSITY FOR ACW 14-MEDIUM MAXIMUM SPECIFIC GRAVITY OF BITUMINOUS PAVING MIXTURES MEDIUM Weight of Bowl in Air (gm) Weight of Bowl in Water (gm) Weight of Bowl and Sample in Air (gm) Weight of Sample (gm) Weight of Bowl and Sample in Water (gm) Asphalt Content of Mix (%) A B C D = (C - A) E G Sample 1 2207.4 1390 3753 1545.6 2296.4 5 Sample 2 2207.4 1389.9 3756.7 1549.3 2296.9 5 = = = = = = SG of Asphalt, Gb = H 1.03 1.03 (F) Max SG of Mix, Gmm = D 2.418 2.412 2.603 2.595 2.450 2.432 2.415 2.398 2.381 OBC=5% Average D+B-E Effective SG of Aggregate, Gse = 100 - G 2.599 (100/F) - (G/H) Gmm at specified of % AC's 4 4.5 5 5.5 6 = 100 (%AC/Gb) + [(100 %AC)/Gse] 94 THEORETICAL MAXIMUM DENSITY FOR ACW10-MEDIUM MAXIMUM SPECIFIC GRAVITY OF BITUMINOUS PAVING MIXTURES MEDIUM Weight of Bowl in Air (gm) Weight of Bowl in Water (gm) Weight of Bowl and Sample in Air (gm) Weight of Sample (gm) Weight of Bowl and Sample in Water (gm) Asphalt Content of Mix (%) = = = = A B C D = (C - A) Sample 1 2207.4 1390 3770.2 1562.8 = = E G 2291.1 6 2298.3 6 SG of Asphalt, Gb = H 1.03 1.03 (F) Max SG of Mix, Gmm = D D+B-E 2.362 2.390 Effective SG of Aggregate, Gse = 100 - G (100/F) - (G/H) 2.574 2.610 Gmm at specified of % AC's = 100 (%AC/Gb) + [(100 %AC)/Gse] 2.410 2.393 2.376 2.360 2.343 OBC=6% 5 5.5 6 6.5 7 Sample 2 2207.4 1390.7 3767.8 1560.4 Average 2.592 95 THEORETICAL MAXIMUM DENSITY FOR ACW14-COARSE MAXIMUM SPECIFIC GRAVITY OF BITUMINOUS PAVING MIXTURES MEDIUM Weight of Bowl in Air (gm) Weight of Bowl in Water (gm) Weight of Bowl and Sample in Air (gm) Weight of Sample (gm) Weight of Bowl and Sample in Water (gm) A B C D = (C - A) E Sample 1 2207.4 1390 3755.9 1548.5 2300 Sample 2 2207.4 1390 3755.7 1548.3 2294.3 = = = = = Asphalt Content of Mix (%) = G 5 5 SG of Asphalt, Gb = H 1.03 1.03 (F) Max SG of Mix, Gmm = D 2.425 2.404 2.611 2.586 2.449 2.432 2.415 2.398 2.381 OBC=5% Average D+B-E Effective SG of Aggregate, Gse = 100 - G 2.599 (100/F) - (G/H) Gmm at specified of % AC's 4 4.5 5 5.5 6 = 100 (%AC/Gb) + [(100 - %AC)/Gse] 96 THEORETICAL MAXIMUM DENSITY FOR ACW10-COARSE MAXIMUM SPECIFIC GRAVITY OF BITUMINOUS PAVING MIXTURES MEDIUM Weight of Bowl in Air (gm) Weight of Bowl in Water (gm) Weight of Bowl and Sample in Air (gm) Weight of Sample (gm) Weight of Bowl and Sample in Water (gm) Asphalt Content of Mix (%) A B C D = (C - A) E G Sample 1 2207.4 1390.3 3817.8 1610.4 2326.2 6 Sample 2 2207.4 1390.5 3819.3 1611.9 2327.6 6 = = = = = = SG of Asphalt, Gb = H 1.03 1.03 (F) Max SG of Mix, Gmm = D D+B-E 2.388 2.389 Effective SG of Aggregate, Gse = 100 - G (100/F) - (G/H) 2.607 2.608 Gmm at specified of % AC's = 100 2.422 2.405 2.388 2.371 2.355 OBC=6% 5 5.5 6 6.5 7 (%AC/Gb) + [(100 - %AC)/Gse] Average 2.608 97 THEORETICAL MAXIMUM DENSITY FOR ACW14-FINE MAXIMUM SPECIFIC GRAVITY OF BITUMINOUS PAVING MIXTURES MEDIUM Sample 1 Sample 2 Weight of Bowl in Air (gm) = A 2207.4 2207.4 Weight of Bowl in Water (gm) = B 1390 1390 Weight of Bowl and Sample in Air (gm) = C 3717.4 3717.8 Weight of Sample (gm) = D = (C - A) 1510 1510.4 Weight of Bowl and Sample in Water (gm) = E 2275.3 2276.1 Asphalt Content of Mix (%) = G 5 5 SG of Asphalt, Gb = H 1.03 1.03 (F) Max SG of Mix, Gmm = D 2.417 2.419 2.602 2.604 2.453 OBC=5% Average D+B-E Effective SG of Aggregate, Gse = 100 - G 2.603 (100/F) - (G/H) Gmm at specified of % AC's 4 = 100 (%AC/Gb) + [(100 - %AC)/Gse] 4.5 2.436 5 2.418 5.5 2.401 6 2.384 98 THEORETICAL MAXIMUM DENSITY FOR ACW14-FINE MAXIMUM SPECIFIC GRAVITY OF BITUMINOUS PAVING MIXTURES MEDIUM Sample 1 Sample 2 Weight of Bowl in Air (gm) = A 2207.4 2207.4 Weight of Bowl in Water (gm) = B 1390.4 1390.2 Weight of Bowl and Sample in Air (gm) = C 3772 3773.4 Weight of Sample (gm) = D = (C - A) 1564.6 1566 Weight of Bowl and Sample in Water (gm) = E 2296.4 2297.8 Asphalt Content of Mix (%) = G 6 6 SG of Asphalt, Gb = H 1.03 1.03 (F) Max SG of Mix, Gmm = D 2.376 2.378 2.592 2.595 2.411 OBC=6% Average D+B-E Effective SG of Aggregate, Gse = 100 - G 2.594 (100/F) - (G/H) Gmm at specified of % AC's 5 = 100 (%AC/Gb) + [(100 - %AC)/Gse] 5.5 2.394 6 2.377 6.5 2.361 7 2.344 99 APPENDIX H GRADATION LIMIT FOR ACW 10 AND ACW 14 Table 4.1(a): Gradation Limit for ACW 10 (Medium) Sieve Size (mm) Gradation Limit Percentage Passing Percent Retained 14 100 100 0 10 90 – 100 95 5 5 58 – 72 65 30 3.35 48 – 64 56 9 1.18 22 – 40 31 25 0.425 12 - 26 19 12 0.15 6 – 14 10 9 0.075 4-8 6 4 ACW10 (MEDIUM) 120 % Passing 100 80 Lower Limit 60 Upper Limit 40 % Passing Medium 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 ^0.45 Sieve Size Figure 4.1(a): Gradation Limit for ACW 10 (Medium) 100 Table 4.1(b): Gradation Limit for ACW 10 (Coarse) Sieve Size (mm) Gradation Limit Percentage Passing Percent Retained 14 100 100 0 10 90 – 100 97 3 5 58 – 72 60 37 3.35 48 – 64 49 11 1.18 22 – 40 24 25 0.425 12 - 26 15 9 0.15 6 – 14 9 6 0.075 4-8 6 3 ACW 10 (COARSE) 120 % Passing 100 80 Lower Limit Upper Limit 60 % Passing 40 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 ^0.45 Sieve Size Figure 4.1(b): Gradation Limit for ACW 10 (Coarse) 101 Table 4.1(c): Gradation Limit for ACW 10 (Fine) Sieve Size (mm) Gradation Limit Percentage Passing Percent Retained 14 100 100 0 10 90 – 100 91 9 5 58 – 72 68 23 3.35 48 – 64 60 8 1.18 22 – 40 36 24 0.425 12 - 26 23 13 0.15 6 – 14 12 11 0.075 4-8 6 6 ACW 10 (FINE) 120 % Passing 100 80 Lower Limit 60 Upper Limit 40 % Passing 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 ^0.45 Sieve Size Figure 4.1(c): Gradation Limit for ACW 10 (Fine) 102 Table 4.1(d): Gradation Limit for ACW 14 (Medium) Sieve Size (mm) Gradation Limit Percentage Passing Percent Retained 20 100 100 0 14 90 – 100 95 5 10 76 – 86 81 14 5 50 – 62 56 25 3.35 40 – 54 47 9 1.18 18 – 34 26 21 0.425 12 – 24 18 8 0.15 6 – 14 10 8 0.075 4-8 6 4 ACW14 (MEDIUM) 120 % Passing 100 80 Lower Limit 60 Upper Limit 40 % Passing Medium 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 ^0.45 Sieve Size Figure 4.1(d): Gradation Limit for ACW 14 (Medium) 103 Table 4.1(e): Gradation Limit for ACW 14 (Coarse) Sieve Size (mm) Gradation Limit Percentage Passing Percent Retained 20 100 100 0 14 90 – 100 98 2 10 76 – 86 85 13 5 50 – 62 51 34 3.35 40 – 54 40 11 1.18 18 – 34 20 20 0.425 12 – 24 13 7 0.15 6 – 14 9 4 0.075 4-8 6 3 ACW 14 (COARSE) 120 % Passing 100 80 Lower Limit 60 Upper Limit 40 % Passing 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 ^0.45 Sieve Size Figure 4.1(e): Gradation Limit for ACW 14 (Coarse) 104 Table 4.1(f): Gradation Limit for ACW 14 (Fine) Sieve Size (mm) Gradation Limit Percentage Passing Percent Retained 20 100 100 0 14 90 – 100 92 8 10 76 – 86 79 13 5 50 – 62 54 25 3.35 40 – 54 48 6 1.18 18 – 34 31 17 0.425 12 – 24 20 11 0.15 6 – 14 12 8 0.075 4-8 6 6 ACW 14 (FINE) 120 % Passing 100 80 Lower Limit 60 Upper Limit 40 % Pass ing 20 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 ^0.45 Sieve Size Figure 4.1(f): Gradation Limit for ACW 14 (Fine) 105