PERFORMANCE AND EVALUATION OF GRAPHITE WHEN MACHINING HARDENED STEEL ASSAB 718 RADWAN AHMED SAEED AHMED A project report submitted in partial fulfilment of the requirements for the award of the degree of Master of Engineering (Mechanical - Advanced Manufacturing Technology) Faculty of Mechanical Engineering Universiti Teknologi Malaysia NOVEMBER 2009 iii To My Beloved Father, Mother, Wife, Brothers, Sisters and my Daughter Last but not least to all the prayers, courage, and confidence and trust that you all gave to me. May Allah bless all people that I love and it is my honor to share this happiness with my loved ones. iv ACKNOWLEDGMENTS First and foremost, I would like to express my deepest, sincerest gratitude to my supervisors Associate Professor Dr izman sudin and Associate Professor Hamidon Musa for their guidance and advice, without which I would never have been able to accomplish the objectives of my project. Their intelligence and determination have been a source of inspiration, their demands for quality and perfection, a challenge which taught me lessons beyond the reach of my classroom textbook. Secondly, I would like to dedicate my thanks to all the technical staff at Production Lab, Metrology Lab and Material Science Lab especially to En. Ali, En. Aidid, En. Sazali, En.Ayub for lending me their help and support in completing this project. Their time and patience for providing many useful advices and ideas through the trials and tribulations during this project execution are very much appreciated. Lastly, I would also like to express my special thanks to my wife, Mother and my family members for believing in me and continuously supporting me throughout this project. Last but not least, I would like to thank those who have contributed directly or indirectly towards the success of this research study. v ABSTRACT This project presents the machining of ASSAB718 hardened steel using sinker electro-discharge machining involving two different graphite electrodes. POCO EDM4 and POCO EDM200 The main purpose of this study was to investigate the influence of various parameters on the machining characteristics, namely, surface roughness (Ra), Material removal rate (MRR), Electrode wear rate (EWR), and Microcracks depth after undergoing sinker EDM process. The Full Factorial Design of Experiment (DOE) approach with two-levels was used to formulate the experimental plan and, to analyze the effect of each parameter on the machining characteristics four factors under study were pulse interval (A), pulse duration on (R), peak current (P) and servo voltage (SV). Confirmation tests were conducted for the optimum conditions for each machining characteristics in order to verifying and comparing. Design Expert software was utilized to analyze the above results. The, servo voltage and pulse of signal have appeared to be significant to all responses investigated. Overall, the results from the confirmation tests showed that the percentage of performance was acceptable due to all the results obtained were within the allowable value which was less than 11% of margin error for EDM200 and 7.23% for EDM4 electrodes respectively. vi ABSTRAK Projek ini mengkaji pemesinan keluli keras (ASSAB718) menggunakan pemesinan nyahcas elektrik (EDM) melibatkan dua jenis elektrod grafit. Tujuan utama kajian ini ialah untuk mengkaji pengaruh pelbagai parameter dalam EDM pembenam acuan, iaitu kekasaran permukaan (Ra), kadar pembuangan bahan (MRR), kadar kehausan elektod (EWR) dan kedalaman mikrorekahan selepas melalui proses EDM pembenam acuan. Pendekatan reka bentuk eksperimen (DOE) faktoran penuh melibatkan dua aras digunakan untuk menyediakan susun atur eksperimen, untuk menganalisis pengaruh setiap parameter ke atas ciri pemesinan dan untuk menganggarkan penetapan optimum bagi setiap parameter EDM iaitu sela denyutan (A), tempoh denyutan on, (R), arus puncak (P), dan voltan servo (SV). Ujian pengesahan juga dijalankan pada keadaan optimum bagi setiap ciri pemesinan bertujuan untuk membanding dan mengesahkan keputusan anggaran secara teori menggunakan perisian Design Expert. Dalam kajian ini, pemesinan dilakukan menggunakan mesin EDM CNC jenis Roboform 100 (4 paksi). Pengukuran Ra pula menggunakan Mitutoyo Formtracer CS-5000 dan kedalaman mikrorekahan diukur menggunakan Mikroskop Imbasan Elektron XL40. Umumnya, keputusan yang diperolehi menunjukkan yang denyutan on dan arus puncak adalah bererti terhadap kesemua sambutan yang dikaji. Secara keseluruhannya, keputusan ujian pengesahan boleh diterima kerana kesemua hasil memberikan jidar ralat kurang daripada 11%. vii TABLE OF CONTENTS CHAPTER 1 TITLE PAGE DECLARATION ii DEDICATION iii ACKNOWLEDGEMENTS iv ABSTRACT v ABSTRAK vi TABLE OF CONTENTS vii LIST OF TABLES xi LIST OF FIGURES xiii LIST OF SYMBOLS xv LIST OF APPEENDICES xvi INTRODUCTION 1.1 Introduction 1 1.2 Background of the Project 1 1.3 Problem Statement 2 1.4 Objective 3 1.5 Scope 3 1.6 Significance of study 4 1.7 Project Structure 4 viii 2 LITERATURE REVIEW 2.1 Introduction 5 2.2 EDM Die Sinking process: 6 2.2.1 Limitation of EDM 9 2.3 EDM Electrodes 9 2.4 3 2.3.1 Electrodes Material 10 2.3.2 Graphite Material 10 2.3.3 Graphite Grades within Classifications 11 EDM Machining Parameter 16 2.4.1 Discharge voltage: 17 2.5.2 Pulse (On-time) and pulse interval (Off) 18 2.5.3 Polarity 19 2.5.4 Electrode gap 20 2.5.5 Dielectric Fluid 20 2.5.6 Concentration of EDM 21 2.5.7 Type of dielectric flushing 23 2.5.8 Surface Finish 23 2.5.9 Surface Integrity 24 2.5.10 White Layer 25 2.5 Machining Characteristics 30 2.7 summary 32 METHODOLOGIES 3.1 Introduction 33 3.2 Research Methods and Procedures 33 3.1.2 Workpiece Material 36 3.2.2 Electrode Materials 36 3.2.3 Machining Parameters 37 3.3 4 Measuring of Responses 39 3.3.1 Volumetric relative wear 40 3.3.2 Material Removal rate (MRR) 40 3.3.3 Microcracks 41 3.3.4 Surface Roughness 41 ix 3.4 4 41 RESULTS AND DATA ANALYSIS 4.1 Introduction 46 4.2 Experimental Results EDM4 46 4.2.1 Machining Time 47 4.2.2 Weighing Process 48 4.2.3 Surface Roughness 49 4.2.4 Microcracks 50 4.2.5 ANOVA Analysis 51 4.3 4.4 5 Experimental Equipment 4.2.5.1 Analysis Results for Ra 52 4.2.5.2 Analysis Results for MRR 54 4.2.5.3 Analysis Results for EWR 56 4.2.5.4 Analysis Results for Microcracks 58 4.2.6 60 Confirmation Tests 4.2.6.1 Comparison Tests for EDM4 61 4.2.7 62 Comparison of Test Results for EDM4 Experimental Results EDM200 64 4.3.1 Weighing Process 64 4.3.2 Microcracks 65 4.3.3 ANOVA Analysis 66 4.3.3.1 Analysis Results for Ra 67 4.3.3.2 Analysis Results for MRR 69 4.3.3.3 Analysis Results for EWR 71 4.3.3.4 Analysis Results for Microcracks 73 4.3.4 Confirmation Tests for EDM200 76 4.3.5 Comparison of Test Results for EDM200 77 summary 78 DISCUSSIONS 5.1 Introduction 78 5.2 Surface Roughness, Ra 79 x 6 5.3 Material Removal Rate MRR 79 5.4 Electrode Wear Rate EWR 80 5.5 Microcracks 80 5.6 Summary 81 CONCLUSIONS 6.1 Conclusions 82 6.2 Recommendations 84 REFERENCES 85 Appendices A-E 88-114 xi LIST OF TABLES NO. TITLE PAGE 2.1 POCO Graphite grade EDM4 12 2.2 Graphite electrode weights 13 2.3 Classification of EDM Graphite Electrodes 14 2.4 Specification of electrodes 16 2.5 peak current and pulse duration effect to work machined surface 27 2.6 sinking EDM parameters affect the surface integrity of hardened steel 28 2.7 sinking EDM parameters affect the tool wear of hardened steel 29 3.1 Classification for the material to be used in the experiment 36 3.2 electrode properties 37 3.3 General machining parameter 38 3.4 The parameters and the value used in experiment 39 4.1 Machining Time when using EDM4, EDM200 47 4.2 Weighing of workpiece (lift) and Weight of EDM$ electrode (right) 48 4.3 MRR &EWR for Electrode EDM4 49 4.4 Surface Roughness (Ra) for Electrodes EDM4 and EDM200 50 4.5 Machining response results for Electrode EDM4 51 4.6 ANOVA for surface roughness, Ra 52 xii 4.7 ANOVA for Material Removal Rate MRR 54 4.8 ANOVA for Electrode Wear Rate EWR% 57 4.9 ANOVA for Microcracks 59 4.10 Quality characteristics of the machining performance. 61 4.11 Confirmation test results for surface roughness, Ra) 61 4.12 Confirmation test results for Microcracks 61 4.13 Confirmation test results for Material Removal Rate MRR. 62 4.14 Confirmation test results for Electrode Wear Rate EWR %.) 62 4.15 Comparison test results for all responses. EDM 4 63 4.16 Weighing of workpiece (lift) and Weight of EDM200 electrode (right) 64 4.17 MRR &EWR for Electrode EDM4 65 4.18 Machining response results for Electrode EDM200 66 4.19 ANOVA for surface roughness, Ra 67 4.20 ANOVA for surface roughness, MRR. 70 4.21 ANOVA for Electrode Wear Rate (EWR %) 72 4.22 ANOVA for Microcracks 74 4.23 Quality characteristics of the machining performance200. 76 4.24 Confirmation test results for surface roughness, Ra. 76 4.25 Confirmation test results for microcracks 76 4.26 Confirmation test results for Material Removal Rate MRR 77 4.27 Confirmation test results for Electrode Wear Rate EWR% 4.28 Comparison test results for all responses.EDM200 78 5.1 The comparison of setting parameters with previous researchers 92 . 77 xiii LIST OF FIGURES FIGURE NO. TITLE PAGE 2.1 CNC EDM Die Sinking Machine Roboform 100 (4 Axis) 6 2.2 The Process die sinking1 8 2.3 The Process die sinking2 8 2.4 The Process die sinking3 8 2.5 EDM4 specification 15 2.6 EDM200 specification 15 2.7 List of process factors for EDM 17 2.8 Actual profile of a single EDM pulse 18 2.9 jet flushing using flushing nozzles 21 2.10 Structure material layers 26 2.11 Sparking gap 31 3.1 Overall summary of Research Methodology 34 3.2 The view of work piece 36 3.3 Electrode cross-section view 37 3.4 CNC EDM Die Sinking Machine Robform 100 (4 Axes) 42 3.5 The Digital Rockwell Hardness Tester machine 42 3.6 Formtracer CS - 5000 Mitutoyo 43 3.7 High Power Optical Microscope – Zeiss Axiotech 43 3.8 Balancer device 44 3.9 MECATONE T201A 44 3.10 The sand grind and the polish machine 45 4.1 Half Normal probability plots for Ra EDM4 53 4.2 Main Interactions for Ra EDM4 53 4.3 Half Normal probability plots for MMR EDM4 55 xiv 4.4 Interaction plot for MMR EDM4 56 4.5 Half Normal probability plots for EWR%. EDM4 57 4.6 Interaction plot for EWR%. EDM4 58 4.7 Half Normal probability plots for Microcracks EDM4 59 4.8 Interaction plot for microcracks EDM4 60 4.9 Half Normal probability plots for Ra.EDM200 68 4.10 Interaction plot for Ra EDM200 69 4.11 Half Normal probability plots for MRR. EDM200 70 4.12 Interaction plot for MRR EDM200 71 4.13: Half Normal probability plots for EWR% EDM200 72 4.14: Interaction plot for EDM200 73 4.15 Half Normal probability plots for Microcracks EDM200 75 4.16 Interaction plot for EDM200 75 xv LIST OF SYMBOLS EDM - Electrical Discharge Machining WEDM - Wire Electrical Discharge Machining MRR - Material Removal Rate EWR - Electrode Wear Ratio Ra - Surface Roughness LMC - Length of Microcracks SEM - Scanning Electron Microscopy V - Machining Voltage P - Peak Current A - Pulse Duration (On-time) R - Pulse Interval Time (Off-time) CNC - Computer Numerical Control DOE - Design of Experiment ASSAB718 Hardened Steel Working Material, ASSAB Steel Grade EDM4, 200 Electrode Grade Level We Weight of Electrode Wm Weight of Working Material xvi LIST OF APPENDICES APPENGIXS TITLE PAGE References 98 A The overall results for surface roughness EDM4 103 B The overall results for surface roughness EDM200 109 C The overall results for Microcracks structure EDM4 115 D The overall results for cracks structure EDM200 122 1 CHAPTER 1 INTRODUCTION 1.1 Introduction This chapter discusses the basic ground of the project. It is followed by Problem statement, project objective, scopes and finally project structure. 1.2 Background of the Project Electrical discharge machining, commonly known as EDM, is a process that is used to remove metal through the action of an electrical discharge of short duration and high current density between the tool and the work piece. There are no physical cutting forces between the tool and the workpiece involved. EDM has proved valuable especially in the machining of super-tough, electrically conductive materials such as the new space-age alloys. It can be used to produce parts with intricate shape that is impossible when using conventional cutting tools. 2 This machining process is continually finding further applications in the metal machining industry. It is being used extensively in the plastic industry to produce cavities of almost any shape in metal moulds. Other applications include production of critical parts for aerospace, electronics and medical industries. Although the application of EDM is limited to the machining of electrically conductive work piece materials, the process has the capability to cut these materials regardless of their hardness or toughness (Li Li, Y.S. Wong January 2001) In recent years, EDM researchers have explored a number of ways to improve the sparking efficiency including some unique experimental concepts that depart from the EDM traditional sparking phenomenon. Despite a range of different approaches, this new research shares the same objectives of achieving more efficient metal removal coupled with a reduction in tool wear and improved surface quality .Research areas in EDM fall under three major headings. The first relates to machining performance measures such as material removal, tool wear and surface quality (SQ). The second area describes the effects of process parameters including electrical and non-electrical variables, which are required to optimize the stochastic nature of the sparking process on the performance measures. Finally, research concerning the design and manufacture of electrodes has also been reported (S.T. Newman 2003) 1.3 Problem Statement EDM is commonly used in tool, die and mould making industries for machining heat-treated tool steel materials. The heat-treated tool steel material falls in the difficult-to-cut material group when using conventional machining process. 3 1) Comparing the Performance of POCO EDM4 and POCO EDM200 electrodes from material removal rate MRR, electrode wear rate EWR, achievable roughing surface finish and Microcracks. 2) To evaluate the optimal condition for each electrode. by using DOE soft wear and conformations tests 1.4 Objectives The objectives of this research were: 1. To evaluate the performance of sinker electro-discharge machine(EDM)on hardened steel(ASSAB718) 2. To evaluate the performance of graphite electrode in term of surface roughness, material removal rate, electrode wear rate and microcracks 1.5 Scope The scopes of this project were limited to the following 1. Workpiece material used was hardened steel ASSAB 718 with hardness up to 59 HRC 2. Electrode material was limited to two types of graphite materials. 4 3. Variable machining parameters were limited to current, voltage, pulse off/on and pulse width while other parameters were fixed. 4. Chermill Robofirm 100 Electrical discharge machine EDM die sinking were used. for conducting experimental. 1.6 Significance of study The current study focused on the evaluation of the performance of graphite electrodes when machining hardened steel material. It was hoped that the findings could be used by industrial practitioners to select the most suitable cutting parameters for hardened steel and realizing its economic potential to the fullest. Generally, the significance of study can be summarized by the following points: 1. Better understanding of graphite electrode behaviors when machining hardened steel at various conditions. 2. Information gathered from the study becomes useful especially for die and mould making industries to consider graphite as a candidate for replacing copper electrode particularly for varying works 1.7 Project Structure This project were include about six chapters with references and appendixes were all illustrated in the contents 5 CHAPTER 2 LITERATURE REVIEW 2.1 Introduction This chapter discusses the effects of EDM machining parameters and the working principle of each EDM parameters. 2.2 EDM Die Sinking Process The electrical discharge process is based on thermal effects; electrical discharges between two electrodes, the tool and the work-piece have material removing potential. Electro-discharge machining (EDM) is a widely used method for shaping conductive materials. EDM removes material by creating controlled sparks between a shaped electrode and an electrically conductive work piece. As part of the material is eroded, the electrode is slowly lowered into the work piece, until the resulting cavity has the inverse shape of the electrode. Dielectric fluid is flushed into 6 the gap between the electrode and work piece to remove small particles created by the process and to avoid excessive oxidation of the part surface and the electrode. The applications of EDM lie mainly in the tooling industry where it is applied on materials which are too hard to be machined with conventional techniques, such as milling or turning. The parts for these applications are usually larger than 1 mm; therefore conventional methods can be applied for fabricating the electrodes. Due to the fact that EDM can achieve very fine surface finishes, it has been trialed in the micromachining of conductive materials. For this purpose, two grades of graphite electrodes (EDM4 and EDM200) are used with CNC EDM Die Sinking Machine Rob form 100 (4xis) have been used as die-sinking electrodes. Figure 2.1 shows the EDM die sinking machine that available at Universiti Teknologi Malaysia (UTM). Figure 2.1: CNC EDM Die Sinking Machine Rob form 100 (4 Axis) During the EDM process, a series of non-stationary, timed electrical pulses remove material from a work piece. The electrode and the work piece are held by the 7 machine tool, which also contains the dielectric. A power supply controls the timing and intensity of the electrical charges and the movement of the electrode in relation to the work piece. At the spot where the electric field is strongest, a discharge is initiated. Under the effect of this field, electrons and positive free ions are accelerated to high velocities and rapidly form an ionized channel that conducts electricity. The plasma zone quickly reaches very high temperatures, in the region of 8,000 to 12,000' Centigrade, due to the effect of the ever-increasing number of collisions; this causes instantaneous local melting of a certain amount of the material at the surface of the two conductors. When the current is cut off, the sudden reduction in temperature causes the bubble to implode, which projects the melted material away from the work piece, leaving a tiny crater, The eroded material then re-solidifies in the dielectric in the form of small spheres and is removed by the dielectric. All this without the electrode ever touching the work piece Making EDM a no-contact machining process allowing you to achieve tighter tolerances and better finishes in a wide range of materials that are otherwise difficult or impossible to machine with traditional processes. The physical principle working of EDM can be explained as EDM machining is performed, as an electric sparks who jump between two electrodes subjected to a given voltage in the submerged of insulating liquid (dielectric fluid). Figures 2.2, 2.3 and 2.4 show how the electricity used to machining the electrode materials. Since the two electrodes are in a dielectric or insulating medium, the voltage applied to them must be sufficient to create an electric field which is greater than the dielectric rigidity of the fluid. 8 Figure 2.2: The process of die sinking As a result of the action of this electrical field, free positive ions and electrons are accelerated, creating a discharge channel which becomes a conductor, and it is precisely at this point where the spark jumps. This causes collisions between the ions (+) and the electrons (-). A channel of plasma is thus formed. Figure 2.3: The process of die sinking These collisions create high temperatures in both poles and a ball of gas is formed around the plasma channel, which begins to grow. At the same time, the high temperatures in the two poles melt and vaporize part of the material of the part, while the electrode itself suffers only very slight wear. Figure 2.4: The process of die sinking 9 2.2.1 Limitation of EDM Clearly, the benefits of EDM are considerable, and it is often appropriate to EDM instead of using conventional manufacturing processes. Below show some of the restrictions of EDM: i. EDM tapering: The maximum taper angle is ±45 degrees. The maximum height/angle is 30 degrees at 40.64 cm high. In the maximum electrical resistance for work piece and fixture is approximately 0.5-5.0 ohm centimeter for sinker EDMs. ii. The accuracy of an EDM is limited to about ±0.00245mm(2.5µm) iii. Surface finish is about (5.08 micro meter) for EDMs sinkers. 2.3 EDM Electrodes The EDM electrodes are the important component in this process. This is because of the reaction between the work piece and the electric currents through this electrode. These electrodes should be a conductor of electricity so that they can conduct this current from the machine to the work piece. The shape of this electrode will affect the shape of the product. In this study round shape electrodes are used for experimental involving copper electrode and square shape for electrode graphite. The basic characteristics need for electrodes: i. Good conductors of electricity and heat ii. Easily machined to shape that is needed iii. Produce efficient metal removal from the work piece iv. Resist deformation during the erosion process v. Exhibit low electrode (tool) wear rates 10 2.3.1 Electrodes Materials Electrical discharge machining (EDM) is a non-conventional machining process where material is removed electro-thermally by a series of successive discrete discharges or sparks between two electrically conductive objects, i.e., the electrode and the machined work piece. The performance of the EDM process, to a large extent, is dependent on the material and the design of the electrodes. EDM electrode material must have basic properties such as electrical and thermal conductivity, a high melting temperature, low wear rate, and resistance to deformation during machining. In general, the electrode is the ―cutting‖ tool in the EDM process. With normal EDM machining applications, the work piece is the positive terminal of the power supply and called anode. The electrode, called the cathode is the negative terminal. The size and shape of the electrode determines the size and shape of the work piece produced with the clearance that existed. 2.3.2 Graphite Materials One of the electrodes used is graphite. Graphite is a crystalline form of carbon having a layered structure of basal planes or sheets of close-packed carbon atoms. Although brittle, graphite has high electrical and thermal conductivity and resistance to thermal shock and high temperature [although it begins to oxidize at 500°C (930°F)]. It is therefore an important material for application such as electrodes, heating elements, brushes for motors, high-temperature fixtures and furnace parts, mold material such as crucibles for melting and casting of metals, and seals (because of low friction and wear). Unlike other materials, the strength and stiffness of graphite increase with temperature. This material is available in many different grades from large grain sizes (200 μm), used in rough EDM operations, to 11 very fine grains (1 μm) for finish EDM operations, particularly in steel. The costs of graphite vary from inexpensive, for coarse-grain sizes, to very expensive for finegrain sizes. It provides a high material removal rate and low electrode wear depending on the EDM parameter settings - as compared to metallic electrodes. At the present there is a trend to incorporate the entire geometrical configuration of the work piece onto a single large electrode, instead of partitioning the tool in many small pieces. Thus, the weight of the electrode becomes very important because it affects many factors in handling construction and use of the electrode. Graphite has a much lower density than copper, which makes it the best material for large electrodes. Although graphite is very abrasive it is relatively easy to be machined by all the conventional machining processes. Milling, drilling, turning, grinding and ultrasonic machining provide excellent finishes in graphite. The major drawback of graphite is the fine dust it produces during its machining. It is able to settle on the guides of the machine tool and when mixed with the machine's cutting fluid it will act like a lapping compound, which eventually reduces the accuracy of the machine. Precautions must be taken when machining graphite. 3.3.3 Graphite Grades within Classifications The physical properties of each grade of graphite determine the ranking within classifications. The properties that influence performance are particle size, flexural strength and shore hardness. These properties along with a photomicrograph of the microstructure are the best tools for predicting graphite performance. The best graphite in any classification has tightly packed particles with little variation in size. This kind of uniform material resists wear caused by the thermal nature of the EDM process. Particle size is generally stated as an average size. When particle size spans a small range, the microstructure of the material becomes more uniform with reduced porosity. The porosity in the graphite is boundary between 12 particles. The particles are bound together by chemical or mechanical means and the failure of this system is what releases particles into the gap when EDMing. If the material's particles are small, uniform in size and tightly packed, erosion of the electrode is minimal. Particle size has a bearing on the minimum surface finish that the material will produce. Since the electrode reproduces its structure in the cavity, fine surface finishes cannot be obtained with graphite grades that have large particle and non-uniform microstructure. [www.moldmakingtechnology.com]. The following tables 2.1 and 2.2 shows the different grade of EDM machined with proper suitable graphite electrode types, according to POCO Graphite Production: Table 2.1 POCO GRAPHITE GRADE 13 Table 2.2 Graphite Electrode Weights a) EDM Graphite Electrodes Graphite is isotropic, very fine grain graphite with high strength, high density, electrical conductivity, providing high metal removal rate, excellent surface finish, and high resistance to electrode wear makes it an excellent EDM electrode material. Spark Graphite is light in weight, dimensionally stable and is easily machining into any size or shape from larger size EDM graphite electrode to thin and intricate EDM graphite electrodes. 14 Table 2.3 Classification of EDM Graphite Electrodes Classification of EDM Graphite Electrodes Fine Application Large Forging Dies, Die Casting Dies and Plastic Moulds. Precision Forging Dies , Die Casting ,Plastic Moulds, Superfine Rubber & Glass Moulds Very precision - Threading Electrodes, Engraving, Ultrafine Stamping Dies & Aerospace Applications Fine detailed Engraving electrodes, Delicate electrode & Angstrofine intricate Mould and Dies PRODUCT SPECIFICATIONS OF POCO GRAPHITE Grade Average Flexurl Compres Classification Particle Strength Strength Size (psi) (psi) Electrical Hardness Resistivity (Shore) Microohm/inch EDMAF5 Angstrofine <1 17,000 27,000 87 680 EDMC3 Ultrafine <5 16,500 30,000 67 120 EDM-4 Ultrafine <4 15,800 23,000 76 500 EDM-3 Ultrafine <5 13,500 21,500 76 540 EDM-2 Ultrafine <5 10,000 18,000 73 620 EDM-1 Ultrafine <5 7,500 15,000 70 740 EDM200 Superfine 10 9,000 16,000 64 480 EDMC200 Superfine 10 13,000 23,000 60 70 EDM150 Fine 14 7,800 14,500 68 570 EDM100 Fine 20 6,500 12,500 58 480 COA PHI 15 b) EDM-4 4 Poco‘s EDM-4 is the premier offering in the ultrafine grain classification. This highly isotropic grade combines extraordinary strength with moderate hardness, yielding superior electrode fabrication characteristics. EDM-4 has superior EDM performance characteristics for metal removal rates, wear and surface finish. c) Superfine-Graphite-EDM-200 Poco's EDM-200 is anisotropic superfine particle graphite providing good strength, surface finish, and wear resistance. Moderately priced, EDM-200 provides excellent repeatability from electrode to electrode and from job to job. Table 2.3 and Figure2.5, 2.6 below shows the specification of the graphite electrode Figure 2.5 EDM4 specification Figure 2.6 EDM200 specification 16 Table 2.4: Specification of electrodes Physical properties EDM4 EDM200 Electrical resistivity (μΩ/inch) 500 480 Hardness ss (shore) 76 64 Compressive vies strength (psi) 23000 16000 Melting point (°C) 3350 3125 Flexural strength (µsec) 15800 9000 classification ultrafine Super fine Coefficient of thermal expansion (×10 −6 °C−1) 7.8 2.4 6.9 EDM Machining Parameter Generally, EDM parameters are categorized into two groups which have electrical and non-electrical parameters. The electrical parameters comprise of polarity, peak current, pulse duration and power supply voltage. The non-electrical parameters include circumferential speed of the electrode, reciprocating speed, gap size and flushing of dielectric. According to Mohd. Amri the electrical group usually has more significant affects to the machining characteristics than non-electrical group. This is based on his research that showed the most significant parameter in machining tungsten carbide is pulse duration, followed by machining voltage, peak current and interval time. By referring to figure 2.7 there are many factors that can affect machining characteristics in EDM process found by previous researcher ,however, in this study the emphasis will be given more on the electrical parameters only such as machining voltage, peak current, pulse duration (on-time) and interval time (off-time). 17 Figure 2.7 List of process factors for EDM. Furthermore, many researchers also have suggested that it is more desirable and economical to familiar with parameters that would control the machining process before planning and designing the machining process. Therefore, in order to have better understanding of EDM parameters, they are briefly explained as below based on reports and journals written by former researchers: 2.4.1 Discharge voltage Discharge voltage in EDM is related to the spark gap and breakdown strength of the dielectric (Kansal.italic 2005). Before current can flow, the open gap voltage increases until it has created an ionization path through the dielectric. Once the current starts to flow, voltage drops and stabilizes at the working gap level. The preset voltage determines the width of the spark gap between the leading edge of the electrode and work piece. Higher voltage settings increase the gap, which improves the flushing conditions and helps Fig.2.8 Actual profile of a single EDM pulse (Fuller, 1996).To stabilizes the cut. MRR, tool wear rate (TWR) and surface roughness increases, by increasing open circuit voltage, because electric field strength increases. However, the impact of changing open circuit voltage on surface hardness after machining has been found to be only marginal. 18 Figure 2.8 Actual profile of a single EDM pulse 2.4.2 Pulse duration (On-time) and pulse interval (Off-time) Each cycle has an on-time and off-time that is expressed in units of microseconds. Since all the work is done during on-time, the duration of these pulses and the number of cycles per second (frequency) are important. Metal removal is directly proportional to the amount of energy applied during the on-time (Singh italic. 2005). This energy is controlled by the peak amperage and the length of the on-time. Pulse on-time is commonly referred to as pulse duration and pulse off-time is called pulse interval. With longer pulse duration, more work piece material will be melted away. The resulting crater will be broader and deeper than a crater produced by shorter pulse duration. These large craters will create a rougher surface finish. Extended pulse duration also allow more heat to sink into the work piece and spread, which means the recast layer will be larger and the heat affected zone will be deeper. However, excessive pulse duration can be counter-productive. When the optimum pulse duration for each electrode—work material combination is exceeded, 19 material removal rate starts to decrease. A long duration can also put the electrode into a no-wear situation. Once that point is reached, increasing the duration further causes the electrode to grow from plating build-up. The cycle is completed when sufficient pulse interval is allowed before the start of the next cycle. Pulse interval will affect the speed and stability of the cut. In theory, the shorter the interval, the faster will be the machining operation. But if the interval is too short, the ejected work piece material will not be swept away by the flow of the dielectric and the fluid will not be deionizer. This will cause the next spark to be unstable. Unstable conditions cause erratic cycling and retraction of the advancing servo. This slows down cutting more than long, stable off-times. At the same time, pulse interval must be greater than the deionization time to prevent continued sparking at one point (Fuller, 1996), typical ranges are from 2to 1000 second. Therefore, the selection of EDM parameters is important in determining and getting the accuracy and surface finish for a particular application, all the pervious parameters descried can be adjusted either the manually or by using CNC control unit or programmable controllers. 2.4.3 Polarity The polarity of the electrode can be either positive or negative. The current passing through the gap creates high temperatures causing material evaporation at both electrode spots. The plasma channel is composed of ion and electron flows. As the electron processes (mass smaller than anions) show quicker reaction, the anode material is worn out predominantly. This effect causes minimum wear to the tool electrodes and becomes of importance under finishing operations with shorter ontimes. However, while running longer discharges, the early electron process predominance changes to positron process (proportion of ion flow increases with 20 pulse duration), resulting in high tool wear. In general, polarity is determined by experiments and is a matter of tool material, work material, current density and pulse length combinations. 2.4.4 Electrode gap The tool servo-mechanism is of considerable importance in the efficient working of EDM, and its function is to control responsively the working gap to the set value. Mostly electro-mechanical (DC or stepper motors) and electro-hydraulic systems are used, and are normally designed to respond to average gap voltage. The most important requirements for good performance are gap stability and the reaction speed of the system; the presence of backlash is particularly undesirable. The reaction speed must be high in order to respond to short circuits or open gap conditions. Gap width is not measurable directly, but can be inferred from the average gap voltage (Crook all and Heuvelman, 1971). 2.4.5 Dielectric Fluid The EDM setup consists of a power supply whose one lead is connected to the work piece immersed in a tank having dielectric coil. The tank is connected to a pump, oil reservoir, and a filter system. The pump provides pressure for flushing the work area and moving the oil while the filter system removes and traps the debris in the oil. The oil reservoir restores the surplus oil and provides a container for draining the oil between the operations as shown in figure 2.9. 21 (a) (b) Figure 2.9 Jet flushing using flushing nozzles The main functions of the dielectric fluid are: i. To flush the eroded particles produced during machining, from the discharge gap and remove the particles from the oil to pass through a filter system. ii. To provide insulation in the gap between the electrode and the work piece. iii. To cool the section that was heated by the discharge machining. For most EDM operations kerosene is the common die electric used with certain additives that prevent gas bubbles. Silicon fluids and mixture of these fluids with petroleum oils have excellent results. 2.4.6 Concentration of EDM Flash point: This is the temperature at which the vapors of the fluid will ignite. This explanation is a little simplistic as conditions for testing are more involved but for the sake of discussion and safety‘s sake, the higher this number, the better. 22 Dielectric strength: This is the ability of the fluid to maintain high resistivity before spark discharge and in turn the ability to recover rapidly with a minimal amount of OFF time. Oil with a high dielectric strength will offer a finer degree of control throughout the range of frequencies used, especially those used when machining with high duty cycles or poor flushing conditions. This will provide for better cutting efficiency coupled with a reduced potential arcing. Viscosity: The lower the viscosity of the fluid the better is the accuracy and finishes that can be obtained. In mirror finishing or close tolerance operations, spark gaps can be as small as 0.005 or less. With such tight, physical restrictions such as this, it is much easier to flush small spark gaps with lighter and thinner oil. Good finishing EDM oils are on the thin side. Specific gravity: Often confused with viscosity, this is the ―weight‖ of a substance measure by a hydrometer. The ―lighter‖ the oil or lower its specific gravity, faster the heavier particles (chips) settle down. This reduces the gap contamination and possibilities of secondary discharge and/or arcing. Color: All dielectric oils will eventually darken with use, but it seems only logical to start with a liquid that is as clear as possible to allow viewing of the submerged part. Clear or ―water-white‖ should be your choice, because any fluid that is not clear when brand new certainly contains undesirable or dangerous contaminants. Preventive Maintenance: Depending on the use of the oil and maintenance the oils can last several years. Regularly filtered oil prevention of water contamination will extend its useful life considerably. Water contamination cannot be eliminated completely as condensation will occur on the electrode surface when the surface heats up. Graphite electrodes will contribute more to the condensation than the metallic electrodes as they have a porous structure and absorb moisture from 23 the air. That is the reason why the graphite electrodes should be stored in dry areas. Some shops will keep the electrodes in dry ovens the night before they are used. 2.4.7 Type of dielectric flushing Basic characteristics required of a dielectric in EDM are high dielectric strength and quick recovery after breakdown, effective quenching and flushing ability. TWR and MRR are affected by the type of dielectric and the method of its flushing (Wong et al., 1995). Most dielectric fluids are hydrocarbon compounds or water. Demonized water is used for wire-EDM and high precision die-sinking because of its low viscosity and carbon-free characteristics. The dielectric fluid is flushed through the spark gap to remove gaseous and solid debris during machining and to maintain the dielectric temperature well below its flash point. A control feature that is available on many machines to facilitate chip removal is vibration or cyclic reciprocation of the servo-controlled tool electrode to create a hydraulic pumping action. Orbiting of the tool or work piece has also been found to assist flushing and improve machining conditions (Levy and Ferroni, 1975). 2.4.8 Surface Finish During each electrical discharge, intense heat is generated, causing local melting or even evaporation of the work piece material. With each discharge, a crater is formed on the work piece and a smaller crater is formed on the tool electrode. Of the molten material produced by the discharge, only 15% or less is carried away by the dielectric [Serope Kalpakjian, (1992)]. The remaining melt re-solidifies to form an undulating terrain. After magnification, the surface is observed to be covered with overlapping craters, globules of debris, and pockmarks or ‗chimneys‘, formed by entrapped gases escaping from the re-deposited material. 24 The crack formation usually occurred due to the development of high thermal stresses exceeding the ultimate tensile strength of the material, as well as with plastic deformation [Mohd. Amri, L. (2002). - Sandvik CIC Rolls]. According to Lee et al. [V.García Navasa] cracks normally exist in the recast layer, initiating at its surface and traveling down perpendicularly towards the parent material. In the vast majority of cases, the cracks terminate within the white layer or just on the interface of the white layer and the parent material. Sometimes the cracks also may observe within the crater as the result of thermal stress during discharge. It has been observed that the occurrence and the extension of the cracks can be greatly influenced by choosing suitable operating conditions [Earaerts, W. (2004).]. 2.4.9 Surface Integrity Surface integrity is defined as the inherent or enhanced condition of a surface produced in a machining or other surface generating operation. The nature of the surface layer has been found in many cases to have a strong influence on the mechanical properties of the part. This association is more pronounced in some materials and under certain machining operations. Surface integrity has two important parts. The first is surface texture, which governs principally surface roughness, which essentially is a measure of surface topography. This subject has been and being pursued by many investigators. The second is surface metallurgy which is a study of the nature of the surface layer produced in machining. Surface integrity of a surface produced by a metal removal operation includes the nature of both surface topography as well as surface metallurgy on the mechanical and physical properties of a material in its chosen environment. Typical surface integrity problems include: i. Grinding burns on high strength steel landing gear components. ii. UN tempered marten site in drilled holes. iii. Effect of cutting fluid on the stress corrosion properties of titanium. iv. Grinding cracks in root section of cast nickel base gas turbine buckets. 25 v. Lowering of fatigue strength of parts processed by EDM or ECM. vi. Distortion of thin components. vii. Residual stress induced in machining and its effect on distortion, fatigue, and stress corrosion. Surface integrity broadly defined not only topological (geometric) features of surfaces and their physical and chemical properties, but also the metallurgical and mechanical state of the machined surface. It‘s can be assessed using micro hardness measurements or micro structural analyses which reveal cracks, phase transformation, melted and re-deposited layers and similar features. Surface integrity is an important consideration in manufacturing operations because its influences properties, such as fatigue strength, resistance to corrosion and service life. Several defects produced during manufacturing operation these defects are usually caused by combination of factors, such as: i. Defect in the original material, caused by a casting or metal working process ii. The method by which the surface is produced iii. Lack of proper control of process parameter, which can result in excessive stresses, excessive temperature or surface deformation. 2.4.10 White Layer White layer also known as recast layer that occur in EDM machining because of the machining parameters used in experiment. Due to thermal nature of the electro discharge machining process, a heat-affected zone, consisting of several layers is created at the surface of the work piece. The white layer includes some particles resolidified on the surface and not flushed away. This material was taken to the molten state but neither ejected nor removed by the flushing action of the dielectric. 26 According to [Luo, Y. F. and Mater, J. (1998) Process Technology] under the white layer, other layers may be seen, and the number of layers differs from sample to sample also reported that a white layer has been observed to form under all machining conditions even when using water as dielectric, though this white layer differs from the one found on samples machined in an oil dielectric. The average thickness of the white layer decreases with a decrease in energy. The thickness of the layer also appears thicker when machining with a graphite electrode as compared when machining with a copper electrode. Due to high temperature during EDM process, a molten pool is formed at the surface of the work piece and the dielectric takes place resulting in diffusion carbon in the material. This carbon goes into solution in the molten metal. The iron and the carbon combine to form iron carbides, which solidify in dendrite structures, oriented along the direction of the highest cooling gradient, which is perpendicular to the surface. This phenomenon leads to a significant increase in the micro hardness value of the white layer. Based on the findings of the different workers, it is found that irrespective of the EDM machining conditions used (such as pulse current and pulse on-time) the occurrence of the white layer depends on two main factors, namely, the initial carbon content of the work piece and the type of dielectric fluid used. If these two conditions are met, then the resulting thickness of the white layer will depend upon the magnitude of the pulse energy (pulse current and/or pulse on-time). The white layer or recast layer shown on figure 2.11 Figure 2.10 Structure material layers 27 i. A summary of previous researchers regarding the effects of EDM parameters on the surface roughness on various types of steel is shown in Table 2.5. Table 2.5 Peak current and pulse duration effect to work machined surface EDM process and electrode types Lee S H and Die sinking Ki X P(2001) Graphite, copper and [Lee, S.H. and Li, X.P. copper tungsten. (2001).] Author (Year) Mohd Amri (2002) [Lauwers, B., Liu, W. and Earaerts, W. (2004).] Puerto‘s et al. (2004) [C.F. Hu Y.C. Zhou , Y.W. Bao (2006).‖] work piece Steel (en31) Findings i) For all three electrodes used the surface roughness of the work piece increases with the increasing peak current. ii) Copper exhibits the best performance with regard of surface finish and graphite is the poorest. iii) The negative tool polarity gives better surface roughness. iv) Surface roughness increase with the increase of open-circuit voltage, peak current and pulse duration. . i) To obtain minimum surface roughness (Ra), minimum voltage and peak current coupled with maximum pulse duration and interval time. ii) For higher surface roughness, must inverse the parameters. iii) The results showed peak current have the major influenced to Ra, followed by interval time, machining voltage and pulse duration. iv) Optimal machining parameters for Ra are machining voltage -120 V, peak current 8 A, pulse duration 50 µm and interval time 800 µm, Die sinking Graphite: (ELLOR30) negative polarity, Ø 9 mm AISI P20 tool steel Die sinking Copper: negative polarity, jet flushing pressure 20 kPa AISI P20 tool i) Design factor of intensity have great steel influence on surface roughness for any value of duty cycle. ii) Duty cycle is less influenced in surface roughness parameter. iii) To obtain good surface finish of AISI P20 tool steel, low value of both intensity and pulse time must be used. Most of the researchers also agreed that peak current and pulse duration have the significant effect to work machined surface. Other factors such as flushing pressure and duty cycle have no significant influenced to surface roughness. 28 However, without proper flushing used during EDM process, good machining conditions cannot be achieved [Sandvik CIC Rolls]. ii. A summary of previous researchers regarding the effects of EDM parameters On the Cracks (surface integrity) on various types of steel is shown in Table 2.6 Table 2.6 Sinking EDM parameters affects the surface integrity of hardened steel is Author (Year) Rebelo Morao Dias(1997) EDM process and electrode types Die sinking Graphite, copper work piece Findings HRC55 i) The dimensions of random overlapping surface craters increase with machining pulse energy and density and penetration depth of the cracks in the re-cast layer increases with the machining pulse energy. ii) Network crack formation is associated with the development of high tensile stresses . Luis, Die sinking conductive i) Flushing pressure, it was verified Puertas Graphite, ceramic that an increase in the latter (within the and G. (siliconise considered work interval, 20–60 kPa) Villa d silicon resulted in a decrease in The wear on (2003) carbide) the electrode. (SiSiC) ii) Factors over material removal rate (MRR) and Electrode wear (EW) has been carried out. . intensity (I), pulse time (ti), duty cycle (η), opencircuit voltage (U) and flushing pressure (P), iii) Large micro cracks formed in materials B, D And E (depth = 10 µm). . Hu , Zhou Die sinking Ti3SiC2 i) The acceleration of the material and Y.W. Graphite, removal rate increases with the Bao (2006) copper discharge current and working voltage, but decreases with increasing pulse duration ii) Melting and decomposing are confirmed as the Main material removal mechanisms. iii) Despite the formation of micro cracks in the re-solidified layer and the loose grains in the subsurface 29 Lee and Die sinking Tai Graphite, reported, copper (2006) [C.F. Hu Y.C. Zhou , Y.W. Bao (2006).‖] H13 tool i) The surface roughness is broadly steel and D2 similar for D2 and H13, and, in both cases, it is found to increase as pulse current and pulse-on Duration increase. ii) white layer thickness, it is noted that the thickness of this layer on H13 is slightly Greater than the layer on D2. iii). white layer thickness increases as pulse current and pulse-on duration increase The literature reports showed that the information on details how sinking EDM parameters affects the surface integrity of hardened steel is still scarce and rather vague in the open literature. Particularly, a systematic study on how sinking EDM parameters affect the surface integrity especially in the presence of cracks. iii. A summary of previous researchers regarding the effects of EDM parameters on the Tool Wear on various types of steel is shown in Table 2.7 Table 2.7 Sinking EDM parameters affect the tool wear of hardened steel EDM process and Author (Year) electrode types Die sinking Amorim, Graphite, Weingaertner copper October-366 work piece Findings AISI P20 (a) For electrodes at positive tool steel polarity, graphite and copper presented similar results in terms of the values of Vw. Probably the 10 μm grain size of the graphite used for the experiments should be applied with higher discharge currents, when the working gap width would be larger and the EDM performance could be more stable. (b) The lower levels of volumetric relative wear J were attained for EDM with graphite and copper at positive polarity despite the EDM 30 parameter settings. (c) The best surface roughness Ra was obtained for copper electrodes under negative polarity. . Che Haron. Die sinking Ghani, Graphite, .Burhanuddin, copper Y.K. Seong, C.Y. Swee 2007 XW42 tool 1. The material removal rate of steel XW42 tool steel with copper electrode is greater than that with graphite electrode. 2. Copper electrode is suitable for roughing process, whilst graphite electrode is suitable for finishing process. Combination of both electrodes will improve machining characteristics and surface finish. 3. The electrode wear rate of copper is lower than graphite electrode when machining XW42 tool steel. The literature reports showed that the information on details how sinking EDM parameters affects the tool wear of hardened steel material is still scarce and rather vague in the open literature. Particularly, a systematic study on how sinking EDM parameters affect the tool wears especially in the presence of wear. 2.5 Machining Characteristics In this section, the machining characteristics that investigate are cracks, surface roughness, and thickness of recast layer in the previous study. Each of this features are usually occurred at the machined surface and may caused failure to the work piece. These defects are explained in the following: 31 i. Cracks Since surface cracking is a potential source of component failure, it is necessary to qualify the degree of cracking by means of some objective standard. However, to quantify the cracking in terms of an estimation of width, length or depth of crack, or even the amount of cracking is not easy. In this study, crack is defines as a ―surface crack density‖, for instances the total length of cracks (cm) in a unit area (cm2). ii. Sparking gap Spark gap of the electrode used during machining is measured using optical microscope in order to study the correlation between the machining parameters and the spark gap. The unit used in this measurement is mm. Figure 2.12 showed the actual length of spark gap in the mathematical equation. Figure 2.11 Sparking gap 32 2.7 Summary 1) Most of the researchers also agreed that peak current and pulse duration have significant effect to work machined surface. Other factors such as flushing pressure and duty cycle have no significant influenced to surface roughness. However, without proper flushing used during EDM process, good machining conditions cannot be achieved [Sandvik CIC Rolls]. 2) The literature reports showed that the information on details how sinking EDM parameters affects the surface integrity of hardened steel is still scarce and rather vague in the open literature. Particularly, a systematic study on how sinking EDM parameters affect the surface integrity especially in the presence of cracks. 3) The literature reports showed that the information on details how sinking EDM parameters affects the tool wear of hardened steel material is still scarce and rather vague in the open literature. Particularly, a systematic study on how sinking EDM parameters affect the tool wears especially in the presence of wear. 33 CHAPTER 3 METHODOLOGY 3.1 Introduction This chapter describes the research methods and procedures covered in this study it consist of four main elements namely, research design and data analysis, variables, research procedures and instrumentations 3.2 Research Methodology The flow chart in Figure 3.1 shows the overall steps involved in the experimental works. It is divided in to three main parts, i.e. 1) Workpiece and electrode materials 2) EDM machine and parameters to vary 3) Responses to be evaluated Detailed descriptions of those are explained in the following section. 34 Work piece Material Equivalent ASSAB 718 High steel material with hardness range 55HRC Electrode Graphite Graphite Parameters Current (A) Voltage (v) 24-48 Pulse interval (µSec) 80-120 100-400 Pulse Duration 0.2-3.8 Measuring Response Material Rate Removal MRR Electrode Wear Ratio EWR Electronic Balance/weighing m/c Surface Roughness Ra Microcrack Surface Roughness Tester Measuring Equipments CNC EDM Die sinking M/c Robform 100(4axis) Mitutovo Formtracer CS-5000 Scanning Electronic Micro Scopy SEM (XL40) Figure 3.1: (a) Overall summary of Research Methodology 35 Workpiese Material: ASSAB718 (59HRC) Material Electrode Material: Poco EDMK4 & EM200 Chermilles Machine: Roboform 100 Experiment Trials Experimental Method: Full factorial, 2level, 4fectors &4cener points Parameters to vary: Current: Voltage: Pulse Interval: Pulse duration: 24-48 80-120 100-400 0.8-3.2 A V µsec µsec Material removal Rate (MRR) Using Electronic balance Responses Electrode Wear Ratio (EWR) Roughness (Ra) Microcracks (LOC) Formtraser CS5000 Scanning Electron (µ/scope) High power (µ/scope) Figure 3.1: (b) Overall summary of Research Methodology 36 3.2.1 Workpiece Material Work piece of hardened steel ASSAB718 was cut to the cube shape with dimension of 10mm x10mmx10mm and cut by the EDM Wire Cut. Figure 3.5 shows the shape and dimension of the work piece. Table 3.1 provides the specification of the working material. Work piece size = 10x10x10 mm Hole size = 5x 5x5 mm Figure 3.2: The view of work piece Table 3.1 Classification for the material to be used in the experiment (ASSAB718) ASSAB718 C Nominal composition (wt. %) 0.33 3.2.2 Cr Ni W V F e 0. 1.8 0.9 0 0 Mn Si 1.4 Hardness 59 HRC Density 7.87kg/cm³ 0 Electrode Materials Two different types of electrodes were examined in this project for rough EDM machining hardened steel .These two electrodes were poco EDM4 and EDM200. 37 Table 3.2 shows the properties of poco electrodes used in the experiment, while the cross-section view shows in figure 3.3 Table 3.2 electrode properties Grade EDM4 EDM200 Average Classification Particle Size Flexural Strength (psi) Compress Hardness Strength (Shore) (psi) Electrical Resistivity Microohm/inch Ultrafine <4 15,800 23,000 76 500 Superfine 10 9,000 16,000 64 480 5mm 5mm 5mm (a) 5mm (b) Figure3.3 Electrode cross-section view 3.2.3 Machining Parameters: The experiments were conducted using Charmilles CNC EDM Machine Roboform 100 the machine is equipped with energetic generator, which means that it is possible to set , among others EDM parameters , the discharge duration (te) and pulse interval (to) which control the ignition delay time (td) as a percentage of (te). In this work (td) was kept as 30% of (te) for all the experiments It means that low energy would be applied with longer ignition delay time. The detailed specifications of EDM used in this experiment are given in table 3.3 appendix 38 The selection of EDM parameters is important in determining the accuracy and surface finish for a particular application. The parameters that were used in EDM machining include voltage, current, pulse On-time and also pulse Off-time. These parameters were manually adjusted using CNC control unit or programmable controllers. This research the parameters were varied include pulse voltage, pulse current, pulse-on duration (ON-time), and pulse-off duration (OFF-time).Table 3.3 summarized the factors and levels of the parameters Table 3.3 General machining parameter Level Factor Low (-) High (+) Discharge Voltage (V) volt 80 120 Peak Current (P) amp. 24 48 Pulse interval (A) µsec 100 400 Pulse duration( Off /On- time ) (R) µsec 0.8 3.2 Table 3.4 shows the planning of experimental trials after considering all factors and levels given in table 3.3 39 Table 3.4: The parameters and the value used in experiment No of Trial 3.2.4 Voltage Peak Current Pulse Interval Pulse Duration V (volt) P(Ampere) A(µsec) R(µsec) 1 -1 -1 -1 -1 2 +1 -1 -1 -1 3 -1 +1 -1 -1 4 +1 +1 -1 -1 5 -1 -1 +1 -1 6 +1 -1 +1 -1 7 -1 +1 +1 -1 8 +1 +1 +1 -1 9 -1 -1 -1 +1 10 +1 -1 -1 +1 11 -1 +1 -1 +1 12 +1 +1 -1 +1 13 -1 -1 +1 +1 14 +1 -1 +1 +1 15 -1 +1 +1 +1 16 +1 +1 +1 +1 17 -1 -1 -1 -1 18 +1 -1 -1 -1 19 -1 +1 -1 -1 20 +1 +1 -1 -1 Measuring of Responses There are four (4) responses variables evaluated in this experiment and are discussed in the following section. 40 3.2.4.1 Volumetric relative wear This value represents the ratio of electrode wear rate to material removal rate and expressed in percentage. Electrode wear ratio (EWR) can be defined as electrode wear weight divided by work piece removal weight. [Khairul Nizar bin Omar (2004)] The efficiency of the electrode used, calculated EWR% = 𝑊𝑒₁−𝑊𝑒₂ 𝑊𝑚₁−𝑊𝑚₂ X100 3.1 Where, We₁= Weight of electrode before machining We₂= Weight of electrode after machining Wm₁ = Weight of material before machining Wm₂ = Weight of material after machining Or, Electrode wear ratio (EWR) can be expressed by the following expression EWR = volume of material removed from electrode Volume of material removed from part 3.2.4.2 Material Removal Rate (MRR) This response variable was selected for this study r to indicate the speed of the EDM process, in removing workpiece MRR = reduction in weight of work piece or electrode (gm) Density of work piece or electrode (g/mm³) × machining time (min) 3.2 41 3.2.4.3 Microcracks Scanning electron microscopy (SEM) was used to measure cracks on the specimens after machining with EDM die sinking. The specimens were grind using silicon carbide paper with grit size from 400 to 4000 to obtain smooth surface. Final polishing was performed on rotating disc of cotton cloth followed by slevyt cloth. The diamond of 6µm particles was used during polishing with cotton cloth. The slevyt cloth was used together with a suspension solution consisting of SiO₂ particle to get better result. Then specimens were examined under the optical image analyzer and SEM. 3.2.4.4 Surface Roughness The surface finish of machined specimens was measured using a surface roughness tester. (Mitutoyo Formtracer CS5000). The length of measurement was 1.5mm and measure with 0.8mm cut off. The Ra values were measured three times for each trial to get the average value 3.4 Analytical Equipments Figure 3.4 shows the EDM die sinking machine that is available at the production laboratory, Unversti Teknologi Malaysia. All the experimental trail were conducted using this machine 42 Figure 3.4: CNC EDM Die Sinking Machine Robform 100 (4 Axes) Hardness of the specimens was tested using Digital Rockwell hardness tester machine (see figure 3.5) Figure 3.5 The Digital Rockwell Hardness Tester machine Mitutoyo Formtracer CS-5000) was used to measure the surface finish of specimens (see figure 3.6) 43 Figure 3.6 Formtracer CS - 5000 (Surface Roughness machine Calibration block was used to calibrate the surface roughness taking before measurement was took place. Each specimen was measured using and 0.8mm cut off Style. Brand/Model : (Mitutoyo Formtracer CS-5000) Accuracy : 0.001 µm The Philips XL40 Microscope Scanning Electron was used to measure cracks on the specimens that occur after EDMed machining. The sample was sectioned prior to the measurement of cracks. At low magnification, high power optical Microscope (see figure 3.7) was used to capture the specimens images on cracks Figure 3.7: High Power Optical Microscope – Zeiss Axiotech. 44 Figure 3.13 shows the balancer used to weigh the workpiece materials ASSAB 718 and the electrodes (EDM4 and EDM200) before and after machining. (See figure 3.8) Figure 3.8 Weighing Machine MECATONE was used to section the workpiece material prior to microcracks measurements by using Scanning Electron Microscope (see figure 3.9) Figure 3.9 MECATONE T201A 45 The measured workpieces were grind with sand paper and polish with polishing machine. Figure 3.10 shows these equipements Figure 3.10: The sand grind and the polish machine 3.5 Summary This chapter discusses the research methodology used in this project. Any others, the experiment plane, workpiece and electrode materials and finally the analytical equipments used to measure and evaluate the response variables 46 CHAPTER 4 RESULTS AND DISCUSSIONS 4.1 Introduction This chapter presents the experimental results on Sinker EDM of hardened steel material using graphite electrodes (EDM200 and EDM4). As was noted earlier, the full factorial design was used for both designing and analyzing the experiment. DOE was used to determine the significant process variables surface roughness (Ra), electrode wear rate (EWR), material removal rate (MRR) and length of Microcracks (LMC). 4.2 Experimental Results-EDM4 In this study, randomization of the run order to be carried out and analysis sequences were carried out according to the run order organized by Design Expert software as summarized table 3.4. Full factorial design of four factors with two levels each was conducted which consist of 16 runs plus four center points which resulted in a total number of 20 trials. The machining responses that were record are surface 47 roughness (Ra), Electrode wear rate (EWR), Material removal rate (MRR) and Length of Micro-Cracks (LMC). 4.2.1 Machining Time The time consumed for each run in this study was recorded by the machine time indicator. Machining time starts as the electrode touch the workpiece and ends at a fixed distance of 5 mm Table 4.1 Machining Time when using EDM4, EDM200 No of Trial Run (volt) V Peak Current (Ampere) P 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 15 12 8 6 5 1 2 4 13 12 9 10 17 14 11 17 16 20 16 3 80 120 120 120 80 80 120 120 80 120 80 80 80 120 80 120 80 120 120 120 24 48 24 48 24 24 24 24 48 48 24 24 24 48 48 48 48 48 48 24 Voltage Pulse width (µsec) A 400 400 100 100 100 100 400 100 400 100 400 100 100 100 400 100 100 400 100 400 Pulse Off/On time (µsec) R Machining Time (minute) EDM4 Machining Time (minute) EDM200 0.8 0.8 0.8 3.2 0.8 0.8 0.8 3.2 3.2 0.8 3.2 0.8 3.2 0.8 0.8 0.8 3.2 3.2 0.8 3.2 100.8 29.01 45.06 57.14 67.45 35.32 112.34 85.03 105.42 46.63 178.36 21.48 67.00 38.20 34.15 19.94 65.42 89.49 29.46 265.80 96.31 25.55 41.22 55.38 51.15 54.40 97.09 105.2 274.30 35.07 218.28 107.58 144.09 62.01 137.30 21.09 226.26 373 82.46 179.0 48 4.2.2` Weighing Process With the help of electronic balancer we got the differences weight between the working material and cutting tool electrode before and after machining operations as shown in Table 4.2.While machining responses (MRR and EWR) shown in Table 4.3 are calculated by equations shown after. Table 4.2 Weighing of workpiece (lift) and Weight of EDM$ electrode (right) No. of Initial Weight (gm) Final Weight (gm) Difference In Weight (gm) Initial Weight (gm) Final Weight (gm) Difference In Weight (gm) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 8.0315 8.1542 7.5692 8.2895 7.7863 8.0420 7.9130 8.0214 8.1260 7.8731 7.9125 7.9788 7.9965 7.7665 7.8792 7.9324 8.0300 7.8265 8.1424 6.8180 6.9258 6.5780 7.1650 6.7008 7.0116 6.8560 7.0756 6.9748 6.6947 6.9900 6.9760 7.2670 6.8000 6.7660 6.9380 7.3200 6.6740 6.8920 1.2135 1.2284 0.9912 1.1245 1.0855 1.0304 1.0570 0.9458 1.1512 1.1784 0.9225 1.0028 0.7295 0.9665 1.1132 0.9944 0.7100 1.1523 1.2504 4.7128 4.7821 4.3722 4.6032 4.8508 4.7130 4.8099 4.5894 4.9623 5.2364 4.5247 4.4120 4.4920 4.3757 4.7792 4.4060 4.7160 4.7640 5.2912 4.6660 4.7140 4.3300 4.5567 4.8088 4.6692 4.7900 4.5760 4.9580 5.2262 4.4770 4.3280 4.4440 4.3240 4.7290 4.3540 4.6536 4.7110 5.1895 0.0468 0.0681 0.0422 0.0465 0.0488 0.0438 0.0199 0.0134 0.0043 0.0102 0.0477 0.0840 0.0480 0.0517 0.0502 0.0520 0.0624 0.0050 0.1017 20 7.9898 6.9360 1.0538 4.6067 4.5552 0.0510 Trial 49 Table 4.3 MRR &EWR for Electrode EDM4 No. of Trail 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 4.2.3 Volume of material Removal (mm³) 155.179 157.084 126.752 143.798 138.8107 131.765 135.166 120.480 147.210 150.690 11.795 128.240 93.280 123.590 142.350 127.160 90.079 147.350 159.890 134.750 Machining Time (min.) Response 1 (MRR) mm³/min Response 2 (EWR)‰ 100.8 29.01 45.06 57.14 67.45 35.32 112.34 85.03 105.42 46.63 178.36 21.48 67.00 38.20 34.15 19.94 65.42 89.49 29.46 265.80 1.5395 5.4148 2.8129 2.5155 2.0579 3.7306 1.2032 1.4169 1.3964 3.2316 0.0661 5.9699 1.3923 3.2354 4.1685 6.3772 1.3878 1.6466 5.4274 0.5069 3.8566 5.5438 4.2575 4.1352 4.4915 4.2508 1.8827 1.4168 0.3735 0.8656 5.1707 8.3764 6.5798 5.3492 4.5095 5.2293 8.7887 4.3391 8.1334 4.8396 Surface Roughness Table 4.4 shows the summary of surface roughness measurements for 20 trials. All the measurements were conducted using Mitutoyo Formtracer CS-5000 with 5 µm stylus tip and 40º of tip angle. Each section was measured for three times before the average results were obtained. However, the data indicated in Table 4.4 is only the summary of measurements obtained and the full measurement results of surface roughness can be seen in Appendix B. 50 Table 4.4 Surface Roughness (Ra) for Electrodes EDM4 and EDM200 No. of Trail surface roughness for bottom surface EDM4 µm surface roughness for bottom surface EDM200 µm Ttrail 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 4.2.4 Ra1 Ra2 Ra3₃ Av. Ra Ra1 Ra2 Ra3 Av. Ra 7.765 10.110 8.631 8.784 10.716 9.858 10.105 9.981 11.688 12.923 10.865 11.585 10.222 11.939 10.412 10.317 10.579 8.377 8.951 9.165 11.182 9.282 9.672 9.948 10.243 10.381 9.985 10.148 8.670 13.618 9.531 9.100 8.334 8.594 8.178 8.322 8.457 8.862 9.831 8.659 10.023 9.424 9.567 9.645 11.270 9.862 10.025 9.943 9.903 10.242 9.789 9.931 9.325 12.167 10.018 9.671 11.473 10.588 10.260 8.737 15.118 8.924 8.825 10.260 4 8798 7.610 8.120 8.162 11.732 22.241 11.305 11.518 10.661 10.957 9.885 10.347 11.336 11.972 9.235 11.654 8.787 9.583 9.028 9.107 9.392 8.282 8.631 8.456 11.567 11.080 10.871 11.097 5.254 10.640 9.516 10.078 7.686 11.083 8.726 9.055 7.240 8.123 10.670 7.681 9.488 10.801 9.256 9.700 10.360 9.794 9.600 9.697 11.057 9.800 10.012 10.220 13.894 13.790 14.977 13.842 9.720 10.344 9.157 9.594 9.600 11.769 9.351 9.475 11.569 11.724 11.462 11.554 11.181 10.028 9.820 9.924 12.667 11.957 11.213 1.755 9.530 12.998 9.725 9.627 9.032 12.172 9.320 9.961 10.447 11.150 10.266 10.356 12.179 8.324 9.251 9.751 17.996 18.380 17.403 18.188 Microcracks Table 4.5 shows the summary of Length of Microcracks for 20 trials, all the measurements were conducted using Scanning Electron Microscope (SEM) Philips XL40. Each section was measured for three times before the average results were 51 obtained. However, the data indicated in Table 4.5 shows the machining results response for EDM4 electrode. Table 4.5 Machining response results for Electrode EDM4 Factors No of Trial 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 Response V (volt) P (amp) A (µsec) R (µsec) 80 24 400 0.8 120 120 120 80 80 120 120 80 120 80 80 80 120 80 120 80 120 120 120 48 24 48 24 24 24 24 48 48 24 24 24 48 48 48 48 48 48 24 400 100 100 100 100 400 100 400 100 400 100 100 100 400 100 100 400 100 400 0.8 0.8 3.2 0.8 0.8 0.8 3.2 3.2 0.8 3.2 0.8 3.2 0.8 0.8 0.8 3.2 3.2 0.8 3.2 Ra µm 8.784 11.585 9.165 10.148 8.322 9.645 9.931 10.260 8.162 10.347 9.107 11.097 9.055 9.700 10.220 9.594 11.554 1.755 9.961 9.751 L.MC µm MRR mm³/min EWR ‰ 100.38 1.5395 3.8566 63.12 5.4148 5.5438 96.35 2.8129 4.2575 71.42 2.5155 4.1352 25.63 2.0579 4.4915 64.7 3.7306 4.2508 40.1 1.2032 1.8827 28.56 1.4169 1.4168 55.1 1.3964 0.3735 56.85 3.2316 0.8656 34 0.0661 5.1707 55.93 5.9699 8.3764 72.62 1.3923 6.5798 44.2 3.2354 5.3492 89.57 4.1685 4.5095 40.77 6.3772 5.2293 50.93 1.3878 8.7887 95.53 1.6466 4.3391 69.91 5.4274 8.1334 84.12 0.5069 4.8396 4.2.5. ANOVA Analysis All data obtained for Electrode EDM4 were then used as input to the Design Expert software for further analysis, according to steps outline for full factorial design Table 4.5 52 4.2.5.1 Analysis Results for Surface Roughness, Ra Based on Table 4.6, there are only three factors affecting the surface roughness, Ra. According to the analysis done in the Design Expert software, when the values of probability (Prob>F) are less than 0.05, it shows that the factor is significant. In this case, the pulse 0ff (off) and servo voltage (SV) and peak current (IP) were significant to the Ra, but there were no interaction of any of these factors observed in the ANOVA table. For the other factors namely pulse on (ON), is not significant since the probability values were greater than 0.1. Therefore, they will not show in the Table 4.9. In this investigation, 95% of confidence interval (CI) is used. Table 4.6 ANOVA for surface roughness, Ra Based on Figure 4.1, the significant factors were observed better in the half normal probability plot of the standardized effects. As displayed in the Figure 4.1, the significant factors highlighted were pulse off time (OF) servo voltage (SV) and 53 peak current (IP)which denoted as A, B and AD respectively. In order to have clearer observation and better understanding of the response, the main effect plot is available. Therefore, only the main effect of Ra which are pulse off time (OF) servo voltage (SV) and peak current (IP) were showed. Figure 4.1 Half Normal probability plots for Ra. From the interactions plot, it was clearly showed that whenever peak current (IP) increased from 24 µs to 48 amps. The value of (Ra) also increased dramatically from 9.3315 to 10.2777. Meanwhile, a reverse result was observed for SV effect as the graph showed that Ra increased 9.64425 to 10.5055 when SV increased from 80 volt to 120 volt. Therefore, no interaction graph can be show in this section. In order to obtain better Ra during EDM Sinker of hardened steel, IP should be set at 48A.and SV at 120 V. Figure 4.2 Main Interactions for Ra 54 4.2.5.2 Analysis results for Material Removal Rate MRR Next analysis is to determine which factor and interaction affecting the response of material removal rate (MRR). This was done by considering the result from ANOVA obtained from the software. According to Table 4.7, there is only one factor affecting the material removal rate (MRR). According to the analysis done in the Design Expert software, when the values of probability (Prob>F) are less than 0.05, it shows that the model is significant. In this case, and pulse width was significant to the MRR, but there were no interaction of this factor observed in the ANOVA table. For the other factors namely pulse off (OFF), servo voltage (SV) and peak current (IP), are not significant since the probability values were more than 0.05. Therefore, they will not show in the Table 4.7. In this investigation, 95% of confidence interval (CI) is used. The information was better illustrated in half normal probability plot as shown in Figure 4.3. This graph is required in order to check for normality of residuals of the factors studied. Table 4.7 ANOVA for Material Removal Rate MRR 55 As displayed in the Figure 4.3, the significant factors highlighted were the pulse on (ON)only while the other parameter was not significant which denoted as C and ABD In order to have clearer observation and better understanding of the response, the main effect plot is available. Therefore, only the main effects of MRR which are pulse on (ON) were show. Figure 4.3 Half Normal probability plots for MRR. Figure 4.4 show the interaction plot, it was clearly showed that when SV increased from 80 volt to 120 volt. The increasing of MRR was from 2.68275 to 3.07. Meanwhile, the value of (Ra) also increased dramatically. From 2.62075 to 4.16325 Based on the ANOVA analysis, IP and SV were affecting the MRR In order to obtain better MRR during EDM Sinker of hardened steel; IP should be set at 48A.while SV at 120 V. 56 Figure 4.4 Interaction plot for MMR 4.2.5.3 Analysis Results for Electrode Wear Ratio (EWR %) The third analysis is to determine which factors and interaction that affects the Electrode Wear Ratio (EWR), similar procedures were done in analyzing the significant factor and the possible interaction as discussed in previous section, whatever factors that have the “Prob>F” less than 0.05 are considered significant for EWR with the confidence interval (CI) used is 95%. Therefore, based on ANOVA analysis and half normal probability plot shown in Table 4.8 and Figure 4.5 respectively, only CD which is the products of C and D factors were effects on the Electrode Wear Ratio (EWR). In this section, the interaction plot is given in Figure 4.6 in order to provide a better illustration of the phenomena. 57 Table 4.8 ANOVA for Electrode Wear Rate EWR% Figure 4.5 Half Normal probability plots for EWR%. 58 Results in Figure 4.6 showed that, Electrode Wear Ratio (EWR) was affected by the product of pulse on (ON) and pulse off (OFF), Based on the graph, EWR increased dramatically from 1.69625 to 5.4165 mm/min as ON was increased Meanwhile, EWR was observed to decrease as OFF were decreased from [4.5815 to 3.01074] Based on this relationship, maximum EWR. Can be obtained when the parameters are set at ON = 400 µs, OFF = 3.2 µs, IP = 24 A and SV = 80 V. Figure 4.6 Interaction plot for EWR%. 4.2.5.4 Analysis Results for Microcracks Results of the ANOVA Table 4.9 and the half normal probability plot figure (4.7) indicated that all factors are not significant. As explained before, although pulse off (OFF) as shown in the ANOVA and normal probability plot, it was not considered as the main factor because of the “Prob>F” value was more than 0.05. However, it is indicated in the variance analysis in order to support the hierarchy in the experiment design analysis. For clearer observation and understanding on the response and main effects of the results obtained, the main effect plot and the interaction plot were provided. 59 Table 4.9 ANOVA for Microcracks Figure 4.7 Half Normal probability plots for Microcracks 60 From the graph shown in Figure 4.8, it was obvious that both factors were able to increase the microcracks when the setting parameters were increasing. as shown in the graphs, cracks an increment from50.2 to 87.2 µm when servo voltage was increased from 80v to 120 v. Similar pattern was observed as pulse off was increased from 0.8 to 3.8µs the increment of microcrack was 54.8 to 55.02.Apparently based on the analysis, the maximum length of crakes can be achieved by setting pulse-off and SV at 0.8 µs and 120 V respectively. Figure 4.8 Interaction plot for Microcracks 4.2.6 Confirmation Tests Once the analyzing process for all the four responses were completed, the factors need to be confirmed according to the effects correlation and met with the objective and goal of each response. In the other words, the confirmation tests needs to be carried out in order to ensure that the theoretical predicted roles suggested by the software were accepted. All the parameters used in the confirmation tests were suggested by the Design Expert software. Three confirmation tests were conducted in order to compare the experimental results from the prediction made. Table 4.10 indicates the expected of quality characteristics for each response that required in the 61 process optimization. This is followed by the confirmation test results for Ra, EWR, MRR and microcracks as shown in Tables 4.11 to 4.14 respectively. All data and related pictures involved in this analysis were attached in Appendix B and C. 4.2.6.1 Comparison Tests for EDM4 Table 4.10 Quality characteristics of the machining performance. Machining Characteristics Quality Characteristics Surface roughness (Ra) Maximum Material Removal Rate (MRR) Maximum Electrode Wear Rate (EWR) Minimum Microcracks Minimum Table 4.11: Confirmation test results for surface roughness, Ra. Exp. Trial Trial condition Repeat 1 Ra (µm) 19 ON = 100µs OFF = 3.2 µs IP = 2.4 A SV = 120 v 12.667 Repeat 2 Ra (µm) Repeat 3 Ra (µm) Total Average (µm) 11.957 11.213 11.755 Table 4.12: Confirmation test results for Microcracks Confirmation test results for micro-cracks Exp. Trial Trial Condition 14 ON = 400µs OFF = 0.8 µs IP = 48 A SV = 120 v Repeat 1 (µm) Repeat 2 (µm) Repeat 3 (µm) Total Average (µm) 35.46 52.94 38.5 44.2 62 Table 4.13: Confirmation test results for Material Removal Rate MRR. Exp. Trial Trial Condition 17 ON = 100µs OFF =.0.8 µs IP = 48 A SV = 120 v Material Removal Rate MRR Confirmation Test Results Repeat 1 Repeat 2 Total Average mm³/min mm³/min mm³/min 6.85 5.88 6.38 Table 4.14: Confirmation test results for Electrode Wear Rate EWR%. EWR%. Confirmation Test Results Exp. Trial Trial Condition 20 ON = 400µs OFF = 0.8 µs IP = 48 A SV = 120 v Repeat 1 Repeat 2 Repeat 3 Total Average 4.51 4.39 3.85 4.26 4.2.7. Comparison of Test Results As mentioned before, three confirmation runs were conducted in order to measure the reliability of optimization solutions obtained from the software analysis. The comparison of test results between the theoretically prediction and confirmation test results was the final consideration that will evaluate whether the optimum parameters predicted were in the allowable range. The margin of error from the prediction and experimental results was set at 7.523% (below than 10 %.)Margin error was calculated using the equation below Margin error % = [(Confirmation on test result – Predicated result) / Predicated result] * 100% 4.1 63 According to the Final Equation in Terms of Coded Factors and Final Equation in Terms of Actual Factors given in ANOVA table analysis ,we can found the value of the prediction and confirmation test results which illustrated in appendix (E) Prediction equation = f x (Duty fact, pulses, current, SV) 4.2 Tables 4.22 indicated the comparison of test results between theoretical prediction and confirmation runs for Ra (7.01%), micro-cracks (2.31%), MRR (11.54%) and EWR% (9.23%) respectively. Therefore, the overall margin of error percentage was 7.523% Table 4.15: Comparison test results for all responses. EDM 4 Response factors Prediction (Design Expert) Experimental (Confirmation Test) Error Margin (%) Ra 10.99 11.76 7.01 MRR 5.72 6.38 11.54 EWR 3.90 4.26 9.23 Crack 43.20 44.2 2.31 64 4.3 Experimental results –EDM200 All the experiment results were shown in the following sections. 4.3.1 Weighing Process With the help of electronic balancer we got the differences weight between the working material and cutting tool electrode before and after machining operations as shown in Table 4.16.While machining responses (MRR and EWR) shown in Table 4.17 are calculated by equations shown after. Table 4.16 Weighing of workpiece (lift) and Weight of EDM200 electrode (right) No of Trial 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 Initial Weight (gm) Final Weight (gm) Difference In Weight (gm) Initial Weight (gm) Final Weight (gm) Difference In Weight (gm) 8.0632 7.1004 0.9628 4.1023 4.0588 0.0435 8.0185 7.1110 0.9075 4.4130 4.3668 0.0462 8.1592 7.1648 0.9944 4.3747 4.3320 0.0427 7.9248 6.8942 1.0306 4.0363 3.9905 0.0458 7.7323 6.7100 1.0223 4.5191 4.4760 0.0431 7.9010 6.8828 1.0182 3.9890 3.9542 0.0348 7.9580 6.8975 1.0605 4.4513 4.4149 0.0364 8.1092 7.1504 0.9588 4.2383 4.2005 0.0378 7.9875 7.0192 0.9683 4.2586 4.2185 0.0401 8.1262 7.1210 1.0052 4.3277 4.2885 0.0392 8.0758 7.1261 0.9497 4.6044 4.5608 0.0436 7.9325 6.9220 1.0105 4.2129 4.1698 0.0431 8.0131 7.1668 0.9895 4.2982 4.2610 0.0372 8.1027 7.0236 0.9419 4.2101 4.1740 0.0361 7.8302 6.7683 1.0619 4.4089 4.3780 0.0309 7.8288 6.8537 0.9751 4.1270 4.0931 0.0339 8.0213 6.9717 1.0496 4.4649 4.4187 0.0462 7.7778 6.7855 0.9923 4.4168 4.3623 0.0545 8.0244 7.1329 0.8916 4.5265 4.4940 0.0325 706267 6.7200 0.9067 4.2685 4.2420 0.0215 65 Table 4.17 MRR &EWR for Electrode EDM4 No. of Trail 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 4.3.2 Volume of material Removal (mm³) 0.1231 0.1161 0.1272 0.1318 0.1307 0.1302 0.1356 0.1226 0.1238 0.1289 0.1214 0.1292 0.1265 0.1204 0.1358 0.1247 0.1342 0.1268 0.1140 0.1159 Machining Time (min.) Response 1 (MRR) mm³/min Response 2 (EWR)‰ 96.31 25.55 41.22 55.38 51.15 54.40 97.09 105.2 274.30 35.07 218.28 107.58 144.09 62.01 137.30 21.09 226.26 373 82.46 179.0 1.2782 4.5440 3.0859 2.3799 2.5558 2.3934 1.3966 1.1654 0.5030 3.6755 0.5602 1.2009 0.8779 1.9416 0.9891 5.9127 0.6100 0.5100 1.3825 0.7082 4.5181 5.0910 4.2940 4.4440 4.2159 3.4178 3.4323 3.9424 4.1413 0.0389 4.5909 4.2652 3.7595 3.8327 2.9098 3.4766 4.4016 5.4922 3.6451 2.3712 Microcracks Table 4.18 shows the summary of Length of microcracks for 20 trials, all the measurements were conducted using Scanning Electron Microscope (SEM) Philips XL40. Each section was measured for three times before the average results were obtained. However, the data indicated in Table 4.5 shows the machining results response for EDM200 electrode. 66 Table 4.18 Machining response results for Electrode EDM200 Factors Response No of Trial V (volt) P (amp) A (µsec) R (µsec) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 80 24 400 4.3.3 120 120 120 80 80 120 120 80 120 80 80 80 120 80 120 80 120 120 120 48 24 48 24 24 24 24 48 48 24 24 24 48 48 48 48 48 48 24 400 100 100 100 100 400 100 400 100 400 100 100 100 400 100 100 400 100 400 Ra µm L.O.C µm MMR mm³/min EWR ‰ 0.8 9.981 35.13 1.2782 4.5181 0.8 10.317 26.54 4.5440 5.0910 0.8 9.9477 40.88 3.0859 4.2940 3.2 9.100 66.9 2.3799 4.4440 0.8 8.659 45.26 2.5558 4.2159 0.8 9.943 21.41 2.3934 3.4178 0.8 9.671 75.45 1.3966 3.4323 3.2 8.825 71.11 1.1654 3.9424 3.2 11.518 152.35 0.5030 4.1413 0.8 11.654 35.18 3.6755 0.0389 3.2 8.456 207.85 0.5602 4.5909 0.8 10.078 40.1 1.2009 4.2652 3.2 7.681 219.2 0.8779 3.7595 0.8 9.697 38.49 1.9416 3.8327 0.8 13.842 60.35 0.9891 2.9098 0.8 9.475 80.5 5.9127 3.4766 3.2 9.924 44.04 0.6100 4.4016 3.2 9.627 82.42 0.5100 5.4922 0.8 10.356 37.77 1.3825 3.6451 3.2 18.188 64.25 0.7082 2.3712 ANOVA Analysis All data obtained for Electrode EDM4 were then used as input to the Design Expert software for further analysis, according to steps outline for full factorial design Table 4.19 67 4.3.3.1 Analysis Results for Surface Roughness, Ra Based on Table 4.19, there are two factors affecting the surface roughness, Ra. According to the analysis done in the Design Expert software, when the values of probability (Prob>F) are less than 0.05. In this investigation, 95% of confidence interval (CI) is used. The information was better illustrated in half normal probability plot as shown in Figure 4.9. This graph is required in order to check for normality of residuals of the factors studied. Table 4.19 ANOVA for surface roughness, Ra 68 As displayed in the Figure 4.9, the significant factors highlighted were pulse width (ON) and servo voltage (SV) which denoted as A,C,AD,CD, and ABD respectively. In order to have clearer observation and better understanding of the response, the main effect plot is available.. Therefore, only the main effects of Ra which are pulse width (ON) and servo voltage (SV) were showed. Figure 4.9 Half Normal probability plots for Ra. From the interaction plot, it was clearly showed that whenever IP increased from 24 A. to 48 A, the value of Ra also decreased dramatically. From 10.905to 9.0625, meanwhile, a reverse result was observed for SV effect as the graph showed that Ra decreased when SV increased from 80 volt to 120 volt. The decreasing of Ra was 11.48 to 8.11. Based on the ANOVA analysis, to obtain better Ra during EDM Sinker of hardened steel, IP should be set at 48A.while SV at 80 V. 69 Figure 4.10: Interaction plot for Ra 4.3.3.2 Analysis Results for Material Removal Rate MRR Next analysis is to determine which factor and interaction affecting the response of material removal rate (MRR), this was done by considering the result from ANOVA obtained from the software. According to Table 4.20, there is no any factor affecting the material removal rate (MRR). According to the analysis done in the Design Expert software, when the values of probability (Prob>F) are less than 0.05, it shows that the entire factors are not significant. In this investigation, 95% of confidence interval (CI) is used. The information was better illustrated in half normal probability plot as shown in Figure 4.11. Based on Figure 4.11, the significant factor was observed better in the half normal probability plot of the standardized effects. In order to have clearer observation and better understanding of the response, the main effect plot is available, .therefore, only the main effects of MRR which are peak current (IP) and pulse ON were showed. 70 Figure 4.11 Half Normal probability plots for MRR. Table 4.20 ANOVA for surface roughness, MRR 71 Figure 4.12: Interaction plot for MRR Figure 4.12 show the main effects plot, it was clearly showed that when IP increased from 24 amps to 48 amps. The decreasing of MRR was about 2.4975 to 1.805 meanwhile, but, when pulse ON increasing from100µs to 400µs. the decreasing of MRR from 1.9375 to 1.0125.Based on the ANOVA analysis, ON and IP were affecting the MRR, therefore, in order to obtain better MRR during EDM Sinker of hardened steel, ON should be set at 100 µs while IP at 24 A. 4.3.3.3 Analysis Results for Electrode Wear Rate (EWR %) The third analysis is to determine which factors and interaction that affects the Electrode Wear Ratio (EWR) Similar procedures were done in analyzing the significant factor and the possible interaction as discussed in previous section, whatever factors that have the “Prob>F” less than 0.05 are considered significant for EWR with the confidence interval (CI) used is 95%.Therefore, based on ANOVA analysis and half normal probability plot shown in Table 4.21 and Figure 4.13 respectively, all factors were effects were are not significantly . 72 Table 4.21 ANOVA for Electrode Wear Rate (EWR %) Figure 4.13 Half Normal probability plots for EWR% 73 Figure 4.14 shows that, Electrode Wear Ratio (EWR) was affected by servo voltage SV, and peak Current IP, Based on the graph, EWR increased dramatically from 3.805 to 4.5325 Meanwhile, EWR was observed to decrease as SV increased, were decreased from 4.1575 to 4.0575.Based on this relationship, maximum EWR. Can be obtained when the parameters are set at IP = 48 A, and SV = 120 V. Figure 4.14: Interaction plot for EWR% 4.3.3.4 Analysis Results for Microcracks Last analysis is to determine which factor and interaction affecting the response of microcracks, this was done by considering the result from ANOVA obtained from the software, according to the table 4.22, the factors which are affecting the Microcracks are servo voltage S.V and pulse off, according to the analysis done in the Design Expert software, when the values of probability (Prob>F) are less than 0.05, it shows that factors are significant to the microcracks, in this investigation, 95% of confidence interval (CI) is used. The information was better illustrated in half normal probability plot as shown in Figure 4.15. This graph is required in order to check for normality of residuals of the factors studied. 74 Table 4.22 ANOVA for Microcracks Based on Figure 4.15, the significant factors were observed better in the half normal probability plot of the standardized effects. As displayed in the Figure 4.15, the most significant factors highlighted were pulse OFF and servo voltage (SV) which denoted as A, D, and AD respectively. In order to have clearer observation and better understanding of the response, the main effect plot is available. Therefore, only the main effects of micro-cracks which are servo voltage (SV) and pulse off were showed. 75 Figure 4.15 Half Normal probability plots for microcracks From the interaction plot, it was clearly shown that whenever IP increased from 24 A to 48 A, the value of microcracks will be decreased dramatically from 96.1275µm to 65.1325 µm. Meanwhile, when SV increased from 80 v to 120 v, the decreasing of microcracks from 112.98 µm to 30.405 µm. In order to obtain better Microcracks during EDM Sinker of hardened steel, IP should be set at 48A.while SV at 80 volt. Figure 4.16: Interaction plot for Microcracks 76 4.3.4 Confirmation Tests for EDM200 Table 4.23 Quality characteristics of the machining performance.EDM200 Machining Characteristics Quality Characteristics Surface roughness (Ra) Maximum Material Removal Rate (MRR) Maximum Electrode Wear Rate (EWR) Minimum Micro-cracks Minimum Table 4.24: Confirmation test results for surface roughness, Ra. Exp. Trial Trial condition Repeat 1 Ra (µm) Repeat 2 Ra (µm) Repeat 3 Ra (µm) Total Average (µm) 12 ON = 100µs OFF = 3.2 µs IP = 24 A SV = 120 v 17.996 18.38 17.40 18.21 Table 4.25: Confirmation test results for microcracks Confirmation test results for micro-cracks Exp. Trial Trial Condition 2 ON = 400µs OFF = 0.8 µs IP = 48 A SV = 120 v Repeat 1 (µm) Repeat 2 (µm) Repeat 3 (µm) Total Average (µm) 34.27 41.27 37.01 37.72 77 Table 4.26: Confirmation test results for Material Removal Rate MRR. Exp. Trial Trial Condition 6 ON = 100µs OFF =.0.8 µs IP = 44 A SV = 120 v Material Removal Rate MRR Confirmation Test Results Repeat 1 Repeat 2 Total Average mm³/min mm³/min mm³/min 6.01 5.88 5.91 Table 4.27: Confirmation test results for Electrode Wear Rate EWR%. EWR%. Confirmation Test Results 4.3.5 Exp. Trial Trial Condition 2 ON = 100µs OFF = 0.8 µs IP = 48 A SV = 120 v Repeat 1 Repeat 2 Repeat 3 Total Average 3.41 4.01 3.65 3.645 Comparison of Test ResultsEDM200 As mentioned before, three confirmation runs were conducted in order to measure the reliability of optimization solutions obtained from the software analysis. The comparison of test results between the theoretically prediction and confirmation test results was the final consideration that will evaluate whether the optimum parameters predicted were in the allowable range. The margin of error from the prediction and experimental results was set below than 11 %.( 10.72%) Margin error was calculated using the equation below Margin error % = [(Confirmation on test result – Predicated result) / Predicated result] x 100% 78 According to the Final Equation in Terms of Coded Factors and Final Equation in Terms of Actual Factors given in ANOVA table analysis ,we can found the value of the prediction and confirmation test results which illustrated in appendix (E) Prediction equation = f x (Duty fact, pulses, current, SV) Table 4.28: Comparison test results for all responses.EDM200 Response factors Prediction (Design Expert) Experimental (Confirmation Test) Error Margin (%) Ra 16.49 18.19 10.31 MRR 4.68 5.91 26.28 EWR 3.05 4.26 39.67 Crack 56.62 37.72 -33.38 NOTE: All the mathematical relations for prediction result and confirmation test are illustrated in appendix (E). 4.4 Summary This chapter discusses the results and discussions on this project. The experimental results for EDM4 and EDM200, where each one included the experiment results tables, ANOVA ANALYSIS and confirmation tests and finally to determined the margin of error from the prediction and experimental results for each EDM electrodes. 78 CHAPTER 5 PERFORMANCE COMPARISON BETWEEN GRAPHITE ELECTRODES 5.1 Introduction This chapter focuses more on the significant parameters that have great influence on the performance of machining characteristics such as, surface roughness (Ra), Material Removal Rate (MRR), Electrode Wear Rate (EWR) and Microcracks. Additionally, an explanation on why there was almost no observation of Microcracks presence in this study will also is included. Although DOE has greatly contributed to the analysis of all studied responses, the information provided was still lacking in understanding the EDM sinker process for ease of optimization. The information which was provided through statistically process was only based on numbers and plotted graphs; therefore it is required for further interpretation and discussion in terms of relating them back to the actual machining process. In this chapter, the discussions are made unilaterally according to each response. 79 5.2 Surface Roughness, Ra According to the results obtained from the Design Expert software tables 4.6 and 4.19, servo voltage (SV) was the main factors that affect on the roughness response (Ra) were found that when SV increase from 80 volt to 120 volt., Ra (for EDM4) increased from 9.64425 to 10.5055 while for EDM200 decreased 11.48 to 8.11 While the maximum value found with EDM4 which is about 11.7µm while with EDM200 only 18µm.Therefore, the optimal signal setting to get maximum amount for Ra with EDM4 are ON = 100µ ,OFF = 3.2 µs ,IP = 2.4 A and SV = 120 v. and for EDM200 was ON = 100µs, OFF = 3.2 µs, IP = 24 A and SV = 120 v Finally, the margin error obtained from the comparison test for the Surface Roughness, Ra EDM4 was 7.01%.,while for EDM200 was 10.31% 5.3 Material Removal Rate MRR From the analysis it could be see that the servo voltage and pulse width ON are the most significant factor compared to another factors. As given by the Design Expert software tables 4.7 foe EDM4, but with EDM200 there were no significant factors. Therefore, the maximum value of material removal rate for EDM4 was 6.4mm/min, while for EDM200 the maximum value of material removal rate was 5.9 mm/min where the value of the servo voltage is increased from 80 v to 120 v. the increasing of MRR was from 2.68275 to 3.07mm/min, while in EDM4 was. Increased from 2.68275 to 3.07mm/min .Therefore, the optimal signal setting to get maximum amount for MRR with EDM4 are ON = 100µs, OFF =.0.8 µs, IP = 48 A and SV = 120 v., and for EDM200 was ON = 100µs, OFF =.0.8 µs, IP = 44 A and SV = 120 v .finally, the margin error obtained from the comparison test for the material removal rate for the EDM4 was 6.38%. While for EDM200 was 26.28% 80 5.4 Electrode Wear Rate EWR From the analysis it observed that the pulse off and pulse width ON are the most significant factor compared to another factors, as given by the Design Expert software tables 4.8 foe EDM4, but with EDM200 there were no significant factors. Therefore, the maximum value of electrode wear rate for EDM4 was 8.8, while for EDM200 the maximum value of electrode wear rate was 5.49 where the value of the pulse off is increased from 0.8 v to 3.8 µsec. the increasing of EWR from 3.805 to 4.5325 while in EDM4 was increased dramatically from 1.69625 to 5.4165 Therefore, the optimal signal setting to get maximum amount for EWR with EDM4 ON= 400µs ,OFF = 0.8 µs ,IP = 48 A ,and SV = 120 v., and for EDM200 was ON = 100µs, OFF =.0.8 µs, IP = 48 A and SV = 120 v .finally, the margin error obtained from the comparison test for the material removal rate for the EDM4 was 9.23%. While for EDM200 was 39.6% 5.5 Microcracks According to the results obtained from the Design Expert software tables 4.9 and 4.22, servo voltage (SV) and pulse off was the main factors that affect on the microcracks were found that when SV increase from 80 volt to 120 volt., cracks (for EDM4) increased from50.2 to 87.2 µm while for EDM200 decreased 112.98 µm to 30.405 µm While the maximum value found with EDM4 which is about 11.7µm while with EDM200 only 18µm.Therefore, the optimal signal setting to get maximum amount for Ra with EDM4 are ON = 400µ ,OFF = 0.8 µs ,IP = 48 A and SV = 120 v. and for EDM200 was ON = 400µs, OFF = 0.8 µs, IP = 48 A and SV = 120 v Finally, the margin error obtained from the comparison test for the Surface Roughness, Ra EDM4 was 2.31%.,while for EDM200 was -33.38% 81 5.6 summary Generally, the result obtained and data analysis is acceptable. All the results obtained one in agreement with the general trends obtained by other researchers. According to the actual design of experiment, replication of experiment is important to ensure that all data is accurate and acceptable..But due to several difficulties during this project ,only one replicate has been done for each electrode experiment and these experiment just follow the P-value from the response surface analysis ,also this experiment has been conducted 100%random manner . The die-sinking electrical discharge machine model Chamilles ROBOFORM 100 is a CNC machine if the machining conditions are not suitable for the machine, the machine stops or the duration of interval between two pulses and the withdrawal time duration of pulsation are changed automatically. This affected the accuracy of the responses. EDM requires that the axis of the electrode be parallel to the direction of feed for true reproduction of the electrode shape .It was difficult to obtained this because of the way that the tool were machined and the machine`s condition which also effected on the accuracy of responses . 82 CHAPTER 6 CONCLUSION AND RECOMMENDATIONS 6.1 Conclusions Basically, this study evaluates the machining performance of hardened steel material (ASSAB718) when machined using two different grades of graphite electrodes. All the experiments trials, planning and analysis were executed using two-level full factorial design of experiment. The purposes of DOE method applied in this study were to determine the optimum condition of machining parameters and the significance of each parameter to the performance of machining characteristics. The total experiment runs performed in this study was 20 trials for each electrode using randomized parameters and analyzed using by Design Expert software. The following conclusions are drawn based on the performance of machining characteristics studied in this research work. 1) Within the range of parameters tested using EDM4 electrode material the recommended condition to get maximum MRR are the machining voltage at level 120 v, peak current 48 A, and pulse ON time at 100 µsec .While for EDM200 electrode, the recommended conditions to get maximum MRR are the machining voltage at level 80 v, peak current 48 A, and pulse ON time at 400µsec. The 83 machined workpiece surface roughness increases steadily with increasing MRR; therefore, referred to the overall machining results tables in chapter 4 EDM4 is better to used for hardened steel material to produced high Material Removal Rate (MRR), low roughness, less length of Microcracks and short machining time, but with high EWR%. 2) The most significant factors that effecting the quality of machining Characteristic is the servo voltage was the most significant factor affecting the responses, According to ANOVA ANALAYSIS tables studied in chapter 4. Finally, the objective of this project is generally achieved. From the design of experiment methodology, it is found that the, servo voltage and pulse of signal have appeared to be significant to all responses investigated. Overall, the results from the confirmation tests showed that the percentage of performance was acceptable due to all the results obtained were within the allowable value which was less than 11% of margin error for EDM200 and 7.23% for EDM4 electrodes respectively .Even though there is a lot of variation influencing the data. The results in this project could be used as a basis for further investigation in electrical discharge machining of hardened steel ASSAB718 6.2 Recommendations Based on the current findings, the following recommendations for future works are proposed as follows: 1. Use of different grades of graphite as the tool electrode for better understands 84 its effect upon the machined surface and machining parameters in machining hardened steel material. 2. Study the effects of additives in dielectric fluid increasing the effectiveness of material removal rate 3. Study on the effect of residual stress on the specimens after being machined at high removal rate. 4. 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(2002). “Machining Characteristics of Al2O3 / 6061 Al Composite Using Rotary EDM with a Dislike Electrode.” The International Journal of Advances Manufacturing Technology, 16: pp. 322-333. 88 APPENDIX A THE OVERALL MEASUREMENT RESULTS FOR SURFACE ROUGHNESS EDM4 ELECTRODE 89 RUN #1: RUN#2 RUN #3: RUN #4 90 RUN #5: RUN #6: 7) RUN #8: RUN #7: 91 9) RUN #9: 11) RUN #11 10) RUN #10 12) RUN #12 92 13) RUN #13 14) RUN #14 15) RUN #15 16) RUN #16 93 17) RUN #17 18) RUN #18: 19) RUN #19 20) RUN #20 94 APPENDIX B THE OVERALL MEASUREMENT RESULTS FOR SURFACE ROUGHNESS EDM200 ELECTRODE 95 1) 3) RUN #1: RUN #3: 2) RUN #2: 4) RUN #4: 96 5) RUN #5: 6) RUN #6: 7) RUN #7: 8) RUN #8: 97 9) RUN #9: 10) RUN #10: 11) RUN #11: 12) RUN #12: 98 13) RUN #13: 14) RUN #14: 15) RUN #15: 16) RUN #16: 99 17) RUN #17: 18) RUN #18: 19) RUN #19: 20) RUN #20 100 APPENDIX C THE OVERALL MEASUREMENT RESULTS FOR MICROCRAKES STRUCTURE EDM4 ELECTRODE 101 1) RUN #1: 2) RUN #2 4) 3) 4) RUN #4 RUN #1: 102 5) RUN #5 6) RUN #6 7) RUN #7 8) RUN #8 103 9) RUN #9 10) RUN #10 11) RUN #11 12) RUN #12 104 13) 15) RUN #13 RUN #15 14) RUN #14 16) RUN #16 105 17) RUN #17 18) RUN #18 19) RUN #19 20) RUN #20 106 The microcracks on the surface of EDM machining at 250x magnification on trial 2 of graphite electrode Microcracks at 160volt, 64amperes, and 50µsecond of pulse interval (magnification 2500x) on graphite electrode 107 APPENDIX D THE OVERALL MEASUREMENT RESULTS FOR MICROCRAKES STRUCTURE EDM200 ELECTRODE 108 1) RUN 1 2) RUN 2 1) RUN 3 4) RUN 4 109 6) RUN 5 7) RUN 7 6) 9) RUN 8 RUN 6 110 8) RUN 9 10) RUN 10 10) RUN 11 12) RUN 12 111 13) RUN 13 14) RUN 15 14) 16) RUN 14 RUN 16 112 17) RUN 17 17) RUN 19 18) 20) RUN 18 RUN 20 113 NOTE: All the above diagrame of creacs are taken with magnification optical (10 *50) 500x Microcracks at 80volt, 48amperes, and 100µsecond of pulse interval (magnification 2500x) on graphite electrode EDM4 Microcracks at 80volt, 24amperes, and 4000µsecond of pulse interval (magnification 2500x) on graphite electrodeEDM200 114 APPENDIX E THE OVERALL ANALYSIS RESULTS FOR PREDICTED AND ACTUAL COMFORIMATION TESTS FOR EDM200 AND EDM4 ELECTRODES 115 EDM4 Analysis Results for Surface Roughness, Ra 116 Analysis Results for Material Removal Rate MRR 117 Analysis Results for Electrode Wear Ratio (EWR) 118 Analysis Results for Microcracks 119 Analysis of Results for EDM200 electrode Analysis Results for Surface Roughness, Ra 120 Analysis Results for Material Removal Rate MRR 121 Analysis Results for Electrode Wear Ratio (EWR) 122 Analysis Results for Microcracks