M. S. RAMAIAH INSTITUTE OF TECHNOLOGY BANGALORE-54 Autonomous Institute, Affiliated to VTU SYLLABUS (For the Academic year 2015 - 2016 VII and VIII Semester B. E. CHEMICAL ENGINEERING M.S. RAMAIAH INSTITUTE OF TECHNOLOGY, BANGALORE – 560 054 DEPARTMENT OF CHEMICAL ENGINEERING 1. History of the Institute: M. S. Ramaiah Institute of Technology was started in 1962 by the late Dr. M.S. Ramaiah, our Founder Chairman who was a renowned visionary, philanthropist, and a pioneer in creating several landmark infrastructure projects in India. Noticing the shortage of talented engineering professionals required to build a modern India, Dr. M.S. Ramaiah envisioned MSRIT as an institute of excellence, imparting quality and affordable education. MSRIT being a part of Gokula Education Foundation, has grown over the years with significant contributions from various professionals in different capacities, ably led by Dr. M.S. Ramaiah himself, whose personal commitment has seen the institution through its formative years. Today, MSRIT stands tall as one of India’s finest names in Engineering Education and has produced around 35,000 engineering professionals who occupy responsible positions across the globe. 2. History of the Department: Instituted in 1978, the Department was the first to offer a course in Chemical Engineering by a selffinancing engineering institution in Bangalore and the fifth in MSRIT. Since its inception the department has moved steadily towards the fulfillment of its mission and is emerging as a significant player in the academic landscape of Chemical Engineering education in our country. The Department is certified thrice in succession by the National Board for Accreditation, once by National Assessment and Accreditation Council and is also ISO 9001:2008 certified for imparting quality education. Over 1900 students have graduated in 32 batches. The Department has secured majority of the university ranks. The expertise of the faculty covers a wide range of disciplines and they are engaged in cutting edge technological research. The average experience of faculty in the department is more than twenty years and they are alumni of IISc, IIT and NITs. The Department follows Outcome Based Education system which is designed for students to achieve the specified outcomes of the course. Enriching insights by eminent dignitaries from the practicing world is arranged under the activities of Society of Chemical Engineers, a body comprising of chemical engineering community of the institute. The Department is approved as Research Center by VTU for higher qualifications like M.Sc. Engg. (by Research and Ph.D. degrees. Research Projects from DRDO, AICTE and VTU have been successfully completed. The Annual Technical Symposium organized by the department for students – RASAYAN encompasses a plethora of events such as Paper presentations, Poster presentations, M.S. Ramaiah Memorial Technical Quiz etc to challenge the young minds. The Bangalore Regional Centre of the Indian Institute of Chemical Engineers is functioning from this Department for more than a decade. The country’s most prestigious event in Chemical Engineering, Indian Chemical Engineering Congress - CHEMCON-2011 was organized here. The department offers excellent infrastructure and students have won various prestigious awards, international internships and high accolades for innovative projects. 3. Faculty List: Sl. Name of the Faculty No. 1 Dr. Archna 2 Dr. Y J Rao 3 Dr. V.Venkatesham 4 Sri. S. Swaminathan 5 Sri. Ravi Sadasivan 6 Sri. K.A. Badarinarayana 7 Dr. G. M. Madhu 8 Dr. Brijesh 9 Dr. Rajeswari M. Kulkarni 10 Sri. Ramasivakiran Reddy 11 Sri. Koteswara Rao Jammula 12 Smt.V. Shravanti 13 Ms. Annapurna S M Qualification Designation M.E, Ph.D. M. E, Ph.D. M. E, Ph.D. M. E. M.S.(Research), (Ph.D) M.Tech. M.E., Ph.D. M.Tech., Ph.D. M.Tech, Ph.D. M.Tech. (Ph.D) M.Tech., (Ph.D) M.Tech., (Ph.D) M.Tech. Professor and Head Professor Emeritus Associate Professor Associate Professor Associate Professor Associate Professor Associate Professor Associate Professor Assistant Professor Assistant Professor Assistant Professor Assistant Professor Assistant Professor 4. Vision & Mission of the Institute: The Vision of MSRIT: To evolve into an autonomous institution of international standing for imparting quality technical education. The Mission of the Institute in pursuance of its Vision: MSRIT shall deliver global quality technical education by nurturing a conducive learning environment for a better tomorrow through continuous improvement and customization. 5. Vision & Mission of the Department: Vision: To be a leading chemical engineering centre for quality technical education and progressive research at global level. Mission: 1. To provide a state of art environment and a rigorous academic program that trains students to excel in fundamental science, chemical and allied engineering fields. 2. To offer programme that inculcates creative thinking and lifelong learning, contributing to the advancements of chemical sciences and its application. 3. To foster principles of sustainability and promote environmentally benign technologies for the benefit of society. 6. Process of deriving the Vision & Mission of the Department: Institute’s Vision and Mission Department Faculty Alumni Definition of of Vision and Mission of the department by the committee Industry Students Management 7. Process of Deriving the PEO’s of the Programme: Institute Vision & Mission Department Vision & Mission Committee formation & preparation of questionnaire Conduction of survey Students Industry Alumni Collect data (Department Committee) Deliberate Analyze and summarize the data in Board of Studies Approved in Academic Council & Governing Council PEOs 8. PEO’s of the programme offered: The B.E. Chemical Engineering Program at M. S. Ramaiah Institute of Technology aims to provide a strong foundation of scientific and technical knowledge in a state of art learning ambience. It equips the graduates with problem solving abilities, teamwork, and communication skills necessary throughout their careers. They are consistent with the following Educational Objectives: 1. To provide a strong foundation and understanding of the fundamental principles of mathematics, science, and engineering enabling graduates to pursue their careers as practicing chemical engineers in Chemical and Allied Engineering Industries. 2. To produce graduates who are prepared to pursue their post graduation and Research in the fields of Chemical Engineering and Petrochemicals, Material Science, Biotechnology, Nanotechnology, Environmental Engineering, any emerging allied areas and Business. 3. To produce graduates who posses skills with contemporary grounding in professional responsibility, ethics, global and societal impact of engineering decisions to assume professional leadership roles and administrative positions. 4. To provide students with opportunities to participate in various multidisciplinary teams and to develop and practice written and oral communication skills. 9. Process of deriving PO’s: The Programme outcomes are defined by taking feedback from faculty, alumni, Industry, professional bodies, guidelines suggested by regulatory bodies (UGC, AICTE, VTU and Graduate Attributes suggested by National Board of Accreditation. The established PEO’s are in line with programme educational objectives. The following Figure indicates the information flow. 10. PO’s of the programme offered: The Chemical Engineering Graduates of MSRIT are expected to have the following abilities/ qualities. a. An ability to apply knowledge of mathematics, science and engineering fundamentals. b. An ability to design and conduct experiments, and to analyze and interpret experimental results with working knowledge of chemical process safety. c. An ability to design systems, components, or processes to meet specified objectives within all the realistic constraints of sustainable technology. d. An ability to identify, formulate, and solve complex chemical engineering problems. e. An ability to use techniques, skills and modern engineering tools necessary for engineering practice. f. An ability to understand the professional, societal and ethical responsibility. g. An ability to work as a member of multidisciplinary teams, and have an understanding of team leadership. h. To have good written and oral communication skills. i. An ability to understand the impact of engineering solution in a global, economic and societal context. j. An ability to have motivation and engage in lifelong learning. k. An ability to have knowledge of recent happenings/contemporary issues. l. To have the knowledge of project management and finance requirements and able to write project proposals. 11. Mapping of PEO’s & PO’s: Programme Educational Objectives 1 2 3 4 a X X b X X c d X X X X X Programme Outcomes e f g h i X X X X X X X X X X j X k X X l X X X 12. Curriculum breakdown structure: 13. BOS composition as per VTU Guidelines: SCHEME OF TEACHING AND EXAMINATION – VII SEMESTER B.E. CHEMICAL ENGINEERING (2015-16 Sl. No. Subject Code Title of the Subject Credits (L:T:P Teaching Dept. Teaching hours/week L T P Marks End Exam (Hrs CIE SEE Total 1 CH701 Process Integration 3:0:0 CH 3 0 0 03 50 50 100 2 CH702 Process Control 3:1:0 CH 3 2 0 03 50 50 100 3 CH703 Transport Phenomena 3:1:0 CH 3 2 0 03 50 50 100 4 CHPE03x Elective – Group C 3:0:0 CH 3 0 0 03 50 50 100 5 CHPE04x Elective – Group D 3:0:0 CH 3 0 0 03 50 50 100 6 CHL701 Process Simulation Laboratory 0:0:2 CH 0 0 3 03 50 50 100 7 CHL702 Process Control Laboratory 0:0:2 CH 0 0 3 03 50 50 100 8 CH704 Design Project 0:0:2 CH 0 0 2 03 50 50 100 9 CH705 Inplant training/ Industrial visit Compulsory for completing the course 23 21 8 4 8 Elective –Group C Elective-Group D CHPE031 Principles of Food Processing and Preservation CHPE041 Polymer Processing Technology CHPE032 Advance Bioprocess Engineering CHPE042 Interfacial Phenomenon and Surface Engineering CHPE033 Electrochemical Technology CHPE043 Separation Techniques CHPE034 Process Optimization CHPE044 Multicomponent Distillation CHPE035 Modeling of Chemical Processes CHPE045 Applied Mathematics in Chemical Engineering Open Electives Offered CHOE01 Green Technology 9 SCHEME OF TEACHING AND EXAMINATION – VIII SEMESTER B.E. CHEMICAL ENGINEERING (2015-16 Sl. No. Subject Code Title of the Subject 1 CH801 2 CHPE05x 3 HSS802 4 OE 5 CH803 Credits (L:T:P Economics and Entrepreneurship Elective – Group E Teaching Dept. Teaching hours/week L T P Marks End Exam (Hrs CIE SEE Total 4:0:0 CH 4 0 0 03 50 50 100 3:0:0 CH 3 0 0 03 50 50 100 Principles of Management Open Elective-I 3:0:0 CH 3 0 0 03 50 50 100 3:0:0 AL 3 0 0 03 50 50 100 Project Work 0:0:14 CH 0 0 28 03 100 100 200 10 0 28 27 Elective –Group E CHPE051 Solid Waste Management CHPE052 Scale Up of Chemical Processes CHPE053 Environmental Impact Assessment CHPE054 Introduction to Nanotechnology CHPE055 Research Methodology and Technical Report Writing Open Electives Offered CHOE01 Green Technology Legend: CH- Chemical Engineering Department, AL- Other departments, L-Lecture, T-Tutorial, P-Practical, CIE-Continuous Internal Evaluation, SEE-Semester End Examination. 10 Semester VII PROCESS INTEGRATION Sub Code: Credit: CIE: CH701 3:0:0 50 Marks Contact Hours: 42 SEE: 50 Marks Pre-requisites: Process Heat Transfer, Mass Transfer I and II Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Study the need for integration and pinch technique for direct recycle problems. 2. Learn graphical techniques for direct recycle and synthesis of mass exchange networks. 3. Learn algebraic approach for direct recycle and Heat integration technologies. 4. Learn graphical and algebraic methods for Heat and Power integration. 5. Learn Optimization by mathematical approach to direct recycle and synthesis of mass & heat exchange networks.. 6. Learn mathematical Techniques for mass integration, Initiatives and applications and few Case studies. Course Content: Unit I Introduction to Process Integration: Graphical Techniques. Overall mass targeting. Unit II Synthesis of Mass Exchange Network: Graphical approach. Direct recycle strategies. Unit III Visualization Strategies: For development of mass integrated system. Algebraic approach to targeting direct recycles Unit IV Algebraic Approach: To targeting mass exchange. Network. Recycle strategies using property integration. Heat Integration: Synthesis of Heat Exchange Networks (HENs, Heat Exchange Pinch Diagram, Screening of Multiple Utilities Using the Grand Composite Representation Unit V Combined heat and power integration. Optimization: Mathematical approach to direct recycle. Text Books: 1. Robin Smith, Chemical Process Design & Integration , Wiley, 2005. 2. Mahmoud. M., El – Hawalgi, Process Integration, Elsevier, 2006. 11 Reference Book: 1. Kemp I.C, Pinch Analysis and Process Integration - A user guide on process integration for efficient use of energy, 2nd Edition, Butterworth – Heinneman, 2006. Course Outcomes: On successful completion of this course students will be able to S. No. Course Outcome 1. Explain the need for Mass and Heat integration in chemical industries. 2. Calculate the minimum amount of heat required in heat integration and minimum quantity of fresh reactant require in mass integration by graphical and algebraic methods. 3. Calculate the minimum fresh solvent required in mass exchange networks by graphical and algebraic methods. 4. Calculate the minimum heating and cooling requirements for given process using pinch analysis by graphical and algebraic methods 5. Able to find the quality heating requirements in process flow diagram and able to optimize of mass and heat integration problems by Linear programming method. 12 Programme Outcomes Satisfied a,c,d,e,f,j a,c,d,e,f,j a,b,c,d,f a,c,d,e,f,j a,c,d,e,f,j PROCESS CONTROL Sub Code: Credit: CIE: CH702 3:1:0 50 Marks Contact Hours: 70 SEE: 50 Marks Pre-requisites: Engineering Mathematics II Course coordinator: Department of Chemical Engineering Course Objectives: The student will 1. Understand the dynamics of the behaviour of I and II order type processes. 2. Understand closed loop systems and Controllers (P, I, D and On – Off modes 3. Study the transient response of above control systems 4. Learn the stability criteria - Routh and Bode – root locus diagrams 5. Learn to tune controllers, identify processes.Study the basics of advanced control techniques: (Cascade Control, Ratio control, Feed forward Course Content: Unit I First order systems: Thermometer, level, mixing tank, STR: Linearisation: I order systems in series. Response for various input forcing functions. Second order systems: Characteristics. Transfer functions. Response for various input forcing functions. Transportation lag. Unit II Control System: Basic components, Servo and Regulator control. Controllers: P,I,D and on-off modes. Controller combinations. Final Control Elements: Valves, actuators, valve positioners, valve characteristics. Close Loop: Block diagram. Closed loop transfer function. Unit III Transient response of servo and regulator control systems with various controller modes and their characteristics. Unit IV Stability: Stability of linear control systems. Routh Test. Frequency Response – Bode diagrams, Bode criterion. Control system Design by Frequency Response:. Gain and Phase margins. Ziegler – Nichols rules. Root Locus: Root locus techniques, plotting. Unit V Controller tuning: Ziegler – Nichols method, Cohen & Coon method. Process Identification Advanced Control Techniques: Introduction to Cascade Control, Ratio control, Feed forward control, Adaptive control. 13 Text Books: 1. Cougner, D.R., Process System Analysis and Control, 2nd Edition, McGraw Hill, 1991. 2. Stephanopolous, G., Chemical Process Control- An Introduction to Theory and Practice, Eastern Economy Edition, 2008. Reference Book: 1. Harriott, Process Control, Tata McGraw Hill, 1982. Course Outcomes: On successful completion of this course students will be able to S. Course Outcome No. 1. Analyze simple I and II order systems Programme Outcomes Satisfied a,b,e, j 2. Derive and understand the behaviour of different controllers. a,c,d,e,j,k 3. Analyze the transient response of feedback systems. a,c,d,e,h,i,j,k 4. Design stable control systems for processes. a,c,d,e,f,h,i,j,k 5. Identify process transfer functions.Understand the behaviour a,c,d,e,g,i,j,k of advanced control techniques. 14 TRANSPORT PHENOMENA Sub Code: Credit: CIE: CH703 3:1:0 50 Marks Contact Hours: 70 SEE: 50 Marks Pre-requisites: Momentum Transfer, Process Heat Transfer Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Learn the mechanisms and Laws transport phenomena, Effect of temperature and pressure on transport properties 2. Study velocity distributions in laminar flow for simple fluid flow situations by shell balances 3. Study temperature distributions in solids and in laminar flow for simple heat transfer situations by using shell balances 4. Study Concentration distributions in laminar flow for simple mass transfer situations by using shell balances 5. Learn and derive transport equations in all dimensions and apply them to solve above physical situations and study the analogies between Momentum, Heat and Mass Transport and apply these to common chemical engineering problems Course Content: Unit I Introduction: Momentum Energy and Mass Transport Newton’s law of viscosity (NLV. Newtonian and Non-Newtonian fluids. Fourier’s law of heat conduction (FLHC. Fick’s law of diffusion (FLD.Effect of temperature and pressure on transport properties of fluids. Numerical problems on the application and use of NLV, FLHC and FLD. Unit II Velocity Distribution in Laminar Flow: Steady state Shell momentum balances, Flow over a flat plate, Flow through a circular tube and Annulus, Flow between parallel plates and a slit. Numerical problems on the above situations. Flow of falling film on outside of a circular tube, annular flow with inner cylinder moving, Non Newtonian flow in a tube and over flat plate (Power law and Bingham fluids Unit III Temperature Distribution in Solids and in Laminar Flow: Steady State Shell Energy Balances, Different situations of heat transfer: Heat conduction with internal generation by electrical, nuclear, viscous energy sources. Heat conduction in a cooling fin: Forced and free convection heat transfer. Numerical problems. Unit IV Concentration Distributions in Laminar Flow: Concepts and definitions on transport velocities in a multicomponent system, Steady state Shell mass balances. Diffusion through stagnant gas and liquid films (isothermal and non isothermal films. Equimolar counter diffusion. Numerical problems. 15 Diffusion with homogeneous and heterogeneous reaction. Diffusion into falling film – Forced convection mass transfer. Unit V Analogies between Momentum, Heat and Mass Transport: Reynold’s, Prandtl’s and Chilton & Colburn analogies. Numerical problems. Equations of Change: Equation of continuity Equation of motion; Navier – Stokes equation. Application of these equations in solving simple steady state problems previously discussed. Text Book: 1. Bird, Stewart and Lightfoot, Transport Phenomena, John Wiley, 1994. Reference Books: 1. Welty, Wicks and Wilson, Fundamentals of Momentum, Heat and Mass Transport, 3rd Edition, John Wiley, 1983. 2. Mujumdar, A.S., Advances in Transport Processes, Wiley Eastern Ltd., 1980. Course Outcomes: The student should be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Explain different fundamental laws of transport and know the behaviour of transport properties to changes in operating conditions Derive mathematical equations by shell balance technique for different practical flow situations Derive mathematical equations by shell balance technique for different practical heat transfer problems Derive mathematical equations by shell balance technique for different practical mass transfer situations Apply transport equations to any kind of physical problem and develop mathematical equations representing the physics and explain and apply different analogies to common chemical engineering problems a,b,d,j 16 a,b,c,d,e,i,j a,b,c,d,e,i,j a,b,c,d,e,i,j a,b,d,e,j Sub Code: Credit: CIE: PRINCIPLES OF FOOD PROCESSING AND PRESERVATION CHPE031 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Nil Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Learn characteristics of foods, perishability of unmodified foods and objectives of preservation and processing of foods 2. Gain knowledge on Low temperature Preservation and processing of foods and storage and post-storage handling of foods, along with freezing techniques 3. Study high temperature methods of preservation and processing of foods by heat treatment 4. Learn methods of Preservation and processing by Dehydration with all relevant technological aspects 5. Study processing of milk and milk products, meat and meat products, vegetables and fruits Course Content: Unit I Basic consideration: Quality attributes of food, aim and objectives of preservation and processing of foods, food deterioration, causes of quality deterioration and spoilage of foods, unit operations in food processing. Unit II Low temperature Preservation and Processing of foods: Chilling temperatures: Considerations relating to storage of foods at chilling temperature, applications and procedures, controlled and modified atmosphere storage of foods, post-storage handling of foods. Freezing temperature: Freezing process, slow and fast freezing of foods and its consequences, other occurrences associated with freezing of foods. Technological aspects of pre-freezing, Actual freezing, frozen storage and thawing of foods. Unit III High temperature preservation and processing of foods: Basic concepts in thermal destruction of microorganisms-D, Z, F, values Heat resistance and thermophilisms in microorganisms. Cooking, blanching, pasteurization and sterilization of foods. Assessing adequacy of thermal processing of foods, general process of canning of foods, spoilages in canned foods. Unit IV Preservation by Dehydration and concentration: Principles, technological aspects and applications of concentration processes, drying and dehydration of food. Other techniques in preservation: Food irradiation, microwave heating, ohmic heating 17 Unit V Processing and preservation of food products: Processing and preservations of milk and milk products, vegetables and food, beverages, meat and meat products. Text Books: 1. Potter, N.N. and Hotchkiss, J.H., Food Science, 5th Edition, CBS Publishers and Distributors, 2006. 2. Sivasankar, B., Food Processing and Preservation, Eastern Economy Edition, 2005. Reference Books: 1. Shakuntala, N., Manay and Shadaksharamurthy, M., Foods: Facts and Principles, 3rd Edition, New Age International, 2008. 2. Subbulakshmi, G., and Udupi, S.A., Food Processing and Preservation, 1st Edition, New Age International ,2006. 3. Sahu, J.K., Fundamentals of Food Process Engineering, Narosa Publishing, 2014. Course Outcomes: The student should be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Know different characteristics of food along with the processing and preservation methods Explain low temperature preservation and processing systems and for storage of foods Explain high temperature preservation and processing of foods Explain other preservation techniques for food Understand processing and preservation of some important food products a,c,e,f,j,k 18 a,c,d,e,j,k a,c,d,e,j,k a,c,d,e,j,k a,c,e,f,i,j,k Sub Code: Credit: CIE: ADVANCE BIOPROCESS ENGINEERING CHPE032 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Biochemical Engineering Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Learn the design principles of biological reactors, like chemostat with & without recycle including multistage operation and cell growth kinetics. 2. Learn to develop transport models for bioprocess systems and techniques of enzyme immobilization. 3. Learn about the multiphase bioreactor systems used in bioprocess industry including plant and animal cells and also mixed culture systems 4. Know the methods of biological waste treatment and technology of some important Industrial Bioprocesses. 5. Learn basics of genetic engineering. Course Content: Unit I Design and analysis of biological reactors: Review of bio reactors-chemostat with & without recycle, multistage operation. Sterilization of Reactors. Sterilization of Medium (Batch and continuous. Cell Growth Kinetics: Review of Unstructured Models and Introduction to Structured models of Cell Growth. Unit II Transport phenomena in bioprocess systems: Overall Kla Estimation, and power requirements (review for sparged and agitated vessels. General heat and mass transfer correlations applicable to biological systems. Enzyme Immoblisation: Review of methods. Immobilised enzyme kinetics: Effects of diffusion and reaction on kinetics of immobilized enzymes, Effect of other environmental parameters like pH and temperature. Immobilized Cells: Formulations, Characterization and Applications. Unit III Multiphase bioreactors: Packed, fluidized and trickle bed reactor. Bubble column reactor, design equations with their applications. Fermentation Technology: Animal and Plant Cell Reactor Technology. Mixed Cultures: Introduction. Major Classes of Interactions: Simple Models describing mixed cultures, Industrial utilizations of mixed cultures. 19 Unit IV Biological Waste Treatment: Methods, Conversion of waste water to useful products. Industrial Bioprocess: Anaerobic process: lactic acid, acetone-butanol production. Aerobic Processes: Citric Acid, Baker’s Yeast, High fructose corn syrup production. Unit V Introduction to Genetic Engineering (GE: Aim. Techniques. Achievements and prospects of GE;Translation & Transcription of genetic code. DNA Replication and Mutation and Alteration of cellular DNA. Viruses and Phages. Genetic manipulation: Plasmids. Recombinant DNA Technology. Text Book: 1. Bailey and Ollis, Biochemical Engineering Fundamentals, 2 nd Edition, McGraw Hill, 1976. 2. Shuler M L and Kargi F, Bioprocess Engineering, 2nd Edition, Prentice Hall, 2002. Reference Books: 1. Aiba, S., Biochemical Engineering, Academic Press, London, 1965. 2. Atkinson, A., Biochemical Reactors, Pion Ltd, London. 1975. 3. Pelczar, Microbiology Concept and Application, 5th Edition, McGraw Hill, 2001 Reprint. 4. Doran, P.M., Bioprocess Engineering Principles, Academic Press. Course Outcomes: The student will be able to S. Course Outcome No. 1. Explain the design principles of biological reactors, like chemostat with & without recycle including multistage operation and cell growth kinetics. 2. Develop transport models for bioprocess systems and techniques of enzyme immobilization. 3. Explain about the multiphase bioreactor systems used in bioprocess industry including plant and animal cells and also mixed culture systems. 4. Apply the methods of biological waste treatment and technology of some important Industrial Bioprocesses. 5. Explain Genetic Engineering concepts. 20 Programme Outcomes Satisfied b,c,d,e,j b,c,d,e,j b,c,d,e,j b,c,d,e,j,k b,c,d,e,j,k Sub Code: Credit: CIE: ELECTROCHEMICAL TECHNOLOGY CHPE033 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Engineering Chemistry Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Learn the Fundamentals: Faradays laws, mechanism of conduction in solids, fluids, ionic melts, metals and semiconductors. 2. Study different electrode processes and their kinetics along with double layer theory 3. Learn applications of potentiometry and ion-selective electrodes and polarography. 4. Study mechanisms of Electrode deposition of metals and alloys 5. Learn use and principles of working of different cells: Primary, Secondary and Fuel Cells. Study the corrosion principle and methods of its prevention. Course Content: Unit I Introduction to theoretical aspects: Faradays laws, mechanism of conduction in solids, liquids and gases and in ionic melts. Conduction in metals and semiconductors. Unit II Reversible electrodes and potentials, electrode processes and electrode kinetics. Various types of overpotentials. Polarisation. Butler-volmer for one electron and mute electron steps. Models of electrical Double layer. Unit III Applied aspects: Potentiometry and ion-selective electrodes. Polaroraphy. Unit IV Electrode deposition of metals and alloys. Primary, Secondary and Fuel Cells. Unit V Corrosion and its prevention. Electro winning. Electro organic and inorganic synthesis (and some typical examples. Environmental electrochemistry. Bio-electro chemistry. Text Books: 1. Bockris, J.O.M., & Reddy, A.K.N., Modern Electrochemistry, Vol.1 & 2, Plenum, New York. 2. Kuhn, Industrial Electrochemical Processes, Elsevier, Amsterdam. Reference Books: 1. Lingane, J.J., Electro Analytical Chemistry, John Wiley, New York. 2. Potter, E.C., Electrochemistry, Principles and Applications, Cleaverhume Press, London. 3. Baizer, M.M., Marcel Dekker, Organic Electrochemistry, John Wiley, New York. 21 Course Outcomes: The student will be able to S. No. 1. 2. 3. Course Outcome Programme Outcomes Satisfied Explain different fundamental laws of electro chemical technology Derive different kinetic theories of electrode processes Apply potentiometric and polarographic principles to practical a,b,c,d a,b,c,d a,b,c,d systems 4. 5. Design a simple methodologies for metals and alloys deposition on surfaces Put into practice Primary, Secondary and Fuel Cells. Apply the principles of corrosion and its prevention to different environmental conditions in a chemical process industry 22 a,b,c,d a,b,c,d,j,k PROCESS OPTIMIZATION Sub Code: Credit: CIE: CHPE034 3:0:0 50 Marks Contact Hours: 42 SEE: 50 Marks Pre-requisites: Engineering Mathematics IV Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Learn to develop mathematical model for problems and determine degrees of fredom. 2. Learn to formulate objective function and basic concepts 3. Study concepts of optimization for unconstrained function. 4. Learn methods for multivariable optimization 5. Learn linear programming and its applications. Course Content: Unit I The Nature and Organization of Optimization Problems: Scope and Hierarchy, Applications, General procedure, obstacles. Developing models for optimization: Classifications of models, building models, selecting functions to fit empirical data, factorial experimental design, degrees of freedom. Unit II Formulation of objective function: Economic objective function, time value of money in objective function. Basic concepts of optimization: Function continuity, NLP programming, convexity and its application, quadratic approximation, conditions for extremum of an unconstrained function. Unit III Optimization of unconstrained function: One dimensional search: Numerical methods for optimization a function with one variable, scanning and bracketing procedure, polynomial approximation methods. Unit IV Unconstrained multivariable optimization: Methods using functions values only- Random search, grid search, univariate search, simplex search, conjugate search. Methods using first derivative-steepest descent, conjugate gradient. Newtons method, Quasi Newtons method. Unit V Linear Programming and its applications: Geometry of linear programs, Simplex algorithm, Barrier method, Sensitivity analysis, Linear mixed integer program. 23 Text Book: 1. Edgar, T.F., Himmelblau, D.M., Ladson, L.S., Optimization of Chemical Processes, Mc Graw Hill Reference Book: 1. Rose, L.M., Applications of Mathematical Modeling to Process Development and Design, Applied Science Publishers Ltd., London. Course Outcomes: The student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Develop mathematical models for chemical engineering problems. Optimize functions with single variable using numerical methods. Optimize unconstrained functions. Optimize multivariable problems using numerical methods. Apply linear programming methods in optimization 24 Programme Outcomes Satisfied a,b,c,d,e,g,j a,b,c,d,e,g,j a,b,c,d,e,g,j a,b,c,d,e,g,j . a,b,c,d,e,g,j Sub Code: Credit: CIE: MODELING OF CHEMICAL PROCESSES CHPE035 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Engineering Mathematics I and II, Momentum Transfer, Process Heat Transfer, Chemical Reaction Engineering-I, Chemical Process Calculations Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Study the principles of model building and precautions,learn the approach to solution by the method of shell balances and a review of continuity equation, energy equation, equation of motion, transport equation of state equilibrium and Kinetics. 2. Learn the classification of mathematical models 3. Develop the models and solutions by applying above methods to the basic Chemical engineering problems in mass, heat and momentum transfer. 4. Develop models for the cases involving reaction with diffusion in a tubular reactor, with heat transfer in a packed bed reactor and reactors in series. 5. Study the procedures for flow sheeting, Property estimation, tearing and flow sheeting, Modular and Equation-solving approach (Elementary treatment only. Course Content: Unit I Modeling: Models and model building, principles of model formulations, precautions in model building, Fundamental laws: Review of shell balance approach, continuity equation, energy equation, equation of motion, transport equation of state equilibrium and Kinetics, classification of mathematical models. Unit II Mathematical Modeling and Solutions to the Following: Basic tank model – Level V/s time. Multi component flash drum. Batch Distillation – Vapor composition with time. Batch Reactor. Solvents extraction (steady & unsteady state, stirred tank (steady state and unsteady state, multistage gas absorption, multistage distillation. Unit III Models in heat transfer operation: Heat conduction through cylindrical pipe (steady & unsteady state, cooling of tanks, unsteady state heat transfer by conduction. Models in fluid flow operation: Fluid through packed bed column, flow & film on the outside of a circular tube. Unit IV Models in Reaction Engineering: Chemical reaction with diffusion in a tubular reactor, chemical reaction with heat transfer in a packed bed reactor, reactor in series. Unit V 25 Introduction to flowsheeting: Property estimation, tearing and flowsheeting, Modular and Equation-solving approach (Elementary treatment only. Text Books: 1. Luyben , W.L., Process Modeling Simulation and Control for Chemical Engineering, 2 nd Edition, McGraw Hill, 1990. 2. Babu, B.V., Process Plant Simulation, Oxford Press. Reference Books: 1. Fogler, H.S., Elements of Chemical Reaction Engineering, 2nd Edition, Prentice Hall, 2001. 2. Smith, J. M. and Vanness, H.C., Introduction to Chemical Engineering Thermodynamics, 5 th Edition, MGH 1996. 3. Himmelblau, D.M., Basic Principles and Calculations in Chemical Engineering, Pearson, 7 th Edition. Course Outcomes: The student should be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Apply the shell balance method and similarly use the continuity & transport equations to simple chemical engineering problems . Develop the models for practical engineering problems of mass transfer Develop the strategies for development of models for momentum and heat transfer applications . Apply the methods for the transport problems involving reactions also. Apply tools for flow charting, parameter estimation and modular approach. a,b,c,d,e,g,j 26 . a,b,c,d,e,j a,b,c,d,e,g,j . a,b,c,d,e,j a,b,c,d,e,j Sub Code: Credit: CIE: POLYMER PROCESSING TECHNOLOGY CHPE041 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Nil Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Learn about the different classification of polymer and rubbers and their strength properties 2. Study melt processing as well as low temperature casting process for thermosplastics and thermosets. . 3. Study various shape forming process like injection moulding, extrusion compression moulding, thermoforming, film blowing etc based on end use requirement. 4. Learn to developing mathematical formulations for through put for a given requirement. 5. Study appropriate tests for plastic materials to suit for a given application. Course Content: Unit I Principles of processing of polymers: Melt processing of thermoplastics. Classification of processes. Thermoset plasting processing, crystallization, orientation & shrinkage, co polymers blendings, compounding for engineering application, stress – strain behavior, WLF equation, practical assessment for long term behavior. Unit II Polymer extrusion: Requirements of Polymer for extrusion. Single screw and double screw plasticating extruder zones in extrusion, breaker plates, extruder screw, power calculation. PVC extruder. Die and calibration equipment prime mover for extrusion, co extrusion, extrusion coating, extrusion film blowing reactive extrusion. Extrusion blow moulding for PET bottles, wire drawing-PVC, spinning – various types and applications. Application of various extruded products. Rheological aspects of extrusion and extrusion defects. Operational and maintenance of extrusion equipments. Unit III Injection moulding: Polymer characteristics for injection moulding. Reciprocating screw injection moulding. Single impression mould. Multi impression moulds. Cooling requirements in moulds. Hot runner moulds, gate, mould clamping force calculations. Control of pressure, temperature and time of injection thermostat and fiber reinforced polymer injection moulding, sandwich moulding and injection blow moulding. Rheological aspects and defects of injection. Comparision of injection moulding and extrusion of injection. Operational and maintenance of injection moulding equipments. Reaction injection moulding. Applications. 27 Unit IV Compression moulding: Applications. Principles. Comparison with other processing methods. Derivation of compression mould thickness or compaction force. Transfer moulding. Calendering: Characteristics of polymer for calendering. Principles and operation of calendaring. Derivation of film thickness and pressure required for rollers. Guage control during calendaring. Application of PVC calendered products. Unit V Thermoforming: Basic principles. Vacuum forming. Pressure forming. Description of operations. Product design. Application. Derivation of thermoformed product thickness. Rotational moulding: Principles. Operation & applications. Thickeness. Cooling calculations. Testing of plastics: Thermal, electrical, optical, mechanical properties testing. Text Books: 1. Johnes, M., Principles of Polymer Processing, Chapman and Hall, 1989. 2. Crawford, R.J., Plastic Engineering, 3rd Edition, Butterworth-Hienemann, 1998. Reference Books: 1. McCrum, N.G., Buckley, C.P., Principles of Polymer Engineering, Oxford Press, 1988. 2. Manas Chandha, Polymer Materials –Vol 1,2 & 3, Springer. Course Outcomes: Student will able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Student is able to assess and use equipment and choose a suitable polymer for a material of fabrication Student will be able to study a product design and production rate and choose an appropriate shaping operation He would be capable of testing the manufactured product for a suitability He would be capable of making modifications to moulds and dies for product development He would be capable of suggesting packaging solutions a 28 a,b,d,i,j a,b,c,e,j,k a,b,c,d,e,f,g,i,j,k b,c,d,e,g,h,i Sub Code: Credit: CIE: INTERFACIAL PHENOMENA AND SURFACE ENGINEERING CHPE042 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Chemical Engineering Thermodynamics Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Learn the basic concepts of interface and generalized equation for excess pressure across different surfaces 2. Learn different methods of interfacial tension measurement and thermodynamic analysis 3. Learn kinetics of spreading, contact angle hysteresis. 4. Study the concepts of electrical aspects of surfaces 5. Study different types of surfactants , thermodynamic and mass transfer considerations. Course Content: Unit I Introduction: Concept of Interface and its formation with examples. Mechanical and Thermodynamic approaches to Interface. Equivalence in the concepts of surface energy and surface tension. Applications. Excess Pressure: Generalized equation for excess pressure across a curved surface- the equation of Young and Laplace. Pressure jump across cylindrical surface, flat surface. Vapor pressure of a drop Solubility of drops. Ostwald ripening. Capillary condensation. Super saturation. Nucleation. Unit II Measurement of Interfacial tension: Capillary rise method. Drop weight method, Wilhemy plate method, du nuoy method. Methods based on shape of static drops or bubbles. Dynamic methods-Flow and capillary waves. Thermodynamics of Interfaces: Thermodynamic treatment of interfaces. Free energy at interface. Temperature dependence of the surface tension. Effect of pressure on interfacial tension. Effect of curvature on surface tension. Thermodynamics of binary systems-Gibbs Equation. Surface excess concept. Verification of Gibbs equation. Gibbs monolayers. Unit III Wetting fundamentals and contact angles: Work of adhesion, cohesion. Criteria for spreading of liquids. Kinetics of spreading. Lens formation- three phase systems. Young’s equation. Neumann triangle. Theories of equilibrium contact angles. Contact angle hysteresis. Unit IV Electrical aspects of surfaces: The electrical double layer. Stern treatment of electrical double layer. Free energy of a diffused double layer. Repulsion between two plane double layers. 29 Colloidal dispersions. Combined attractive and electrical interaction-DLVO theory. Kinetics of coagulation. Unit V Surfactants: Anionic and non ionic. Other phases involving surfactant aggregates. Surface films of insoluble surfactants. Thermodynamics of microemulsions. Phase behaviour of oil-watersurfactant systems. Effect of composition changes. Applications of surfactants-emulsions and detergency. Introduction to interfaces in motion: Linear analysis of interfacial stability. Damping of capillary wave motion by insoluble surfactants. Stability and wave motion of thin liquid filmsfoams. Interfacial stability for fluids in motion. Text Books: 1. Miller, C.A. & Niyogi, P., Interfacial Phenomena, Equilibrium and Dynamic Effects, Marshel Deckder, 1985. 2. Adamson, A.W., Physical Chemistry of Surfaces, John Wiley, 5th Edition, 1981. Reference Books: 1. Millet, J.L., Surface Activity, 2nd Edition, Van Nostrad, 1961. 2. Gorrett, H.E., Surface Active Chemicals, Pergemon Press, 1974. Course Outcomes: The student should be able to S. No. 1. 2. 3. 4. 5. Course Outcome Explain mechanical and thermodynamic approaches to interface Derive the equation for excess pressure across different surfaces Explain different methods of interfacial tension measurement. Explain concepts of kinetics of spreading, contact angle hysteresis Explain aspects of electrical aspects of surfaces. Explain thermodynamic and mass transfer considerations of surfactants 30 Programme Outcomes Satisfied a,c,d,j a,c,d,j a,c,d,j a,c,d,j a,c,d,j Sub Code: Credit: CIE: NOVEL SEPARATION TECHNIQUES CHPE043 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Mass Transfer I and II Course coordinator: Chemical Engineering Department The student will 1. Learn the fundamentals of adsorptive separations and modeling and study the Pressure swing & thermal swing adsorption, Counter current separations. 2. Study the basic concepts of chromatography ,design procedures of chromatographic column and types of chromatography 3. Learn different membrane separation technological processes and their design 4. Study the surfactant based separations and learns super critical fluid extraction process with examples. 5. Study the principles of electric, magnetic and centrifugal separation processes Course Content: Unit I Adsorptive separations: Review of fundamentals. Mathematical modeling of column factors. Pressure swing & thermal swing adsorption. Counter current separations. Unit II Chromatography: Chromatography fundamentals. Different types. Gradient & affinity chromatography. Design Calculations for chromatographic columns. Unit III Membrane separation processes: Thermodynamic considerations. Mass transfer considerations. Design of RO &UF. Ion selective membranes. Micro filtration. Electro dialysis. Pervaporation. Gaseous separations. Unit IV Surfactant based separations: Fundamentals. Surfactants at inter phases and in bulk. Liquid membrane permeation. Foam separations. Micellar separations. Super critical fluid extraction: Thermodynamics and physico chemical principles. Process description. Application. Case Study. Unit V External field induced separations: Electric & magnetic field separations. Centrifugal separations and calculations. 31 Other Separations: Separation by thermal diffusion, electrophoresis and crystallization. Text Books: 1. Rousseu, R.W., Handbook of Separation Process Technology, John Wiley & Sons. Reference Books: 1. Kirk-Othmer, Encyclopedia of Chemical Technology, 5 th Edition, 2007. 2. Wankat, P.C., Rate Controlled Separations, Springer, 2005. 3. Wankat, P. C., Large Scale Adsorption Chromatography, CRC Press, 1986. 4. Sourirajan, S., Matsura, T., Reverse Osmosis and Ultra Filtration Process Principle, NRC Publication, Ottawa, 1985. 5. McHugh, M. A. and Krukonis, V. J., Supercritical Fluid Extraction, Butterworth, 1985. Course Outcomes: On completion of this course the student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Explain different types of adsorptive separations such as pressure swing adsorption and thermal swing adsorption and derive the equations for the same Explain the principle of chromatography , different types of chromatography and design the chromatographic columns. Develop design equations for membrane separation processes such as RO&UF Explain concepts of surfactant based separations, physico chemical aspects and applications of Super critical fluid extraction. Explain the applicability of electric, magnetic and centrifugal separation processes for practical situations a,bg,c,d,e,i,k 32 a,b,c,d,e,k . a,b,e,h,j,k a, b,c,d,e,h,i,k . a,b,c,i,j,k Sub Code: Credit: CIE: MULTICOMPONENT DISTILLATION CHPE044 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Mass Transfer-II, Chemical Engineering Thermodynamics, Engineering Mathematics IV. Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Study the criteria for phase equilibra and thermodynamic relations. 2. Study the process of multicomponent distillation and numerical methods applied to estimate parameters. 3. Study various methods of multicomponent distillation. 4. Study reactive distillations and numerical methods applications to estimate the parameters. Course Content: Unit I Phase Equilibria: For Multi component distillation. Thermodynamic relationships for multi component mixture, prediction of phase equilibria. Use of fugacities and activities. Introduction to the method of convergence characteristics. The Theta method for converging temperature. Profile-Development & application to conventional distillation columns. The 2N NewtonRaphson method- Introduction and the Algorithm. The method of successive approximations. Unit II Methods of multicomponent distillation: Azeotropic and extractive distillation processqualitative characteristics and applications. Unit III Phase behaviours at constant pressure: Homogeneous and Heterogeneous azeotropes. Unit IV Reactive Distillation: Distillation accompanied by chemical reaction. Application of the theta method of convergence in reactive method. Formulation of N[r+2] Newton Raphson method. Unit V Complex Mixture: Determination of minimum number of stages required to effect a specified separation. Optimum and economic design of distillation column for the complex mixtures. Text Books: 1. Holland, C.D., Fundamentals of Multicomponent Distillation, Prentice Hall, 1969. Reference Books: 1. King, C.J., Separation Processes, McGraw Hill, 1980. 2. Kai Sundmacher, Achim Kienle, Reactive Distillation, Wiley, 2003. 3. Billet, R., Distillation Engineering, Chem. Publ. Co. NY,1979. 33 Course Outcomes: The student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Predict phase equilibria and determine thermodynamic properties Apply numerical methods to determine parameters for multicomponent distillation Explain different types of multicomponent distillation Explain reactive distillation and applications Determine the number of stages for multicomponent distillation. a,c,d,e,j a,c,d,e,j 34 a,c,d,e,j a,c,d,e,j a,c,d,e,j Sub Code: Credit: CIE: APPLIED MATHEMATICS IN CHEMICAL ENGINEERING CHPE045 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Engineering Mathematics I, II, III Course coordinator: Chemical Engineering Department Course Objectives: The student will study 1. Basic laws for formulation of mathematical models 2. Methods to solve the chemical engineering problems on ordinary differential equations 3. Methods of solving partial differential equations related to chemical engineering 4. Applications of numerical techniques, finite differences and laplace transforms in chemical engineering Course Content: Unit 1 Mathematical Formulation of the Physical Problems: Applications of laws of conservation of mass, energy. Statement of the problem. Modeling. Examples and problems. Unit II Ordinary Differential Equations: Formulations of ordinary differential equations involving chemical engineering problems. Solutions- Equations of first order and first degree. Solutions Equations of first order and second degree. Bernoulli equation. Euler equation. Simultaneous linear differential equations. Unit III Partial Differential Equations: Formulations of partial differential equations involving chemical engineering problems. Solutions. Fourier series. Unit IV Numerical Methods: Solutions of ordinary differential equations for chemical engineering problems. Solutions of partial differential equations for chemical engineering problems. . Unit V Finite Differences: Difference operator, linear difference equations, analysis of stage-wise, Processes. Laplace transforms and their applications to chemical engineering. Text Books: 1. H.S. Mickley, T.K. Sherwood and C.E.Reed, Applied Mathematics in Chemical Engineering, 3rd Edition, Tata McGraw Hill, 1999. 2. S. Pushpavanam, Mathematical Methods in Chemical Engineering, Eastern EconomyEdition, 2004. 35 Reference Books: 1. V.G. Jenson & G.V. Jeffreys, Mathematical Methods in Chemical Engineering, Academic Press, London, 1977. 2. L.M. Rose, Applications of Mathematical Modeling to Process Development and Design, Applied Science Publishers Ltd., London, 1998. Course Outcomes: The student will be able to S. No. 1. 2. 3. 4. Course Outcome Programme Outcomes Satisfied Basic laws for formulation of mathematical models Methods to solve the chemical engineering problems on ordinary differential equations Methods of solving partial differential equations related to chemical engineering Applications of numerical techniques, finite differences and laplace transforms in chemical engineering a,b,c,d,e,g,j a,b,c,d,e,g,j 36 a,b,c,d,e,g,j a,b,c,d,e,g,j Sub Code: Credit: CIE: PROCESS SIMULATION LABORATORY CHL701 0:0:2 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Nil Course coordinator: Chemical Engineering Department Course Objective: The student will learn to 1. Use a process simulation package 2. Perform simulation studies for equipment or a chemical process. 3. Optimize a process using simulation software List of simulations suggested: 1. 2. 3. 4. Introduction to suggested software available (flow sheeting Simulations Studies of flash drum, Distillation Column, CSTR, PFR, Heat Exchanger. Simulation Studies of pump, compressor, cyclone, heater. Process simulation study involving mixing, reactor, distillation, heat exchanger for any of the following;: a. Ethylene Glycol from Ethylene oxide b. Atmospheric distillation of crude oil c. Propylene Glycol from Propylene oxide d. Aromatic stripper with recycle stream (Benzene, Toluene, Xylene e. Styrene from Ethyl Benzene Software Suggested: ASPEN PLUS, HYSYS, CHEMCAD, DESIGN-II, gPROM, UNISIM Course Outcome: The student will be able to S. Course Outcome No. 1. 1. Use any process simulation software. 2. 1. Simulate and optimize the parameters in a process using simulation software. 37 Programme Outcomes Satisfied a,b,c,d,e,g,j,k a,b,c,d,e,g,j,k PROCESS CONTROL LABORATORY Sub Code: Credit: CIE: CHL702 0:0:2 50 Marks Contact Hours: 42 SEE: 50 Marks Pre-requisites: Nil Course coordinator: Chemical Engineering Department Course Objective: The student will conduct experiment to 1. Understand the principles of control systems 2. Study first and second order systems 3. Study characteristics of control valves. List of experiments: 1. Thermometer 2. Single tank - Step Response 3. Non Interacting Tanks – Step Response 4. Interacting Tanks – Step Response 5. Pressure Tank 6. U – Tube Manometer 7. Single tank - Impulse Response 8. Non Interacting Tanks – Impulse Response 9. Interacting Tanks – Impulse Response 10. Level/Flow/Pressure/pH/Temperature control – P controller 11. Level/Flow/Pressure/pH/Temperature control – PI controller 12. Level/Flow/Pressure/pH/Temperature control – PD controller 13. Level/Flow/Pressure/pH/Temperature control – PID controller 14. Valve characteristics. 15. Flapper Nozzle System 16. Valve Positioner. Note: Minimum 10 experiments from the above are to be conducted. Course Outcome: The student will be able to S. No. 1. 1. 2. 1. 3. 1. Course Outcome Programme Outcomes Satisfied Operate a feedback control system Design a feedback control system Write technical report and the operation and behavior of control system. a,b,c,d,e,g a,b,c,d,e,g,i,k h 38 DESIGN PROJECT Sub Code: Credit: CIE: CH704 0:0:2 50 Marks Contact Hours: 24 SEE: 50 Marks Pre-requisites: Chemical Process Calculations, Process Equipment Design and Drawing Course coordinator: Chemical Engineering Department Course Objective: The student will 1. Select, Plan and design a process. 2. Apply the mathematical, computational engineering and economics knowledge for practical design problems. 3. Understanding the principle of working in teams and the concept of team leadership. 4. Learn flow sheeting and designing of plants. 5. Improve report writing skills. Course Content: A group of students will be assigned a case study, or an analytical problem to be carried out under the supervision of a guide. The group shall not contain more than four students. Guides are allocated in the beginning of the seventh semester and the problem on design of an equipment or process is identified. The project group should complete design project and submit the report at the end of seventh semester. The project is evaluated by the guide and a faculty committee to award the CIE marks. Course Outcomes: The student should be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Carry out literature review for any manufacturing process in chemical engineering Write material and energy balance for a process Design and select various components of the process. Carry out computational and economic analysis Write precise project reports with appropriate drawings, flowcharts and references a,b,c,d,e,f,g,h,i,j,k,l 39 a,b,c,d,e,f,g,h,i,j,k,l a,b,c,d,e,f,g,h,i,j,k,l a,b,c,d,e,f,g,h,i,j,k,l h Sub Code: Credit: CIE: INPLANT TRAINING/ INDUSTRIAL VISIT CH705 0:0:0 Contact Hours: 00 --SEE: ---- Pre-requisites: Nil Course coordinator: Chemical Engineering Department Course Objective: The student will be exposed to various operations and processes in chemical industry. Course Content: Students are required to carry out training in a chemical industry for not less than two weeks or Visit atleast five chemical industries between sixth and seventh semester. They are required to submit a report on the same. Course Outcome: The student should be able to S. No. 1. Course Outcome Programme Outcomes Satisfied Understand functioning of chemical process industry and gain a,b,c,d,e,f,g,h,i,j,k,l knowledge on the recent developments in the area. The training will help him to integrate his theoretical knowledge with practical processes. The student will enhace his communication skills and will learn how people work in interdisciplinary teams in industry. This practical experience would make the student realize his professional and ethical responsibility 40 OPEN ELECTIVES OFFERED BY THE DEPARTMENT GREEN TECHNOLOGY Sub Code: Credit: CIE: CHOE01 3:0:0 50 Marks Contact Hours: 42 SEE: 50 Marks Pre-requisites: Engineering Chemistry Course coordinator: Chemical Engineering Department Course Objectives: The students will 1. 2. 3. 4. 5. Learn the tools of green technology and zero waste systems. Learn basic principles of green chemistry and atom efficiently Learn Life Cycle Assessment methods and tools Learn methods for pollution prevention. Learn to design for environment Course Content: Unit I Introduction: Green chemistry and technology for sustainable development, Environmental laws, carbon credits, environmental management system standards- ISO 14000 series. Unit II Green Chemistry: Principles of Green Chemistry, Atom efficiency, Energy conservation, Waste minimization, Substitution. Unit III Life-Cycle Assessment: History, Process, Methodology, Streamlining and Application. Unit IV Pollution prevention planning: Structure of the pollution prevention process, Environmental Audits. Unit V Design for the environment and improvement in manufacturing operations, case studies. Text Books: 1. Anastas P.T., Warner J.C., Green Chemistry: Theory and Practice. Oxford Science Publications, Oxford, 1998. 2. Paul L. Bishop, Pollution Prevention: Fundamentals and Practice, McGraw Hill,2000. Reference Books: 1. Mike Lancaster, Green Chemistry- An Introductory Text, Royal Society of Chemistry Publishing, 2010 2. Boyle, Godfrey, Bob Everett, Janet Ramage, Energy Systems and Sustainability: Power for a Sustainable Future, Oxford University Press, 2004. 41 Course Outcomes: On successful completion of this course the student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Explain environment laws, carbon credits, ISO 14000 series Explain principles of green chemistry Explain the importance of green technology in sustainable development Explain tools of green technology and life cycle assessment. Conduct pollution prevention planning and environment friendly design c,d,e,i c,d,e,i . c,d,e,i 42 c,d,e,i k,l VIII Semester Sub Code: Credit: CIE: ECONOMICS AND ENTREPRENEURSHIP CH801 4:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Nil Course coordinator: Chemical Engineering Department Objectives: The student will 1. Learn basics of cost estimation, working capital and capital investment and understand time value of money. 2. Study the calculation procedures of depreciation and taxes by different methods 3. Learn the methods of estimation of profitability and break-even analysis. 4. Learn functions and types of entrepreneur; and small scale industries. 5. Understand the institutional support like different schemes (KIADB, KSSICE, KSIMC, etc, single windows agency (SISI, NSIC, SIDBI, etc and preparation of projects. Course Content: Unit I Cost Analysis: Factors involved in project cost estimation, methods employed for the estimation of the capital investment. Estimation of working capital. Time value of money and equivalence. Unit II Depreciation And Taxes: Depreciation calculation methods. Equivalence after Taxes. Cost comparison after taxes. Unit III Profitability: Methods for the evaluation of profitability. Break-even analysis. Unit IV Entrepreneur: Meaning of Entrepreneur; Evolution of the Concept, Functions of an Entrepreneur, types of Entrepreneur, Entrepreneurship qualities, intrapreneurship development. Small Scale Industry: Definition; Characteristics; Need and rationale: Scope; role of SSI in Economic Development. Advantages of SSI. Steps to Start and SSI – Government policy towards SSI; Different Policies of S.S.I., Impact of Liberalization, Privatization, Globalization on S.S.I., IPR for entrepreneurs. Unit V Institutional Support: Different Schemes; TECKSOK; KIADB; KSSICE; KSIMC; DIC Single Window Agency: SISI; NSIC; SIDBI; KSFC. 43 Preparation of Project: Meaning of Project; Project Identification; Project Selection; Project Report; Need and Significance of Report; Contents; formulation; Guidelines by Planning Commission, Identification & evaluation of Business Opportunities: Market Feasibility Study; Technical Feasibility Study; Financial Feasibility Study & Social Feasibility Study. Text Books: 1. Peters and Timmerhaus, Plant Design and Economics for Chemical Engineers, McGraw Hill. 2. Charantimath, P.M., Entrepreneurship Development – Small Business Enterprises, Pearson Education, 2006. Reference Books: 1. Desai, V., Dynamics of Entrepreneurial Development & Management, Himalaya Publishing House. 2. Schweyer, H. E., Process Engineering Economics, McGraw Hill, NY. 3. Gupta, C.B., Kanka, S.S., Entrepreneurship & Small Business Management, S Chand & Sons, 2007. Course Outcomes: The student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Programme Outcomes Satisfied Estimate various costs involved in a process industry. Calculate and analyze the costs of depreciation and taxes. Use different tools to estimate profitability of a company. Demonstrate the ability to find an attractive market that can be reached economically. The project reports to get funding from different agencies. a,,c,d,e,g,i,j,k,l a,c,d, ,i,j, l a,c,d,i,j,l c, f,g,h,i,j,k, e,f,g,h,i,j,k,l SOLID WASTE MANAGEMENT Sub Code: Credit: CIE: CHPE051 3:0:0 50 Marks Contact Hours: 70 SEE: 50 Marks Pre-requisites: Environmental Engineering Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Study the material flow in society and generation of solid waste source 2. Understanding various components of solid waste management 3. Understand the sense of onsite handling storage and collection systems including transportation 4. Understand processing technologies with mechanical volume reduction and thermal volume reduction corporate land filling, deep well injections. 5. Learn to estimate material recovery and energy recovery from a given waste data using case studies. 44 Course Content: Unit I Introduction: Definition, characteristics and perspectives of solid waste. Types of solid waste. Physical and chemical characteristics. Variation of composition and characteristics. Municipal, industrial, special and hazardous wastes. General aspects: Overview of material flow in society. Reduction in raw material usage. Reduction in solid waste generation. Reuse and material recovery. General effects on health and environment. Legislations. Unit II Engineered systems: Typical generation rates. Estimation and factors effecting generation rates. On site handling. Storage and processing. Collection systems and devices. Transfer and transport. Unit III Processing Techniques: Mechanical volume reduction. Thermal volume reduction. Component separation. Land filling and land forming. Deep well injection. Unit IV Material recovery: Mechanical size alteration. Electromagnetic separation. Drying and dewatering. Other material recovery systems. Recovery of biological conversion products. Recovery of thermal conversion products. Energy recovery: Energy recovery systems and efficiency factors. Determination of output and efficiency. Details of energy recovery systems. Combustion incineration and heat recovery. Gasification and pyrolysis. Refuse derived fuels (RDF. Unit V Case studies: Major industries and management methods used in typical industries – Coal fired power stations, textile industry, oil refinery, distillery, sugar industry, and radioactive waste generation units. Text Books: 1. Howard S. Peavy, Environmental Engineering, McGraw Hill International Edition, 1986. 2. Dutta, Industrial Solid Water Management and Land Filling Practice, Narose Publishing House, 1999. Reference Books: 1. Sastry C.A., Waste Treatment Plants, Narose Publishing House, 1995. 2. Lagrega, Hazardous Waste Management, McGraw Hill, 1994. 45 Course Outcomes: The student should be able to S. No. 1. 2. 3. 4. 5. Course Outcome Apply knowledge to characterize the solid waste Should able to understand various components of solid waste and perform calculations. Learn various processing techniques and suitable design considerations for land filling sites. Learn about material recovery and energy recovery from solid waste Develop a management plan for handling solid waste for various process industries and municipalities. Sub Code: Credit: CIE: Programme Outcomes Satisfied a a,b,c,i,j a,b,e,j a,b,e,f,g,i,j c,k,l SCALE UP OF CHEMICAL PROCESSES CHPE052 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Nil Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Study concepts of proto types, models, principle of similarity 2. Study the dimensional analysis methods and differential equations approach 3. Study the regime concept and criteria for static dynamic process and extrapolate the process taking into account boundary effect. 4. Learn to develop scale up techniques for chemical engineering unit operations and process for both batch and continuous process. 5. Learn environmental challenges of scale up. Course Content: Unit I Introduction: Concept of prototypes, models, scale ratios, element. Principles of similarity: Geometric similarity. Distorted similarity. Static, dynamic, kinematics, thermal and chemical similarity with examples. Unit II Dimensional analysis: (Review of Rayleigh’s, Buckingham ∏ methods, Differential equation for static systems, flow systems, thermal systems, mass transfer processes, chemical processeshomogeneous and heterogeneous. Unit III Regime concept: Static regime. Dynamic regime. Mixed regime concepts. Criteria to decide the regimes. Equations for scale criteria of static, dynamic processes, Extrapolation. Boundary effects. 46 Unit IV Scale up: Mixing process, agitated vessel, Chemical reactor systems-Homogeneous reaction systems. Reactor for fluid phase processes catalysed by solids. Fluid-fluid reactors. Unit V Stagewise mass transfer processes. Continuous mass transfer processes. Scale up of momentum and heat transfer systems. Environmental challenges of scale up. Text Books: 1. Bisio, A., Kabel, R.L., Scale up of Chemical Processes, John Wiley & Sons. 2. Johnstone and Thring, Pilot Plants, Models and scale up method in Chemical Engineering. Reference Book: 1. Ibrahim and Kuloor, Pilot Plants and Scale up Studies, IISc. Course Outcomes: The student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Apply similitude principles. Develop relations in terms of dimensionless parameters. Identify process regimes and develop equations for static and dynamic processes. Develop scale up criteria for mixing processes and reactors. Develop scale up relations for mass transfer operations and assess environmental challenges. 47 Programme Outcomes Satisfied a,b,c,d,e a,b,c,d,e a,b,c,d,e a,b,c,d,e, j a,b,c,d,e, j Sub Code: Credit: CIE: ENVIRONMENTAL IMPACT ASSESSMENT CHPE053 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Environmental Engineering Course coordinator: Chemical Engineering Department Course Objectives: The students will 1. Learn to establish a need for impact assessments with respect to legislation and regulation. 2. Learn to discuss the methodologies of collection of data and apply cost benefit analysis. 3. Learn to elucidate the contents of impact assessment report for developmental projects with industry specific examples. 4. Learn to formulate environmental management plans, life cycle assessments, waste and environmental audit. 5. Learn to emphasize clean/cleanup technologies, waste reductions at source and clean synthesis. Course Content: Unit I Introduction and need for impact assessment. Legislation and pollution control acts and Regulations. Methodologies-collection of data and analysis, cost benefit analysis. Unit II Applications of Impact assessment methods in specific developed projects, advantages and disadvantages of different methods, Applicability of specific methods with examples. Unit III Impact assessment report contents for the developmental projects like thermal power projects, refinery process and chemical process industries. Unit IV Ranking of impacts, concepts and contents of environmental management plan. Environmental audits, waste audit, life cycle assessment, industrial symbiosis. Unit V Clean technology Option: Clean technology: Clean technology and clean up technology, material reuse, waste reduction at source and clean synthesis. Text books: 1. Unwin, EIA, theory and practice, Hyman Ltd., 1988. 2. Larry W. Carter, EIA, Mc Graw Hill book Co., 1997. Reference Books: 1. Environmental Health and Safety Auditing Handbook, McGraw Hill, Inc., New York, 1994. 2. Clean Technology and Environment, Edited by RC Kirkwood and A J Longley, Chapman & Hall, 1995. 48 Course Outcomes: On successful completion of this course the students will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Explain the need for environment and ecology of terrestrial atmospheric and marine system. Explain interconnectedness and consequences of all human activities and need of clean technology. Explain perspective of short term and long term impact of human activities. Collect data analyze and prepare a report of impact assessment. Explain legal procedure to get clearance from legal authorities. Explain alternative cleaner technologies and advantages of employing them. 49 Programme Outcomes Satisfied Sub Code: Credit: CIE: INTRODUCTION TO NANOTECHNOLOGY CHPE054 3:0:0 Contact Hours: 42 50 Marks SEE: 50 Marks Pre-requisites: Material Science, Chemical Engineering Thermodynamics Course coordinator: Chemical Engineering Department Course Objectives: The students will study 1. Applied thermodynamic principles 2. Concept of free energy and ideal solutions 3. Determination of thermodynamic equilibrium 4. Various methods of producing nanomaterials 5. Methods of analysis 6. Nanolithography and nanomanipulation Course Content: Unit I Overview to Thermodynamics: The first and second laws of thermodynamics. Thermodynamic functions, heat capacity, enthalpy, entropy. Phase equilibrium in one component system, real gases, the interactions between gases. Ehrenfest classification of phase transition, the physical liquid surface; surface tension, curved surfaces, capillary action. Theory of Solution and related topics: Liquid mixtures: free energy as a function of composition, ideal solutions and excess functions. Equilibrium Electrochemistry; electrochemical cells, Methods for calculation of thermodynamic equilibrium. Electrochemical processes. Unit II Fabrication of Nanomaterials by Physical Methods: -Inert gas condensation, Arc discharge, RFplasma, Plasma arc technique, Ion sputtering, Laser ablation, Laser pyrolysis, Ball Milling, Molecular beam epitaxy, Chemical vapour deposition method and Electro deposition. Unit III Scanning Electron Microscopy (SEM, Scanning Probe Microscopy (SPM, TEM and EDAX analysis, X-ray diffraction. Unit IV Optical Microscope and their description, operational principle and application for analysis of nanomaterials, UV-VIS-IR Spectrophotometers, Principle of operation and application for band gap measurement. Unit V Nanolithography and nanomanipulation, E beam lithography and SEM based nanolithography and nanomanipulation, Ion beam lithography, oxidation and metallization. Mask and its application. Deep UV lithography, X-ray based lithography. Reference Books: 1. Mark James Jackson, Microfabrication and Nanomanufacturing, CRC Press, 2005. 50 2. Principe, E. L., Gnauck, P. and Hoffrogge, P., A Three Beam Approach to TEM Preparation Using In-situ Low Voltage Argon Ion Final Milling in a FIB-SEM Instrument Microscopy and Microanalysis, 11: 830-831 Cambridge University Press, 2005. 3. Shaw, L.L., Processing & properties of structural nano materials, John Wiley and Sons, 2010. 4. Narayanan, K.V., Textbook of Chemical Engineering Thermodynamics, Prentice Hall of India Private Limited, New Delhi, 2001. Course Outcomes: The student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Explain the underlying thermodynamic principles Determine the thermodynamic equilibrium Apply the methods of fabrications and applications of nanomaterials Use applied analytical instruments Explain lithography and its applications. 51 Programme Outcomes Satisfied RESEARCH METHODOLOGY AND TECHNICAL REPORT WRITING Sub Code: CHPE055 Credit: 3:0:0 Contact Hours: 42 CIE: 50 Marks SEE: 50 Marks Pre-requisites: Engineering Mathematics IV Course coordinator: Chemical Engineering Department Course Objectives: The students will study 1. Methods to plan, implement, analyse, and report a scientific experiment. 2. Methods of scientific writing, reviewing, and presentation of texts. Course Content: Unit I Research Methodology: Introduction, Defining the research problem, research design. Unit II Method of data collection: Sampling design. Measurement and scaling techniques, methods of data collection, sampling fundamentals. Unit III Data Analysis: Processing and analysis of data, Testing of Hypotheses parametric, Chi-square test, Analysis of variance and covariance. Unit IV Data Analysis: Testing of hypotheses (non-parametric, Techniques of multivariate analysis. Unit V Report writing and Presentation: Interpretation of results and report writing. Text Books: 1. Kothari, C.K., Research Methodology: Methods and Techniques, 2 nd Edition, 2012 Reprint. 2. Bhattacharya, D.K., Introduction to Research Methodology, Excel Books India, 2009. Reference: 1. Suresh Chandra, Mohit Sharma, Research Methodology, Narosa Publishing, 2013. Course Outcomes: The student will be able to S. Course Outcome No. 1. Explain and apply techniques for scientific writing and research methodology to prepare the writing of a scientific report. 2. Perform investigation using methods, explain and take position on the results as well as summarize related work 3. Apply the knowledge in scientific writing and research 52 Programme Outcomes Satisfied g,h,l g,h,l g,h,l methodology and use the knowledge to write a scientific report. PRINCIPLES OF MANAGEMENT Sub Code: HSS802 Credit: 3:0:0 Contact Hours: 42 CIE: 50 Marks SEE: 50 Marks Pre-requisites: Nil Course coordinator: Humanities/ Chemical Engineering Department Course Objectives: The students will study 1. Principles of management and its functional area. 2. Objectives of planning and steps involved. 3. Types of organization, departmentation and span of control. 4. Process of selection and recruitment. 5. Leadership and motivation. 6. Coordination and control systems. Course Content: Unit I Management: Introduction: Meaning – nature and characteristics of Management, Scope and functional areas of management – Management as a science, art or profession – Management & Administration – Roles of Management, Levels of Management. Unit II Planning: Nature, importance and purpose of planning process – Objectives – Types of plans (Meaning only – Decision making – Importance of planning – Steps in planning & planning premises – Hierarchy of plans. Unit III Organizing And Staffing: Nature and purpose of organization – Principles of organization – Types of organization – Departmentation – Committees – Centralization Vs Decentralization of authority and responsibility – Span of control – MBO and MBE(Meaning only. Nature and importance of Staffing – Process of Selection & Recruitment (in brief. Unit IV Directing & Controlling: Meaning and nature of directing – Leadership styles, Motivation Theories, Communication – Meaning and importance. Unit V Directing & Controlling: Coordination, meaning and importance and Techniques of Co – ordination. Meaning and steps in controlling – Essentials of a sound control system – Methods of establishing control (in brief. Text Books: 1. Tripathi, P.C., Reddy, P.N., Principles of Management, Tata McGraw Hill. 53 2. Koontz , H., Principles of Management, McGraw Hill, 2004. Reference Books: 1. Lusier, R., Thomson, Management Fundamentals – Concepts, Application, Skill Development. 2. Robbins, S., Management, Pearson Education/PHI, 17th Edition, 2003. Course Outcomes: The students will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Explain the role of management and its functions. Explain importance and steps in planning. Explain authority and responsibility, process of recruitment and explain leadership and motivation theories. Explain and analyze modes and barriers in communication. Explain importance and methods of control systems. Programme Outcomes Satisfied f,g,i,j,l f,g,i,j,l f,g,j,l f,g,i,j,l f,g,i,j,l OPEN ELECTIVE Sub Code: Credit: CIE: OE 3:0:0 50 Marks Contact Hours: 42 SEE: 50 Marks Pre-requisites: -Course coordinator: Other Departments 54 PROJECT WORK Sub Code: Credit: CIE: CH803 0:0:14 100 Marks Contact Hours:28 SEE: 100 Marks Pre-requisites: --Course coordinator: Chemical Engineering Department Course Objectives: The student will 1. Identify the upcoming areas of chemical engineering. 2. Plan experimental or theoretical work using multidisciplinary knowledge 3. Apply the mathematical, computational engineering and economics knowledge for practical problems 4. Usage of various instrumental techniques 5. Interact with industry and research centers 6. Understanding the principle of working in teams and the concept of team leadership 7. Learn flow sheeting and designing of plants 8. Improve report writing skills Course Content: A group of students will be assigned an experimental work, case study, or an analytical problem to be carried out under the supervision of a guide. The group shall not contain more than four students. Guides are allocated in the end of sixth semester. The students are required to give a comprehensive presentation in the form of seminar on the project work during the eighth semester and submit the report at the end of the semester. During the semester performance of the students are evaluated by the guide and faculty committee to award the CIE marks. The final project report will be evaluated and examined at the end of the eighth semester for SEE marks. Course Outcomes: The student will be able to S. No. 1. 2. 3. 4. 5. Course Outcome Carry out literature review for the upcoming areas of chemical engineering Write protocols for the experiments to be carried out for the area under study Carry out computational and economic analysis Write precise project reports with appropriate reference Present the work progress from time to time with the results obtained 55 Programme Outcomes Satisfied a,b,c,d,e,f,g,h,i,j,k,l a,b,c,d,e,f,g,h,i,j,k,l a,b,c,d,e,f,g,h,i,j,k,l a,b,c,d,e,f,g,h,i,j,k,l a,b,c,d,e,f,g,h,i,j,k,l