M. S. RAMAIAH INSTITUTE OF TECHNOLOGY
BANGALORE-54
Autonomous Institute, Affiliated to VTU
SYLLABUS
(For the Academic year 2015 - 2016
III and IV Semester B. E.
CHEMICAL ENGINEERING
1
M.S. RAMAIAH INSTITUTE OF TECHNOLOGY, BANGALORE – 560 054
DEPARTMENT OF CHEMICAL ENGINEERING
1. History of the Institute:
M. S. Ramaiah Institute of Technology was started in 1962 by the late Dr. M.S. Ramaiah, our
Founder Chairman who was a renowned visionary, philanthropist, and a pioneer in creating several
landmark infrastructure projects in India. Noticing the shortage of talented engineering
professionals required to build a modern India, Dr. M.S. Ramaiah envisioned MSRIT as an institute
of excellence, imparting quality and affordable education. MSRIT being a part of Gokula Education
Foundation, has grown over the years with significant contributions from various professionals in
different capacities, ably led by Dr. M.S. Ramaiah himself, whose personal commitment has seen
the institution through its formative years. Today, MSRIT stands tall as one of India’s finest names
in Engineering Education and has produced around 35,000 engineering professionals who occupy
responsible positions across the globe.
2. History of the Department:
Instituted in 1978, the Department was the first to offer a course in Chemical Engineering by a selffinancing engineering institution in Bangalore and the fifth in MSRIT. Since its inception the
department has moved steadily towards the fulfillment of its mission and is emerging as a
significant player in the academic landscape of Chemical Engineering education in our country. The
Department is certified thrice in succession by the National Board for Accreditation, once by
National Assessment and Accreditation Council and is also ISO 9001:2008 certified for imparting
quality education. Over 1900 students have graduated in 32 batches. The Department has secured
majority of the university ranks. The expertise of the faculty covers a wide range of disciplines and
they are engaged in cutting edge technological research. The average experience of faculty in the
department is more than twenty years and they are alumni of IISc, IIT and NITs. The Department
follows Outcome Based Education system which is designed for students to achieve the specified
outcomes of the course. Enriching insights by eminent dignitaries from the practicing world is
arranged under the activities of Society of Chemical Engineers, a body comprising of chemical
engineering community of the institute. The Department is approved as Research Center by VTU
for higher qualifications like M.Sc. Engg. (by Research and Ph.D. degrees. Research Projects from
DRDO, AICTE and VTU have been successfully completed. The Annual Technical Symposium
organized by the department for students – RASAYAN encompasses a plethora of events such as
Paper presentations, Poster presentations, M.S. Ramaiah Memorial Technical Quiz etc to challenge
the young minds. The Bangalore Regional Centre of the Indian Institute of Chemical Engineers is
functioning from this Department for more than a decade. The country’s most prestigious event in
Chemical Engineering, Indian Chemical Engineering Congress - CHEMCON-2011 was organized
here. The department offers excellent infrastructure and students have won various prestigious
awards, international internships and high accolades for innovative projects.
2
3. Faculty List:
Sl.
Name of the Faculty
No.
1
Dr. Archna
2
Dr. Y J Rao
3
Dr. V.Venkatesham
4
Sri. S. Swaminathan
5
Sri. Ravi Sadasivan
6
Sri. K.A. Badarinarayana
7
Dr. G. M. Madhu
8
Dr. Brijesh
9
Dr. Rajeswari M. Kulkarni
10
Sri. Ramasivakiran Reddy
11
Sri. Koteswara Rao Jammula
12
Smt.V. Shravanti
13
Ms. Annapurna S M
Qualification
Designation
M.E, Ph.D.
M. E, Ph.D.
M. E, Ph.D.
M. E.
M.S.(Research), (Ph.D.)
M.Tech.
M.E., Ph.D.
M.Tech., Ph.D.
M.Tech, Ph.D.
M.Tech. (Ph.D).
M.Tech., (Ph.D).
M.Tech., (Ph.D).
M.Tech.
Professor and Head
Professor Emeritus
Associate Professor
Associate Professor
Associate Professor
Associate Professor
Associate Professor
Associate Professor
Assistant Professor
Assistant Professor
Assistant Professor
Assistant Professor
Assistant Professor
4. Vision & Mission of the Institute:
The Vision of MSRIT: To evolve into an autonomous institution of international standing for
imparting quality technical education.
The Mission of the Institute in pursuance of its Vision: MSRIT shall deliver global quality
technical education by nurturing a conducive learning environment for a better tomorrow through
continuous improvement and customization.
5. Vision & Mission of the Department:
Vision:
To be a leading chemical engineering centre for quality technical education and progressive
research at global level.
Mission:
1. To provide a state of art environment and a rigorous academic program that trains students to
excel in fundamental science, chemical and allied engineering fields.
2. To offer programme that inculcates creative thinking and lifelong learning, contributing to the
advancements of chemical sciences and its application.
3. To foster principles of sustainability and promote environmentally benign technologies for the
benefit of society.
3
6. Process of deriving the Vision & Mission of the Department:
Institute’s Vision and Mission
Department Faculty
Alumni
Definition of of
Vision and
Mission of the
department by
the committee
Industry
Students
Management
7. Process of Deriving the PEO’s of the Programme:
Institute Vision &
Mission
Department Vision
& Mission
Committee formation & preparation of
questionnaire
Conduction of survey
Students
Industry
Alumni
Collect data (Department
Committee)
Deliberate Analyze and summarize the data in
Board of Studies
Approved in Academic Council & Governing Council
PEOs
4
8. PEO’s of the programme offered:
The B.E. Chemical Engineering Program at M. S. Ramaiah Institute of Technology aims to provide a
strong foundation of scientific and technical knowledge in a state of art learning ambience. It equips the
graduates with problem solving abilities, teamwork, and communication skills necessary throughout
their careers. They are consistent with the following Educational Objectives:
1. To provide a strong foundation and understanding of the fundamental principles of mathematics,
science, and engineering enabling graduates to pursue their careers as practicing chemical engineers in
Chemical and Allied Engineering Industries.
2. To produce graduates who are prepared to pursue their post graduation and Research in the fields of
Chemical Engineering and Petrochemicals, Material Science, Biotechnology, Nanotechnology,
Environmental Engineering, any emerging allied areas and Business.
3. To produce graduates who posses skills with contemporary grounding in professional responsibility,
ethics, global and societal impact of engineering decisions to assume professional leadership roles and
administrative positions.
4. To provide students with opportunities to participate in various multidisciplinary teams and to develop
and practice written and oral communication skills.
9.
Process of deriving PO’s:
The Programme outcomes are defined by taking feedback from faculty, alumni, Industry, professional
bodies, guidelines suggested by regulatory bodies (UGC, AICTE, VTU and Graduate Attributes
suggested by National Board of Accreditation. The established PEO’s are in line with programme
educational objectives. The following Figure indicates the information flow.
5
10. PO’s of the programme offered:
The Chemical Engineering Graduates of MSRIT are expected to have the following abilities/ qualities.
a. An ability to apply knowledge of mathematics, science and engineering fundamentals.
b. An ability to design and conduct experiments, and to analyze and interpret experimental results
with working knowledge of chemical process safety.
c. An ability to design systems, components, or processes to meet specified objectives within all the
realistic constraints of sustainable technology.
d. An ability to identify, formulate, and solve complex chemical engineering problems.
e. An ability to use techniques, skills and modern engineering tools necessary for engineering
practice.
f. An ability to understand the professional, societal and ethical responsibility.
g. An ability to work as a member of multidisciplinary teams, and have an understanding of team
leadership.
h. To have good written and oral communication skills.
i.
An ability to understand the impact of engineering solution in a global, economic and societal
context.
j.
An ability to have motivation and engage in lifelong learning.
k. An ability to have knowledge of recent happenings/contemporary issues.
l.
To have the knowledge of project management and finance requirements and able to write project
proposals.
11. Mapping of PEO’s & PO’s:
Programme
Educational
Objectives
1
2
3
4
a
X
X
b
X
X
c
d
X
X
X
Programme Outcomes
e
f
g
h
i
X
X
X
X
X
6
X
X
X
X
X
X
X
j
X
k
X
X
l
X
X
X
12. Curriculum breakdown structure:
4%
3%
9%
Humanites
18%
8%
Basic Sciences
14%
Engineering
Sciences
44%
13. BOS composition as per VTU Guidelines:
7
SCHEME OF TEACHING AND EXAMINATION – III SEMESTER B.E. CHEMICAL ENGINEERING (2015-16
Sl.
No.
Subject Code
Title of the Subject
Credits
(L:T:P
Teaching
Dept.
Teaching hours/week
L
T
P
End
Exam
(Hrs
Marks
CIE
SEE
Total
1
CHMAT301
Engineering
Mathematics – III
3:1:0
MAT
3
2
0
03
50
50
100
2
CHY302
Technical Chemistry -I
2:1:0
CHY
2
2
0
03
50
50
100
3
CH303
Chemical Process
Calculations
3:1:0
CH
3
2
0
03
50
50
100
4
CH304
Momentum Transfer
3:1:0
CH
3
2
0
03
50
50
100
5
CH305
Materials Science
3:0:0
CH
3
0
0
03
50
50
100
6
CH306
Process Equipment
Drawing
0:1:2
CH
0
2
3
03
50
50
100
7
CHL304
Momentum Transfer
Laboratory
0:0:2
CH
0
0
3
03
50
50
100
8
CHYL302
Technical Chemistry-I
Laboratory
0:0:2
CHY
0
0
3
03
50
50
100
14
10
9
25
8
SCHEME OF TEACHING AND EXAMINATION – IV SEMESTER B.E. CHEMICAL ENGINEERING (2015-16
Teaching hours/week
Credits
(L:T:P
Teaching
Dept.
L
T
P
End
Exam
(Hrs
Engineering
Mathematics- IV
3:1:0
MAT
3
2
0
CH402
Chemical Engineering
Thermodynamics
3:1:0
CH
3
2
3
CH403
Process Heat Transfer
3:1:0
CH
3
4
CH404
Mechanical Operations
3:1:0
CH
5
CHY405
Technical Chemistry-II
2:1:0
6
CHL403
Heat Transfer
Laboratory
7
CHL404
8
CHYL405
Sl.
No.
Subject Code
1
CHMAT401
2
Title of the Subject
Marks
CIE
SEE
Total
03
50
50
100
0
03
50
50
100
2
0
03
50
50
100
3
2
0
03
50
50
100
CHY
2
2
0
03
50
50
100
0:0:2
CH
0
0
3
03
50
50
100
Mechanical Operations
Laboratory
0:0:2
CH
0
0
3
03
50
50
100
Technical Chemistry-II
Laboratory
0:0:2
CHY
0
0
3
03
50
50
100
14
10
9
25
Legend: MAT-Mathematics, CHY-Chemistry, CH-Chemical Engineering, L-Lecture, T-Tutorial, P-Practical, CIEContinuous Internal Evaluation, SEE-Semester End Examination.
9
III Semester
ENGINEERING MATHEMATICS – III
Sub Code:
Credit:
CIE:
CHMAT301
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Engineering Mathematics I and II
Course coordinator: Mathematics Department
Course Objectives:
The students will
1. Learn to solve algebraic, transcendental and ordinary differential equations numerically.
2. Learn to fit a curve, correlation, regression for a statistical data.
3. Learn to represent a periodic function in terms of sines and cosines.
4. Understand the concepts of continuous and discrete integral transforms in the form of
Fourier and Z-transforms.
5. Understand the concepts of calculus of functions of complex variables.
Course Content:
Unit I
Numerical solution of Algebraic and Transcendental equations: Method of false position,
Newton - Raphson method.
Numerical solution of Ordinary differential equations: Taylor series method, Euler &
modified Euler method, fourth order Runge-Kutta method.
Statistics: Curve fitting by the method of least squares, fitting a linear curve, fitting a parabola,
fitting a Geometric curve, Correlation and Regression.
Unit II
Fourier Series: Convergence and divergence of infinite series of positive terms. Periodic
functions, Dirichlet conditions, Fourier series of periodic functions of period 2π and arbitrary
period, Half range Fourier series, Practical harmonic analysis.
Unit III
Fourier Transforms: Infinite Fourier transform, Infinite Fourier sine and cosine transforms,
properties, Inverse transforms, Convolution theorem, Parseval identities (statements only.
Z-Transforms: Definition, standard Z-transforms, Single sided and double sided, Linearity
property, Damping rule, Shifting property, Initial value and Final value theorems, Inverse Ztransforms, Application of Z-transforms to solve difference equations.
5
Unit IV
Complex Variables - I: Functions of complex variables ,Analytic function, Cauchy-Riemann
Equations in cartesian and polar coordinates, Consequences of Cauchy-Riemann Equations,
Construction of analytic functions.
Transformations: Conformal transformation, Discussion of the transformations w = z2,
w=
ez and 𝑤 = 𝑧 +
𝑎2
𝑧
(z ≠ 0, Bilinear transformations.
Unit V
Complex Variables-II: Complex integration, Cauchy theorem, Cauchy integral formula. Taylor
& Laurent series(statements only. Singularities, Poles and residues, Cauchy residue theorem
(statement only.
Text Books:
1. Erwin Kreyszig – Advanced Engineering Mathematics – Wiley publication – 10th edition-2015.
2. B. S. Grewal – Higher Engineering Mathematics – Khanna Publishers – 42nd edition – 2012.
References:
1. Glyn James – Advanced Modern Engineering Mathematics – Pearson Education – 4th
edition – 2010.
2. Dennis G. Zill, Michael R. Cullen - Advanced Engineering Mathematics, Jones
and Barlett Publishers Inc. – 3rd edition – 2009.
3. Dennis G. Zill and Patric D. Shanahan- A first course in complex analysis with
applications- Jones and Bartlett publishers-second edition-2009.
Course Outcomes: On successful completion of this course students
S.
No.
1.
2.
3.
4.
5.
Course Outcome
Programme
Outcomes
Satisfied
Should be able to solve the problems of algebraic, transcendental a,b,e,k
and ordinary differential equations using numerical methods.
Fit a suitable curve by the method of least squares and determine a,b,c,g
the lines of regression for a set of statistical data.
Find the Fourier series expansion of a function in both full range and half a,c,f
range values of the variable and obtaining the various harmonics of the
Fourier series expansion for the given
numerical data.
Find Fourier transforms, Fourier sine and Fourier cosine transforms of
e,f,j,k
functions and solving difference equations using Z-transforms.
Find singularities of complex functions and determine the values of
a,b,c,e,h
integrals using residues.
6
TECHNICAL CHEMISTRY-I
Sub Code:
Credit:
CIE:
CHY302
2:1:0
50 Marks
Contact Hours: 56
SEE:
50 Marks
Pre-requisites: Engineering Chemistry
Course coordinator: Chemistry Department
Course Objectives: The students will
1. Study the basic colligative properties; determine the effects of solutes on boiling point,
freezing point, and osmotic pressure and to calculate the molecular weight of the unknown solute
using freezing point depression.
2. Study liquification, colloidal systems and properties
3. Study of different types of organic reactions and isomerism in organic compounds.
4. Study of various organic named reactions used in different industries to synthesize organic
molecules, drugs etc.
5. Study the use of plants as a source of natural dyes, and synthesis of various dyes, manufacture
of soap and detergents, cleaning action of the soaps.
Course Content:
Unit-I
Chemical thermodynamics
Dilute solutions, Colligative properties, lowering of vapour pressure-Raults law-Determination
of M.W. Elevation of B.P Depression of freezing point determination of M.W, Osmotic pressuredetermination of molecular weight and experimental measurements. Isotonic solutions and
abnormal M.W.
Unit- II
Liquification and the properties of liquids, Colloids, Physical properties and molecular structure.
Unit –III
Organic Reaction Mechanism: Introduction, Types of reactions with mechanism-Addition,
Substitution and Elimination.
Basics of stereochemistry-Isomerism-Structural,-Structural, chain, positional, functional,
metamerism, tautomerism and ring-chain isomerism. Stereo isomerism-cis-trans isomerism,
optical activity of organic compounds, optical isomerism, Configuration- R,S and E, Z.
Conformation.
Unit –IV
Industrially Important Organic reactions: Beckmann Rearrangement, Perkin reaction, The
Hofmann rearrangement, Reamer-Tiemann reaction, Cannizzaro reaction, Skraup synthesis, The
Diels-Alder reaction, Aldol condensation.
Unit –V
Organic Materials of industrial importance:
Dyes-classification–modern theory of colour; Synthesis of methyl orange; congo red, malachite
green, indigo and Alizarin.
7
Oils-Fats Analysis of Oil; Sapanification value, Iodine and acid value of oils, Solvent extraction
of oils, refining of oils, Hydrogenation of oils
Soaps and detergents: Manufacture of soap, Continous jet sapanification method, mechanism of
cleaning action of soap, detergents manufacture, cationic, anionic and non ionic detergents.
Text Books:
1. Morrison B.R. and Boyd L.L., Organic Chemistry 6 th Edition, ELBS, New Delhi, 1999.
2. B.R. Puri, L.R. Sharma & Pathania, M.S., Principles of Physical Chemistry, 33rd Ed., S.
Nagin chand & Co., 1992.
3. House, H.O., Modern synthetic reactions, ULBS Publishers, New Delhi.
Reference Books:
1. Sykes Peter, Organic Reactions Mechanism, ULBS Publishers, and New Delhi.
2. Finar, Organic Chemistry Vol I & II ULBS Publishers, New Delhi.
3. Sharma B.K., Industrial Chemistry, 11TH edition, Chand S, and Co. New Delhi, 2001.
4. Tiwari Melhotra and Vishnoi, Organic Chemistry, 7 th Edition, Chand S. and Co. New Delhi,
1996.
5. Bahl, A. and Bahl B.S., A Text Book of Organic Chemistry, 15th Edition.S. Chand and &
Co, New Delhi, 1998.
6. Bikerman, J.J., Surface Chemistry: Theory and Applications, Academic press, New York,
1972.
7. Adamson, A.W., Physical Chemistry of Surfaces, Interscience Publishers Inc. New York.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
Course Outcome
Programme
Outcomes
Satisfied
1. Explain the effects of solutes on boiling point, freezing point, and a,c,g,i,k
osmotic pressure and to calculate the molecular weight of the
unknown solute using freezing point depression.
2. Explain catalytic reactions and the manufacture of dyes and a,b,c,g,l
applications in industry.
3. Write reaction mechanisms in various types of reactions.
a,c,g,k
4. Identify the different organic reactions using the various industries
a,c,e,g,j
in the manufacture of drugs and organic compounds.
5. Explain manufacture of soap and detergents, and their cleaning
action mechanism.
8
a,b,c,e,g,j
CHEMICAL PROCESS CALCULATIONS
Sub Code:
Credit:
CIE:
CH303
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Learn basic principles involving units and dimensions; Expressing compositions of
mixtures; Graphs used for data representation in chemical engineering
2. Learn laws related to about the behavior of gases, liquids and solids; Representation of
vapour-gas mixtures
3. Understand systematic skills, enhance confidence, and generate careful work habits in
solving problems involving different unit operations
4. Learn to adapt above procedures in solving problems involving chemical reactions.
5. Learn what energy balances are, and how to apply them and finally, to learn how to deal
with the complexity of larger problems.
Course Content:
Unit I
Basic Chemical Calculations: Fundamentals and derived units. Conversion of units.
Dimensional consistency of equations. Dimensionless groups and constants. Conversion of
equations. Concept of mole, mole fraction etc. Compositions of mixtures of solids and liquids
and gases. Concept of molarity, molality, normality and ppm. Use of semilog and log-log graphs,
Triangular graphs.
Unit II
Vapour-Gas Concepts: Ideal gas law calculations, Vapour pressure concepts and calculations
for miscible and immiscible systems. Humidity related terms, humidity chart, humidification and
dehumidification operation.
Unit III
Material Balance Without Reaction: General material balance equation for steady
and unsteady states. Typical Steady state material balances in mixing, evaporation, drying,
distillation, absorption, extraction, crystallization and evaporation. Material balances involving
Bypass, Recycle and Purging.
Unit IV
Steady State Material Balance With Reaction: Principles of stoichiometry, Concept of
limiting and excess reactants and inerts, fractional and percentage conversion, fractional yield
and percentage yield, Selectivity, related Problems – without reactions and with reactions.
Fuels and Combustion: Ultimate and Proximate analysis of fuels, Calculations involving
burning of solid, liquid and gaseous fuels, excess air, Air – fuel ratio calculations.
9
Unit V
Energy Balance: General Steady State Energy Balance equation, Thermophysics: Heat
Capacity, Thermochemistry and laws. Heat Capacity. Enthalpy, Heat of Formation, Heat of
Reaction, Heat of Combustion and Calorific Value. Heat of Solution, Heat of Mixing, Heat of
Crystallization. Determination of ∆HR at standard and elevated temperature. Theoretical and
flame temperatures and adiabatic flame temperature.
Text Books:
1. Hougen, O.A., Waston, K.M. and Ragatz, R.A., Chemical Process Principles Part – I,
Material and Energy Balances, Second Edition, CBS publishers and distributors, New Delhi,
1995.
2. Himmelblau, D.M., Basic Principles And Calculations In Chemical Engineering, 6 th Edition,
Prentice Hall Of India, New Delhi, 1997.
Reference Books :
1. Bhatt, B.L. and Vora, S.M., Stoichiometry (SI Units, Third Edition, 1996, Tata Mc Graw Hill
Publishing Ltd., New Delhi, 1996.
2. Richard M. Felder and Ronald W. Rousseau, Elementary Principles of Chemical Processes,
John Wiley & Sons,3rd Edition, 2005.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
Course Outcome
Programme
Outcomes Satisfied
1. Clear idea of various types of unit systems and they will be able to a
convert units from one form of the unit to other and able to find
the equations for fitting data.
2. Sound strategy for solving problems involving gases, vapours etc. a,b,d,i,j
3. Adopt the tools learned from the course to solve numerical a,b,c,e,j,k
problems which contain one or more unit operations.
4. Ability to solve material balance problems involving reactions
a,b,c,d,e,f,i,j,k
5. Develop mathematical relations for both mass and energy balances a,b,c,d,e,f,i,j,k
for different processes.
10
MOMENTUM TRANSFER
Sub Code:
Credit:
CIE:
CH304
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Engineering Mathematics
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Understand concepts on nature and types of fluids, stress and velocity relations, boundary
layer relations, pressure concepts and measurement of pressure by various experimental
methods and by mathematical relations and enhancement of problem solving skills.
2. Understand relationship between kinetic energy, potential energy, internal energy and work
complex flow systems using Bernoulli’s equation with application to industrial problems.
3. Understand clear concepts on Flow of incompressible fluids in conduits and thin layers and
friction factor variations with velocity and friction losses using Bernoullis Equations and they
will be demonstrated experimentally.
4. Study Flow of compressible fluids, Dimensional analysis, Dimensional homogeneity and
various dimensionless numbers and their applications.
5. Understand principles and working of various types of pumps, transportation and metering of
fluids using various experimental techniques and applications to industry.
Course Content:
Unit I
Fluid Statics And Its Application: Concept of unit operation, concept of momentum transfer,
nature of fluids and pressure concept, variation of pressure with height – hydrostatic equilibrium,
barometric equation, measurement of fluid pressure – manometers.
Fluid Flow Phenomena: Types of fluids – shear stress and velocity gradient relation, Newtonian
and Non Newtonian fluids, Viscosity of gases and liquids. Types of flow-laminar and turbulent
flow, Reynolds stresses, Eddy viscosity, Flow in boundary layers, Reynolds number, Boundary
layer separation.
Unit II
Basic Equations Of Fluid Flow: Average velocity, mass velocity, continuity equation, Euler
and Bernoulli’s equations, Modified equation for real fluids with correction factors. Pump work
in Bernoulli’s equations. Angular momentum equation.
Unit III
Flow of Incompressible Fluids In Conduits And Thin Layers: Laminar flow through circular
and non circular conduits. Hagen-Poisuelle equation, Laminar flow of non Newtonian liquids,
turbulent flow in pipes and closed channels, friction factor chart. Friction from changes in
velocity or direction. Form friction losses in Bernoulli’s equation. Flow of fluids in thin layers.
11
Unit IV
Flow of Compressible Fluids: Continuity equation, concept of Mach number, Total energy
balances, Velocity of sound, ideal-gas equations. Flow through variable area conduits, Adiabatic
frictional flow. Isothermal frictional flow (elementary treatment).
Dimensional Analysis: Dimensional homogeneity, Rayleigh and Buckingham-π method.
Significance of different dimensionless numbers. Elementary treatment of similitude between
model and prototype.
Unit V
Transportation and Metering Of Fluids: Pipes, fittings and valves, measurement of liquid and
gas flow rates by orifice meter, Venturi meter, Rota meter and Pitot tube. Flow through open
Channels- weirs and notches. Performance and characteristics of pumps–positive displacement
and centrifugal pumps. Fans, compressor and blowers. Introduction to Unsteady State Flow–
Time to empty the liquid from a tank.
Text Books:
1. McCabe, W.L., Unit operations of Chemical Engineering, 5th Edition, McGraw Hill, New
York, 1993.
2. Kumar, K.L, Engineering Fluid Mechanics, 3rd Edition, Eurasia publishing House (P Ltd., New
Delhi., 1984.
Reference Books:
1. Coulson and Richardson J.F., Chemical Engineering Vol. 1, 3rd edn., Pergamon
Press, 1991.
2. Badger, W.I. and Banchero, J.T., Introduction to Chemical Engineering, Tata Mc Graw Hill,
New York, 1997.
3. Foust, A.S., Principles Of Unit Operation, III Edition, John Wiley and Sons, New York,
1997.
4. Bansal, R.K., Fluid Mechanics and Hydraulic Machines, 7th Edition, Laxmi Publications,
2007.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1.
2.
3.
4.
5.
Course Outcome
Programme
Outcomes
Satisfied
Analyze different types of fluids and they will be able to measure pressure a,b,d,e,i,k
difference for flow of fluids.
Understand and analyze the relationship between kinetic and potential a,b,c,d,e,k
energy, internal energy, work, and heat in complex flow systems using
Bernoulli’s equation, perform macroscopic energy balances.
Analyze and calculate friction factor for different types of flow in various a,b,c,d,e,f,i,k
types of constructions.
Develop mathematical relations using Dimensional analysis by Rayleighs a,d,i
and Buckinghm –π method.
Have knowledge on various types of pumps, transportation and metering a,b,c,d,e,i,k
devices for fluid handling.
12
MATERIALS SCIENCE
Sub Code:
Credit:
CIE:
CH305
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Engineering Chemistry
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Understand concepts on properties and selection of metals, ceramics, and polymers for
design and manufacturing.
2. Study variety of engineering applications through knowledge of atomic structure, electronic
structure, chemical bonding, crystal structure, x-rays and x-ray diffraction, defect structure.
3. Study Microstructure and structure-property relationships, Phase diagrams, heat treatment of
steels.
4. Study detailed information on types of corrosion and its prevention.
5. Learn information on selection of materials for design and manufacturing.
Course Content:
Unit I
Introduction: Introduction to Materials Science, Classification of Engineering Materials, Levels
of Structure, Structure-Property relationship in materials, Primary and secondary bonds.
Crystal Geometry and Structure Determination: Geometry of crystals- the Bravais lattices,
Crystal directions and Planes- Miller indices, Structure determination-X – ray diffraction- Braggs
Law, the power method.
Unit II
Crystal Imperfections: Point Imperfections, Line imperfections- edge and screw dislocations,
Surface imperfections.
Phase Diagram And Phase Transformations: Phase rule, Single component systems, Binary
Phase Diagrams, Lever rule, Typical Phase diagrams for Magnesia-Alumina, Copper-Zinc, Ironcarbon system, Nucleation and growth, Solidification, Allotropic transformation, Cooling curves
for pure iron, Iron-carbon equilibrium diagram, Isothermal transformations (TTT curves.
Unit III
Deformation of Materials: Metals - Elastic deformation, Plastic deformation, Dislocation and
Strengthening mechanism, Failure – Fracture, Fatigue.
Brittle fracture, Stress-Strain behavior, Plastic deformation
Visco-elastic deformation, Fracture, Elastomer deformation.
Unit IV
Materials Processing: Metals and Alloys – Fabrications – Forming, Casting.
Thermal Processing: Annealing, Heat treatment of Steels. Surface hardening methods.
Ceramics – Fabrication and processing of glass
Polymers – Polymerization, Additives, Forming methods, Fabrication of elastomers and fibres.
13
Unit V
Corrosion And its Prevention: Electro-chemical corrosion, Galvanic cells, High temperature
corrosion, Passivity, Corrosion rate and its prediction, Prevention of corrosion. Corrosion charts.
Materials Selection and Design Considerations, Environmental considerations and recycling
Text Books:
1. William D. Callister, Materials Science and Engineering: An Introduction, 6th Edition,
Wiley, 2006.
2. Hajra Choudhary S. K., Material Science and Processes, Indian Book Distributing Co., 1982.
Reference Books:
1. Van Vlack, H.L., Elements of Materials Science, 2 nd Edition, Addision-Wesly Publishing
Company, NY, 1964.
2. Raghavan V., Material Science and Engineering- A First Course, 3rd Edition, Prentice Hall
of India Pvt. Ltd., New Delhi, 1996.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
3
4
5
Programme
Outcomes Satisfied
Course Outcome
Classify different types of engineering materials depending on
structure property, crystal geometry and X-Ray diffraction
Explain atomic structures, types of bonding and crystal
imperfections.
Draw phase diagrams of different metals, TTT curves and explain
deformation of materials.(
Suggest different type of heat treatment techniques depending on
the type of the material and they can analyze different types of
corrosions and suggest preventive methods.
Select materials depending on type of application.
14
a,b,e,j,i,j,k
b,c,d,e,h,k
c,e,f,g,h,i,j,k,l
f,g,i,k
b,c,i,j,k,l
PROCESS EQUIPMENT DRAWING
Sub Code:
Credit:
CIE:
CH306
0:1:2
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Engineering Drawing
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Learn to draw sectional views of the equipments, hatching and sectional planes, piping
symbols, vessel enclosures and supports.
2. Learn to draw proportionate drawings of process equipments like distillation column and heat
exchangers.
3. Learn to draw various assembly drawings of pipe joints, and valves.
4. Learn to draw centrifugal pump and gear pump drawings.
5. Learn basics of AutoCAD
Course Content:
Sectional Views: Representation of the sectional planes, sectional lines and hatching, selection
of section planes and types of sectional views.
Proportionate Drawing 0f Process Equipment: Equipment and piping symbols, vessel
component, vessel opening, Manholes, Vessel enclosures, Vessel Support, jackets, Shell and
tube heat exchanger, reaction vessel and Evaporator, Distillation column
Assembly Drawing: Joints - Cotter with sleeve, cotter joint, Socket and Spigot joint, Stuffing
box and Expansion joint (Screw type or Flanged type
Valves - Stop Valve, Junction Stop Valve, Globe Valve, Stop cock and Gate Valve, Screw down
Stop Valve, Rams Bottom safety Valve, Non – Return Valve.
Pumps - Centrifugal pump, gear pump.
AutoCAD: Introduction, Flanged joint, Union Joint.
Text Books:
1. Gopal Krishna, K.R, Machine Drawing, 9th Edition, Subhas Stores, Bangalore, 1995.
2. Joshi, M.V., Process Equipment Design, 3rd Edition, Macmillan India Publication, New
Delhi.
Reference Books:
1. Walas, S.M., Chemical Process Equipment, Butterworth Heinemann Pub. 1999.
2. Ludwig E.E., Applied process Design, 3rd Edition, Gulf Professional Publishing, New Delhi,
1994.
3. Bhatt, N.D., Machine Drawing, 29th Edition, Charotar publishing House, Anand, 1995.
4. Maidargi, S.C., Chemical Process Equipment Design, Vol. I, PHI Learning Pvt. Ltd., 2012.
15
Note: AutoCAD for only Internal Assessment. In SEE 30% marks to be allocated for memory
drawing and 70% marks for assembly drawing.
Course Outcomes: The students will be well versed to do the following
S.
No.
1
2
3
4
5
Programme
Outcomes Satisfied
Course Outcome
Clear idea of various types of conventions for drawing as per IS696 and chemical engineering symbols.
Know the components of chemical process equipment and sketch
them freehand.(
Draw assembled views of couplings and pipe joints from views
of individual parts.
Draw assembled views of valves and pumps from views of
individual parts.
Be able to specify hardware and software requirements for
computer aided drawing.
16
a,e
c
e
e
a,e
MOMENTUM TRANSFER LABORATORY
Sub Code:
Credit:
CIE:
CHL304
0:0:2
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Engineering Mathematics
Course coordinator: Chemical Engineering Department
Course Objective: The student will perform experiment
1. To determine frictional losses in flow systems
2. Measure flow rate of incompressible fluids
3. To study pump characteristics.
The experiments should be based on the following topics:
1. Friction in Circular Pipes
2. Friction in Non-Circular Pipes
3. Friction in Helical/Spiral Coils
4. Flow rate measurement using Venturi/ Orifice meters
5. Local velocity measurement using Pitot tube
6. Flow over Notches
7. Hydraulic coefficients – Open Orifice
8. Pressure drop in Packed bed
9. Minimum fluidization velocity-Fluidized bed
10. Study of characteristics for Centrifugal pump
11. Study of Pipe Fittings and their equivalent lengths
12. Reynolds apparatus
13. Positive displacement pump
14. Bernoulli’s apparatus
Note: A minimum of 10 experiments are to be conducted.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
3
Course Outcome
Determine energy loss due to friction in flow systems
Measure flow rate of incompressible fluids
Determine pump characteristics and recommend for specific
usage.
17
Programme
Outcomes Satisfied
a,b,c,d,e,h,j,k
a,b,d,e,h,j,k
a,b,c,d,e,h,j,k
TECHNICAL CHEMISTRY-I LABORATORY
Sub Code:
Credit:
CIE:
CHYL302
0:0:2
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Engineering Chemistry
Course coordinator: Chemistry Department
Course Objective: The student will perform experiments on
1. Determination of chloride, nickel and iron in samples.
2. Preparation of organic compounds acetanilide, P-amino benzoic acid
3. Analysis of oils and fats
4. Effect of salt on CST
5. Study of Kinetics of the reaction
Following experiments are suggested:
1. Determination of Chloride content in the given sample of water using N/40 AgNO 3
2. Determination of partition coefficient of iodine between water and carbon tetrachloride.
3. Study of Kinetics of the reaction between K2S2O8 and KI.
4. Effect of Salt on the critical solution temperature of phenol-water system.
5. Determination of nickel as nickel dimethyl glyoximate gravimetrically (after separating Iron
in the given stainless steel solution.
6. Determination of iron as ferric oxide gravimetrically (after separating copper in the given
Chalcopyrite ore solution.
7. Preparation of acetanilide by acetylation of aniline using acetic anhydride.
8. Preparation of P-amino benzoic acid.
9. Analysis of oils and fats- acid value, and iodine value.
10. Estimation of carboxylic acid by Iodometric method
11. Adsorption of heavy metal ions (Cr+3 from solution using different adsorbents and estimation
by colorimetry.
Reference Books:
1. Arthur, I. Vogel’s Qualitative Inorganic analysis including elementary instrumental analysis,
ELBS, Longmann group, 5th Edition, 1989.
2. Clair N. Sawyer and Perry L, McCarty, Chemistry for Environmental Engineering, Third
Edition, McGraw-Hill Book Company, New York, 1978.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
3
4
5
Course Outcome
Determination of chloride, nickel and iron in samples
Preparation of organic compounds acetanilide, P-amino benzoic
acid
Analysis of oils and fats
Effect of salt on CST
Study of Kinetics of the reaction
18
Programme
Outcomes Satisfied
a,b,c,d,e,f,g,h,i,j,k
a,b,d,f,g,h,i,j,k
a,b,c,d,f,g,h,j,k
a,c,d,f,g,h,j,k,l
a,c,d,f,g,h,i,j,k,l
IV Semester
ENGINEERING MATHEMATICS – IV
Sub Code:
Credit:
CIE:
CHMAT401
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Engineering Mathematics I, II and III
Course coordinator: Mathematics Department
Course Objectives: The students will
1 Learn the concepts of finite differences, interpolation and it applications.
2 Understand the concepts of PDE and its applications to engineering.
3 Learn the concepts of consistency, methods of solution for linear system of equations and
eigen value problems.
4 Learn the concepts of Random variable and probability distributions.
5 Construct the various tests essentially needed for the testing of small samples for the testing of
hypothesis.
Course Content:
Unit I
Finite Differences and Interpolation: Forward, Backward differences, Interpolation, NewtonGregory Forward and Backward Interpolation formulae, Lagrange interpolation formula and
Newton divided difference interpolation formula (no proof.
Numerical Differentiation and Numerical Integration: Derivatives using Newton-Gregory
forward and backward interpolation formulae, Newton-Cotes quadrature formula, Trapezoidal
rule, Simpson 1/3rd rule, Simpson 3/8th rules.
Partial Differential Equations - I: Introduction to PDE , Solution of PDE – Direct integration,
Method of separation of variables.
Unit II
Partial Differential Equations-II: Classification of second order PDE, Derivation of one dimensional heat and wave equations, Numerical solution of One - dimensional heat and wave
equations, Two - dimensional Laplace equation, Poisson equation.
Unit III
Linear Algebra: Elementary transformations on a matrix, Echelon form of a matrix, rank of a
matrix, Consistency of system of linear equations, Gauss elimination and Gauss – Siedel method
to solve system of linear equations, eigen values and eigen vectors of a matrix, Rayleigh power
method to determine the dominant eigen value of a matrix, diagonalization of a matrix, system of
ODEs as matrix differential equations.
Unit IV
Random Variables: Random Variables (Discrete and Continuous, Probability density function,
Cumulative density function, Mean, Variance, Moment generating function..
19
Probability Distributions: Binomial distribution, Poisson distributions, Normal distribution,
Exponential distribution, Uniform distribution, Joint probability distribution (both discrete and
continuous, Conditional expectation.
Unit-V
Sampling Theory : Sampling, Sampling distributions, Standard error, Weak law of large
numbers(without proof, Central limit theorem(no proof, Test of Hypothesis for means,
Confidence limits for means, Student’s t-distribution, F-distribution, Chi-Square distribution as a
test of goodness of fit.
Text Books:
1. Erwin Kreyszig – Advanced Engineering Mathematics – Wiley publication – 10th edition-2015.
2. B.S.Grewal-Higher Engineering Mathematics-Khanna Publishers-42nd edition-2012
3. R.E. Walpole, R. H. Myers, R. S. L. Myers and K. Ye – Probability and Statistics for
Engineers and Scientists – Pearson Education – Delhi – 8th edition – 2007.
Reference Books:
1. Glyn James- Advanced Modern Engineering Mathematics-PearsonEducation-4th edition2010
2. Kishor S. Trivedi – Probability & Statistics with reliability, Queuing and Computer
Science Applications – PHI – 2nd edition – 2002.
3. Murray R. Spiegel, John Schiller & R. Alu Srinivasan - Probability & Statistics Schaum’s outlines -2nd edition - 2007.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
3
4
5
Course Outcome
Should be able to use a given data for equal and unequal intervals to
find a polynomial function for estimation. Compute maxima, minima,
curvature, radius of curvature, arc length, area, surface area and
volume using numerical differentiation and integration.
Solve partial differential equations analytically and numerically
Find the rank of a matrix, test the consistency and the solution by
Gauss elimination and Gauss Siedel iteration methods.
Apply the concepts of probability distributions to solve the
engineering problems.
Use the concepts of sampling to enable a student to take a
decision about the hypothesis.
20
Programme
Outcomes
Satisfied
a,b,h
a,b,c,f,i
c,d,j
f,g,h
c,d,g,i
CHEMICAL ENGINEERING THERMODYNAMICS
Sub Code:
Credit:
CIE:
CH402
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Learn fundamentals of thermodynamics such as types of properties, processes and laws of
thermodynamics for flow and non flow process.
2. Understand the clear concepts on P-V-T behavior, Equations of state, thermodynamic
diagrams and compressibility charts, entropy, irreversibility and problem solving skills.
3. Learn the thermodynamic properties of pure fluids, energy relations and fugacity concepts
and study the estimation of partial molar properties, property changes of mixing, and ideal
and non ideal solutions.
4. Learn the fundamentals of phase equilibrium, concept of chemical potential and generation
and consistency check for VLE data.
5. Understand fundamentals of chemical reaction equilibrium to find feasibility and extent of
conversion for the industrial reactions.
Course Content:
Unit I
Basic Concepts and First Law: System, surrounding, processes, state and properties- intensive
and extensive properties, State and path functions, Reversible & irreversible processes, Zeroth
law of thermodynamics. General statement of first law of thermodynamics, First law for cyclic
process and non flow processes, Heat capacity. Derivation for closed system and steady state
flow process- flow calorimeter and heat capacity.
Unit II
P-V-T Behaviour: P-V-T behaviour of pure fluids, Equations of state and ideal gas law,
Processes involving ideal gas law: Constant volume, constant pressure, Constant temperature,
adiabatic and polytropic processes, Equations of state for real gases: Van der Waals equation,
Redlich – Kwong equation, Peng – Robinson equation, Virial equation, Principles of
corresponding states, Generalized compressibility charts, Thermodynamic diagrams.
Second Law of Thermodynamics: General statements of the Second law, concept of Entropy,
Carnot’s principle, Calculations of entropy change, Clausius Inequality, Entropy and
Irreversibility, Third law of thermodynamics.
Unit III
Thermodynamic Properties of Pure Fluids: Work function, Gibbs free energy, Fundamental
property relations, Maxwells equations, Equations for U and H, Effect of temperature on U, G, H
and S, Entropy heat capacity relations, Relationship between Cp, Cv, Clapeyron equation, GibbsHelmholtz equation, Fugacity and fugacity coefficient, determination of fugacity of pure fluids.
21
Properties of Solutions: Partial molar properties, estimation, Gibbs-Duhem equation, Chemical
potential, Fugacity in solutions, Henry’s law and dilute solutions, Activity in solutions, Activity
coefficients, Property changes of mixing, excess properties (Qualitative treatment Activity &
Activity coefficients. Ideal and non-ideal solutions.
Unit IV
Phase Equilibria: Chemical potential, criterion for VLE for ideal solutions, Raoult’s law, P-x,y
and T-x,y diagrams, Non ideal solutions- Azeotropes types, VLE at low pressures, VLE
correlations- van laar, Margules and Wilson equation. Co-existence equation, G-D equation for
VLE, Consistency tests, VLE at high pressures, Liquid-liquid equilibrium.
Unit V
Chemical Reaction Equilibrium: Reaction stoichiometry, Criteria of chemical reaction
equilibrium, Equilibrium constant and standard free energy change, Effect of temperature,
pressure on equilibrium constants and other factors affecting equilibrium conversion, Liquid
phase reactions, Heterogeneous reaction equilibria, Phase rule for reacting system.
Text Books:
1. Smith, J.M. and Vanness, H.C., Introduction to Chemical Engineering Thermodynamics, 5th
Edition, McGraw Hill, New York 1996.
2. Narayanan, K.V., Textbook of Chemical Engineering Thermodynamics, Prentice Hall of
India Private Limited, New Delhi, 2001.
Reference Book:
1. Rao, Y.V.C., Chemical Engineering Thermodynamics, New Age International Publication,
Nagpur, 2000.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
3
4
5
Programme
Outcomes Satisfied
Course Outcome
Calculate the heat and work requirements for the given flow or
non-flow processes.
Analyze and find properties such as Pressure, Volume and
temperature for equations of states and form the fundamentals of
first law of thermodynamics.Calculate entropy for the processes,
and various types of energies such as internal energy, enthalpy,
Helmholtz free energy and Gibbs free energy.
Differentiate between ideal and non-ideal solution and estimate
partial molar properties.
Generate Vapor Liquid Equilibrium data for ideal and non-ideal
solutions and check for their consistency by various methods.
Find the feasibility and extent of conversion for any reaction.
22
a,b,f,h,i,k
a,b,c,d,f,I,j,k
a,b,d,e,j,k
a,b,c,d,e,j,k
a,b,c,d,j,k
PROCESS HEAT TRANSFER
Sub Code:
Credit:
CIE:
CH403
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Engineering Mathematics
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Study various modes of Heat transfer and their fundamental relations. Study conduction heat
transfer and develop mathematical relations for different geometrical solids.
2. Understand properties of insulation and critical thickness of insulation.
3. Understand different types of heat transfer coefficients and their estimations in various types
of flows in different geometries. Study the Boiling and condensation phenomenon.
4. Understand the working of Heat exchangers and to learn design of double pipe, shell and
tube heat exchangers and design of evaporators and conduct experiments and to submit the
report.
5. Understand the phenomenon of radiation, radiation shields and estimation of emissivity.
Study the performance and types of evaporators.
Course Content:
Unit I
Introduction: Various modes of heat Transfer.
Conduction: Fourier’s law, Steady state unidirectional heat flow through compound walls,
Numerical Problems. Heat conduction with heat generation in a slab, cylinder and sphere.
Unit II
Insulation: Properties of insulation materials. Types of insulation, Critical and optimum
thickness of insulation.
Extended Surfaces: Types of fins, fin efficiency. Fin effectiveness. Elementary treatment of
unsteady state heat conduction- Biot number, Lumped heat capacity model, Unsteady state heat
conduction through a slab, Numerical Problems.
Unit III
Convection: Individual and Overall heat transfer coefficients, LMTD, Empirical correlations for
forced and natural convection. Analogy between momentum and heat transfer-Reynolds,
Colburn and Prandtl.
Heat Transfer With Phase Change: Boiling phenomenon, nucleate boiling and film boiling,
Condensation- Film and drop wise condensation. Nusselt equation.
23
Unit IV
Heat Transfer Equipment: Construction and working - Double pipe heat exchanger. Shell and
tube heat exchangers. Condensers.
Design of Heat Transfer Equipment: Elementary design of double pipe heat exchanger. Shell
and tube heat exchanger and condensers.
Unit V
Evaporators: Types, Performance of tubular evaporator- evaporator capacity, evaporator
economy, Multiple effect evaporators.
Radiation: Properties and definitions, Stefan-Boltzmann law, Wein’s displacement law,
Kirchoff’s law, View factors, Radiation between surfaces, Radiation involving gases and vapors.
Radiation shields.
Text Books:
1. McCabe, Unit Operations of Chemical Engineering, McGraw Hill, NY, 5 th Edition, 2000.
2. Coulson, J.M and Richardson, J.F, Chemical Engineering, Vol 1, Chemical Engineering,
Pergemon and ELBS, 5th Edition, McGraw Hill, 2000.
Reference Books:
1. Rao, Y.V.C., Heat Transfer, I Edition, University Press (India Ltd, New Delhi, 2000.
2. Hollman, J. P., Heat Transfer, 8th Edition.
3. Kern, D. Q., Process Heat Transfer, McGraw Hill, NY, 1965.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
3
4
5
Programme
Outcomes Satisfied
Course Outcome
Write all fundamental heat transfer laws and relations. Derive
equations for the calculation of heat flux and estimation of
intermediate temperatures in multilayer systems.
Calculate critical thickness of insulation and its significance.
Derive relation for heat flow through fins and its relevance to
industry.
Application for various correlations of convective heat transfer to
different problems. Estimate LMTD and heat transfer coefficients
for different types of flows.
Design Shell and tube and double pipe heat exchanger and
Evaporator. Explain radiation in different type of solids and
estimate emissivity.
Perform emissivity calculation and also calculate the economy and
capacity of evaporators.
24
a,b,i,j,k
a,b,c,d,e,k
a,c,d,e,f,g,i,j,k
a,b,c,d,i,j,k
a,c
MECHANICAL OPERATIONS
Sub Code:
Credit:
CIE:
CH404
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Pre-requisites: Engineering Mathematics
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Study properties of particulate solids, handling and separation of solid particles using
industrial screens.
2. Study principles of communition and different types of equipment used for size reduction
like crushers and grinders.
3. Learn the basics of fluid flow past immersed bodies and motion of particles through fluids.
4. Understand the principles, working and construction of filtration and sedimentation
equipments.
5. Understand energy requirements in solids handling, agitation and mixing, solid conveying
and storage.
Course Content:
Unit I
Particle Technology: Particle shape, particle size, different ways of expression of particle size,
shape factor, sphericity, mixed particles size analysis, screens – ideal and actual screens,
differential and cumulative size analysis, effectiveness of screen, specific surface of mixture of
particles, number of particles in a mixture, standard screens industrial screening equipment,
motion of screen, grizzly, gyratory screen, vibrating screen, trommels, sub sieve analysis – Air
permeability method, sedimentation and elutriation methods.
Unit II
Size Reduction: Introduction – types of forces used for communition, criteria for communition,
characteristics of communited products, laws of size reduction, work index, energy utilization,
methods of operating crushers – free crushing, choke feeding, open circuit grinding, closed
circuit grinding, wet and dry grinding, equipment for size reduction – Blake jaw crusher,
gyratory crusher, smooth roll crusher, tooth roll crusher, impactor, attrition mill, ball mill, critical
speed of ball mill, ultra fine grinders, fluid energy mill, colloid mill, cutters – knife cutter.
Unit III
Flow of Fluid Past Immersed Bodies: Drag, drag coefficient, pressure drop – Kozeny –
Carman equation, Blake- Plummer, Ergun equation, fluidization, conditions for fluidization,
minimum fluidization velocity, types of fluidization, application of fluidization, slurry transport,
pneumatic conveying.
Motion of Particles Through Fluids: Mechanics of particle motion, equation for one
dimensional motion of particles through a fluid in gravitational and centrifugal field, terminal
velocity, drag coefficient, motion of spherical particles in Stoke’s region, Newton’s region and
intermediate region, criterion for settling regime, hindered settling, modification of equation for
25
hindered
settling,
centrifugal
separators,
cyclones
and
hydro
cyclones.
Unit IV
Sedimentation: Batch settling test, application of batch settling test to design of continuous
thickener, Coe and Clevenger theory, Kynch theory, thickener design, determination of thickener
area.
Filtration: Introduction, classification of filtration, cake filtration, clarification, batch and
continuous filtration, pressure and vacuum filtration constant rate filtration and cake filtration,
characteristics of filter media, industrial filters, sand filter, filter press, leaf filter, rotary drum
filter, horizontal belt filter, bag filter, centrifugal filtration – suspended batch centrifuge, filter
aids, application of filter aids, principles of cake filtration, modification of Kozeny – Carman for
filtration
Unit V
Agitation And Mixing: Application of agitation, Agitation equipment, Types of impellers –
Propellers, Paddles and Turbines, Flow patterns in agitated vessels, Prevention of swirling,
Standard turbine design, Power correlation and Power calculation, Mixing of solids, Types of
mixers- change can mixers, Muller mixers, Mixing index, Ribbon blender, Internal screw mixer,
Tumbling mixer.
Sampling, Storage and Conveying of Solids: Sampling of solids, storage of solids, Open and
closed storage, Bulk and bin storage, Conveyors – Belt conveyors, Chain conveyor, Apron
conveyor, Bucket conveyor, Bucket elevators, Screw conveyor.
Text Books:
1. McCabe W.L., Unit Operation Of Chemical Engineering, V Edition, McGraw Hill
International, Singapore, 2000.
2. Badger, W.L. and Banchero J.T., Introduction to Chemical Engineering, III Edition, McGraw
Hill International, Singapore, 1999.
3. Coulson, J.M. and Richardson, J.F., Chemical Engineering Vol.2, 4, Particle Technology and
Separation Process, 1998.
Reference Books:
1. Brown G., Unit Operation, I Edition, CBS Publishers, New Delhi, 1995.
2. Perry, R and Green, W.D., Perry’s Chemical Engineering Hand book, VII Edition, McGraw
Hill International Edition, New York, 2000.
3. Foust, A.S. et.al, Principles of Unit Operation, III Edition, John Wiley and Sons, New York,
1997.
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
Course Outcome
Classify and suggest different type of separation processes
required for a given feed material.
Suggest suitable equipment from different types of size reduction
methods such as crushing, grinding milling depending on the type
and size of the material.
26
Programme
Outcomes Satisfied
b,c,d,e,fg,g,h,j,k
a,b,c,e,h,j,k
3
4
5
Calculate the terminal velocity of the particles and understanding
of fluid flow through packed and fluidized beds to apply them in
practice.
Explain how to solve filtration problems and find area of the
thickener.
Explain the mixing processes, conveying of solids and calculate
the power requirements for different type of mechanical
operations.
27
a,b,d,e,g,i,j,k
a,b,d,e,i,j,k
a,b,d,e,g,j,k
TECHNICAL CHEMISTRY-II
Sub Code:
Credit:
CIE:
CHY405
2:1:0
50 Marks
Contact Hours: 36
SEE:
50 Marks
Pre-requisites: Engineering Chemistry, Technical Chemistry-I
Course coordinator: Dr. M N Manjunatha
Course Objectives
Students shall develop the need for
1. To understand the fundamentals, principles and applications of Spectroscopy and
Electronic spectroscopy.
2. To understand the fundamentals, principles and applications of Infrared spectroscopy and
Mass spectrometry.
3. To understand the fundamentals, principles and applications NMR spectroscopy.
4. To understand the principles and applications of Flame photometry and Atomic
Absorption spectroscopy.
5. To understand the principles, working and applications of GC, TLC and HPLC.
Course Content:
UNIT I
Spectroscopy: Introduction: Interaction of electromagnetic radiation, energies corresponding to
various kinds of radiations, types of spectroscopy, representation of a spectrum, atomic and
molecular transitions, selection rules.
3 hours
Electronic spectroscopy: Introduction, Principle of electronic spectroscopy, Beer-Lamberts law
definition, derivation and its limitations, terminology associated with electronic spectroscopy,
Intensity shifts, types of absorption bands. Electronic energy levels and electronic transitions in
organic molecules. Woodward-Fisher rules for conjugated dienes and carbonyl compounds.
Quantitative applications.
UNIT II
Infrared spectroscopy: Introduction, Regions of infrared region spectrum, Theory-correct
wavelength of radiation and change in electric dipole moment of a molecule. Types of vibrations,
Factors affecting the group frequencies, electronic effects and hydrogen bonding. Force constant,
coupled interactions, Instrumentation FTIR spectroscopy. Applications, Numerical problems.
Mass Spectrometry: Introduction, basic principles, instrumentation, methods of generating
positively charged ions-electron impact, molecular ion peak, base peak, metastable peak and
isotopic peak, modes of fragmentation.
28
UNIT III
NMR Spectroscopy: General introduction, Theory of NMR, Types of nuclei, chemical shift
definition, factors affecting chemical shift, spin-spin interaction, shielding mechanism of
measurement, Instrumentation, sample handling, representation of NMR spectrum, NMR spectra
of ethanol, methanol and simple organic molecules. Applications.
UNIT IV
Flame Photometry and Atomic Absorption Spectroscopy: Introduction, principle,
instrumentation, applications-qualitative and quantitative determination of alkali and alkaline
earth metals, advantages and disadvantages of FES and AAS. Types of flames used in AAS and
flame spectra, variation of emission intensity with flame, metallic spectra in flame, comparative
study of flame emission spectroscopy and atomic absorption spectroscopy.
Chromatography: Introduction, Classification-Theory-distribution coefficient, rate of travel,
retention time, adjusted retention time, retention volume, adjusted retention volume, net retention
volume, specific retention volume, column capacity, separation number, peak capacity, shapes of
chromatic peak, column efficiency, resolution, optimization of column performance, Numerical
problems.
UNIT V
Thin layer chromatography: Principle, experimental procedure, applications.
Gas chromatography: Principle, instrumentation, sample injection, detectors (TCD, FID, ECD,
atomic emission detector.
High performance liquid chromatography: Principle, instrumentation, column, sample
injection, detectors (absorbance, refractive index, electrochemical.
TEXT BOOKS:
1. Spectrometric Identification of organic compounds, R.M. Silverstein and W.P.
Webster,Wiley & Sons, 1999.
2. Instrumental Methods of Analysis. H.H. Willard, L.L. Merritt and J.A. Dean and F. A.
Settle, CBS Publishers, 7th Edition, 1988.
REFERENCE BOOKS:
1. Instrumental methods of Chemical Analysis, G.W. Ewing, 5th Edition, McGraw-Hill, New
York, 1988.
2. Principles of Instrumental Analysis, Skoog, D.A, S.J. Holler, T.A. Nilman, 5th Edn.,
Saunders college publishing, London, 1998.
3. Spectroscopy by H. Kaur, Pragati Publication, Eighth Edition 2013.
29
4. Principles of Electroanalytical Methods, T. Riley and C. Tomilinsom, John Wiley and
Sons.
5. Instrumental Methods of Chemical Analysis, B.K. Sharma, Goel Publishing House Meerut
2000.
6. Vogel’s Text Book of Quantitative Inorganic analysis, Jaffery, Gill, Basset. J et al 5th
Edn., ELBS, 1998
Course Outcomes: On successful completion of this course students will be able to
S.
No.
1
2
3
4
5
Course Outcome
Understand the electronic spectra of simple organic molecules.
Understand the IR and Mass spectra of simple organic molecules.
Understand the NMR spectra of simple organic molecules.
Working knowledge of Flame photometry and Atomic absorption
spectroscopy.
Working knowledge of GC, TLC and HPLC.
.
30
Programme
Outcomes Satisfied
a,b,c,d,e,f,g,h,i,j,k,l
a,b,d,f,g,h,i,j,k,l
a,b,c,d,f,g,h,i,j,k,l
a,b,c,d,e,f,g,h,i,j,k,l
a,b,c,d,e,f,g,h,i,j,k,l
PROCESS HEAT TRANSFER LABORATORY
Sub Code:
Credit:
CIE:
CHL403
0:0:2
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objective: The student will conduct experiment
1. To study the performance of various types of heat exchangers
2. Determine emissivity
3. Assess insulation thickness for pipes.
List of experiments suggested:
1. Natural Convection in Bare and Finned tube
2. Vertical Shell and Tube Heat exchanger (Condenser
3. Horizontal Shell and tube Heat exchanger (Condenser
4. Helical Coil Heat Exchanger
5. Emissivity Determination
6. Effect of Geometry on Natural Convection
7. Heat Transfer in Packed Beds
8. Double Pipe Heat Exchanger
9. Heat Transfer in Jacketed Vessel
10. Determination of Insulation Thickness
11. Transient Heat Conduction
12. Heat Transfer in Fluidized Beds
13. Evaporator
14. Solar Heater
15. Spiral Plate Heat Exchanger
16. Cross Flow Heat Exchanger
Note: A minimum of 10 experiments are to be conducted.
Course Outcome: On completion of the laboratory, the student will be able to
S.
No.
1
2
3
Programme
Outcomes Satisfied
Course Outcome
Determine the design parameters for design and selection of heat
exchangers.
Evaluate the performance of different types of heat exchangers.
Explain the necessity of insulation and fins.
31
a,b,h
a,b,c,d,e,g
a,d,e,f,g
MECHANICAL OPERATIONS LABORATORY
Sub Code:
Credit:
CIE:
CHL404
0:0:2
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objective:
1. Study various mechanical operations associated with different solids as well as fluid.
Experiments mainly deal with size reduction, size separation, clarification, solid fluid
separation etc.
2. Understand and apply engineering experimentation techniques and safety procedures
common to the chemical industry.
3. Apply principles developed in chemical engineering courses for the analysis of chemical
engineering processes and unit operations.
4. Improve technical writing skills.
5. Improve skills necessary for group work interpersonal skills, coordination of the efforts
of several persons, leader and subordinate roles, etc.
The experiments should be based on the following topics:
1. Air elutriation
2. Air permeability
3. Ball mill
4. Batch sedimentation
5. Beaker decantation
6. Cyclone separator
7. Drop weight crusher
8. Froth flotation
9. Grindability index
10. ICI sedimentation
11. Jaw crusher
12. Leaf filter
13. Plate and frame filter press
14. Pneumatic conveyor
15. Screen effectiveness
16. Sieve analysis
17. Thickener
Note: A minimum of 10 experiments are to be conducted.
Course Outcome: On successful completion of the laboratory the student will be able to
S.
No.
1
Programme
Outcomes Satisfied
a,b,c,d,g,j,k
Course Outcome
Perform particle size analysis
32
2
3
Evaluate performance of size reduction and filtration equipments.
Suggest their applications.
33
a,b,c,d,e,g,j,k
a,b,d,h
TECHNICAL CHEMISTRY LABORATORY-II
Sub Code:
Credit:
CIE:
CHYL405
0:0:2
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Engineering Chemistry laboratory
Course coordinator: Dr. M N Manjunatha
Course Objectives
1. To understand the basic concepts of spectroscopic techniques.
2. To understand the various techniques of Flame photometry and Atomic Absorption
spectroscopy.
3. To understand the working of GC, TLC and HPLC.
List of Experiments
1. Conductometric estimation of Li2SO4 using standard BaCl2 (Precipitation titration
2. Determination of sulphate in the given sample of water using Nephelometer.
3. Determination of nitrate in the given sample of water using spectrophotometer.
4. Determination of % composition of binary mixture using Ostwald’s viscometer.
5. Separation of dyes by thin layer chromatography.
6. Potentiometric titration: FAS><KMnO4.
7. Gas Chromatography (Demo
8. Flame photometric estimation of Ca/K present in the given sample of water.
9. Determination of % of metal present in the given sample using AAS (Demo.
10. To determine (a λmax of a cobalt chloride (b Verify Beer’s law and apply to it find the
concentration of the given CoCl2 solution.
11. Estimation of esters by hydrolysis
12. Estimation of aminogroup by acetylation
13. Spectrophotometric analysis of the chromium ion
Referenece books:
1. Laboratory manual
2. Text book of Organic analysis-IL Finar
3. Vogel text book of quantitative inorganic analysis, Jaffery, Gill, Basset. J et al 5th edn.,
ELBS, 1998.
Course Outcomes On successful completion of the laboratory the student will be able to
S.
No.
1
2
3
Course Outcome
Interpret the various spectra using spectroscopic techniques.
Analyzing the various samples using AAS and FES.
Have concept on using GC, TLC and HPLC for chemical analysis.
34
Programme
Outcomes Satisfied
a,b,c,d,e,f,g,h,i,j,k,l
a,b,d,f,g,h,i,j,k,l
a,b,c,d,f,g,h,i,j,k,l