Journal of Structural Geology xxx (2012) 1e12 Contents lists available at SciVerse ScienceDirect Journal of Structural Geology journal homepage: www.elsevier.com/locate/jsg Surface roughness evolution on experimentally simulated faults François Renard a, b, *, Karen Mair b, c, Olav Gundersen b a ISTerre, University of Grenoble I, CNRS, BP 53, F-38041 Grenoble, France Physics of Geological Processes, University of Oslo, Norway c Department of Geosciences, University of Oslo, Norway b a r t i c l e i n f o a b s t r a c t Article history: Received 3 October 2011 Received in revised form 17 February 2012 Accepted 20 March 2012 Available online xxx To investigate the physical processes operating in active fault zones, we conduct analogue laboratory experiments where we track the morphological and mechanical evolution of an interface during slip. Our laboratory friction experiments consist of a halite (NaCl) slider held under constant normal load that is dragged across a coarse sandpaper substrate. This set-up is a surrogate for a fault surface, where brittle and plastic deformation mechanisms operate simultaneously during sliding. Surface morphology evolution, frictional resistance and infra-red emission are recorded with cumulative slip. After experiments, we characterize the roughness developed on slid surfaces, to nanometer resolution, using white light interferometry. We directly observe the formation of deformation features, such as slip parallel linear striations, as well as deformation products or gouge. The striations are often associated with marginal ridges of positive relief suggesting sideways transport of gouge products in the plane of the slip surface in a snow-plough-like fashion. Deeper striations are commonly bounded by triangular brittle fractures that fragment the salt surface and efficiently generate a breccia or gouge. Experiments with an abundance of gouge at the sliding interface have reduced shear resistance compared to bare surfaces and we show that friction is reduced with cumulative slip as gouge accumulates from initially bare surfaces. The relative importance of these deformation mechanisms may influence gouge production rate, fault surface roughness evolution, as well as mechanical behavior. Finally, our experimental results are linked to Nature by comparing the experimental surfaces to an actual fault surface, whose striated morphology has been characterized to centimeter resolution using a laser scanner. It is observed that both the stress field and the energy dissipation are heterogeneous at all scales during the maturation of the interface with cumulative slip. Importantly, we show that the formation of striations on fault planes by mechanical abrasion involves transport of gouge products in the fault plane not only along the slip direction, but also perpendicular to it. Ó 2012 Elsevier Ltd. All rights reserved. Keywords: Faulting Fracture Frictional sliding Earthquake mechanics Heat dissipation 1. Introduction Earthquake traces appear as more or less linear trends on the Earth’s surface, however a closer examination reveals that these ruptures in fact display a rich morphological complexity. Similarly, exhumed fault planes have been observed to show striations at all scales (Brown and Scholz, 1985), that can be described using a selfsimilar or self-affine (i.e. fractal) approximation (Power et al., 1987; Renard et al., 2006; Sagy et al., 2007; Bistacchi et al., 2011). Such striations have been used to characterize directions of slip either right after an earthquake or to characterize several slip events on the * Corresponding author. ISTerre, University of Grenoble I, CNRS, BP 53, F-38041 Grenoble, France. E-mail address: francois.renard@ujf-grenoble.fr (F. Renard). same fault (Jackson and McKenzie, 1999; Liu-Zeng et al., 2010). They represent kinematic indicators to infer large scale tectonic processes (Petit, 1987; Marrett and Allmendinger, 1990; Mercier et al., 1992; Yin et al., 1999; Zeilinger et al., 2000) and may be used to calculate paleostress tensors (Angelier, 1979; Fry, 1999). They are also found in other geological systems associated with large scale friction, for example bedrock below an ice-sheet (Eyles and Boyce, 1998) or the imprints left by submarine landslides on the sea floor (Gee et al., 2005). The complex morphology of striated fault surface records a plethora of mechanical processes, such as abrasion, damage and crack interactions through branching, all at work during faulting and rupture propagation both at seismic and low velocity. Since fault roughness contributes to the heterogeneity observed in fault properties, this parameter has been proposed to account for the variability of earthquake source parameters (Venkataraman and Kanamori, 2004; Choy and Kirby, 2004; Schmittbuhl et al., 2006), 0191-8141/$ e see front matter Ó 2012 Elsevier Ltd. All rights reserved. doi:10.1016/j.jsg.2012.03.009 Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 2 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 such as static stress drop (Candela et al., 2011a), and final slip distribution during an earthquake (Candela et al., 2011b). Since faults are non-planar, stress concentrations occur at topographic heights and valleys during slip. Numerical simulations of slip on fractal faults have shown that the stress can reach the yield limit at geometric irregularities, leading to secondary off-fault damage whose amount depends non-linearly on the initial roughness of the fault (Dieterich and Smith, 2009). This leads to non-linear scaling between slip distance and fault length, and importantly, damage is produced all over the fault and not only at its propagating tips (Griffith et al., 2010). As a consequence, off-fault damage represents an efficient way to dissipate plastic energy out of the fault plane. However, part of the energy can also clearly be dissipated along the fault plane, through melting or grain comminution of the gouge material. In the present study we show that an additional dissipation mechanism may be at work: the production of the gouge particles at the origin of surface striation, coupled to grain reworking through a ploughing effect can also dissipate energy along the fault plane (in directions parallel and perpendicular to slip), and not only off-fault. Several mechanisms are responsible for the maturation of a fault and the development of well-developed fault zones, e. g. (Caine et al., 1996): fragmentation of particles into smaller pieces, branching of cracks on the fault plane, wear due to the drag of hard particles in the fault zone, transient stress concentrations at the rupture tip, and damage due to the propagation of seismic waves (i. e. dynamic pulverization, see for example (Dor et al., 2006; Doan and Gary, 2009)). All these mechanisms contribute to the development of the complex morphology of slip surfaces and may control how the frictional resistance evolves with cumulative slip. They also lead to the formation of a fault gouge, observed to have a scale-free particle size distribution (Storti et al., 2003). Such processes have been reproduced experimentally on natural rocks (Wang and Scholz, 1994; Amitrano and Schmittbuhl, 2002), however, it has been difficult to observe in situ both the developing microstructures and the dissipation during deformation. In this study we investigate energy dissipation during frictional sliding on analogue models of geological faults. We focus on the development of roughness on simulated faults, demonstrating that the roughness produced on a mature fault not only involves the formation of striations parallel to slip but also results in a lateral component of the roughness pattern. This indicates that lateral ploughing and fracturing processes in the direction perpendicular to sliding (but still in the fault plane) are also important in accommodating slip. Moreover, roughness development is accompanied by gouge formation, that modifies the shear strength of the interface. 2. Experimental method 2.1. Experimental set-up We have built a shear loading apparatus, where a 3 3 cm2 cleaved monocrystal of halite (NaCl), a surrogate for an active fault rock, was in contact with a rough sandpaper substrate (Struer #80 grit, with an average sand grain size in the range 190e201 microns) or a gouge layer (Fig. 1). We have chosen halite (i.e. salt) because it is both brittle and plastic at room temperature, depending on the intensity and localization of stress. The presence of cleavages in halite partly controls fracture propagation and initial damage production at the onset of sliding. During experiments, the halite slider bore a constant normal load of 12 kg (0.13 MPa normal stress). Then a horizontal sliding velocity of 1.7, 0.9 or 0.6 mm/s was applied to the sandpaper substrate (Table 1) using a step motor and an endless screw connected to the plate that supports the sandpaper. An Omega load cell (LCL-040) connected to the plate allows measurement of the shear force during sliding with a resolution close to 0.25% of the measured force. This apparatus is similar to that used in a previous study where the heat dissipation of a sliding interface was analyzed (Mair et al., 2006). We conducted series of experiments either on bare cleaved or roughened halite surfaces or where a thin layer of granular gouge, infra-red objective dead weight VD step motor HD V sand paper ball bearing load cell stiff aluminum frame NaCl slider 30 mm Fig. 1. Shear loading apparatus to measure heat dissipation during frictional sliding. A halite (NaCl) slider bonded to a stiff aluminum frame and subjected to a constant (dead weight) load is in contact with a coarse sandpaper substrate (or gouge layer). The substrate is pulled at a constant velocity (V) by a stepper motor to generate shear at the slider sandpaper (or gouge) interface. Horizontal (HD) and vertical (VD) displacements are monitored using displacements sensors and shear force is recorded using a load cell. An infrared camera, focused at the interface between the slider and the sand paper (or gouge), records the heat dissipation. Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 Table 1 List of experiments. B: bare surface, Ro: initial rough surface, GB: salt gouge, GS: glass beads gouge. Friction: mss. Hurst exponent in the direction parallel to slip (Hpa) or perpendicular (Hpe). Root-mean square roughness parallel/perpendicular to slip: rmspa, rmspe. Slip velocity (V) and cumulative slip (d). Experiment Type V mm/s mss d mm Hpe Hpa Rmspe mm Rmspa mm cleaved os014 os017 os021a os021b os025 os026 os027 os028 os029 os031 os032 os033 os034 os048 os049 os041 os042 os039 os040 os047 os052 os053 os054 os055 os056 B B B B B B B GB GB GB Ro Ro Ro Ro Ro Ro Ro Ro Ro Ro Ro GS GS GS GS Ro 0 1.7 1.7 0.6 0.6 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 0.9 0.9 0.6 0.6 0.6 1.7 1.7 0.9 0.6 1.7 0 e e e e 1.08 1.09 0.27 0.28 0.28 1.03 1.00 0.98 0.99 0.92 0.93 0.84 0.84 0.90 0.96 0.81 0.61 0.60 0.53 0.59 0.94 0 50 50 50 100 53 50 27 44 35 111 167 213 250 662 709 454 477 410 422 615 831 873 897 913 957 e 0.35 0.44 0.45 0.50 0.12 0.22 0.33 0.26 0.35 e e e e e e e e e e e e e e e 0.44 e 0.15 0.08 0.09 0.09 0.01 0.13 0.03 0.33 0.40 e e e e e e e e e e e e e e e 0.26 0.008 0.212 0.170 0.107 0.147 0.119 0.050 0.035 0.008 0.021 e e e e e e e e e e e e e e e 0.179 0.002 0.045 0.032 0.041 0.057 0.038 0.050 0.015 0.0008 0.022 e e e e e e e e e e e e e e e 0.045 3 a thermistor onto a black body. The resolution is 0.06 K for temperature differences, and the accuracy to absolute temperature is 0.5 K. In the current experiments a field of view of 7 9 mm was imaged. Due to low normal stress, the range of temperature increase was modest (e.g. usually less than 1 ) and the produced heat did not modify the frictional properties of the interface during sliding. Therefore, infra-red imaging is used here for identifying plastic deformation (Mair et al., 2006). 2.3. Topography measurements After the friction experiments were conducted, optical images of the interface were taken with a binocular microscope. The topography of several samples was measured using white light interferometer micrography (Wyko 2000 Surface Profiler from Veeco). This involves a microscope using a broad-band white light source coupled to a Michelson interferometer. A reference arm creates interference fringes with maximum intensity at equal optical path lengths of the imaging beam and reference beam. By vertical movement of the sample and simultaneous image capturing, the interference intensity envelope and thereby the relative height of the imaged surface at each pixel is determined with a vertical resolution of 3 nm. The horizontal resolution depends on the lens used and with the highest magnification it is at the diffraction limit of white light, of about 0.5 mm. In the present study, a horizontal resolution of 1.57 mm was selected. The height fields were processed to remove the planar tilt of the surface. 3. Results initially w1 mm thick, separated the interfaces (Table 1). The hardness of the gouge grains was either equal to (sieved halite grains, 180e250 microns) or greater than (SiO2 sand grains Aldrich 50 þ 70 mesh, 211e297 microns) the slider hardness. We monitored horizontal and vertical displacements using linear variable displacement transducers (LVDT) with sub-micron resolution and measured shear resistance to imposed sliding with the load cell. These parameters were recorded at 2 kHz and tests were conducted at ambient room temperature and humidity. In the experiments with initially bare surfaces, gouge products were produced during slip and a gouge layer several grains thick developed. For gouge experiments, even if the system was not confined laterally, a continuous layer of grains remained trapped at the interface (negligible amounts of gouge escaped from the sides of the slider). Finally, we have presented experiments where a single indenter (glass bead, 1 mm diameter) was dragged onto a cleaved halite surface, to produce a single groove, with associated damage. Two experiments of this kind were performed, varying the orientation of the produced groove with respect to the main cleavage directions of the salt crystal (Sarwar, 2008). 2.2. Infra-red light imaging of the interface Since halite is transparent to infra-red light, we can monitor heat emission at the sliding surface by looking through the slider using a high resolution infra-red camera located above the halite sample and focused at the slider interface undergoing shear (Fig. 1). We used a Phoenix infra-red camera with a 12-bit InSb matrix sensor that captures infra-red emissions in the 3e5 mm range. The result is a time-lapse movie of the infra-red radiations emitted during frictional sliding, with 256 320 pixels images at a pixel resolution of 28.7 micron and a capturing rate of 50 frames per second. The infra-red signal is transformed into approximate temperature values by calibration using a Pelletier element and 3.1. Friction, infra-red emission, and damage The typical mechanical behavior and infra-red emission observed during sliding experiments is presented in Fig. 2. Friction (shear force/normal load) increases initially during the loading phase before reaching a peak friction at the onset of sliding. Then friction slightly decreases and fluctuates about a relatively constant steady-state value. At the onset of sliding a small dilatant behavior is observed, usually less than 100 mm. The different experimental conditions e bare surface and sand gouge e show distinct behaviors, the friction level being systematically higher for bare surface experiments than those containing a layer of gouge material. Average temperature change is calculated for a 7 9 mm area on sliding surface using the infra-red emissions. Both types of experiments exhibit a moderate increase in average temperature during sliding (Fig. 2b), always smaller than 1 K. We can therefore neglect the effect of temperature increase on any change in shear resistance during sliding. The average temperature rise in the bare surface experiments increases monotonically with slip, whereas the gouge experiments show an initial increase followed by a leveling off or saturation after some characteristic time. This leveling off is thought (Mair et al., 2006) to reflect a plateau where heat production and thermal diffusion through the gouge are equivalent. Thermal diffusion through bare surfaces is likely to be less and hence the heating term dominates throughout. Close up thermal images (Fig. 3) highlight the heterogeneity of the thermal signal associated with the development of a deformation groove in the halite slider. The signal is dominated by a ‘fat head’ region, where the highest infra-red emission is concentrated, and a ‘narrow tail’ where heat emission is elevated compared to the undeformed slider but less than at the head. The width of the ‘head’, where most of the plastic strain is located, is 3e4 times larger than for the ‘tail’. Each head corresponds to an asperity of the sandpaper that is dragged along the salt surface, damages it, and produces a striation. The fact that infra-red emission extends 34 Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 4 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 shear load / normal load a secondary fractures, 3e4 times the groove diameter, develops (Fig. 5aeb); whereas the scratch is oriented in the direction of the cleavages, the width of the damage zone is 1e2 times the groove diameter (Fig. 5c). 1.5 bare surface gouge 1 3.2. Topography The topography of a freshly cleaved surface and several striated surfaces that had undergone various amount of slip were measured using white light interferometry (Table 1). The data obtained, for each sample, is a 2D topographic height field of the roughness over a selected area, from which 1D roughness profiles were extracted (Fig. 6). For each surface, 1D profiles were characterized by their root-mean-square roughness xrms defined as: 0.5 0 0 10 20 30 time (s) temperature increase (°C) b xrms 0.5 bare surface gouge 0.4 0.3 0.2 0.1 0 0 10 20 30 time (s) Fig. 2. Time evolution of sliding friction (a) and heat emission (b) during experiments for imposed velocity V ¼ 1.7 mm/s. Data are presented for bare surface experiments, where the halite slider directly contacts sand paper, and sand gouge experiments where the slider contacts the sandpaper via a thin (initially 1 mm thick) layer of sand. Heat emission is presented as average temperature change occurring on a 7 9 mm area imaged by the infra-red camera and located at the center of the sample sliding surface. times the width of the produced striae indicates that dissipation processes (wear, grain fragmentation, fracturing) occur in a volume much larger than the size of the ploughing asperity. This is verified on optical images of a slip surface (Fig. 4), where striae and gouge products are clearly visible. The grooves have developed through a ‘ploughing’ effect of the sandpaper asperities. Interestingly, on the sides of many grooves we observe oblique fractures (labeled F in Fig. 4aeb) that have damaged the surface, tearing out fragments that become part of the gouge. Each sandpaper asperity thus inflicts damage both at the actual contact with the salt, but also in its vicinity. The particles produced are then presumably dragged and accumulate at the bottom of each groove (Fig. 4c) or are evacuated sideways. A sketch of this process (Fig. 4d) shows that volume of the whole damage area is 3e4 times larger than the diameter of the ploughing asperities. To better image the damage around a single striae, we have also performed experiments where a single asperity (glass bead, 1 mm diameter) was dragged onto a fresh cleaved halite surface, producing a single scratch (Sarwar, 2008). The resulting damage (Fig. 5) shows the development of secondary fractures that propagate in a volume around the main scratch. Depending on the orientation of the scratch with respect to the cleavage directions of the salt slider, the damage is more or less pronounced: if the scratch is oriented at 45 to the main cleavage directions, a wide zone of sffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi ðxi xÞ2 ¼ n (1) where xi is the height at the pixel i, and x is the average height of the profile. When the average height of the profile is set to zero, xrms is equal to the standard deviation, and quantifies the importance of height variations in the profile. To calculate xrms , several 1D parallel profiles were extracted from the 2D surface. For each profile, the mean trend was removed, before xrms was calculated according to Eq. (1). Then, the xrms of all parallel profiles were averaged (see Table 1). The freshly cleaved halite surface is almost flat, with xrms less than 10 mm (Fig. 6a). Striated surfaces exhibit larger xrms, between 0.03 and 0.2 mm. Moreover, as striated surfaces are strongly anisotropic, xrms is two to five times larger perpendicular to the direction of slip, than parallel to it (see Fig. 6b, c). During all experiments, the vertical displacement measured was small, in the range of the depth of the grooves produced. For experiments with gouge, a slight compaction was observed, on the order of 1e2 gouge grain diameters. This is interpreted to be due to the evolution of the gouge towards a more compacted state, as gouge loss on the sides of the slider was found to be negligible. Importantly, the formation of this roughness involves several processes: formation of grooves along direction of slip, fracturing on the sides of these grooves, and transport of grains from the grooves to their sides in a snow-plough like manner (Fig. 7). We have also characterized the scaling properties of the rough surfaces. For this, we have extracted several hundreds of profiles in the direction of slip and perpendicular to it to analyze the statistical properties of the slider surface. A Fourier power spectrum method, which has been shown to be robust and reliable, was used to characterize scaling properties of rough surfaces and search for self-affine properties, that are often observed on natural faults (Renard et al., 2006; Sagy et al., 2007; Candela et al., 2009; Bistacchi et al., 2011). A 2-D rough profile is self-affine if it remains statistiH cally invariant under the scaling transformation dx/ldx; dz/l dz, where x is the coordinate along the 2-D profile, z the roughness amplitude and H the so-called Hurst exponent. In such a system, the roughness amplitude depends on the magnification l, following a power law relationship. If the power law scaling exponent H lies in the range 0 < H < 1, different magnification factors will be needed in the directions parallel and perpendicular to the profile for a small portion of the profile to appear statistically similar to the entire profile. Then, the profile is called self-affine. If H ¼ 1, the profile is called self-similar. For all white light interferometry data of rough slip surfaces, the topography shows a self-affine geometry. The different slip surfaces analyzed cover approximately 2 decades of length scales and show a scaling relationship with a Hurst exponent H that varies with cumulative slip (Fig. 9). H is close to 0.5 for profiles perpendicular to the slip direction and slightly smaller along slip (see Table 1). Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 5 slip temperature (°C) 2 mm 0.4 0.3 0.2 1 mm left-over groove active damage zone temperature (°C) 0.1 0.35 0.3 0.25 active asperity Fig. 3. (Top) Infra-red imaging of heat spots localized at the tip of grooves at the frictional interface of the slider. The striations produced correspond to sand paper asperities that induce permanent damage on the slider surface. The temperature increase due to friction is less than 0.5 C. The slip direction is indicated by the arrow. (Bottom) A zoom on the active damage zone, which concentrates most of the heat dissipation, shows it is 3e4 times wider than the produced striation. The size of the sand paper asperity is indicated. 3.3. Effects of cumulative slip The effects of cumulative slip are presented in terms of mean steady state friction and root-mean square roughness in Fig. 8. Each point on the graph is a single experiment. In some cases an individual halite sample was used for a series of experiments, therefore total cumulative slips of 1000 mm were possible on a single sample although the slip of an individual experiment was w50 mm. The data sets are split into three groups: bare surface; sand gouge; and halite gouge. Mean steady state friction level (calculated for the portion of the friction curve considered to be steady state, e.g. Fig. 2) is highest, w0.8e1.0, for bare rough samples and bare cleaved surfaces. Experiments having a layer of sand gouge result in intermediate levels of friction w 0.6, whereas those with halite gouge yielded lower friction w 0.4. A slight mechanical weakening, characterized by a reduction in steady state friction coefficient, is observed with increasing amounts of slip for bare rough surfaces. Interestingly, the Hurst exponent evolves with slip from lower values to a more or less constant value reached after around 50 mm cumulated slip. Here, the initial increase of Hurst exponent (Fig. 9) is due to the fact that the slip starts on an initial bare surface with H ¼ 0 and the roughness evolves after a small cumulative slip only towards a more or less constant value. For an initially bare surface, the amplitude of the roughness (calculated as the root-mean-square) increases during the first w50 mm of slip, then appears to stabilize at larger slips (Fig. 8b) at a value that stays constant within the error bar of measurements. For this value of slip, all the initially flat surface is covered with striations. The root-mean-square roughness values for a 2D surface and profiles parallel and perpendicular to slip direction are compared. The roughness of a profile measured perpendicular to slip is highest, the profile parallel to slip direction is lowest and perhaps unsurprisingly, the roughness of the 2D surface falls inbetween. In the experiments, presented in Fig. 9, the Hurst exponent, calculated in the direction perpendicular to slip is always larger than for the slip direction. This is also what is generally observed on natural faults, where H is smaller in the direction of slip (e.g. (Renard et al., 2006)) than perpendicular to it. A difference is a smaller Hurst exponent (0.3e0.4) in the experiments, compared to natural fractures (0.6e0.8). These experimental data of slip surface anisotropy confirm and extend previous studies showing the self-affine anisotropy properties of fault surfaces (Power Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 6 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 Fig. 4. Optical images of the slip surface of sample OS017 showing the main characteristics of the grooves (aeb). On the sides of striae, damage is produced in the form of secondary fractures (F) that wear the slip surface. c) At the bottom of each groove, particles of halite having a grain size in the range 5e20 microns are observed. These particles are interpreted as the gouge produced. d) Sketch showing active asperities at the extremity of grooves. Most of these grooves show a well-defined striae and secondary fractures, the whole volume of the damage zone being 3e4 times larger than the asperity diameter. Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 7 Fig. 5. Optical images of a single scratch on cleaved halite surface. A bead of silica was dragged on the surface, creating a groove and secondary fractures (labeled F). The amount of damage depends on the crystallographic orientation. aeb) Groove along the main crystallographic (100) direction, with fractures forming at 45 , along cleavage directions. c) Groove along the cleavage direction (at 45 from Fig. a), showing much less secondary fractures (Sarwar, 2008). et al., 1987; Renard et al., 2006; Sagy et al., 2007; Bistacchi et al., 2011). 4. Discussion 4.1. Striations on natural faults Fault roughness development represents an important issue in terms of how stresses are distributed, concentrated, and dissipated during the seismic cycle (Power et al., 1988). Fault roughness, which can be measured accurately using high resolution profilometers (Power et al., 1987) or laser distance meters (Power et al., 1987; Renard et al., 2006; Sagy et al., 2007; Candela et al., 2009; Bistacchi et al., 2011) exhibit scale invariance properties over several decades of spatial scales. The rough interface can be interpreted either as a limit between the core of the fault zone that contains a gouge and fault rocks (Caine et al., 1996) and the wider damage zone, or between two adjoining fault blocks. The latter interpretation applies to those cases where the thickness of the fault core is much smaller than the length scale at which the fault is characterized. Several mechanisms have been proposed to explain the formation of gouge particles during sliding, such as dynamic pulverization (Reches and Dewers, 1987; Doan and Gary, 2009), fault branching (Power et al., 1988), grain fragmentation (e.g. Abe and Mair (2005) and references therein), or asperity ploughing (see Fig. 10). The latter mechanism can be observed on natural faults when a hard object is dragged along the fault plane leaving a permanent damage imprint. This is observed, for Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 Fig. 6. White light interferometry technique is demonstrated by a surface topography image (left) and linear topography transects (right) in two perpendicular directions (X along slip, Y perpendicular to slip). The black arrow indicates the direction of sliding. (a) Transects on a flat portion of the interface without damage (i.e. fresh surface). (b) Transects at the bottom of a groove. (c) Transects on the side of a groove where a marginal ridge is observed. Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 9 Fig. 7. Topography images, obtained using white light interferometry, highlight different features developed after increasing amounts of cumulative slip. (aee) Bare salt surface over sandpaper, with the initial cleaved surface indicated (C). The formation of striations sub-parallel to the slip direction occurred by fragmentation of the salt along grooves (G), fractures (F), and plastic deformation of the salt that was pushed on the sides of the grooves, producing marginal ridges (R). (f) Topography of an interface where a gouge was initially present during shearing, demonstrating the lower level of damage production. example, on the Vuache Fault (French Alps), where high resolution topography measurements have been acquired using laser surveying (Renard et al., 2006). On this left-lateral slip fault in limestone, the direction of slip is indicated by striations at all scales that form a self-affine morphology of the slip surface. In Fig. 10 the topography of a 11 8 m2 area of the fault, showing meter wide striations is displayed. Making the analogy with our experiments, we infer that some of these striations correspond to grooves produced by the ploughing effect of an asperity that was harder than the material lying at the sliding surface. In our experiments we observed that the ploughing effect created damage not only inside the groove, but also in a region 3e4 times wider than the groove itself. Moreover, the wear products are pushed not only in the direction of slip, but also sideways (i.e. lateral to slip) hence potentially amplifying the generation of roughness in that direction by forming marginal ridges. 4.2. Faulting processes in laboratory experiments To reproduce slip and faulting in laboratory experiments, one can use conditions of stress and temperature similar to those along a fault plane at depth and study the quasi-static growth of microcracks, leading to fracturing (e.g. Lockner et al. (1991). To study dynamic fracture, one can visualize 2D ruptures using photoelasticity (Xia et al., 2004; Nielsen et al., 2010) or 3D ruptures using ultrafast ultrasonic imaging in analogue materials (Latour et al., 2011). However, in such experiments, direct imaging of damage processes in the fault plane itself are generally not possible. In the present study, damage processes along the slip surface can be visualized and energy dissipation measured through the use of infra-red emission. This provides additional information on the localization of fracturing and plastic deformation processes that may operate in natural systems. Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 10 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 H, perpendicular to slip H, along slip 0.9 0.8 0.7 1.2 Hurst exponent steady−state friction coefficient a 1 0.8 0.6 0.5 0.4 0.3 0.6 0.2 0.4 0.1 0.2 0 0 0 0 500 1000 cumulative slip (mm) 250 200 150 100 50 0 0 500 100 200 300 400 500 600 700 cumulated slip (mm) 800 900 1000 Fig. 9. The Hurst exponent (see text) is calculated and plotted parallel and perpendicular to slip as a function of cumulative slip. 2D surface 1D perpendicular to slip 1D along slip b rms of surface roughness (µm) 1 Bare cleaved surface Bare rough surface Rough surface + salt gouge Cleaved surface + salt gouge Rough surface + sand gouge 1000 cumulative slip (mm) Fig. 8. a) Steady-state friction of the sliding interface is plotted as a function of increasing cumulative slip for different initial conditions. b) Root-mean square of the roughness, for initial flat slider, as a function of cumulative slip. The data are presented in the direction of slip, perpendicular to it, and for the whole 2D surface. These data show that the roughness increases from zero (flat surface) to a value that remains more or less constant after a small amount of cumulative slip (less than 100 mm). The experimental conditions we apply are clearly far from conditions at depth in a fault, however the experiments do share common properties with faults: the presence of a material that can behave in both a brittle and ductile manner, the formation of gouge particles, the presence of strong asperities that can pin the interface during sliding, and a slight dilatancy at the onset of sliding. Such dilatancy is measured experimentally when faulting rocks are deformed under upper crust conditions (see Scholz (2002), Figure 1.24) and slowly vanishes when reaching the ductile regime. Finally, our experiments are dry, whereas fluids are known to play an important role during slip in natural faults, due to variations of pore pressure or chemical effects. The experimental data indicate that the roughness of an initially flat interface develops rapidly with slip. Both root-mean-square roughness and Hurst exponent reach a more or less constant value after less than 50 mm of cumulative slip, which corresponds to the distance necessary to cover the initial flat surface with striations. In the experiments, the initial surfaces are flat, and hence somewhat like natural joints in rocks. The amplitude of striations reach a steady state that we interpret as imposed by the constant grain size of the sand paper or the initial sand gouge. In the experiments the friction coefficient continues to decrease (Fig. 8a) even if the surface roughness does not evolve much. A possible explanation would be related to the production of gouge particles, whose rolling effect could decrease the resistance to shear (Oda et al., 1982). Another explanation is that the striations that form fit the sand paper asperities, such that erosion of the sand grains becomes less efficient. The evolution of fault roughness under the effect of asperity ploughing has two consequences on damage, as evidenced by the experimental results. Firstly, the damage zone around the asperity is much larger than the produced groove, as demonstrated by the infra-red emissions (Fig. 3) and we see the formation of fractures that grow sideways, i.e. oblique to slip (Figs. 4 and 7). In the experiments, the orientation of these fractures is partly controlled by the crystallographic orientation (i.e. the fractures labeled on Fig. 4aeb corresponds to directions of cleavage) of the salt slider and by the strong elastic contrast between the sandpaper and the slider. In Nature, these fractures are controlled both by variations in local stress orientation and by the presence of heterogeneities in material properties. There too, a strong elastic contrast may exist between damaged fault rocks and a strong asperity dragged into the fault zone. Secondly, the gouge material produced is pushed on each side of the groove, forming a marginal ridge. This indicates that, during wear, gouge material is transported not only along the slip direction, but also perpendicularly. The mechanics of scratching indenters is well-studied in the engineering community for now more than 40 years (Bowden and Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009 F. Renard et al. / Journal of Structural Geology xxx (2012) 1e12 11 Fig. 10. Topographic images of the Vuache fault surface (from the French Alps) are presented. The fault plane has been measured using a 3D laser scanner to obtain the Digital Elevation Model of the fault roughness shown. This fault shows clear striations at all scales. Some of these grooves (G) appear to have been created by a ploughing effect of an asperity that was dragged into the fault zone during slip. Tabor, 1966; Gee, 2001), and has been, for example, applied to machine drill bits (Beste et al., 2004). For example, scratch tests are performed on various materials to measure the erosion, friction and wear produced. Several experimental results on various materials have shown the presence of positive ridges developing on the sides of a striation (Li et al., 1996). The presence of ridges is observed and numerically simulated in ductile materials (Barge et al., 2003), whereas secondary fractures also develop in more brittle materials such as soda-lime glass (Li et al., 1998), ceramics (Lee et al., 2000), or minerals (Broz et al., 2006). The formation of these cracks was successfully modeled using finite elements (Holmberg et al., 2003) for scratches forming on steel coated with TiN ceramic and showing that tensile stress is generated around the contact, allowing for fracturing. This secondary damage therefore apparently plays an important role in dissipating strain within, but also outside of the main zone of wear production. Such structures appear to be analogous to those we observe in our halite experiments. 5. Conclusions Our experiments demonstrate that wear production and plastic dissipation (monitored by the infra-red emission) along a rough sliding interface is highly heterogeneous when strong asperities produce striations on slip surfaces. Heterogeneities, both structural features and stress concentrators, can strongly damage the fault surface through various deformation processes (gouge production, asperity ploughing, fracturing), that represent a significant contribution to the overall friction coefficient. Importantly, the fault interface is not only damaged parallel to slip direction, but also perpendicularly to slip due to fracturing and ploughing effects that transport material at various angles to the sliding direction. With cumulative slip, these combined damage effects appear to result in a gradual decrease in the friction coefficient due to the development of striations themselves and the accumulation of gouge particles that dissipate strain by a rolling effect. Acknowledgments This work was supported by a Center of Excellence grant from the Norwegian Research Council to PGP (Physics of Geological Processes) at the University of Oslo and the grant ANR-09-JCJC0011-01 from Agence Nationale de la Recherche. The authors acknowledge the contribution of Munib Sarwar and Stephane Santucci, whose single indentor scratch experiments (presented in Fig. 5) along with those conducted by the authors, gave additional insights into the roughness evolution we present in this paper. Appendix A. 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Please cite this article in press as: Renard, F., et al., Surface roughness evolution on experimentally simulated faults, Journal of Structural Geology (2012), doi:10.1016/j.jsg.2012.03.009