Burning of high T c bridges M. E. Gaevski,a) T. H. Johansen, Yu. Galperin,a) and H. Bratsberg Department of Physics, University of Oslo, P. O. Box 1048 Blindern, N 0316 Oslo, Norway A. V. Bobyl, D. V. Shantsev, and S. F. Karmanenko State Technical University, 195251 St. Petersburg, Russia ~Received 4 February 1997; accepted for publication 24 September 1997! Burning of superconducting thin film bridges by large transport currents ~up to densities of 2 3107 A/cm2 ) is investigated by magneto-optical imaging of flux distribution and low-temperature scanning electron microscopy providing T c maps. It is shown that the destruction is preceded by significant penetration of magnetic field inside a weak-pinning region. In bridges containing extended defects magneto-optic investigation is sufficient to locate the incipient burning region. In high-quality bridges free from such defects only a combination of the two techniques will allow prediction of the place of fatal destruction. © 1997 American Institute of Physics. @S0003-6951~97!01847-0# In order to optimize the performance of devices made from high T c superconductors ~HTSs! it is important to have space-resolved information about the material and its response properties. Today, several techniques have been developed for this purpose. One of them is low-temperature scanning electron microscopy ~LTSEM!,1 which monitors the transition into the normal state under the local heating by an electronic beam. This method allows one to determine the local values of the critical temperature T c . Another powerful technique—magneto-optical ~MO! imaging ~see e.g., Ref. 2 and references therein!—enables one to monitor the distribution of magnetic field perpendicular to a plane adjacent to the HTS surface. In this work we combine these two nondestructive techniques to investigate the performance of HTS bridges carrying large transport currents. When an HTS device carries a transport current, I T , approaching the critical value, I c , one expects that local variations in the material become increasingly important and eventually determines where the device is destroyed. The usual source of destruction is thermally induced motion of magnetic flux which leads to further heat dissipation and local increase in the temperature. This, in turn, causes reduced flux pinning locally, and a process having the character of an avalanche3 leads to strong overheating or burning. While HTS films carrying small transport currents have been studied previously by the MO method,4–7 there exists so far no such study focusing on the behavior when I T ;I c . In this work we show that MO images of self-fields from I T correlated with T c maps obtained by the LTSEM technique8 can be used to predict the location of burning in HTS films. Superconducting YBa2 Cu3 O72 d ~YBCO! films were prepared by dc magnetron sputtering of a ceramic stoichiometric target. The films were grown on ~100! LaAlO3 substrates at a rate of 2 nm/min at T5680 K in a gaseous mixture of Ar and oxygen. Subsequent heat treatment at T 5500 K for 20 min in pure oxygen at a pressure of 1 atm and cooling for 1 h resulted in a high oxygen saturation of the YBCO lattice.9 The film thickness was 300 nm. X-ray a! Also with A. F. Ioffe Physico-Technical Institute, 194021 St. Petersburg, Russia. Appl. Phys. Lett. 71 (21), 24 November 1997 analysis confirmed good quality and a ~100! orientation of the films. According to scanning electron microscope ~SEM! studies, the films contained no inclusions or outgrowths >1 m m normal to the surface. Micro-bridges 1003500 ( m m!2 were formed by a standard photolithographic procedure. To optimize conditions for MO studies we fabricated samples with all contact plates placed on the same side of the structure at a sufficient distance from the bridge. The contact pads were covered by Ag, and Au wires were attached by a thermal compression. Two typical bridges were studied. One of them ~see Fig. 1! referred to as ‘‘good,’’ had a critical current density ;106 A/cm2 at 77 K as determined by current-voltage (I-V) measurements. The other sample, referred to as ‘‘bad’’ had critical current ;53104 A/cm2 at 77 K. As shown below, the burning process for the two samples showed distinctly different features. MO images of the ‘‘good’’ sample at 15 K are shown in Figs. 1~b!–1~f!. Here bright areas correspond to large absolute values of the perpendicular magnetic field. As an MO indicator we use Bi-doped YIG film with in-plane anisotropy, and an optical cryostat system described in Ref. 10. In the current-carrying states with I T 53 A and 6 A, Figs. 1~b! and 1~d!, respectively, the field is seen to concentrate near the edges. Note that the MO indicator does not discriminate between the ‘‘up’’ and ‘‘down’’ directions of the perpendicular field when using the present crossed polarizer setting on the microscope, and hence the images are essentially symmetric about the center line of the bridge. ~By changing the polarizer settings the two directions are easily distinguished.! The increased intensity near the corners is due to bending of the current flowlines as they are governed by the bridge geometry.11 The uniform dark appearance of the inner part of the bridge demonstrates a very good homogeneous screening. In the remanent state after switching off the current, Fig. 1~c!, one can clearly observe two pairs of bright bands near the edges separated by the dark shielded area. The inner two bands show the trapped flux, which has opposite direction in the two bands. The outer two bands show re-magnetized regions, i.e., the return field of the trapped flux partly penetrat- 0003-6951/97/71(21)/3147/3/$10.00 © 1997 American Institute of Physics 3147 FIG. 1. ~a! Sketch of the bridge geometry. ~b!–~f! MO images of the ‘‘good’’ bridge @scale bar in ~b! is 100 m m long#. ~b!,~d! The self-field distributions for currents I T 53 and 6 A, respectively. ~c!,~e! The remanent state after switching off the 3 and 6 A currents, respectively. ~f! Destroyed bridge in an external field of 5 mT. In this frame the the bright areas near the contact pads are due to the magnetic prehistory of the sample, and thus irrelevant for the illustration of the burned region, which appears as a bright channel near the center. ~Right! T c map of the ‘‘good’’ sample: ~black! 90 K, ~white! 92 K. ing into the film. The flux bands therefore represent an oscillating flux profile across the bridge where the field changes sign three times, as predicted by theory.12 A more detailed comparison is presented in a forthcoming paper. Increasing the current above 6 A caused burning, i.e., J c 523107 A/cm2 at 15 K, leaving the bridge in the remanent state shown in Fig. 1~e!. More than 50% of the bridge appears dark because the trapped flux escaped this region during the heating. In order to localize where fatal destruction took place an external field was applied to the sample. Figure 1~f! shows such an MO image with an applied field of 5 mT. The destroyed region is the bright channel crossing the bridge. From the details of the pre-burning MO images the bridge had two regions near the edge, marked by arrows, showing enhanced flux penetration in the current carrying state. Other irregularities can also be seen in the flux front, but these are of less magnitude. Of the two major defects the one associated with region 1 is the more pronounced, and should therefore be the most probable candidate to initiate the burning. Surprisingly, the bridge ‘‘chooses’’ instead region 2, as evident from Fig. 1~f!. Note also that none of the defects at any pre-burning stage extends across a substantial part of the bridge even when J T .J c , as in Fig. 1~d!. It is therefore clear that MO imaging alone is not capable of pre3148 Appl. Phys. Lett., Vol. 71, No. 21, 24 November 1997 dicting the burning location in a bridge which is free from extended defects. This situation is quite different from the case studied in Ref. 5, and also for the ‘‘bad’’ sample discussed below, where pronounced extended defects dominated the behavior. Using the LTSEM technique, described in detail elsewhere,8 we made prior to the MO investigation, a map of the local T c for each bridge. Such a T c map of the ‘‘good’’ bridge is shown in Fig. 1~right! where the dark regions correspond to reduced values of T c . Here one clearly recognizes regions 1 and 2 from the MO images as also being areas with relatively low T c . If one assumes that regions with low T c also have reduced J c it is evident that region 2 is the more probable candidate as the area of low T c here percolates across the entire bridge. Indeed, the channel of destruction seen in the MO image strongly correlates with the percolating path of low T c . One can also notice that a low T c path exists near the upper boundary of the bridge. The reason why we believe that this region is not fatal is as follows. First, the MO images show no distinct features in this part of the bridge, indicating that the region has an enhanced concentration of pinning centers which prevents reduction in J c in spite of low T c . Second, the central part of the bridge is likely to be in the worst situation with respect to thermal stability. Thus Gaevski et al. FIG. 2. ~a!–~e! MO images of the ‘‘bad’’ sample. ~a! Remanent state obtained by switching off a field of 150 mT. ~b!–~d! Increase of transport current up to 3 A. ~e! The destroyed bridge in an external field of 5 mT. The scale bar is 100 m m long. ~f! SEM image of the area marked by white rectangle on ~e!. one expects that the device will burn at some ‘‘weak region’’ close to the central part. The MO images of the ‘‘bad’’ bridge are shown in Figs. 2~a!–2~e!. In 2~a! one sees an image of the remanent state after applying a magnetic field of 150 mT which caused full penetration. In this case, the pair of dark lines separate the uni-directed trapped flux in the center from the reversely directed return flux. Adding now a transport current, the field distribution becomes asymmetric, as shown in 2~b!–2~d!. According to Ref. 12 an additional line with B z 50, i.e., with dark appearance, should exist within an interval of I T values. Figure 2~b! gives clear evidence for this prediction of the theory, not previously verified for a state with such a combined magnetic prehistory. The main observation here, however, is that in this sample an extended defect is visible in the MO images. The flux pattern in Fig. 2~c! is severely distorted near a ‘‘weak region’’ where the field penetrates more than half of the bridge width. Note however that, at large I T close to the critical value as in 2~d!, the field distribution becomes more symmetric. We believe that in this regime the transport current drives the cross section containing the ‘‘weak region’’ into a resistive state with resistivity of the same order of magnitude as in the nondefected part. Finally, at I5I c 53 A, the bridge burns out. From 2~e! showing how the destroyed Appl. Phys. Lett., Vol. 71, No. 21, 24 November 1997 bridge shields an external field it is clear that the burning took place in the ‘‘weak region.’’ The micro-photograph of Fig. 2~f! shows that the damaged part of the film consists of a narrow straight line, not directly across the bridge, but instead forming a certain angle. The ‘‘bad’’ bridge was evidently destroyed along a linear defect present in the film. We conclude therefore that MO imaging can be used to locate extended defects which become fatal for HTS bridges carrying large transport currents. In films showing no extended defects, like the ‘‘good’’ sample in our study, the situation is more complex. From MO imaging one can find several candidates for the location of burning, and hence additional diagnostics is required. The method of LTSEM mapping of T c provides another set of candidates, which in general do not completely overlap with the ones from MO images. We have shown that bands of low T c extending across the bridge, and also overlapping with edge defects seen by MO imaging, are the actual place of fatal destruction when I T >I c . The burning is usually seen to take place near the central part of the bridge. This indicates that in order to optimize the performance of superconducting bridge devices it is important to design them in a convex shape in order to increase the heat transfer. In spite of the considerable field amplification near the sharp corners, see e.g., Fig. 1~d!, we found that burning never takes place here. Thus, a design with rounded corners will probably not improve the strength of the bridge with respect to burning. The authors thank The Norwegian Research Council and the Russian State Program on HTSC ~Grant No. 94048! for financial support. 1 R. P. Huebener, in Advances in Electronics and Electron Physics, edited by P. W. Hawkes ~Academic, New York, 1988!. Vol. 70, p. 1. 2 M. R. Koblischka and R. J. 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