LIBRARY COPY HYDnRAliC GRADIEf AND OP ON A PERFORAD PLM P$ISUHE by Robert T. Hucks, Jr. S.B., Lehigh University (1950) and t William P. Thomsonm S.B*, Purdue University _ (1948) Submitted in Partial Fulfillment of the Requirementsfor the Degree of MA$2EROF SCIENCE at the MASSACHUSS INSTT 1951 Signatures of Authors a!.aa a . ., O * a. e a a* * *$S a, * J Signature of Supervising Professor .. o $ a. * OF TECNOLOGY ... rW.- .. . . . -_- - - - - * . ... . .. lw. -ar a- ...... o e * .. Signature of Chairman, Department Committee on Graduate Studies ....... . .a. . ...e es ........ * a * I 52M-126 HYDRAULIm D=If ANDPRESUE DROP ON A PERAM PLI Robert T. Hucks, r Willian P. homson By: Submitted for the degree of Master of Science in the Department of hemi cal Engineering at the Massachusetts Institute of Technology on August 24, 1951, Hydraulic gradient and pressure drop on a perforated plate were studied using a 120" x 1 A 60" : 10" section of the plate was perforated with 1/8" holes on 1/4" equilateral liquid 1/2" test section of 14 gauge sheet steel, triangular flow. The inlet enters, the long dimension being parallel to and outletcalming sections were each 24" long, All data were taken using a air-water system. The superficial air velocity was varied from 57 to 7 ft per seej; water rate was varied from 0 to 24 gpm/ift; and weir height was varied from 1/4 to 1". Hydraulic gradient data were correlated using a anntring-type friction expression: } ft Vf2 N 2g rh Whereft was correlated against Re': Re3 rh Vf /f 52M-l 26 The pressure drop data were correlated using the following expression for the drop through the perforations: ho CVp2 The total plate pressure drop was found to consist of this drop, a loss due to suface tension effects, and a loss equivalent to the hydrostatic head of the liquid above the perforationsa Nethods were developed for predicting the hydraulic gradient and pressure drop on a perforated plate operating in the range of variables studied. Thesis Supervisor: E. R. Gilliland Title Professor of ChemicalEngineering . Chemical Engineering Department Massachusetts Institute of Technology Cambridge 39, Massachusetts August 23, 1951 Professor ;oseph S. Newell Secretary of the Faculty Massachusetts Institute of Technology Cambridge 39, Massachusetts Dear Sir: In accordancewith the regulations of the Faculty, this thesis, entitled "Hydraulic Gradient and Pressure Drop on a Perforated Plate," is hereby submitted in partial fulfillment of the requirements for the degree of Master of Science in Chemical Engineering. Respectfully submitted. Robert T. Hucks, Jr. William P. Thomson A -EWIEDg The authors wish to express their appreciation to Professor E. .his R. Gilliland for manyhelpful suggestions in supervisingthis thesis. Credit is also due to Mr. H. H. Engineering Shop under the direction their cooperation, arter and the Chemical of Mr H 0. Chasen for TABIZ OF CONTENTS Page I Sumary o. . . .. . . II Introduction . . *r 1 . 4 . . . .. A. Object of the Investigation. . Limitations of the Investigation C. Ter inology . . . . * . ... B, . Or I . . . .. D, Previous Wkork... c..... .. a... III 5 7 8 Procedure A. E rerimental Progra, a B. Description Of aratus . * O . O a . a 16 . . Experimental Procedure a s . . . . . a . D. Method of Correlation 1. Hydraulic Gradient 2 Pressressure Drop IV Results 3 o. 19 21 .. . .*o .o 15 .. £ 8 0 0 a a a a * * a, a a a a a * a * a a a a a1 a 0 21 22 0 23 V Discussionof Results A. HYdraulic Gradient Correlation B. CI. Pressure VI VII * * ,e Calculation Procedure for Predicti D. . rop Correlation . * 0 0 36 a $ * $ 0 37 0 08 * * a.. **,*a draulic Gradient . * . . . .. a 0 43 Pressure Drop Calculation Procedure Conclusions Recommendations , *o . * . a .. * * o · * * . S *· . . * $ a 45 47 TABX OFF CBNTfNT (Continued) Page VIII Appendix SumnarizedGradient Data . . . a a a a ak a a 8 Su;marized Pressure Drop Data . . 56 . A. Saple Calculations. 49 . . . . 5 * 0 ... 65 B, Plate Leveling Procedure . . . 67 0. Calibration of Flowneters . . 68 D, Nomenclature .o . ,o E. Literature Citations a .. . a . a a a a a s 89 a * a a a a a a* 71 ........ . OF FIGLRMS 2 Figure Page 1 Flow Diar 2 Perforated Plate 3 Hydraulic Gradient 4 Hydraulic Gradient vs. Air Velocity . .... 5 Pressure Drop on Dry Perforated Plate . . . . 6 Total Plate Pressure Drop vs. Air Velocity . 7 Total Plate Pressure Drop vs. Water Rate . . . * 28 8 FrictionFactorCorrelation- f' vs. Re' . . .. . 33 9 Friction Factor Correlation- f'T vs. Re' . . . 10 of Apparatus Layout . . . . . .. vs. Water Rate . . . . . . . . .. , . . * . . . Table **..*. 18 20 24 25 26 27 35 . PlatePressureDrop vs. Air Velocity . . . . . . ID IX 40 OF TABLES * * . A Ia Summarized Gradient Data A Ib Sumarized Gradient Data - Calculated Results A 3I Summarized Pressure Drop Data - Dry Plate . A III SummarizedPressure Drop Data WaterRate. Liquid on Plate - Negligible A IV . Sumnarized Pressure Drop Data - Plate. . . . Liquid FlowingAcross . 49 ·* 53 · 0 s * * · .. · 56 60 1 The successful operation of a perforated plate depends to a large extent on the hydraulic gradient of liquid on the plate and the pressure drop of the vapor in passing through the plate. little At the present time, information is available in the literature concerningthese phenomena and no satisfactory method for predicting them has been pro- posed. The purpose of this thesis is to develop a practical method of predicting the pressure drop andhydraulic gradient on a perforated plate. Data were taken using an air-water system and a perforated plate having 1/8-inch perforations on l/4-inch equilateral triangular centers. The range of operating conditions studied involved liquid rates up to 24 gpm/ft*, vaporsuperficial velocities up to 7 ft./see., and seals up to 2 inches. This range was considered compatible with present day commercialpractice in designing towers. Data were also taken using the plate with no liquid on it. The following conclusions for hydraulic gradient and pressure drop on a perforated plate were drawn from the data of this investigation: 1. The hydraulic gradient increases rate. 2* The hydraulic gradient increases with decreasing exit weir th increasing liquid flow height. 3. The hydraulic gradient may be predicted by use of a anning- type friction expression. 4. The hydraulic gradient on a perforated plate is about 17% of that on a bubble-cap plate operating at the same liquid rate per unit of plate width and the same exit weir height. 2 5, The pressure drop through the perforations for both a dry plate and wet plate is a function of the square of the vapor velocity, 6, The total plate pressure drop increases with increasing vapor velocity. 7? The total plate pressure drop increases with increasing liquid rate, 8, The total plate pressure drop increases with increasing exit weir height, 9,b nowing the vapor velocity through the perforations, weir height, and liquid flowrate, the total plate pressure drop may be calculated by use of the equation: = - h t ht + 046 h, 10o The total plate pressure drop on a perforated plate is about 92%of that on a bubble-cap plate operating at the same vapor rate per unit area of plate, the sameliquid rate per unit of plate width, andthe sameliquid level on the plate. If the samecomparisonis madewith the plates operating at equal seals (liquid level on the perforated plate equal to the height of liquid above cap slots of thebubble-cap plate), the perforated plate drop is about 68%of that on the bubblecap plate. The hydraulic gradient data were correlated very well by the use of a anning-type friction expression: ft Vf2 N 2grh Where f' was correlated against Ret: Re" This correlation gradient rh,'7fp was used to develop a method forpredicting hydraulic on a perforated plate hich height and the liquid rate, depends only upon the exit weir The plate pressure drop on a perforated plate was correlated with the expression: ho = OVp2 With a perfectly dry plate, the constant was found to be 0o00029, However, with liquid on the plate, the pressure drop through the perforations was greater than predicted using this constant, and the constant 0.00047 was found to apply, The higher pressure drop was believed to be a result of regions of inactive perforations present during stable runs, The total plate pressure drop was found to consist of the above-mentioneddrop through the perforations, a loss due to surface tension effects, and a loss equivalent to the hydrostatic hea. of the liquid above the perforations, A procedure was developed for predicting the total plate pressure drop on a perforated plate in the studied,This procedure depends only upon the range of variables vapor rate, liquid rate, and exit weir height. 4 II INTRODUCTION A. Object of the Investigation This thesis has two main objectives: 1. To develop a simple method of predicting pressure drop on a perforated plate. 2. To present a practical method of predicting hydraulic gradient on a perforated plate. At the present time perforated plates are used to a limited extent in fractionating columns as a means for promoting vapor-liquid contact, Their simplicity of construction makes the cost of both fabrication and maintenance low in comparison to that of the commonly employed bubble-cap plates. They have proven effective for liquids containing suspended solids, such as the beer mashes in alcohol production, which tend to clog bubble-caps The chief objection to the use of perforated plates is their tendency to t'dump"or "prime" more easily than bubble-cap plates so that they operate satisfactorily liquid within a narrower range of vaporand rates, The successful operation of a perforated plate depends to large extent on the pressure drop of the vapor in passing a through the plate and on the hydraulic gradient of the liquid passing over the plate, As the vapor flow rate in a column is increased, the pressure drop per plate increases until it reaches the point where liquid can no longer flow dom the dovnpipes and may even begin to flow upward, resulting in "priming." As the liquid flow rate is increased in the tower, liquid flowing across a plate suffers increasing energy losses due to flow friction, resulting in increased hydraulic gradient. Particularly in columnsof large diameter, a liquid flow rate is finally reached where the gradient is large enough to prevent the flow of vapor through the perforations at the upstream end of the plate. On further increasing liquid flow rate, the liquid at the upstream end of the plate may actually dump"through the perforations so that the plate is by-passed by a portion of the liquid stream. Bubble-cap plates also experience the phenomenaof dumping' and priming." The caps are constructed, however, so that they will function properly over a wider range of vapor and liquid rates than the perforated plates. At the present time there is little information available in the literature whichis of value in predicting either pressure drop or hydraulic gradient for a perforated plate. It is hopedthat this thesis will be a substantial contribution for makingsuch predictions. B. Limitations of the Investigation All data in this investigation were taken for an air-water system. In general, maxim superficial air velocity was 7 ft. per sec., while the maximum water flow rate was 24 gpm per ft. of plate width. Data for higher water rates could not- be taken since the plate operation becameunstable at higher rates with the air velocities attainable. mercially, While these rates are not the maximumrates used eom. it is believed that the rates do cover the ranges ordinarily encountered. The minimumsuperficial air velocity included in this investigation was 5.7 ft. per sec., since at lower air velocities the plate became unstable. The minimnu water flow rate was zero. 8 The maximumexit weir height for standard operation was 1 inch. With higher weirs, it was found impossible to operate the plate stably at the air velocities attainable with the apparatus. The limiting factor for maximum weir heights and liquid rates was found to be the capacity of the air blower. By covering one-half to three-quarters of the perforated area, the maximum superficial air velocity was increased to about 25 ft. per see., while the maximum water rate was increased to about 90 gpa per ft. of plate width. With three-quarters of the perforated plate covered, the plate operation was observed to be promising at a superficial air velocity of about 20 ft. per sec. with a seal of about 5 inches of clear water. With one-half of the plate covered, some quantitativedata were taken using a 1 1/2" exit weir. The superficial air velocity in this case was about 12 ft. per see., while the water rate was varied from no flow to about 50 gpm/ft. Some qualitative observations at this air velocity using a 1" exit weir. Starting with rate, the operation was stable. was reached were made a low water Increasing the water rate, a point where the plate was unstable (approximately40 g/ft.). In this region of operation, masses of foam moved back and forth diagonally across the plate giving a "washing machine action." action "dumped"large quantities of water through the plate. This As the water rate was increased, the above action gradually disappeared until the plate was operating with fair stability at a water rate of about 65 gpm/nft The high velocity of the water across the plate evidently allowed no chance for these oscillations to take place. With further increase in water rate, the stability continued to improve until the 7 operation of the plate, at a water rate of about 90 gpm/ft., appeared to be as good as, if not superior to, the operation at any other range of water rate. In conclusion, the ranges of water and air rates used are considered to be representative of those which might be encountered in industry. 0. Terminology ry Plate - A perforated plate with no liquid on it, i.e., completely dry. Dmping - The action of a plate when liquid flows down through the perforations so that the plate is by-passed by a portion of the liquid. Hdraulic Gradient ({Ah) The two points on a plate. difference in head between any Tiless otherwise stated, the difference in head betweenthe inlet calmingsection and the outlet calming section. Hydrostatic Head- (h) - The pressure exerted at any point in the liquid by the liquid above. Unless otherwise stated, the pressure exerted on the plate at any point along its length by the liquid above. Instability - A plate is considered unstable when the quantity of water passing down through the perforations becomes area. greater than 0.2 gpm/ft*2 of perforated Piming - If the level of the liquid at the upstream side of plate plus the height of the liquid columnwithin the the 8 downspout, equivalent to the pressure drop between plates, exceeds the height of the downspout, liquidwillbackup the downspoutto the plate above. This action is referred to as priming. Seal - of clear liquid present on the plate, The height Unless stated, the hydrostatic head at the downstream otherwise calming section expressed in inches of Su erficial Air Velocity - The air velocity clear liquid. based of the bubbling section expressed in ft. on the area per seea Since data of this investigation were limited to regions of stable operation, the area of the bubbling section was 4.17 square feet TotalPlate Pressure Drop (hT) -The difference in pressure between the vapor in the space below the plate and the vapor above the liquid on the plate. A perforated plate with liquid, either standing on Wet Plate it or flowing across it. D. Previous Work Previous investigations of hydraulic gradient have been confined largely to bubble-cap plates. Klein (6) using The most recent work was carried out by an air-water system, He was able to correlate success- fullythe hydraulic gradient on a bubble-cap plate with operational variables by the use of a anning-type friction expression. His conclusion was that the hydraulic gradient on a plate is a result of the frictional losses suffered by the liquid in platse It has been found flowing across the that frictional drag is much higher for 9 aerated than for non-aerated flow. The energy lost as a result of friction is compensatedby a loss of hydrostatic head whichproduces the hydraulic gradient. lein found that the hydraulic gradient increases with increased liquid rate, increases slightly with increased air rate up to the point of complete aeration, and decreases with increased skirt clearance, seal, and weir height. Basedon the gradient correlation, a relatively simple design procedure for the of hydraulic gradient was developed depending only upon prediction the exit weir height and the liquid rate. The operation of perforated plate columnshas been investigated by Eirschbaum().* He found that perforated plate efficiency, general conditions being equal, is superior to that of a cap-type plate. With efficiency drops off rapidly because of decreasing vapor velocity, withplate liquid dripping through the plate ("dumping")* In columns spacing great enough to prevent entrainment from becoming an important factor, enrichment increases as vapor velocity increases until the optimum load is exceeded. It then decreases evenly because of decreased vapor-liquid contact time. At excessive vapor velocity, the perforated plate pressure drop is so excessive as to cause "priming." Kirstbaua mentions also that the capacity of perforated plates to carry low vapor loads diminishes as plate diameter increases, while the upper load limit, imposed by priming," stays almost constant. Plates of larger diameters also exhibit better efficiencies in their operating range. Kirschbaumattributes the pressure drop of the vapor between plates to twotypes of losses; a static loss due to the head of liquid 10 on the plate, and a streaming loss whichis analogousto fluid flow through an orifice and is a function of the square of the superficial The pressure drops encountered by Eirschbaum may have vapor velocity. been excessive because he employedplates with small perforations on relatively large centers. used by him had A representative plate B25 rm4 holes on 9 mm equilateral triangular centers. Kirschbaum also investigated increasing efficiency by employing atomizing effects on perforated plates using no exit uwir. He found that the atomizing effect was not sufficiently perfect to obtain comparableto that which can be realized rectification layer using a weir. He also tested a orrugated the sides of the corrugations. with the foam plate with holes in With this plate and no weir, he obtained a cross-current, atomizing effect between liquid and vapor. The results proved no better. Kirsehbaum's work is valuable from a qualitative point of view because he tested various modifications of the perforated plate. By varying perforation diameter and pitch, he obtained varying amounts of vapor passage area. Increasing the area of vapor passage decreased the plate pressure drop but did not remove the dependence of the pressure drop on the square of the vapor velocity. small a ratio of pitch He found that too to diameter for the perforations led to merging of vapor streams above the holes and, therefore, loss in efficiency of vapor-liquid ontact. However, Kirschbaum attempted no quantitative correlation of hydraulic gradient andpressure dropwith vapor and liquid loading. The perforations on a perforated plate function as submerged orificese. Mcoldrick (7) attempted a correlation of the pressure drop 11 through a single submerged orifice with vapor velocity and liquid head above the orifice. Using various liquids and air as a vapor, he found that the pressure drop throughan 1/8 in. orifice and liquid above was affected by the liquid height, air rate, liquid surface tension, and liquid density. water He proposed the following correlation for an air- systema Pw a 0.003 Where ()2+ H h. x P total pressure drop in inches of water. q rateof airflow in cubic feet per hour volumetric through the 1/8 in. orifice. Hh m Hydrostatichead in inches of water. Correction factor due to surface tension* X This correlation indicates that the pressure drop corrected for hydrostatic head is essentially that of air through a dry orifice. the surface tension corrections to be small in McGoldrickfound comparisonto the other factors and essentially constant. However, at high vapor rates, the air funnels through the liquid and the surface tension factor becomes negligible. The dry orifice loss is similar to that predicted by Kirschbaum(). McGoldrick fails to present a general correlation for the pressure drop through a submerged orifice, since his equation involved the experimental factor LX Robinson and Gilliland (), h6wsver, suggest the following equation for the pressure drop through the perforations: Whexe r pressure dropthrough perforations, inches of liquid. I m surface tension, dynes per oni Pr 2 vapor density, lb. per ou, ft. /2 * liquid density, lb. per ou. ft. =--velocity based on total perforation S m diameter of area, ft. per sec. perforation, in, Kirschbaumxand Andrews () have found that incorrect leveling produces unevenliquid distribution to a greater degree with perforated plates than with bubble-cap plates. With low vapor velocities, impossible to arrange conditions so that equal distribution it was of vapor flow was maintained over the whole surface of the plate, although the plate could be precisely leveled with adjusting screws. Gunness and Baker () made etensive tests on a 5 1/2 ft. diamater beer still being used to separate alcohol from a beer mash. Perforated plates with 1/2 in. holes on 1 1/8 in. equilateral triangular centers ware employed at 18 in. spacings in the column. perforations. ach plate had 2,500 Rates of flow and pressure drops over each plate were measured. The column operated at a feed rate of 720 lbo/min. and a steam rate of 162 lb./min. Pressure drops per plate averagedbetween 2 and 3 in. H20 with a vapor velocity of 17 ft./sec. through the perforations. The results indicated that the perforated plates gave efficiencies lower than those attainable with bubble-eap plates. The nature of the mash made use of perforated plates desirable because of the difficulty involved in cleaning clogged cap plates. The investi- gators made runs Justafter the plate had been cleaned several weeks after the column had been in operation. The fact that and also 13 perforated plates can efficiently handle ontaminating liquids is borne out by the results, The most recent quantitative investigation oncerningbydraulic gradient on perforated plates was carried out by Hutchinson, Buren and Miller ( ) The objective of their investigation was to obtain data which would indicate the type of liquid depth to be used for hydraulic gradient correlations. They developeda theoretical analysis of aerated flow which indicated that the proper depth factor for correlation was an effective aerated seal (that is, the hydrostatie head of the foammeasured in terms of clear liquid flowing), They correlated their data on this basis. The investigation was carried out on a stainless steel plate having 1/8 in. perforations on 3/16 in. equilateral triangular centers with the long dmension parallel to liquid flow. The perforated area was 23 in. wide and 47 in. long, the upstream calming section varied from 16 in. to 30 in., and the downstream calming section was 20 in. long. The length of the aerated section was varied from 47 in. to 30 in. by blanking off the upstream holes, and the width was reduced by half for high liquid rates (over 2,000 gph/ft.). were madewith a 1%forward tilt velocities up to 9 ft./sec. of the plate. Three sets of runs Superficial air and liquid rates up to 4,000 gph/ft. were used. Hutchinson, Buren and Miller found it necessary to consider the effects of aeration in interpreting fluid flow data on the perforated plate. factors: These effects were included in the correlation by the following 14 deP i Aerationfactored _ Density faotor =iaerated densit clear density wherethe subscripts "a"and b" refer to to liquid depths at the samepoint on the plate under different flow conditions. dA P pressure drop through the plate. - clear liquid head on the plate. ;/0 clear liquid density. They also found that: 1. Hydraulic gradient increased with increased liquid rate. 2* The gradient decreased with increased seal. 35.For a sloped plate, the absolute gradient increased compared to a flat plate under the same conditions$but the relative to the sloped plate decreased. gradient 4. There was a logarithmic variation of gradient with average seal,. 5. The gradient decreased with decreased length of the aerated section. The previous literature appears to lack suitable correlations of both hydraulic gradient and pressure drop with the variables; liquid rate, vapor rate, andweir height. The object of this thesis is to makethese correlations 15 III PO,DURN A- Experimental Program To develop a correlation for the pressure drop on a perforated plate, it was felt necessary to first investigate the pressure drop with no liquid on the plate. hese data led to the conclusion that the pressure drop was similar to an orifice-type loss and could be calculated with the standard orifice equation. The next step was to see if the pressure drop through the perforations was similar when liquid was held on the plate. investigation, For this data were taken using various weir heights with a negligible liquid flow rate to offset leakage at the downstreamweir and through the perforations. The hydrostatic head readings in the bubbling section were averaged and, together with a calculated pressure loss due to surface tension, subtracted from the total plate pressure drop. The remaining loss was that due to passage of the air through the perforations and proved greater than that for a dry plate. During the investigation, it was noticed that although the plate was operating in a stable range, regions of perforations were inactive whenthe plate was viewed from the underside by means of plastic windowsin the air chamber. t was reasoned that this phenomenon was responsible for the eessive pressure drop on the wet plate. The quantity of liquid leaking through the plate was measured and proved to be alight. Previous work with Fanning friction hydraulic gradient bubble-cap plates (6) has shown that a factor type expression can be used to correlate data. To test its applicability to a perforated plate, runs were madevarying liquid and air flow rate and also weir 16 height. The gradient was measured by subtracting the downstream clear liquid level from that upstream. Becauseof the horizontal direction in which air was led to the air chamberbelowthe plate, the air leaving the perforations had a velocity vector in the downThis tended to raise the level in the downstream stream direction, calming section above that in the upstream calming section, giving a reverse hydraulic gradient effect when no liquid was flowing. Several runs were made to measure this effect at various air rates and liquid seals with no liquid flow and a plot of correction values was developed. These corrections were applied to the hydraulic gradients measured during liquid flow runs to make them equivalent to gradients measured on a plate ith vertical air flow to the perforations. Applying the sanning-typefriction factor expression to the hydraulic gradient data as a method of correlationyielded results that were quite satisfactory. To investigate plate operation at high air velocities, it was necessary to blank off the upstream half of the perforated area. Because the air vector effect mentioned above was more pronounced and errors involved in measuring hydraulic gradient doubled, the data taken at high air velocity and high liquid seal proved unsatisfactory. However, the runs served in obtaining qualitative information regard- ing plate operation. B. Description of Apparatus The apparatus by Ghormley () used in this thesis was adapted from that constructed and Seuren ( and more recently used by Klein (). The 17 apparatus was originally constructed and used for the investigation of the operating characteristics of bubble-capplates. The apparatus consisted of an air-tight covered 2-EP. by the perforated Gould centrifugal measuring devices, chamber which was plate; a 15-HP. Sturtevant blower; two pumps; three 55gallon drums; and various such as manometers and orifices. The regionabove the plate was enclosed so as to allow for liquid flow. The forward side was constructed of three panes of glass to allow observation of action on the plate. T~vplastic windowswere located in the air chamberenabling observation of the underside of the plate during operation. Figure 1 is a schematic representation of the apparatus. blower was Joined to the air-tight The chamber by means of an 8-inch duct, makingit possible to force air through the perforated plate. The maximumair capacity was 2,000 fmtagainst atmospheric pressure. The air rate was regulated by means of a slide damperin the blower discharge line and was measured by means of an orifice. later was pumpedover the perforated plate from the three drums, which were oined in parallel, by the two centrifugal pumps connected in parallel having a maximumcapacity of 140gpm. The water rate was controlled by a globe valve in the 2-inch water line leading from the pumps to the upstream end of the perforated plate and was measured by an orifice. An inlet weir was used to insure even distribution the water flow across the plate section. of In succession, the water flowed through an inlet calming section, over the perforated section ~~~_ of the plate, through an outlet - k l- -- calming section, and over an adjustable 18 _ __ ©_ I f-4 c w a Z4 ;o m ,;c _ i. - I 1118-- i. _ ___ outlet weir to the surge drums completing the cycle. The perforated plate was constructed by WickwireSpencer, Ic, from 14 gauge steel sheet to the following approximate dimensions: Over-all dimensions 120" Upstream edge to inlet weir Length of inlet calming section Length of perforated section 12" 24" 60" Widthof perforated 10" section Length of outlet calming section 13 1/2" 24" The perforations were 1/8" diameter on 1/4" equilateral triangular centers, the long dimension parallel to liquid flow. Figure 2 indicates the location of taps in the plate which allowedmeasurement of the hydrostatic head at various points along the length of These taps were connected to open-end manometers. the plate. in indicated Also igure 2 are the three taps located in the air chamber for measuring the total plate pressure drop. These taps were connected to open-end water manometers. For the runs in which no liquid was used on the plate, straightening vanes were inserted beneath the plate and perpendicular to the air flow for better air distribution and to produce a more vertical air flow through the perforations. These vanes were removed during runs with liquid on the plate because they reduced air flow through the perforations directly above them. rimental Procedure C. The operation of the apparatus was essentially the samefor all runs in which liquid was used. A typical run is outlined below: 1. The hydrostatic head manometer lines were purged of air by forcingwater throughthem fromthe plate / taps. After this 20 _ _ _ _ - - _ - i FIGURS ?1P FORAT3D PL.A, 2 LAYOUT I "I I R w,7E HYIn DRO an90 S, IA ?R3SUR DR TAPS (I,II, I II kF3RATD SECTION III IRH 8 /* -'/ _ _I____ I ~-1----~1w---- - ----- -- I procedure, the water levels in the manometers should be the Ii same and should lie on a horizontal line. If they did not, adjustments were made to level the plate by means of leveling boltson the legs of the apparatus. (See Appendixfor details of plate leveling.) 20 The desired exit weir was installedo 3. The air blower was started with the damper fully opened. 4. The pump (or pumps) was started and the globe valve in the water line adjusted for proper flow rate. 5. With the plate covered with water and liquid flowing over the exit weir, the air damperwas adjusted to give the desired flow rate. 6. The lines leading to the pressure drop taps were drained of any water that had collected in them. The taps themselves were shielded against water droplets from the plate, and the draining procedure was necessary only during very unstable plate operation. 7. After about three minutes were allowed to reach steady state, readings were taken of the hydrostatic head manometers, the plate pressure drop manometers, the water and air orifice manometers, the air temperature, the air pressure upstream of the air orifice, andthe weir height. D. Method of Correlation 1. Hydraulic Gradient The hydraulic gradient data were correlated by a anning friction factor type expression by plotting a modified friction - _e 22 factor as a function of the Reynolds number, 2. Pressure Drop The pressure drop data were correlated by plotting the air velocity through the perforations against the pressure drop of the air passing through the perforations. With both the dry and the wet plate, curves were obtained which indicated the dependence of the pressure drop through the perforations on the square of the air velocity. A completedescription of the abovecorrelations is given in the section II titled DISCUSSION O RESULTS. _ __ I WV The hydraulic gradients RESULTS measured on the plate and corrected for the air velocity vector (see Section III) are shown in Figures and 4 plotted against the operational variables. In Figure 3 the hydraulic gradient is plotted against the water rate at various weir heights. Figure 4 showsthe effect of air rate on the hydraulic gradient at various weir heights. It can be seen that increasing water rate and decreasing weir height both tend to increase the hydraulic gradient, whereas varying the air rate has little effect on the gradient. This latter feature indicates that operation was in the range of full ( alein's aeration and verifies is independent of vapor velocity. conclusion that hydraulic gradient The trend of the 1-inch weir data in Figure 4 might indicate that aeration was not complete at the low air rates with this liquid levels The pressure drop on a dry perforated plate is plotted against air rate in Figure 5. logarithmic The straight line with a slope of tw on paper indicates the dependence of the pressure drop on the square of the air velocity. The total plate pressure drops are shown in Figures 6 and plotted against the operational variables. Figure 6 is a plot of the total pressure drop against air rate at various weir heights with negligible heights weir water flow. on the total The effect pressure of the water flow rate at various drop is illustratedin Figure 7. 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I ~~~. t -. ..... -.I 1, I -- X ' !····I1.i l-- ~_, -1----r· -T;T' ..... ~...)....q. :I J- --..,~ , ' i-' .............. . ,. ,I... , . / i . ' *. *',· !. i" " * ' I I . :. :· '.-. i.t· .: . ::' . ~~ ~~~· :-*,-f -- -.... . .t.. I..= . .:~ j -,," .. I--,---,_~...,.... ~~~~~~~ : .. · , : .- . . { . I ', , ,.w. . . . ' . 1 .... ',~~~~~~~~~~~~~~~~~~~~~~~~~~~ I· . . - ... .,- :...... I _. ~ .... .p --:- ........ I--··· . . ....... . = ,... , , ... ... F ...........- ,f i;1ii~ i .. c~j .... ...... ...;.. ....... . .... ..... . . ..... -F L' '~ ...., ., '~~'' L--=," "~~~,,,.···I [..~~~~~~~~~~~i ,;.i~~i . .. ..------' ......,.., ,. . ..- i... . I.... -,: ,. I~~.~....... J.. . ....-::..-------'·:.---~' '-.: --: ~~"':.,:..... ,.. .':.-. : ' ...... -. ~ _--d.. .............................. . . 4..... ....."F:I~ ...-I--=-" '-. ;· '"." r~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ i '" * -!.. ....... i. : . . -~-._ _~/f ... . , ,~.. ~·i---~*----[ : . .i~'....~.............. _, :'-~........... i~~ . ~~~~~~~~~~~~~~.......-.:~ ._ ,1~~~~~~~~~~~~~~~~~~~~ . .... . .. i:.~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ,-----'~: "' ,..[-:-: t.---. ~~~~~ . , i~~~~~~~~[--:** *--." .... i-..i .1 .. " ; i ........ '~rq .. +' ' ....,*:f ..: ~ '. ,i t . .. ·I I~~~~~ ', - t I......... , ... '7 I- · I .. I.I , , ~: , I I :! ~ I' r...., I . ~ .. J /7---:-~-- [ J ~~~~~~~~~~~~~~~~~~~~~ i .................~~~~~~~~~~ I .......... '.i ...'r .l 'l·I ........... .b* ,' : !I ... .. , ... " r ... ~. , .... ... 1 ... , 1., , ..~~~~~~7T; J.. ~~ ~-:~ IB -- L , .... , ....... ........... , ,....'-'" -r- -4._ _.....-...... i The hydraulic gradient and pressure dropdata shown in these Figures were used to develop correlations and methods of prediction (see Section V - DISTU3SI[ OF EStULTS). The mainresults of this thesis are: A. A correlation for the hydraulic gradient data. B. A alculation procedure for predicting hydraulic gradient. 0. A correlation for the pressure drop data. D. A calculation procedure for predicting pressure drop. 30 V DISCUSSION OF RS1LTS A. _ydraulic Gradient Correlation In his investigation of hydraulic gradient on bubble-capplates, Klein(6) found the gradient to be independent of vapor velocity reaching the point of full liquid aeration after He further found that the bulk of the hydraulic gradient occurred in the bubbling section and that the hydraulic gradient data were correlated by meansof a Fanning- type friction factor A study of the hydraulic gradient data in Figure 4 for the perforated plate both indicates that operation was in the region of full aeration and verifies Klein's conclusion that hydraulic gradient is independentof vapor velocity The flow of liquid across a perforated plate is essentially the same as that across a bubble-cap plate. In each case there is a constancy of liquid or foam velocity and area available for flow It seemed reasonable, therefore, to assume that the bulk of the gradient muld occur in the bubbling section of the perforated plate and that the hydraulic gradient data muld be correlated by a Fanning-type friction factor, The hydraulic gradient data were used to calculate a modified friction factor from the expression.: F a f' Vf 2 N 2gc rh Where F - nergy loss across the bubbling section h = hydraulic gradient (in. of H20). () 24 h (ft.of HpO). Pf I Vf W velocity of foam (ft/sec.), N m length of bubbling section (ft.), gravitational constant (ft./sec. 2 ), c rh modified friction factor, = hydraulic radius (ft.)., The hydraulic radius was obtained from the equation: rh WJhere b m Lc - (2) bL channel width (ft.). calculated foam height hydrostatic head (ft.) twice the downstream (6), The foam velocity was calculated from the equation: G Vf (3) (60) 7-46L' Where G' liquid flow rate (gpm/ft. plate width), Q+= fractional volume of the foam occupied by the liquid = 1/3 (. The modified friction factor was plotted as a function of the Reynolds number of the foam which was obtained from the equation: Ret Where Re' _ rh v Pf 4 Reynolds number of foaMn :f .- effective foam viscosity (lb./fto-sec.)* /O ::s effective foam density (b/ft. The foam density,/4 3 ), , is essentially the weight of liquid contained in a unit volume of foam. Since is defined as the I fractional volume of foam occupied by the liquid, it follows that may be calculated from the expression: P Pi /M 1 Where (5) density of the clear liquid (lb./ft.3). There being no simple, accurate expression for calculating foam amounts of air and water in the foam, a viscosity from the relative similar expression was used for oalculating f: Af:Af Where 1 (6) clear liquid viscosity. Any error introduced by use of the above equation affects the correla- tion only by shifting the plot of the friction factor, f', along the Re' axis. )Figure8 showsthe modified friction factor, f', plotted vs. the Reynolds number for various weir heights. The points for each weir height are seen to lie on a straight line. As the weir height and, consequently, the seal increases, the friction factor for a given Reynolds number increases. It would be convenient to draw the lines for the various weir heights into a single line. Since f' and Re' are dimensionless, the factor used to draw the lines of Iigure 8 together should be dimension- less. Several factors were tried, andthe factor T was chosen: (57) he - Dp Where Dp diameter of the perforations (in.). he =-dowastream hydrostatic head (in. of H2 0). 33 9i:iii;i:~i i ...::;::.. 9:::;~:::: -·--- ··· ............- ::I:: ::-:...:::::::-. :::: .: ....... ........ ....... .... ~~ ~ ~ ··~]!I:l ~ ;:~:::[;,r::;!iiir:!:! :::t. --,~~ : ::!.: :-::... :: .~~~~~~~~~~ .................... ;........, .... ! '.. I d#:![ IU ll I' ..... . ".....?' ...... .-- . l 1. ........ . !'.::.Z 't:! [ {I. { : !!:;: ! i;:!!·: :i!!~::h:lii ji' {~: !Z'.' ' { ...... .... :.... . ..... ... . ,. ;.. ... ~~~~~~~~~~~~~~~~~~~~~':;.'iZ ":-:.. ;il/! '::/:.::;d:'.T'.' . ;:' . :::':' :: T .. :: : . . ........... ~~~~~~~~~.:.::......:~ ;.r .... . .· : {~ .I .......... .............. . ::::::::::::::::::::::: :. ::::::: ...... .. i...... .: ................ :: :: ::::::.iIri ii ii:;:.::~~~~~~~~~~~~~~::::·:: .... t...'..... .....i.: I....................... ............... ...... . .. [iiii~jil~i :'":1 . . ...... .............F. .~ . :-i!~.i= ::::::::::::::::::::::::i :4~: . ..~~~~:::::I:...... . ~ ~ ~,:.::::::: ...... ............. ~ . ,.;:' ~ .'........ ... ..... .......... .~~.. : ....... .. .... . ..-' :::~': ::: ::::!;-~ i: :. :-""' :!:':~::::"::::':: i '::li~ ~:::{~'_ iiiiiiI~::,I ::: :::::::.: k;::::1::: ::.:': ; ~I,;:1::: ':::-: ::;:::: . ..- ~::::;i: ~',.-;~:!:.~ii ::..;:.,.::.:.::: :::::::::::::: ..!.?h :~,J::r:,t'·i!i!; " .. i~...::...! ......... ...... ........ [:" ... ::-~ ~J:kL'-' ...... }......~...... :;; '.::::::::::::::::::::::::.: :o- j :::::= ::::::I:::',' ~~~~~ ifff~~~~~~~~~~~~~~:.i : ':':.: ::.':;l:.'. :::::::" ..... :::: I·r:'::: ; ::::":::;': '.lll ' .::i :::!F.::!::: : !!:ui~:~:~ i-.:"F '! i: :: Iii i:/:~::":..::.: il,:.-ji : iib! q [,"T .. isiii~il ~':,: , ::. J} :: .. ........... ~~~~~~~........... ...... ;; ': ' I ... "~ ' := ........ ['':J' ~· ' iiiiii 1 ;;".;'';; iti..... .... :·--· :' J: J j: . . .·· .. ...- , .. ;..;;;; ;:; :":;.!: :::: : .[.... : .. {Ill -~·. .. ; . I..-..-i.:.: :. ...... :· ri. : 1:.···.:: ........ t i ' j: ' ;::.: : :::::· ,::::: ' :]{ :J .... : J ; . f: : I tlt i~'~:;: ; t :,::::::: PIoo :: 3 j { ........ ,......:_:: . ""'... ~~ :::::::::: ~~~~~~~~~~~~~ ..:~::::::: :t"{:: a :::: ............ . . ~ ........... ~ ......... : ~:~:: ~ ............................... ~ ~ ~ . ~ ............ ::'':: : ::::iilii:': :.~:::~. ~ :::::::::{:?:'::;':':iF:::::':; 't*.... *-,t ~o.............. +:...... liilii~li .-.~,~.~ : ,.,~,.,, :::,::::::::: .'...... ~::::::~ 3~~~~~~~~~~~~~~~~~~~: .J . ......... :i~~~~~~~~~~~.:iiiiiiili~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ t 'T'' '-!.. . J,0 ~~~...;... ~~~~~~~ · . : · :~ · · · . ... .. JJ t........: !. ............. i :: :.:'::F: .:..... ............. T'r~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ....... ~~~~~~~~~~~~~~~~~~~~~~~~~~~......;. ,................... ::':......... . .......... " ............ . ~'-' '' 'r: :': ....... :::. ; NZ.ll~~'41~ . ' : ;::! ....... .;.::::::::::::: ::::: ·· ::: · ;.;~.;;;;; :::i::::i':::;· ;;-· ::!', ;::::::;:::: ...:;ti ::{::::::::::::::::::::::::':: .. I- :.J ''t-" .... ,~; . JI :~,, :;'t":..'"'TJT'] r"'[: 4 ,"T. T 5 8 7 5,000 Reynolda 8 9 '-:: '' 10 10,000 t;' ' .'-J:. Tf...,. ~2 .:: :·. 3 O50 M 50,=o Number - Re' Pr .*-/3- -/ 6 7 34 This factor was employedwithout a theoretical basis and maynot apply on a plate with a different perforation diameter or perforation The plot pattern of 'T vs. aRe is shown in Figure 9. xcluding the data for the 1 1/2" weir, this plot is seen to correlate the data quite well. Since it was found impossible to obtain data for weirs above " at the vapor velocities attainable with the aparatus, of perforated the half section was covered in order to obtain the data for the 1 1/2" weir. For all weir heights, it was found necessary to correct the hydraulic gradient data for the velocity vector of the air (see section III). This correction was made for the 1 1/2" weir data and the gradient then doubled so as to correspond to a five foot Therefore, bubbling section as in the case of the other weir heights. any error in either the data itself or in the correction for the air velocity vector was doubled. Since all points for the 1 1/2" weir data lie on the "high" side of the line, it is felt by the authors that the correction for the air velocity vector was in error.It is interesting to note that all points for the 1 1/2" weir data lie along a line parallel to the original line if one point is excluded. In summingup the above discussion, it was found that hydraulic gradient for the perforated plate could be predicted by use of a modified anning equation. The modified Fanning friction various weir heights were found to be correlated Re. factors by plotting for f' x T vs. Of noteworthy interest is the fact that the modified Fanning friction factor for the perforated plate is about 17%of the same factor for bubble-cap plates with the sameweir height and operating at equal Reynolds numbers (6). A comparison of hydraulic gradient data 35 ~ rt-- ~ ~ it~~~~~~~~~~~~t ~ li' ~ ~ ""i;'P ~ °;"' ....;i:':.: ':' t I .... ........... ~~~~~~~~~~~ ~~~~~~~~~~~~......... ~~~~~~L ~=,'' ~LLI ~:? i.::fi~~ .. -~:i_ !:: 1::;: : .. : ..:fi~!t:. ~!fif::: :::;ti ,~ti:i:~!:.:: .i:: ~ i' '-:i: :: :: T9 ::::,::::.:,;'f-. .. i~~ ~; :~i~ilii :..:¢ t:ff:firf : ;~??~:!~ ,:; :i t:::.::: t::;:::::!1: t~" i :;': ;~.~ ': '-'~: "' ,,;:~:~. I:: ....... "" ;:::::::: ,,.., :: li'. ;i;: ·___-:...::: _ :....................... =::::........ :::::: ~:: -::::::::':::::::::: ;:,:::::: ::.:... .............. ::: ~ :: ::1::: :::, ~,::: ::;: , : ::::::::::::::::::::::::: ' ..... E~~~~~~~~~~~~~~~. ' :.~:tif IiiJ. 11,!'::::::i........ :::tF;.;:::::;':' ;.M :::::::::t::~! ,.::::!~ i:· l: .............. ...... .. i ~~~ .......... ~~~~~~~~~~~~......... ............ . .................. :::'::"'I:::::::::::':::;:: ..... :.'~I..~ :::fl~:.:... ::::I::::::::.:2.. ~~~~~::- ::::. :::;.:....... : ..,.~~'; '':::liF;'Fl'::::.:: ,...::: ............ t..:-:'.':: .: ;it..~::":::~::::l: ": ~::~~, :~I,::: :..:: J J;::::.::i:;;.:::::;:1·::':' J ' 'J " 6 a ':: ' ::f::: ,:1:::: : j~~:i!::l,, ::,t:..L · ,·t · ·. .·- · .i . .. · ::::~:,':' ; :;:::!:::':::: ::::::::'::::,:::J:.;:~' :::::.::::;.:~::' :::i::::(::::' :.:::r: 'TT-"FTT.'; 2 ..... , .1:: .:::....: .. .... :: · :::: ~~~~~~~~~~~~~......:' :.: ,.·j........ ... ,.r....j.... .. i.., . i '~ : .~,.~ :',~ _,: .:-iii':'-~ ~'~:: .:.J'~. ii:a~ .:::j:;:::: Ow..%;:I~'N;,,::: :;i::TW,?: . .,T is.~~~~~~~: -:-.: :,T,/////. iiii -ii: "-7;' .,i'T :-,::.T'T: · '··.Tt::J: ~~~~~~~~~~~~~~~~~~~~~ · · ....... t:1:j,. ~,i ,,? t : : : ,,t : : :::t: · "~ i:.... '.ff" !'i. [L~.' :;i:.~: : ' ' :' Ii 11'~ : : :" ' ~~~~~~~~:'~:j:;''':;.:i.;..::.. ":::..: :::Ji.' : :: .L:::'; ' :J~'. t.....LL I ............;!.... . ,.::.4::tliiii~l: ..... I.............'. :. :::::::':::·::: ! :::. . ... ::::1:.:.:!:.:.:'::: :.:~:::,. :'....I......t ~. . . ~ ......... ~~~:::::::::::::::::::: ............... ~~~ ~~~ ~~ ,·. :~,i :~,. .:::!::· · -::!: .::; iii::~-_:,. " ·~~~~~~~~~~~~~~~~~~~~~~:~.~~:-~,,:::.:'.~:" ,··:'1 ;; .... .I:::: ,:::~,~.:I'.:: . f:.' 3~~~~~~~~::~:.,, l~:,In....:',:,:,'":::'i . : .... ' :· .I : ~~~~~~t.·: I :: . oo -- ~: ............. · 1~~~......... ':. ~ t ~ I (iLLL1L:~~~ 2,000 : ..- : ....i~:... 1... . .!... ,.:, , .: I~~~~~~~~~~~~~~~~~~~~~~~~~/; '::::!:;'j::.': :·: :',::::;:'..n:,': ....... ... "': ." i:1 ' :. " ,·' ~: i. 5,000 ....., ,i'i I-' i~~~~~~~~~ .1 : :i~ill~j.'..,i' ~ ~t........ ::: i; .:: : :. ... i 3 4 5 50,000 10,000 Reynolds Number- Re' W -J? c/3 6 759r · 36 for the two types of plates operating with the same water rate and weir height verifies the fact that hydraulic gradient on the perforated plate is about 17% of that on a bubble-cap plate* B. Calculation Procedure forPredictirng Hydraulic Gradient On the basis of this investigation, a procedure is offered for calculating hydraulic gradient on a perforated plate operating uGer stable conditions knowingthe liquid flow rate across the plate, the exit weir height, ad assuming complete aeration. l1 The dovmstream clear liquid level, h , is determined from the liquid flow rate and the exit weir height by use of the standard weir equation. 2. The foam height, L, is twice the downstreamhydrostatic head: Lo 2h 3 12 3, (ft.) /f, The effective foam density, is calculated from the expression: 3 - p1(lb./ft. /9£ 4, The value of radius, L ) () is used to determine the hydraulic r , and the foam velocity, Vf : rh bL c bL ( ft.) b + 2LE vf (ft./sec) G= 60 /f (2) (3) Lc 5, The effective foam viscosity, ,, is calculated from the expression: f,C/c ] (lb/f.se.) (6) 37 6.The Reynolds numberof the foam, Ret , is obtained from the equation: 4) r,=rh V( 7. 8. nlowingRet, ft is obtained from Figure 8. The hydraulic gradient, A h, is determined from the modified Flaning equation: f Z1 Wlhere Vf2 N 2 g rh h - 24 (in. of liquid). C. Pressure Drop Correlation The drop in pressure of air passing through a perforated plate with no liquid on it was found to be a function of the square of the air velocity and could be represented by the equation: ho lhere (8) Vp2 ho - pressure drop through perforations (in. of H20), Vp O air velocity through perforations (ft./sec.). eperinental constant 000029. This is the equation of the straight line in ligure 5, obtained by plotting on logarithmic paper the velocity of air through the perforations vs. the pressure drop across the plate. In order to obtain an equation applicable to vapors other than air, Equation 8 maybe converted to the more general standard orifice equation: 2VC ao /P (9) 38 Where Vp vapor velocity through perforations (ft./sec.). ho _ pressure drop through perforations (in. of liquid). liquid density (lb./ft.3). ?01 /Pv - vapor density (lb./ft.S). /34 WhereA. is the hole area (ft. 2) and As is the perforated section area (ft. 2 ). 2 LAaj experimental constant. 0 The experimental constant was found to be 0,86.It is believed that this high constant obtained with a dry plate can be accounted for by reasoning that the air streams leaving adjacent perforations interact and flow characteristics a single orifice. result which differ from those peculiar to The tendency is for the pressure drop to be less air velocity, than for a single orifice at the s Equation with employed usually The constants 9 for a single orifice range from 0.60 to 0.80. The drop in pressure of air passing through with liquidon it was found to consist 1. type An orifice a perforated plate of the followingcomponents: loss which could not be calculatedusing Equation 8, 2. A loss due to surface tension effects. 3. A loss equivalent to the hydrostatic head of the liquid above the perforations. Orifice tpe loss. By subtracting the surface tension effect and the hydrostatic head loss from the total plate pressure drop and plotting the remaining plate pressure drop on logarithmic paper against the 39 air velocity, a straight line with a slope of two was obtained. in Figure 10. The equation of this line is: is illustrated ho = Where This 2 (lo) ho - pressure drop through perforations (in. of HE0) Vp = air velocity through perforations (t/sec), 0 = experimental constant 0*00047 t At equivalent air velocities (based on total area of perforations, Ap),the pressure drop of the air passing through the perforations was found greater for the wet plate than for the dry plate. that this was caused by partial inactivity It is believed of the perforated area which is attributed to the wave otion of tion o the the bubbling liquid on the plate. Since the velocities were calculated from the volumetric air rate to the plate and the total hole area, they did not represent the actual velocity in the case of the wet plate with its inactive regionso Assuming that the pressure drop on the wet plate should be the sa that on a dry plate, Equation S was used to calculse a velocity as from the pressure drop. It was found that about 20%of the perforated area had to be unavailable for air flow during a stable run to cause the higher pressure drop. This agreed with an estimate of 25%inactivity made by viewing the underside of the plae through plastic windows during operation, Although about 20%of the perforations were estimated to be inactive during a stable run, this portion of the plate was not dumping. Regions of high hydrostatic head seemedto moveacross the plate in the direction of liquid flow causing the perforations underneath to be inactive. However,the actual leakage caused by this 40 IC :--"' :" : : B a ....... ' - ... . ' / .. ' ';: ; ~-'; .. :''~~--i·- . ' ~'~',;.' . ' -' 7 '~~ : ' ...... , - '~. I ... :: ;l.. . -- a -;I~~~~~t 5 --- _ t :::'~~~~~~~~~~." !.~~.... t ;=':;'w.................... .·· r-· .l ' _--' .... ........... : ............. ....-c.,"-F . ............ :C... ........ t.........: . ...... t1 ~-'"t-.... , 4 Z : ' ' ~~l,""41f.... 'k~l' ..... .T-_ _ i i'I. ......,...... .....T ......... .,,.......I....' . . :1::;~ _ 14... ....:.. :: .. .. - ; i ~.-- 2-~ .....I.... A...gf ... :__ - - £: -: ~-:--q-· . : : ~~~~~~~~~~~~~~~~~i i:-·.~l._ ::···2,m-:m]'.: ::.'.;::-h '.~: ~_._.o ..... . ...... ·-............ -:1 ............ i .- . ~)·. ~ . IILL-- -~·)·-·-I····1 : ,·····-~· ..................... ,.- I. :: : t-,-:........ i~.~l ........ . . ... ..... .... ..... .L', . , .-...... .,,: ,i· ~· ' / i ' ~ -. L--~ ................ ....... c-~~~~~~~~~~~ , . ....... ~-.~L·lt .....!_·_ : ....................... i =] :' ,'-~. ,~~~~~~~~~." r S ~--.:u:_::: ~ i::r~r:: , TIL~.1_·· :_· f.. :-?.-:: :-::: -~_~ :: : === :' __ c,, ~.:... ....... ~ 1.. .... !;:" .. :-:+-:-: :=========- I.. ,, , :/": ...... ~ ,,.............. I .... - ....*?..... r--I .... , .....f ................. t....... i..............t !.., ...... , 2 ~~~~~~~~~~~~~~~.. J''I J -- --- -, [- ' =L~-, , r-- ........ '-- ,+........ - '. .... - /- ... :· .... ... .... ) ..... .~. - · · . .) [-'- . _.,_L , ~ _ ~ ~ ~ ~~ +.., 1 15 -r .. --- · :· h ' ..... ~....i............ '-.. ' ..-...-. ·-- p'" Ir " t·- . ... ;.,.. -. '. .. -,:'- -,' ..... ' '!::: : :::;:'i: :: ":;'i:' · ::; -·-.-· ·- 2 S 4 S 8 20 30 40 50 60 Air Velocity - Vp (ft./sec.) 4 · 1· t '· :, l....i.. i· · '. · -- t....... Ji : -·- .. " , '--i·--~,, :::::::::::::::::: ~~~~~_ tt--,---- ·-- '--- . .~.' ; , -,-?'" i~· . ' 7 70 a 80 WPT & ·1 9 !· 10 90 100 41 was very slight during stable runs, amunting phnono to approxi- mately 0.015 gpa/ft. 2 perforated areao At higher air velocities than could be obtained with the exist- ing apparatus, it is believed that the inactive areas would gradually disappear and the plate pressure drop would then follow Equation 8. Converting Squation 10 into the more general standard orifice equation, Eiquation 9, yields an experimental constant of Oe68. This constant obtained with a wet plate is more in line with constants usually encountered for use in quation 9. However, it is believed that the velocity used to calculate the constant in this equation, Vp :1 is not the actual velocity on the wet plate as explained above, An alternative explanation for the constant, 068, would be that although regions of inactivity were observed from the underside of the plate, the estimate of 20%inactivity mayhave been too high and actually most of the area was active, If this were true, the velocity used to calculate the constant would have been correct, It is suggested that the clear liquid layer below the foam and ext to the plate greatly reduces the interaction of air streams from adjacent perforations, and flow is more nearly like that through a single I orifice. This would explain the fact that the. more normal constant of 0.68 applied rather than 0,86 which was found to apply with the dry plate. Surface tension loss. To account for the loss in pressure due to surface tension effects, the following equation for the formation 42 of bubble surface was applied: 0.04 Y t Where / D ()11 ht = pressure drop due to surface tension effects (in. of liquid). liquid surface tension(dynes/cm.). 3DP perforation diameter (in.). This lossamounted to 037 inchesof water for the system studied. McGoldrick ( found this equation to apply for a single 1/8-inch orifice and for air velocities similar to those encountered in this thesis. The equation was, therefore, employed and proved satisfactory in correlating the pressure drop data Hydrostatic head loss. The pressure to be overcomeby the air leaving the perforations is equivalent to the hydrostatic head of the liquid above the perforations. plate was found to The hydrostatic head profile for be similar to that encountered with a perforated a bubble-cap plate (6}) A region of low hydrostatic head was formed in the bubbling section.It was found that with weirsup to one inch and air velocities (through the perforations) up to 30 feet per second, the averase hydrostatic head in the bubbling section was p mroimately0.46 times that in the downstream calming section. Comparing data taken by Seuren (9) of the total pressure drop on a bubble-cap plate with the total pressure drop on a perforated plate operating at the same volumetric air rate and water level on the plate reveals the perforated plate drop to be the lower of the two. Seuren S used thirty aps distributed in an area equivalent to the perforated area used in this thesis. level of 232 At an air rate of 34 ofma/capad in. on the plate with no liquid flow, Seuren a liquid measured a total plate pressure drop of 3.10in. of H20o With the same rate of air to the perforated plate, i.e., 1020 cfm, and the same liquid level, a total plate pressure drop of 2.85 in. of HO0was calculatedo This is about 92%of the drop on the bubble-cap plate. The height of liquid above the slots on Seuren's plate was 1.57in With this same liquid seal on a perforated plate, the pressure drop vmuld be 2.10 in. of HI20 or 68%of the bubble-cap plate drop, D, Pressure Drop Calculation Procedure The vapor velocity through the perforations, the liquid rate and the downstream weir height are sufficient data to predict the total plate pressure drop with the following equation: h, he Where . = h o t ht +- 94 6 h (12) hydrostatic head of the clear liquid in the downstream calming section, calculated with the standard weir formula (in. of liquid), The value for h o is calculated from Equation 9 using the constant 0,68. The surface tension effect, ht, is calculated by using Equation ll. Although Figure 10 was developed using data for 1/4, l/2, 3/4 1, and 1 1/4 inch weirs, with no liquid flow, the validity of extending its use to somewhat higher seals vith liquid flow is verified in Table A IV, where calculated and experimental pressure drops are compared. However, it is not recommended that this plot be used for high seals or for liquids with properties differing widely from water 44 At higher water rates it is to be noted that the calculated drop becomea I increasingly lower than the experimental drop. This is partially explained by the fact that the hydraulic gradient on the plate auses a fringe of the upstreamperforations to ease bubbling and in effect reduees the plate hole area. The plot was developed from data with no liquid flow and hence does not include this effect. Whenthe pressure drop is calculated using air velocities corrected for this iactive area, better agreement is obtained between the values of experimental and calculated pressure drop. This is illustrated in Table A AI. 45 VI COONCLUSIONS The conclusions to be drawn from this investigation of hydraulic gradient and pressure drop on a perforated plate are as follows: 1o The hydraulic gradient increases with increasing liquid liquid flow rate. 2, The hydraulic gradient increases with decreasing exit weir height o 3, The hydraulic gradient may be predicted by use of the Fanningtype friction expression: F Where _ _ _______ f't for various weir heights is plotted versus Re': Re' 11 _ ' rhvf f i ii 4. I vs. Ret for various weir heights may be The curves of brought together into a single curve by plotting f'T vs. Re', where: I T Dp h c - Dp This correlation is knomw to be valid only for the data of this investigation. Further study would be necessary to determine whether or not the correlating factor, , is applicable to plates of different perforation size or pattern and to systems other than air-water, 5, The hydraulic gradient on a perforated plate is about 17% of that on a bubble-cap plate operating at the same liquid rate per unit of plate width and the same exit weir height. 6, The pressure drop of vapor passing through the perforations of either a wet or dry plate is a function of the square of the vapor velocity. 7. The pressure drop on a dry perforated plate is lower than the pressure drop through the perforations on a wet plate when operating at equal superficial air velocities. 46 8. The total plate pressure drop increases with increasing vapor velocityo 9. The total plate pressure drop increases with increasing liquid rate and increasing exit weir height. 10. Kowing the vapor velocity through the perforations, exit weir height, and liquid flow rate, the total plate pressure drop may be calculated by use of the equation: h0-+ ht+ haW Where ho may be calculated from the orifice equation: 6 (1l with e 046 C = 0,68, ht 4P may be calculated from the equation: 0.04r t 11. D- At the same superficial air velocity, liquid rate per unit of plate width, and liquid depth, the total plate pressure drop through the perforated plate was found to be 92% of that through a bubble-cap plate. Making the same omparison with equal seals (liquid level on perforated plate equal to height of liquid above cap slots on the bubble-cap the total plate pressure drop through the perforated plate), plate was found to be 68% of that through a bubble-cap plate (9), of a perforated plate in operaheadprofile 12. Thehydrostatic plate()s tion is very similar to that of a bubble-cap 13, In the range perforations of stable operation, leakage down through the was found negligible. The following recommendationsare made for future investigation of hydraulic gradient a-adpressure drop on perforated plates: 1. Investigate validity of applying the correlations madein this thesis to lates of different perforation patterns and with larger perforations. The factor, T, used in correlating f' vs. Re for various weir heights would be 3 of particular interest. 2, Investigate validity of applying the correlations madein this thess .i ts plates operating with higher sealsand greater liquid flow rates by adapting the apparatus to deliver greater vapor velocities. 3, Investigate validity of applying the correlations made in this thesis to plates using liquids andvapors with properties rrom the air-water different system used, 48 I i VIII s IE4, APPEDIX 49 4) Ao 0 0 O 0000000000000 0000000000 0 9 h3 09 a 9 . 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" 1Q ,n .- m L a0W 0 R X4 " os 4 o t4 HH H0 HH9 HH0 H 0H3 H 00H & 0 * 0 0 0 * 1-4 n 0 in 02 00 co a 0 00 0 000 0 o 4 W n3 X tc r P3 e Ol 0 ** 0$ 0e n0 H + 0 *.W HW Ur4, 8C9 40 r-i 9 I. .. ,"3- I x'pa~e lJ 40 W0 X O n 0 * a a 0* * 0 r- 1n qj 1p W M a 1^ 0 ssss !Q 0 0 r-4 d r- H *0 0 aT 91 -i a5 Q H8H8 /Ai * 54 L O0#Ob L b 6sto o 0a: L- 4 ! o909O 9 0o O(1O *0 0 00000000 : %. 4wr O0 I Lb to w L- L- M $ G 00 0o C>O o 9 0 · 9000000000 oo0 7OO a~ "4 0t · t ·r · 6r · · o 0 0 r)3 · 0o 0 PA to w 4t 3 n 0 w 0 0 Co 0 0 O0 O m f 0 04 r 044e .rd 4. %33 i 4 IoaOn g m a H#_ W o cn p-r *I n9 C P~~l: 1IS* i $:ac" o 9 ,- a0 * cN i n to to %n 0 f8 " C r o 1t U 9 L4 O 09 * 0000a o rC + t CoitX C9 W00b ~od Ca990 CQQ 00 0000000 41) C 3 O9 9 90 0 0 o 4A 44 p **90 000* s w aCa W a a 2 LBi= p3E~ ( U1~iS 0 n %Mnwo£ 4. 4. . -.0 0 4. 09 MI tA 0 LD-X3 s to w 0 #1 to w r4mooo -4 w v s4 q ri A A A w- W -0 t 3 *Soa !* 4 4 . .1 I 9 9 * * * , 9 * sw 90 a4 rc~ w 0 0 IV 0 f-4 m tD 02 0 3 - r- r4 r- r- r- 0000wwtto 49a9 9 0 09 eo O3~~ Xs e a w ee 9 3n 3 0"8999920 9 * r4 a0 I I alai uv/s 'leM. e .T o 55 0008800 O 000 0 0000000 o 4a oo8ooo 0 0000000 * , .4 , o 8 93 0M $o a. 4-4 ea n6 434 009 a f®O · · 0000000 ip Id 9g w 0 · iU: C4 L% * *0 0 ·q f %I o 6HHH24· 0 H0 H m A 4- 9~ 4bF Cw n .144-0 4 p , 0 * a * * 00000000 m 4 P 9 * * , *0 a W 0 4 ; tO40 v4 , 0 #I nl Ln u n , 4 01 I 4 (Pe% SA~OD vexe I , .. el f-I popo;xd o ;- cTH) ZIGI mz,/T-T X-------- 56 TABLZ A II S oMAR D PRESSUTE MaP DATA _DR PLATZ Run Air Rate V (/see.) ~~~·"cm~U~ 5.12 6,97 999 12,0 14,4 16.0 17.7 19,2 Average Plate oaloulated Plate Pressure Drop hO (in. Ho0) 0 2 Pressure Drop 0,02 0,02 0.014 0005 0.029 0,042 0.06 0,060 0.08 0.074 0,09 0,092 0*10 0,107 0,120 0,134 0.150 21,5 0.12 0.14 22,7 0O15 253,7 25,0 0,18 28,3 0o20 0*22 30.1 31,0 0,008 003 20,4 29*4 ho (in. 0,18 0.19 0.24 0,26 0.27 0.165 0.185 0.199 0,219 0,231 0,250 0,262 0,279 o 2 0) 57 t N o L-1 n -tp n r t n t 00 0 ob ;4 w 000000000 * , ,- 0 II P4 A02 A of 4 * * *4 4 19I CO ^ - A oHq (BnL 0000000a -O 4o t Osv e o a 00000 90 O O wo w 0202~ xmp HH 44ow ,4 020O aX m v-IH 0202 S s0 t1 ::1 C A b va ON O O C- 000 00000 c O 4 4 * 0 0 0 o0 to , 4 0oto a o i~ .4 -A 0C O0 0 I i"$ H .4 m 0s 00 0 00 0 0- 0 o* 0 O*0a OO 0 A9 OoatedIo44 I t9 R HHHHOO 4O a w0 w 0 0 S to cc QQ 0 4D q- Ig ' A F3 UP ;b H 000000 c0 o 04 04 0 6 4 W404 aO 000 3 0 - o 0 o 0 * 0 * 4 q pq H s r-4 Pd r Pi Q O a 4 8 Q a 0 es e 0 ow 0 e o 2 rdA 44-.-P. 1o~ )A 0 N 34 00 0 O A 44 4C O 0 n 01 aD o H* * mcoOtO 4C4 r O W 0 dQ * . * * 4 00CCOQ 4*4404444o4O CQ Q CcQ / H 0 H B IW&iZ/ 0 0t 119 JTIPA '"I?/1 I I - do 58 i 4 A eoi 00(D V-j W - tD S L- ,* ,Pi n n3n 0 O0 te0 , > So 4i- * n 0 U CQ HowI S IP 42 +0 O O oo m0 CO -P n n 00 O 0 0 H .4A 0 Ve4 411s -g~ 94 1~0 CQ* rH 3 o 8 8 0.- 8 8* - aS 8 O* p *J ~~~.~~o~~~~e$g 19 (ar~9 A9 A 002 w HH H _ P P 8- I a I 0 0:1t pO CQI 4)0 3 I f~e P=~~~ 03 X 8 c8 0 8 * I> r-4 -q ri* oti 0 8 0 8 0 to 0w r-A r-i *--I r-4 r4 0 r-q r1i-4 rk 0 e0 t-I 0 r-4 a H1i 8 fj0 rie 0 e--l r-4 0 0 f8 *4 H3 ps3 ¢mi~ Ea _# 8 CQ CQ C-I 0 ce 04 8 r-i r-t FI 1j* 4 ?-I T-4 f*i o-4 I r ? 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I 4 'DJ_ 02 0a 02 4D i I I 0 0, * H f-4 fC * t) * CA Q CQ 0 n H -i3 ii V-1 f1 HHi H1 p t s V) HH P 0 04 A Uo O0 $ 99 I I~ A4 0 g* g0 C * 0 0 4 t * a v0 0 V4 0 0co *14 WZ II 0 M 0 p E; 0 ., Id -r3 10 pl!Q P%# E e g egO * *3 * %ra Oodlr O @* ts n3 0 1-3 * 0 *v CcO _44 - f- * no * 0 ee + e e e Q-H q *0 e g 4, *r 00 , 0 10 ea g 4 e. q CQ Q a 4' Im -t w 0 P 0 os 0 §t ct · 4o h 64 63 88W 043 0 X % 3C tO cO *5; ip 86X8 az · b *Sa t 'I, 9~W~ I : m 0 0 -P ~~~~~~~~~~0 0 I H tqtt4 61 t9 O 0eOC* I P4.--- c * P4,P- :1 0 tA02 r ,E - o tV OOa# - -C 0 04-0Q2 J Q n· o 0 HHHHHI r -i H H r H HH r-3 H4 r 4 i 0 Hn M - M!C n oU 0cton n 8n n Nt* . n9 0 0* 0 '- oP4 -I * 4 as totoiU') a*d * 00 0 4 HHHH H-I H HH r-HH r P4--.' 0 p o0 C- w TOs ::s W-5 w* n 4n n0 r iHHH H Qb n 0 0 -4 r H a * GiO 0 t v D* lq 0 a 4HH H Hril 4 H4HHH rHHH kh NA P4) n0 000 nLo00n 04 * 0 0 0 0 0 :s 04 0 0 co .~l -4 o 00M 0 0 * Wi0 O * 0 000 to t000 000 0 to 8 Q C C,* C-0 00, 1 i X X CM - - 0 0 0t t t 000 0000000 000000 0 0 o 4-4) 0 * to Ca O£: O b 0000 , C -- - l- a 3 0 4 44* Q tO on 0 S 4 oo 1 0. * b iF- in n o4 60O * 4 40 4 4, \·~ 0E o *40 * * W C0 £ ~20 Q 0s 444 0O0 O* n s O S4 p4 L.- U C s I t: < )QO a a C.O on3 0 o a S to 'U 0 a a, e 0 a i 4 Q ;4 t i to CO 4 A~ ®D 4 0 00 M If 0 94 * *0o · · o 0 o 4 - @ H , 00 0O 0t c4a 4-4 9 J i a ~S*8*93ss k p4 CH~ I T9 iD~~ssI~~·j IMa Of," I O a A SsCQ .1/ / ,~~~g to0ar1 a5 ) '020 0 04 a;v ,,/' M O *<~2 0 0I to o -- 0%a I m 0 'o cxto * 4 r- I 0 Q Q 8· a HHH rOt:3 r-i T A Ca ·Q Ca ?td + no Ototo J 4 $00un aa * H HHl ld 00 -J r-i r- f- - ot - r 0 i - HH H QHA HH 4 r -. ~-# 1 0 00R 4) A H H Qm 4nO-toL sv2 a >3 l.- kh P4 0 mmj -P.s V ~~AL I e1(Id 4 0 4)z 0- 3 p2 S w3 ab o ca o o 00000* 0 0 a 4) 0 0 0 9.4 i i .4 mii !- $4 Pwd o o C4 w .0 e3a to 000 L- L- t *- w M *O k00000 a cz1 oX p o- 0 0 000 0 O0 000* 00 00 0 ooooooo og VI 0 4q hi eaor ~ r4FF4 0 t (D P4D 4)S H4) a. 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Sle Calculations Sample calculations will be arried through for t types of alculations: 1 radient Correlation Hydraulic 2, Pressure Drop Correlation 1, Hydraulic Gradient Correlation Data from Run E-2 are used for the alculations 21 ga rh Z ft vf Where (1) N = 0.22 = Ah 24 00092 24 o = 32.2 ft./sec, = i =b+2I U f L b = 1, 125 ft. 2 bL I, 2he followings = 12 (2) l.22) 12 0,203 ft. rh =1.125 0203) m 1.125 + 2(o.203) = 0.149 ft. (60) (7,46) Lcf (60) (7,46) (0.203) (1/3) 5. plt = 0 t. (j2) (.0-92) (o0516)2 = 00663 32,2) (0,149) (5.o) (3) 0.516ft./see. h - D 0,12 1.22 - 0.12 - f'T - 0.109 0.00723 rh f Pf ~f p 62,4 = 3 Af i(5) 3 20.8 lb,it. 1 (6) 0,000672 t 0.000224 o lb. /ft-se,. 3 t _ (0,.149) (0,516) Re(0.000224) (20.8) 7,14 x 03 2, Pressure Drop Correlation Data from Run E-2 are used in the following calculations: VP X P, A~Pa vp - 27,4 x 42_3 P 0,936 x 407 -Vp= 30,5 ft,/seco = 0.0o Y P01 =0,04 (11) P 72,8 62.4 x 0125 67 nt = 0.37 in. H20 hf = ho+ ht + hay h 1 ho (12) - 0.37 - o.57 = 044 in. E20 (experimental plate pressure drop) ho ,=a VP o (10) o.o000047 (30.5)2 ho = 0.44 in. 20 (calculated plate pressure drop) B, Plate Leveling Procedure The following procedure was employedto insure proper leveling of the perforated plate and zeroing of the manometerchart: 1. Hydrostatic head manometerlines to the taps in the inlet and exit calming sections were purged of air by forcing water through them from the taps. 2. Theperforated area of the plate was blanked off with a piece of sheet metal. 3. An exit weir was installed and water run onto the plate. Water flow was adjusted to be just sufficient weir level. to maintain If leakage under the sheet metal was excessive, air was admitted to the air chamberto build up pressure and stop the leakage. 4. The liquid levels in the upstream and downstream calming sections were measured on the plate and if found unequal, the plate level was adjusted by leveling screws on the legs of the apparatus. 68 5* The manometer sheet was adjusted so that the manometers for the upstream and downstreamcalming sections both read the same, the reading being that measured on the plate. Using this procedure, the plate ends could be leveled to within plus or minus 1 mm# *. Calibration of Flomesters 1. Water Rate Measurement The orifice in the water line was calibrated by direct measurement. The globe valve in the water line was set, the system was allowed to cometo equilibrium, and the water orifice manometerrecorded while water was collected for a measured time interval. The water collected was weighed and the water rate calculated in gallons per minute. This procedure was repeated for various flow rates andthe results plotted to obtain a curve of water rate vs. the water orifice manometerreading. 2. Air Rate Measurement Pitot tube traverses were madeacross the air duct for several air rates. rom these traverses, the air rates were determined by means of graphical integration. The results were used to check the validity of using the standard orifice equation for non-compressible flow. The use of this equation was found to be satisfactory using the experimental constant: C = 00o6 A curve of air rate, in cubic feet per sec., vs. the air rate manometerreading was plotted using the orifice equation. D, Nomenclature AP= Total perforation area (ft.2 ) A8 Area of perforated section (t, ), - Platewidth (ft), b Dp 2 - F - Perforation diameter (in.). riction head loss A h Modified frictionfactor - V (ft. of liquid). 24 2g rh Z Vf ~G = g Volumetric flow rate (gpm/ft, of plate width) Gravitational A h N constant (32,2 ft. lbs. mass/see, 2 lbs. force), Hydraulic Gradient across plate (in, of liquid), h Hydrostatic head (in, hay of liquid). Average hydrostatic head in bubbling section (in, of liquid), hc D aownstream calming section hydrostatic head (in ho Pressure drop through perforations (in, of liquid), ht; Pressure drop due to surface tension effects (in. of liquid). hT~ = Total plate pressure drop (in. of liquid). La = Calculated foam heigh N Pa t e of liquid)a (ft.)h Length of bubbling section (ft,), _ Atmospheric pressure (in. of H20), Ps- Static pressure upstream of air orifice (in. of H20) Qe Volumetric flow rate of air (efm)o 70 rh Hydraulic radius (ft.), Re' - ModifiedReynolds number orrelation factor -- _ h c - Dp T = Vf = Foam velocity (ft/seec.). Vp - Velocity of vapor based on total hole area (ft./see.), Factor r r m rh V in standard orificeequation. /3 Surface tension of liquid (dynes/er,). Foam viscosity (lb./ft. sec.), Liquid viscosity (lb./ft. sec.), 1 = 3 ) oam density (lb,/ft. f /0 Liquid density (lb./ftA,3) Vapor density (lb,/ft 3 ). Density factor effective aerated density clear liquid- density A] 71 2. Literature Citations 1. Ghrmleyt, . L., M.,SThesis, Chem Eng°,MI.T. (1947). 2. Gunaness,R, C., end Baker, 13941400 (1938). 3. Hutchinson, . G., Ind. n:g. Ohem., M. H., Buren, A. G, end Miller, E3 B. P., "Aerated Flow Principal Applied to Sieve Plates," unpublished (1949) 4. Kirschbaum and Andrews, . Inst. Petroleum Tech., 803-20, (1936), 5, Kirschbaum, B., "Distillation and Rectification," Chem. Publishing Co., Inc., New York (1948). 6. Klein, . H., S.D. , 264-76, Thesis, Chem. ng., M.I.T. (1950). 7. McGo1driok, 8. Robinson and Gilliland, "lemsnts of FractionalDistillation," 4th Ed,, McGraw-Hill Book o.,,Inc., New York (1950). 9. Seuren, 10 . E.1,B.S. Thesis, hem. ng., M.I.T. (1950). . R., M.S. Thesis, Chem.Eng.,M.I.T. (1947). Weber, H. O.,"Thermodynamics for Chemical Engineers," John Wiley & Sons, Inc., New York (1939).