ANALYTICAL REPORT 1 2 3

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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: (708)534-5200
TestAmerica Job ID: 500-107612-1
Client Project/Site: UW Stout - 136039
For:
Short Elliott Hendrickson, Inc. dba SEH
10 North Bridge Street
Chippewa Falls, Wisconsin 54729-3374
Attn: Mr. Brian L. Kent
Authorized for release by:
2/23/2016 12:52:41 PM
Sandie Fredrick, Project Manager II
(920)261-1660
sandie.fredrick@testamericainc.com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
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Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
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Page 2 of 29
TestAmerica Chicago
2/23/2016
Case Narrative
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
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Job ID: 500-107612-1
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Laboratory: TestAmerica Chicago
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Narrative
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Job Narrative
500-107612-1
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Comments
No additional comments.
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Receipt
The samples were received on 2/16/2016 10:20 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was -1.4º C.
Receipt Exceptions
Bottle for sample 1 has time of 928, logged per COC. Sample 11 listed twice on COC. Received sample 12 with ID of
JSH16-3F300D-FNTN, logged per COC.
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Page 3 of 29
TestAmerica Chicago
2/23/2016
Detection Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
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Client Sample ID: HH10-4F400G-FNTN
Analyte
Lead
Result Qualifier
7.9 B
Lab Sample ID: 500-107612-1
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: HH10-1F165-FNTN
Analyte
Lead
Result Qualifier
20 B
Result Qualifier
20 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
1.2 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
3.4 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
2.7 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
0.93 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
0.32 J B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
2.2 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
0.79 B
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-9
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: JHSA15-3F300J-FNTN
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-8
Client Sample ID: JT16A-2F201J-FNTN
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-7
Client Sample ID: MH17-2F201N-FNTN
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-6
Client Sample ID: AA19-3F300B-FNTN
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-5
Client Sample ID: VR7-3F300A-FNTN
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-4
Client Sample ID: CFSC8-1F100-FNTN
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-3
Client Sample ID: RSSL12-5F500-FNTN
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-2
Client Sample ID: HH10-1F165-FNTN DUP
Analyte
Lead
1
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-10
RL
0.50
Client Sample ID: MLH11-3F300-FNTN
MDL Unit
0.16 ug/L
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-11
This Detection Summary does not include radiochemical test results.
TestAmerica Chicago
Page 4 of 29
2/23/2016
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Detection Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
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Client Sample ID: MLH11-3F300-FNTN (Continued)
Analyte
Lead
Result Qualifier
0.97 B
RL
0.50
Lab Sample ID: 500-107612-11
MDL Unit
0.16 ug/L
Client Sample ID: JHSA16-3F300D-FNTN
Analyte
Lead
Result Qualifier
0.55 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
0.66 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
0.49 J B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
6.9 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
0.78 B
Result Qualifier
0.67 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
1.0 B
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
9.0
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
2.6
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-19
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: MPC47-2F220-TAPCW
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-18
Client Sample ID: MSC45-2F234-TAPCW
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-17
Client Sample ID: MSC45-2F221-TAPCW
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-16
Client Sample ID: MSC45-2F221-TAPHW DUP
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-15
Client Sample ID: MSC45-2F221-TAPHW
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-14
Client Sample ID: A18-3F301-FNTN
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-13
Client Sample ID: FH2-3F300B-FNTN
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-12
Client Sample ID: CT46-2F200K-FNTN
Analyte
Lead
1
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-20
RL
0.50
Client Sample ID: MPC47-2F208-TAPCW
MDL Unit
0.16 ug/L
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-21
This Detection Summary does not include radiochemical test results.
TestAmerica Chicago
Page 5 of 29
2/23/2016
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Detection Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
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Client Sample ID: MPC47-2F208-TAPCW (Continued)
Analyte
Lead
Result Qualifier
37
RL
0.50
Lab Sample ID: 500-107612-21
MDL Unit
0.16 ug/L
Client Sample ID: MPC47-2F220-TAPHW
Analyte
Lead
Result Qualifier
1.6
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
14
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
22
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
14
RL
0.50
MDL Unit
0.16 ug/L
Result Qualifier
2.3
Result Qualifier
0.82
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-26
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: SHS48-1F117-TAPCW DUP
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-25
Client Sample ID: SHS48-1F117-TAPCW
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-24
Client Sample ID: MPC47-B6-TAPCW DUP
Analyte
Lead
Prep Type
Total/NA
Lab Sample ID: 500-107612-23
Client Sample ID: MPC47-B6-TAPCW
Analyte
Lead
Dil Fac D Method
1
200.8
Lab Sample ID: 500-107612-22
Client Sample ID: MPC47-2F208-TAPHW
Analyte
Lead
1
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-27
RL
0.50
Client Sample ID: MSC45-1F100N-BTTL FLL
MDL Unit
0.16 ug/L
Dil Fac D Method
1
200.8
Prep Type
Total/NA
Lab Sample ID: 500-107612-28
No Detections.
Client Sample ID: MSC45-2F200C-BTTL FLL
Lab Sample ID: 500-107612-29
No Detections.
Client Sample ID: SFC5-2F202-BTTL FLL
Lab Sample ID: 500-107612-30
No Detections.
Client Sample ID: SFC5-1F28-BBTL FLL
Lab Sample ID: 500-107612-31
No Detections.
This Detection Summary does not include radiochemical test results.
TestAmerica Chicago
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2/23/2016
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Method Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
Method
200.8
TestAmerica Job ID: 500-107612-1
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Method Description
Metals (ICP/MS)
Protocol
EPA
Laboratory
TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
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Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
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TestAmerica Chicago
Page 7 of 29
2/23/2016
Sample Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
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2
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Lab Sample ID
500-107612-1
500-107612-2
500-107612-3
Client Sample ID
HH10-4F400G-FNTN
HH10-1F165-FNTN
HH10-1F165-FNTN DUP
Matrix
Water
Water
Water
Collected
Received
02/13/16 09:20 02/16/16 10:20
02/13/16 09:37 02/16/16 10:20
02/13/16 09:37 02/16/16 10:20
500-107612-4
500-107612-5
500-107612-6
RSSL12-5F500-FNTN
CFSC8-1F100-FNTN
VR7-3F300A-FNTN
Water
Water
Water
02/13/16 09:52 02/16/16 10:20
02/13/16 10:09 02/16/16 10:20
02/13/16 10:25 02/16/16 10:20
500-107612-7
500-107612-8
AA19-3F300B-FNTN
MH17-2F201N-FNTN
Water
Water
02/13/16 08:32 02/16/16 10:20
02/13/16 08:41 02/16/16 10:20
500-107612-9
JT16A-2F201J-FNTN
Water
02/13/16 08:49 02/16/16 10:20
500-107612-10
500-107612-11
JHSA15-3F300J-FNTN
MLH11-3F300-FNTN
Water
Water
02/13/16 09:06 02/16/16 10:20
02/13/16 10:37 02/16/16 10:20
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500-107612-12
JHSA16-3F300D-FNTN
Water
02/13/16 09:00 02/16/16 10:20
500-107612-13
500-107612-14
CT46-2F200K-FNTN
FH2-3F300B-FNTN
Water
Water
02/13/16 10:47 02/16/16 10:20
02/13/16 10:56 02/16/16 10:20
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500-107612-15
A18-3F301-FNTN
Water
02/13/16 11:13 02/16/16 10:20
500-107612-16
500-107612-17
500-107612-18
MSC45-2F221-TAPHW
MSC45-2F221-TAPHW DUP
MSC45-2F221-TAPCW
Water
Water
Water
02/13/16 11:32 02/16/16 10:20
02/13/16 11:32 02/16/16 10:20
02/13/16 11:37 02/16/16 10:20
500-107612-19
500-107612-20
500-107612-21
MSC45-2F234-TAPCW
MPC47-2F220-TAPCW
MPC47-2F208-TAPCW
Water
Water
Water
02/13/16 11:45 02/16/16 10:20
02/13/16 12:07 02/16/16 10:20
02/13/16 12:19 02/16/16 10:20
500-107612-22
500-107612-23
500-107612-24
MPC47-2F220-TAPHW
MPC47-2F208-TAPHW
MPC47-B6-TAPCW
Water
Water
Water
02/13/16 12:10 02/16/16 10:20
02/13/16 12:20 02/16/16 10:20
02/13/16 12:40 02/16/16 10:20
500-107612-25
500-107612-26
500-107612-27
MPC47-B6-TAPCW DUP
SHS48-1F117-TAPCW
SHS48-1F117-TAPCW DUP
Water
Water
Water
02/13/16 12:40 02/16/16 10:20
02/13/16 13:09 02/16/16 10:20
02/13/16 13:09 02/16/16 10:20
500-107612-28
500-107612-29
500-107612-30
MSC45-1F100N-BTTL FLL
MSC45-2F200C-BTTL FLL
SFC5-2F202-BTTL FLL
Water
Water
Water
02/13/16 14:08 02/16/16 10:20
02/13/16 14:16 02/16/16 10:20
02/13/16 14:32 02/16/16 10:20
500-107612-31
SFC5-1F28-BBTL FLL
Water
02/13/16 14:39 02/16/16 10:20
TestAmerica Chicago
Page 8 of 29
2/23/2016
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Client Sample Results
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: HH10-4F400G-FNTN
Lab Sample ID: 500-107612-1
Date Collected: 02/13/16 09:20
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
7.9 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: HH10-1F165-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 13:35
Dil Fac
1
Lab Sample ID: 500-107612-2
Date Collected: 02/13/16 09:37
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
20 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: HH10-1F165-FNTN DUP
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 13:39
Dil Fac
1
Lab Sample ID: 500-107612-3
Date Collected: 02/13/16 09:37
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
20 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: RSSL12-5F500-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 13:43
Dil Fac
1
Lab Sample ID: 500-107612-4
Date Collected: 02/13/16 09:52
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
1.2 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: CFSC8-1F100-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 13:58
Dil Fac
1
Lab Sample ID: 500-107612-5
Date Collected: 02/13/16 10:09
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
3.4 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: VR7-3F300A-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:09
Dil Fac
1
Lab Sample ID: 500-107612-6
Date Collected: 02/13/16 10:25
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
2.7 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: AA19-3F300B-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:13
Dil Fac
1
Lab Sample ID: 500-107612-7
Date Collected: 02/13/16 08:32
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
5
6
7
8
Method: 200.8 - Metals (ICP/MS)
Lead
3
4
Method: 200.8 - Metals (ICP/MS)
Lead
1
Result Qualifier
0.93 B
RL
0.50
MDL Unit
0.16 ug/L
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:17
Dil Fac
1
TestAmerica Chicago
Page 9 of 29
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Client Sample Results
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: MH17-2F201N-FNTN
Lab Sample ID: 500-107612-8
Date Collected: 02/13/16 08:41
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
0.32 J B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: JT16A-2F201J-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:20
Dil Fac
1
Lab Sample ID: 500-107612-9
Date Collected: 02/13/16 08:49
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
2.2 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: JHSA15-3F300J-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:24
Dil Fac
1
Lab Sample ID: 500-107612-10
Date Collected: 02/13/16 09:06
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
0.79 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: MLH11-3F300-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:28
Dil Fac
1
Lab Sample ID: 500-107612-11
Date Collected: 02/13/16 10:37
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
0.97 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: JHSA16-3F300D-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:32
Dil Fac
1
Lab Sample ID: 500-107612-12
Date Collected: 02/13/16 09:00
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
0.55 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: CT46-2F200K-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:35
Dil Fac
1
Lab Sample ID: 500-107612-13
Date Collected: 02/13/16 10:47
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
0.66 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: FH2-3F300B-FNTN
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 14:39
Dil Fac
1
Lab Sample ID: 500-107612-14
Date Collected: 02/13/16 10:56
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
5
6
7
8
Method: 200.8 - Metals (ICP/MS)
Lead
3
4
Method: 200.8 - Metals (ICP/MS)
Lead
1
Result Qualifier
0.49 J B
RL
0.50
MDL Unit
0.16 ug/L
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 15:02
Dil Fac
1
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Page 10 of 29
2/23/2016
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11
12
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14
Client Sample Results
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: A18-3F301-FNTN
Lab Sample ID: 500-107612-15
Date Collected: 02/13/16 11:13
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
RL
0.50
6.9 B
MDL Unit
0.16 ug/L
Client Sample ID: MSC45-2F221-TAPHW
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 15:05
Dil Fac
1
Lab Sample ID: 500-107612-16
Date Collected: 02/13/16 11:32
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
RL
0.50
0.78 B
MDL Unit
0.16 ug/L
Client Sample ID: MSC45-2F221-TAPHW DUP
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 15:09
Dil Fac
1
Lab Sample ID: 500-107612-17
Date Collected: 02/13/16 11:32
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
0.67 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: MSC45-2F221-TAPCW
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 15:13
Dil Fac
1
Lab Sample ID: 500-107612-18
Date Collected: 02/13/16 11:37
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
1.0 B
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: MSC45-2F234-TAPCW
D
Prepared
Analyzed
02/17/16 11:00 02/17/16 15:17
Dil Fac
1
Lab Sample ID: 500-107612-19
Date Collected: 02/13/16 11:45
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
9.0
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: MPC47-2F220-TAPCW
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 12:38
Dil Fac
1
Lab Sample ID: 500-107612-20
Date Collected: 02/13/16 12:07
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
2.6
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: MPC47-2F208-TAPCW
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 12:53
Dil Fac
1
Lab Sample ID: 500-107612-21
Date Collected: 02/13/16 12:19
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
5
6
7
8
Method: 200.8 - Metals (ICP/MS)
Lead
3
4
Method: 200.8 - Metals (ICP/MS)
Lead
1
Result Qualifier
37
RL
0.50
MDL Unit
0.16 ug/L
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 12:57
Dil Fac
1
TestAmerica Chicago
Page 11 of 29
2/23/2016
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11
12
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14
Client Sample Results
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: MPC47-2F220-TAPHW
Lab Sample ID: 500-107612-22
Date Collected: 02/13/16 12:10
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
RL
0.50
1.6
MDL Unit
0.16 ug/L
Client Sample ID: MPC47-2F208-TAPHW
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:01
Dil Fac
1
Lab Sample ID: 500-107612-23
Date Collected: 02/13/16 12:20
Date Received: 02/16/16 10:20
Matrix: Water
Analyte
Result Qualifier
RL
0.50
14
MDL Unit
0.16 ug/L
Client Sample ID: MPC47-B6-TAPCW
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:16
Dil Fac
1
Lab Sample ID: 500-107612-24
Date Collected: 02/13/16 12:40
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
RL
0.50
22
MDL Unit
0.16 ug/L
Client Sample ID: MPC47-B6-TAPCW DUP
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:31
Dil Fac
1
Lab Sample ID: 500-107612-25
Date Collected: 02/13/16 12:40
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
RL
0.50
14
MDL Unit
0.16 ug/L
Client Sample ID: SHS48-1F117-TAPCW
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:35
Dil Fac
1
Lab Sample ID: 500-107612-26
Date Collected: 02/13/16 13:09
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
RL
0.50
2.3
MDL Unit
0.16 ug/L
Client Sample ID: SHS48-1F117-TAPCW DUP
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:39
Dil Fac
1
Lab Sample ID: 500-107612-27
Date Collected: 02/13/16 13:09
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
Result Qualifier
0.82
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: MSC45-1F100N-BTTL FLL
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:42
Dil Fac
1
Lab Sample ID: 500-107612-28
Date Collected: 02/13/16 14:08
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
5
6
7
8
Method: 200.8 - Metals (ICP/MS)
Lead
3
4
Method: 200.8 - Metals (ICP/MS)
Lead
1
Result Qualifier
<0.16
RL
0.50
MDL Unit
0.16 ug/L
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:46
Dil Fac
1
TestAmerica Chicago
Page 12 of 29
2/23/2016
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10
11
12
13
14
Client Sample Results
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: MSC45-2F200C-BTTL FLL
Lab Sample ID: 500-107612-29
Date Collected: 02/13/16 14:16
Date Received: 02/16/16 10:20
Matrix: Water
Result Qualifier
<0.16
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: SFC5-2F202-BTTL FLL
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 13:50
Dil Fac
1
Lab Sample ID: 500-107612-30
Date Collected: 02/13/16 14:32
Date Received: 02/16/16 10:20
Matrix: Water
Result Qualifier
<0.16
RL
0.50
MDL Unit
0.16 ug/L
Client Sample ID: SFC5-1F28-BBTL FLL
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 14:01
Dil Fac
1
Lab Sample ID: 500-107612-31
Date Collected: 02/13/16 14:39
Date Received: 02/16/16 10:20
Matrix: Water
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
5
6
7
8
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
3
4
Method: 200.8 - Metals (ICP/MS)
Analyte
Lead
1
Result Qualifier
<0.16
RL
0.50
MDL Unit
0.16 ug/L
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 14:05
Dil Fac
1
9
10
11
12
13
14
TestAmerica Chicago
Page 13 of 29
2/23/2016
Definitions/Glossary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Qualifiers
3
Metals
Qualifier
B
F5
J
1
4
Qualifier Description
Compound was found in the blank and sample.
Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL. The data are considered valid because the
absolute difference is less than the RL.
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
5
6
7
Glossary
Abbreviation
¤
%R
CFL
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
CNF
DER
Contains no Free Liquid
Duplicate error ratio (normalized absolute difference)
Dil Fac
DL, RA, RE, IN
DLC
MDA
EDL
MDC
Dilution Factor
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
Decision level concentration
Minimum detectable activity
Estimated Detection Limit
Minimum detectable concentration
MDL
ML
NC
ND
PQL
QC
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not detected at the reporting limit (or MDL or EDL if shown)
Practical Quantitation Limit
Quality Control
RER
RL
RPD
TEF
TEQ
Relative error ratio
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
8
9
10
11
12
13
14
TestAmerica Chicago
Page 14 of 29
2/23/2016
QC Association Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
1
2
Metals
3
Prep Batch: 323203
Lab Sample ID
500-107612-1
500-107612-2
500-107612-3
Client Sample ID
HH10-4F400G-FNTN
HH10-1F165-FNTN
HH10-1F165-FNTN DUP
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Water
Method
200.8
200.8
200.8
Prep Batch
500-107612-3 DU
500-107612-3 MS
500-107612-4
HH10-1F165-FNTN DUP
HH10-1F165-FNTN DUP
RSSL12-5F500-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
500-107612-5
500-107612-6
CFSC8-1F100-FNTN
VR7-3F300A-FNTN
Total/NA
Total/NA
Water
Water
200.8
200.8
500-107612-7
AA19-3F300B-FNTN
Total/NA
Water
200.8
500-107612-8
500-107612-9
500-107612-10
MH17-2F201N-FNTN
JT16A-2F201J-FNTN
JHSA15-3F300J-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
500-107612-11
500-107612-12
500-107612-13
MLH11-3F300-FNTN
JHSA16-3F300D-FNTN
CT46-2F200K-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
500-107612-13 DU
500-107612-13 MS
500-107612-14
CT46-2F200K-FNTN
CT46-2F200K-FNTN
FH2-3F300B-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
500-107612-15
500-107612-16
500-107612-17
A18-3F301-FNTN
MSC45-2F221-TAPHW
MSC45-2F221-TAPHW DUP
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
500-107612-18
LCS 500-323203/2-A
MSC45-2F221-TAPCW
Lab Control Sample
Total/NA
Total/NA
Water
Water
200.8
200.8
MB 500-323203/1-A
Method Blank
Total/NA
Water
200.8
Lab Sample ID
500-107612-1
500-107612-2
Client Sample ID
HH10-4F400G-FNTN
HH10-1F165-FNTN
Prep Type
Total/NA
Total/NA
Matrix
Water
Water
Method
200.8
200.8
500-107612-3
HH10-1F165-FNTN DUP
Total/NA
Water
200.8
323203
500-107612-3 DU
HH10-1F165-FNTN DUP
Total/NA
Water
200.8
323203
500-107612-3 MS
500-107612-4
HH10-1F165-FNTN DUP
RSSL12-5F500-FNTN
Total/NA
Total/NA
Water
Water
200.8
200.8
323203
323203
500-107612-5
500-107612-6
500-107612-7
CFSC8-1F100-FNTN
VR7-3F300A-FNTN
AA19-3F300B-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323203
323203
323203
500-107612-8
500-107612-9
500-107612-10
MH17-2F201N-FNTN
JT16A-2F201J-FNTN
JHSA15-3F300J-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323203
323203
323203
500-107612-11
500-107612-12
500-107612-13
MLH11-3F300-FNTN
JHSA16-3F300D-FNTN
CT46-2F200K-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323203
323203
323203
500-107612-13 DU
500-107612-13 MS
500-107612-14
CT46-2F200K-FNTN
CT46-2F200K-FNTN
FH2-3F300B-FNTN
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323203
323203
323203
500-107612-15
500-107612-16
500-107612-17
A18-3F301-FNTN
MSC45-2F221-TAPHW
MSC45-2F221-TAPHW DUP
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323203
323203
323203
500-107612-18
LCS 500-323203/2-A
MSC45-2F221-TAPCW
Lab Control Sample
Total/NA
Total/NA
Water
Water
200.8
200.8
323203
323203
MB 500-323203/1-A
Method Blank
Total/NA
Water
200.8
323203
5
6
7
8
9
10
11
12
13
14
Analysis Batch: 323267
Prep Batch
323203
323203
TestAmerica Chicago
Page 15 of 29
4
2/23/2016
QC Association Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
1
2
Prep Batch: 323395
Prep Batch
3
Lab Sample ID
500-107612-19
500-107612-19 DU
500-107612-19 MS
Client Sample ID
MSC45-2F234-TAPCW
MSC45-2F234-TAPCW
MSC45-2F234-TAPCW
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Water
Method
200.8
200.8
200.8
500-107612-20
500-107612-21
MPC47-2F220-TAPCW
MPC47-2F208-TAPCW
Total/NA
Total/NA
Water
Water
200.8
200.8
500-107612-22
MPC47-2F220-TAPHW
Total/NA
Water
200.8
6
500-107612-23
500-107612-23 DU
MPC47-2F208-TAPHW
MPC47-2F208-TAPHW
Total/NA
Total/NA
Water
Water
200.8
200.8
7
500-107612-23 MS
MPC47-2F208-TAPHW
Total/NA
Water
200.8
500-107612-24
500-107612-25
MPC47-B6-TAPCW
MPC47-B6-TAPCW DUP
Total/NA
Total/NA
Water
Water
200.8
200.8
8
500-107612-26
SHS48-1F117-TAPCW
Total/NA
Water
200.8
500-107612-27
SHS48-1F117-TAPCW DUP
Total/NA
Water
200.8
9
500-107612-28
500-107612-29
MSC45-1F100N-BTTL FLL
MSC45-2F200C-BTTL FLL
Total/NA
Total/NA
Water
Water
200.8
200.8
10
500-107612-30
500-107612-31
LCS 500-323395/2-A
SFC5-2F202-BTTL FLL
SFC5-1F28-BBTL FLL
Lab Control Sample
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
11
MB 500-323395/1-A
Method Blank
Total/NA
Water
200.8
4
5
12
13
Analysis Batch: 323537
Lab Sample ID
500-107612-19
500-107612-19 DU
500-107612-19 MS
Client Sample ID
MSC45-2F234-TAPCW
MSC45-2F234-TAPCW
MSC45-2F234-TAPCW
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Water
Method
200.8
200.8
200.8
Prep Batch
323395
323395
323395
500-107612-20
500-107612-21
500-107612-22
MPC47-2F220-TAPCW
MPC47-2F208-TAPCW
MPC47-2F220-TAPHW
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323395
323395
323395
500-107612-23
500-107612-23 DU
500-107612-23 MS
MPC47-2F208-TAPHW
MPC47-2F208-TAPHW
MPC47-2F208-TAPHW
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323395
323395
323395
500-107612-24
500-107612-25
500-107612-26
MPC47-B6-TAPCW
MPC47-B6-TAPCW DUP
SHS48-1F117-TAPCW
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323395
323395
323395
500-107612-27
500-107612-28
500-107612-29
SHS48-1F117-TAPCW DUP
MSC45-1F100N-BTTL FLL
MSC45-2F200C-BTTL FLL
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323395
323395
323395
500-107612-30
500-107612-31
LCS 500-323395/2-A
SFC5-2F202-BTTL FLL
SFC5-1F28-BBTL FLL
Lab Control Sample
Total/NA
Total/NA
Total/NA
Water
Water
Water
200.8
200.8
200.8
323395
323395
323395
MB 500-323395/1-A
Method Blank
Total/NA
Water
200.8
323395
TestAmerica Chicago
Page 16 of 29
2/23/2016
14
QC Sample Results
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Method: 200.8 - Metals (ICP/MS)
3
Lab Sample ID: MB 500-323203/1-A
Matrix: Water
Analysis Batch: 323267
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 323203
MB MB
Result Qualifier
0.173 J
Analyte
Lead
RL
0.50
MDL Unit
0.16 ug/L
Lab Sample ID: LCS 500-323203/2-A
Matrix: Water
Analysis Batch: 323267
Added
100
Result Qualifier
108
Sample Sample
Result Qualifier
20 B
Spike
Added
100
MS MS
Result Qualifier
125
Sample Sample
Result Qualifier
0.66 B
Spike
Added
100
MS MS
Result Qualifier
109
Unit
ug/L
D
Unit
ug/L
D
Unit
ug/L
D
Sample Sample
Result Qualifier
20 B
DU DU
Result Qualifier
19.5
Unit
ug/L
%Rec
105
%Rec
108
Sample Sample
Result Qualifier
0.66 B
DU DU
Result Qualifier
0.534 F5
Unit
ug/L
%Rec.
Limits
70 - 130
RPD
4
RPD
Limit
20
RPD
21
RPD
Limit
20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 323395
MB MB
Result Qualifier
<0.16
RL
0.50
MDL Unit
0.16 ug/L
D
Prepared
Analyzed
02/18/16 11:10 02/18/16 12:27
Dil Fac
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 323395
Spike
Added
100
LCS LCS
Result Qualifier
101
Unit
ug/L
D
%Rec
101
%Rec.
Limits
85 - 115
TestAmerica Chicago
Page 17 of 29
5
6
7
8
10
11
12
%Rec.
Limits
70 - 130
D
4
9
Client Sample ID: CT46-2F200K-FNTN
Prep Type: Total/NA
Prep Batch: 323203
Lab Sample ID: LCS 500-323395/2-A
Matrix: Water
Analysis Batch: 323537
Analyte
Lead
Limits
85 - 115
D
Lab Sample ID: MB 500-323395/1-A
Matrix: Water
Analysis Batch: 323537
Analyte
Lead
%Rec
108
Client Sample ID: HH10-1F165-FNTN DUP
Prep Type: Total/NA
Prep Batch: 323203
Lab Sample ID: 500-107612-13 DU
Matrix: Water
Analysis Batch: 323267
Analyte
Lead
%Rec.
Client Sample ID: CT46-2F200K-FNTN
Prep Type: Total/NA
Prep Batch: 323203
Lab Sample ID: 500-107612-3 DU
Matrix: Water
Analysis Batch: 323267
Analyte
Lead
Dil Fac
1
Client Sample ID: HH10-1F165-FNTN DUP
Prep Type: Total/NA
Prep Batch: 323203
Lab Sample ID: 500-107612-13 MS
Matrix: Water
Analysis Batch: 323267
Analyte
Lead
Prepared
Analyzed
02/17/16 11:00 02/17/16 13:24
LCS LCS
Lab Sample ID: 500-107612-3 MS
Matrix: Water
Analysis Batch: 323267
Analyte
Lead
D
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 323203
Spike
Analyte
Lead
1
2/23/2016
13
14
QC Sample Results
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Lab Sample ID: 500-107612-19 MS
Matrix: Water
Analysis Batch: 323537
Analyte
Lead
Sample Sample
Result Qualifier
9.0
Client Sample ID: MSC45-2F234-TAPCW
Prep Type: Total/NA
Prep Batch: 323395
Spike
Added
100
MS MS
Result Qualifier
110
Lab Sample ID: 500-107612-23 MS
Matrix: Water
Analysis Batch: 323537
Analyte
Lead
Sample Sample
Result Qualifier
14
Analyte
Lead
Spike
Added
100
MS MS
Result Qualifier
117
Sample Sample
Result Qualifier
14
D
%Rec
101
Unit
ug/L
D
%Rec
103
DU DU
Result Qualifier
8.87
Unit
ug/L
D
%Rec.
Limits
70 - 130
Unit
ug/L
D
RPD
2
RPD
Limit
20
RPD
0.09
RPD
Limit
20
TestAmerica Chicago
Page 18 of 29
4
6
7
8
Client Sample ID: MPC47-2F208-TAPHW
Prep Type: Total/NA
Prep Batch: 323395
DU DU
Result Qualifier
13.8
3
5
Client Sample ID: MSC45-2F234-TAPCW
Prep Type: Total/NA
Prep Batch: 323395
Lab Sample ID: 500-107612-23 DU
Matrix: Water
Analysis Batch: 323537
Analyte
Lead
Unit
ug/L
%Rec.
Limits
70 - 130
Client Sample ID: MPC47-2F208-TAPHW
Prep Type: Total/NA
Prep Batch: 323395
Lab Sample ID: 500-107612-19 DU
Matrix: Water
Analysis Batch: 323537
Sample Sample
Result Qualifier
9.0
1
2/23/2016
9
10
11
12
13
14
Lab Chronicle
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: HH10-4F400G-FNTN
Lab Sample ID: 500-107612-1
Date Collected: 02/13/16 09:20
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 13:35 PFK
Client Sample ID: HH10-1F165-FNTN
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 13:39 PFK
Client Sample ID: HH10-1F165-FNTN DUP
Prep Type
Total/NA
Total/NA
Batch
Method
200.8
200.8
Batch
Method
200.8
200.8
Run
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 13:43 PFK
Batch
Method
200.8
200.8
Lab Sample ID: 500-107612-4
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 13:58 PFK
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-5
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:09 PFK
Client Sample ID: VR7-3F300A-FNTN
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-6
Date Collected: 02/13/16 10:25
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
14
Lab
TAL CHI
TAL CHI
Date Collected: 02/13/16 10:09
Date Received: 02/16/16 10:20
Batch
Type
Prep
Analysis
12
13
Dilution
Factor
Client Sample ID: CFSC8-1F100-FNTN
Prep Type
Total/NA
Total/NA
11
Matrix: Water
Date Collected: 02/13/16 09:52
Date Received: 02/16/16 10:20
Batch
Type
Prep
Analysis
8
10
Lab Sample ID: 500-107612-3
Client Sample ID: RSSL12-5F500-FNTN
Prep Type
Total/NA
Total/NA
7
9
Lab
TAL CHI
TAL CHI
Date Collected: 02/13/16 09:37
Date Received: 02/16/16 10:20
Batch
Type
Prep
Analysis
4
6
Lab Sample ID: 500-107612-2
Run
3
5
Lab
TAL CHI
TAL CHI
Date Collected: 02/13/16 09:37
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
1
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:13 PFK
Lab
TAL CHI
TAL CHI
TestAmerica Chicago
Page 19 of 29
2/23/2016
Lab Chronicle
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: AA19-3F300B-FNTN
Lab Sample ID: 500-107612-7
Date Collected: 02/13/16 08:32
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:17 PFK
Batch
Method
200.8
200.8
5
Lab
TAL CHI
TAL CHI
6
Lab Sample ID: 500-107612-8
Date Collected: 02/13/16 08:41
Date Received: 02/16/16 10:20
Batch
Type
Prep
Analysis
3
4
Client Sample ID: MH17-2F201N-FNTN
Prep Type
Total/NA
Total/NA
1
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:20 PFK
7
8
9
Lab
TAL CHI
TAL CHI
10
11
Client Sample ID: JT16A-2F201J-FNTN
Lab Sample ID: 500-107612-9
Date Collected: 02/13/16 08:49
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:24 PFK
Client Sample ID: JHSA15-3F300J-FNTN
13
Lab
TAL CHI
TAL CHI
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:28 PFK
Client Sample ID: MLH11-3F300-FNTN
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-11
Date Collected: 02/13/16 10:37
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:32 PFK
Client Sample ID: JHSA16-3F300D-FNTN
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-12
Date Collected: 02/13/16 09:00
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
14
Lab Sample ID: 500-107612-10
Date Collected: 02/13/16 09:06
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:35 PFK
Lab
TAL CHI
TAL CHI
TestAmerica Chicago
Page 20 of 29
12
2/23/2016
Lab Chronicle
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: CT46-2F200K-FNTN
Lab Sample ID: 500-107612-13
Date Collected: 02/13/16 10:47
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 14:39 PFK
Batch
Method
200.8
200.8
5
Lab
TAL CHI
TAL CHI
6
Lab Sample ID: 500-107612-14
Date Collected: 02/13/16 10:56
Date Received: 02/16/16 10:20
Batch
Type
Prep
Analysis
3
4
Client Sample ID: FH2-3F300B-FNTN
Prep Type
Total/NA
Total/NA
1
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 15:02 PFK
7
8
9
Lab
TAL CHI
TAL CHI
10
11
Client Sample ID: A18-3F301-FNTN
Lab Sample ID: 500-107612-15
Date Collected: 02/13/16 11:13
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 15:05 PFK
Client Sample ID: MSC45-2F221-TAPHW
13
Lab
TAL CHI
TAL CHI
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 15:09 PFK
Client Sample ID: MSC45-2F221-TAPHW DUP
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-17
Date Collected: 02/13/16 11:32
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 15:13 PFK
Client Sample ID: MSC45-2F221-TAPCW
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-18
Date Collected: 02/13/16 11:37
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
14
Lab Sample ID: 500-107612-16
Date Collected: 02/13/16 11:32
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323203 02/17/16 11:00 LWN
323267 02/17/16 15:17 PFK
Lab
TAL CHI
TAL CHI
TestAmerica Chicago
Page 21 of 29
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2/23/2016
Lab Chronicle
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: MSC45-2F234-TAPCW
Lab Sample ID: 500-107612-19
Date Collected: 02/13/16 11:45
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 12:38 PFK
Batch
Method
200.8
200.8
5
Lab
TAL CHI
TAL CHI
6
Lab Sample ID: 500-107612-20
Date Collected: 02/13/16 12:07
Date Received: 02/16/16 10:20
Batch
Type
Prep
Analysis
3
4
Client Sample ID: MPC47-2F220-TAPCW
Prep Type
Total/NA
Total/NA
1
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 12:53 PFK
7
8
9
Lab
TAL CHI
TAL CHI
10
11
Client Sample ID: MPC47-2F208-TAPCW
Lab Sample ID: 500-107612-21
Date Collected: 02/13/16 12:19
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 12:57 PFK
Client Sample ID: MPC47-2F220-TAPHW
13
Lab
TAL CHI
TAL CHI
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:01 PFK
Client Sample ID: MPC47-2F208-TAPHW
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-23
Date Collected: 02/13/16 12:20
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:16 PFK
Client Sample ID: MPC47-B6-TAPCW
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-24
Date Collected: 02/13/16 12:40
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
14
Lab Sample ID: 500-107612-22
Date Collected: 02/13/16 12:10
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:31 PFK
Lab
TAL CHI
TAL CHI
TestAmerica Chicago
Page 22 of 29
12
2/23/2016
Lab Chronicle
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: MPC47-B6-TAPCW DUP
Lab Sample ID: 500-107612-25
Date Collected: 02/13/16 12:40
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:35 PFK
Batch
Method
200.8
200.8
5
Lab
TAL CHI
TAL CHI
6
Lab Sample ID: 500-107612-26
Date Collected: 02/13/16 13:09
Date Received: 02/16/16 10:20
Batch
Type
Prep
Analysis
3
4
Client Sample ID: SHS48-1F117-TAPCW
Prep Type
Total/NA
Total/NA
1
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:39 PFK
7
8
9
Lab
TAL CHI
TAL CHI
10
11
Client Sample ID: SHS48-1F117-TAPCW DUP
Lab Sample ID: 500-107612-27
Date Collected: 02/13/16 13:09
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:42 PFK
Client Sample ID: MSC45-1F100N-BTTL FLL
13
Lab
TAL CHI
TAL CHI
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:46 PFK
Client Sample ID: MSC45-2F200C-BTTL FLL
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-29
Date Collected: 02/13/16 14:16
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 13:50 PFK
Client Sample ID: SFC5-2F202-BTTL FLL
Lab
TAL CHI
TAL CHI
Lab Sample ID: 500-107612-30
Date Collected: 02/13/16 14:32
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
14
Lab Sample ID: 500-107612-28
Date Collected: 02/13/16 14:08
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Matrix: Water
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 14:01 PFK
Lab
TAL CHI
TAL CHI
TestAmerica Chicago
Page 23 of 29
12
2/23/2016
Lab Chronicle
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Client Sample ID: SFC5-1F28-BBTL FLL
Lab Sample ID: 500-107612-31
Date Collected: 02/13/16 14:39
Date Received: 02/16/16 10:20
Prep Type
Total/NA
Total/NA
Batch
Type
Prep
Analysis
Batch
Method
200.8
200.8
1
Matrix: Water
3
4
Run
Dilution
Factor
1
Batch
Prepared
Number or Analyzed Analyst
323395 02/18/16 11:10 LWN
323537 02/18/16 14:05 PFK
5
Lab
TAL CHI
TAL CHI
6
7
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
8
9
10
11
12
13
14
TestAmerica Chicago
Page 24 of 29
2/23/2016
Certification Summary
Client: Short Elliott Hendrickson, Inc. dba SEH
Project/Site: UW Stout - 136039
TestAmerica Job ID: 500-107612-1
2
Laboratory: TestAmerica Chicago
3
The certifications listed below are applicable to this report.
Authority
Wisconsin
Program
State Program
1
EPA Region
5
Certification ID
999580010
4
Expiration Date
08-31-16
5
6
7
8
9
10
11
12
13
14
TestAmerica Chicago
Page 25 of 29
2/23/2016
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2
3
4
5
6
7
8
9
10
11
12
13
14
Page 26 of 29
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2
3
4
5
6
7
8
9
10
11
12
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2
3
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7
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Page 28 of 29
2/23/2016
1
Login Sample Receipt Checklist
Client: Short Elliott Hendrickson, Inc. dba SEH
2
Job Number: 500-107612-1
Login Number: 107612
List Number: 1
Creator: Scott, Sherri L
List Source: TestAmerica Chicago
3
4
5
Question
Answer
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
False
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
6
Comment
7
True
8
9
True
10
-1.4
11
12
13
Refer to Job Narrative for details.
14
True
N/A
True
TestAmerica Chicago
Page 29 of 29
2/23/2016
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