1 2 3 4 ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Tel: (708)534-5200 TestAmerica Job ID: 500-107612-1 Client Project/Site: UW Stout - 136039 For: Short Elliott Hendrickson, Inc. dba SEH 10 North Bridge Street Chippewa Falls, Wisconsin 54729-3374 Attn: Mr. Brian L. Kent Authorized for release by: 2/23/2016 12:52:41 PM Sandie Fredrick, Project Manager II (920)261-1660 sandie.fredrick@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 5 6 7 8 9 10 11 12 13 14 Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Table of Contents Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 3 1 2 3 4 7 8 9 14 15 17 19 4 5 6 7 8 9 10 11 25 26 29 12 13 14 Page 2 of 29 TestAmerica Chicago 2/23/2016 Case Narrative Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 1 2 Job ID: 500-107612-1 3 Laboratory: TestAmerica Chicago 4 Narrative 5 Job Narrative 500-107612-1 6 Comments No additional comments. 7 Receipt The samples were received on 2/16/2016 10:20 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was -1.4º C. Receipt Exceptions Bottle for sample 1 has time of 928, logged per COC. Sample 11 listed twice on COC. Received sample 12 with ID of JSH16-3F300D-FNTN, logged per COC. Metals No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. 8 9 10 11 12 13 14 Page 3 of 29 TestAmerica Chicago 2/23/2016 Detection Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: HH10-4F400G-FNTN Analyte Lead Result Qualifier 7.9 B Lab Sample ID: 500-107612-1 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: HH10-1F165-FNTN Analyte Lead Result Qualifier 20 B Result Qualifier 20 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 1.2 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 3.4 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 2.7 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 0.93 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 0.32 J B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 2.2 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 0.79 B Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-9 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: JHSA15-3F300J-FNTN Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-8 Client Sample ID: JT16A-2F201J-FNTN Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-7 Client Sample ID: MH17-2F201N-FNTN Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-6 Client Sample ID: AA19-3F300B-FNTN Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-5 Client Sample ID: VR7-3F300A-FNTN Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-4 Client Sample ID: CFSC8-1F100-FNTN Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-3 Client Sample ID: RSSL12-5F500-FNTN Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-2 Client Sample ID: HH10-1F165-FNTN DUP Analyte Lead 1 Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-10 RL 0.50 Client Sample ID: MLH11-3F300-FNTN MDL Unit 0.16 ug/L Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-11 This Detection Summary does not include radiochemical test results. TestAmerica Chicago Page 4 of 29 2/23/2016 3 4 5 6 7 8 9 10 11 12 13 14 Detection Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: MLH11-3F300-FNTN (Continued) Analyte Lead Result Qualifier 0.97 B RL 0.50 Lab Sample ID: 500-107612-11 MDL Unit 0.16 ug/L Client Sample ID: JHSA16-3F300D-FNTN Analyte Lead Result Qualifier 0.55 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 0.66 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 0.49 J B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 6.9 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 0.78 B Result Qualifier 0.67 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 1.0 B RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 9.0 RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 2.6 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-19 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: MPC47-2F220-TAPCW Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-18 Client Sample ID: MSC45-2F234-TAPCW Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-17 Client Sample ID: MSC45-2F221-TAPCW Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-16 Client Sample ID: MSC45-2F221-TAPHW DUP Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-15 Client Sample ID: MSC45-2F221-TAPHW Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-14 Client Sample ID: A18-3F301-FNTN Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-13 Client Sample ID: FH2-3F300B-FNTN Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-12 Client Sample ID: CT46-2F200K-FNTN Analyte Lead 1 Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-20 RL 0.50 Client Sample ID: MPC47-2F208-TAPCW MDL Unit 0.16 ug/L Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-21 This Detection Summary does not include radiochemical test results. TestAmerica Chicago Page 5 of 29 2/23/2016 3 4 5 6 7 8 9 10 11 12 13 14 Detection Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: MPC47-2F208-TAPCW (Continued) Analyte Lead Result Qualifier 37 RL 0.50 Lab Sample ID: 500-107612-21 MDL Unit 0.16 ug/L Client Sample ID: MPC47-2F220-TAPHW Analyte Lead Result Qualifier 1.6 RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 14 RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 22 RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 14 RL 0.50 MDL Unit 0.16 ug/L Result Qualifier 2.3 Result Qualifier 0.82 Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-26 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: SHS48-1F117-TAPCW DUP Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-25 Client Sample ID: SHS48-1F117-TAPCW Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-24 Client Sample ID: MPC47-B6-TAPCW DUP Analyte Lead Prep Type Total/NA Lab Sample ID: 500-107612-23 Client Sample ID: MPC47-B6-TAPCW Analyte Lead Dil Fac D Method 1 200.8 Lab Sample ID: 500-107612-22 Client Sample ID: MPC47-2F208-TAPHW Analyte Lead 1 Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-27 RL 0.50 Client Sample ID: MSC45-1F100N-BTTL FLL MDL Unit 0.16 ug/L Dil Fac D Method 1 200.8 Prep Type Total/NA Lab Sample ID: 500-107612-28 No Detections. Client Sample ID: MSC45-2F200C-BTTL FLL Lab Sample ID: 500-107612-29 No Detections. Client Sample ID: SFC5-2F202-BTTL FLL Lab Sample ID: 500-107612-30 No Detections. Client Sample ID: SFC5-1F28-BBTL FLL Lab Sample ID: 500-107612-31 No Detections. This Detection Summary does not include radiochemical test results. TestAmerica Chicago Page 6 of 29 2/23/2016 3 4 5 6 7 8 9 10 11 12 13 14 Method Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 Method 200.8 TestAmerica Job ID: 500-107612-1 1 2 Method Description Metals (ICP/MS) Protocol EPA Laboratory TAL CHI Protocol References: EPA = US Environmental Protection Agency 3 4 5 6 Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 7 8 9 10 11 12 13 14 TestAmerica Chicago Page 7 of 29 2/23/2016 Sample Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 1 2 3 Lab Sample ID 500-107612-1 500-107612-2 500-107612-3 Client Sample ID HH10-4F400G-FNTN HH10-1F165-FNTN HH10-1F165-FNTN DUP Matrix Water Water Water Collected Received 02/13/16 09:20 02/16/16 10:20 02/13/16 09:37 02/16/16 10:20 02/13/16 09:37 02/16/16 10:20 500-107612-4 500-107612-5 500-107612-6 RSSL12-5F500-FNTN CFSC8-1F100-FNTN VR7-3F300A-FNTN Water Water Water 02/13/16 09:52 02/16/16 10:20 02/13/16 10:09 02/16/16 10:20 02/13/16 10:25 02/16/16 10:20 500-107612-7 500-107612-8 AA19-3F300B-FNTN MH17-2F201N-FNTN Water Water 02/13/16 08:32 02/16/16 10:20 02/13/16 08:41 02/16/16 10:20 500-107612-9 JT16A-2F201J-FNTN Water 02/13/16 08:49 02/16/16 10:20 500-107612-10 500-107612-11 JHSA15-3F300J-FNTN MLH11-3F300-FNTN Water Water 02/13/16 09:06 02/16/16 10:20 02/13/16 10:37 02/16/16 10:20 8 500-107612-12 JHSA16-3F300D-FNTN Water 02/13/16 09:00 02/16/16 10:20 500-107612-13 500-107612-14 CT46-2F200K-FNTN FH2-3F300B-FNTN Water Water 02/13/16 10:47 02/16/16 10:20 02/13/16 10:56 02/16/16 10:20 9 500-107612-15 A18-3F301-FNTN Water 02/13/16 11:13 02/16/16 10:20 500-107612-16 500-107612-17 500-107612-18 MSC45-2F221-TAPHW MSC45-2F221-TAPHW DUP MSC45-2F221-TAPCW Water Water Water 02/13/16 11:32 02/16/16 10:20 02/13/16 11:32 02/16/16 10:20 02/13/16 11:37 02/16/16 10:20 500-107612-19 500-107612-20 500-107612-21 MSC45-2F234-TAPCW MPC47-2F220-TAPCW MPC47-2F208-TAPCW Water Water Water 02/13/16 11:45 02/16/16 10:20 02/13/16 12:07 02/16/16 10:20 02/13/16 12:19 02/16/16 10:20 500-107612-22 500-107612-23 500-107612-24 MPC47-2F220-TAPHW MPC47-2F208-TAPHW MPC47-B6-TAPCW Water Water Water 02/13/16 12:10 02/16/16 10:20 02/13/16 12:20 02/16/16 10:20 02/13/16 12:40 02/16/16 10:20 500-107612-25 500-107612-26 500-107612-27 MPC47-B6-TAPCW DUP SHS48-1F117-TAPCW SHS48-1F117-TAPCW DUP Water Water Water 02/13/16 12:40 02/16/16 10:20 02/13/16 13:09 02/16/16 10:20 02/13/16 13:09 02/16/16 10:20 500-107612-28 500-107612-29 500-107612-30 MSC45-1F100N-BTTL FLL MSC45-2F200C-BTTL FLL SFC5-2F202-BTTL FLL Water Water Water 02/13/16 14:08 02/16/16 10:20 02/13/16 14:16 02/16/16 10:20 02/13/16 14:32 02/16/16 10:20 500-107612-31 SFC5-1F28-BBTL FLL Water 02/13/16 14:39 02/16/16 10:20 TestAmerica Chicago Page 8 of 29 2/23/2016 4 5 6 7 10 11 12 13 14 Client Sample Results Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: HH10-4F400G-FNTN Lab Sample ID: 500-107612-1 Date Collected: 02/13/16 09:20 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier 7.9 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: HH10-1F165-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 13:35 Dil Fac 1 Lab Sample ID: 500-107612-2 Date Collected: 02/13/16 09:37 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier 20 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: HH10-1F165-FNTN DUP D Prepared Analyzed 02/17/16 11:00 02/17/16 13:39 Dil Fac 1 Lab Sample ID: 500-107612-3 Date Collected: 02/13/16 09:37 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 20 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: RSSL12-5F500-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 13:43 Dil Fac 1 Lab Sample ID: 500-107612-4 Date Collected: 02/13/16 09:52 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 1.2 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: CFSC8-1F100-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 13:58 Dil Fac 1 Lab Sample ID: 500-107612-5 Date Collected: 02/13/16 10:09 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 3.4 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: VR7-3F300A-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:09 Dil Fac 1 Lab Sample ID: 500-107612-6 Date Collected: 02/13/16 10:25 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 2.7 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: AA19-3F300B-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:13 Dil Fac 1 Lab Sample ID: 500-107612-7 Date Collected: 02/13/16 08:32 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead 5 6 7 8 Method: 200.8 - Metals (ICP/MS) Lead 3 4 Method: 200.8 - Metals (ICP/MS) Lead 1 Result Qualifier 0.93 B RL 0.50 MDL Unit 0.16 ug/L D Prepared Analyzed 02/17/16 11:00 02/17/16 14:17 Dil Fac 1 TestAmerica Chicago Page 9 of 29 2/23/2016 9 10 11 12 13 14 Client Sample Results Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: MH17-2F201N-FNTN Lab Sample ID: 500-107612-8 Date Collected: 02/13/16 08:41 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier 0.32 J B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: JT16A-2F201J-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:20 Dil Fac 1 Lab Sample ID: 500-107612-9 Date Collected: 02/13/16 08:49 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier 2.2 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: JHSA15-3F300J-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:24 Dil Fac 1 Lab Sample ID: 500-107612-10 Date Collected: 02/13/16 09:06 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 0.79 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: MLH11-3F300-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:28 Dil Fac 1 Lab Sample ID: 500-107612-11 Date Collected: 02/13/16 10:37 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 0.97 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: JHSA16-3F300D-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:32 Dil Fac 1 Lab Sample ID: 500-107612-12 Date Collected: 02/13/16 09:00 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 0.55 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: CT46-2F200K-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:35 Dil Fac 1 Lab Sample ID: 500-107612-13 Date Collected: 02/13/16 10:47 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 0.66 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: FH2-3F300B-FNTN D Prepared Analyzed 02/17/16 11:00 02/17/16 14:39 Dil Fac 1 Lab Sample ID: 500-107612-14 Date Collected: 02/13/16 10:56 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead 5 6 7 8 Method: 200.8 - Metals (ICP/MS) Lead 3 4 Method: 200.8 - Metals (ICP/MS) Lead 1 Result Qualifier 0.49 J B RL 0.50 MDL Unit 0.16 ug/L D Prepared Analyzed 02/17/16 11:00 02/17/16 15:02 Dil Fac 1 TestAmerica Chicago Page 10 of 29 2/23/2016 9 10 11 12 13 14 Client Sample Results Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: A18-3F301-FNTN Lab Sample ID: 500-107612-15 Date Collected: 02/13/16 11:13 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier RL 0.50 6.9 B MDL Unit 0.16 ug/L Client Sample ID: MSC45-2F221-TAPHW D Prepared Analyzed 02/17/16 11:00 02/17/16 15:05 Dil Fac 1 Lab Sample ID: 500-107612-16 Date Collected: 02/13/16 11:32 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier RL 0.50 0.78 B MDL Unit 0.16 ug/L Client Sample ID: MSC45-2F221-TAPHW DUP D Prepared Analyzed 02/17/16 11:00 02/17/16 15:09 Dil Fac 1 Lab Sample ID: 500-107612-17 Date Collected: 02/13/16 11:32 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 0.67 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: MSC45-2F221-TAPCW D Prepared Analyzed 02/17/16 11:00 02/17/16 15:13 Dil Fac 1 Lab Sample ID: 500-107612-18 Date Collected: 02/13/16 11:37 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 1.0 B RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: MSC45-2F234-TAPCW D Prepared Analyzed 02/17/16 11:00 02/17/16 15:17 Dil Fac 1 Lab Sample ID: 500-107612-19 Date Collected: 02/13/16 11:45 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 9.0 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: MPC47-2F220-TAPCW D Prepared Analyzed 02/18/16 11:10 02/18/16 12:38 Dil Fac 1 Lab Sample ID: 500-107612-20 Date Collected: 02/13/16 12:07 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 2.6 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: MPC47-2F208-TAPCW D Prepared Analyzed 02/18/16 11:10 02/18/16 12:53 Dil Fac 1 Lab Sample ID: 500-107612-21 Date Collected: 02/13/16 12:19 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead 5 6 7 8 Method: 200.8 - Metals (ICP/MS) Lead 3 4 Method: 200.8 - Metals (ICP/MS) Lead 1 Result Qualifier 37 RL 0.50 MDL Unit 0.16 ug/L D Prepared Analyzed 02/18/16 11:10 02/18/16 12:57 Dil Fac 1 TestAmerica Chicago Page 11 of 29 2/23/2016 9 10 11 12 13 14 Client Sample Results Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: MPC47-2F220-TAPHW Lab Sample ID: 500-107612-22 Date Collected: 02/13/16 12:10 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier RL 0.50 1.6 MDL Unit 0.16 ug/L Client Sample ID: MPC47-2F208-TAPHW D Prepared Analyzed 02/18/16 11:10 02/18/16 13:01 Dil Fac 1 Lab Sample ID: 500-107612-23 Date Collected: 02/13/16 12:20 Date Received: 02/16/16 10:20 Matrix: Water Analyte Result Qualifier RL 0.50 14 MDL Unit 0.16 ug/L Client Sample ID: MPC47-B6-TAPCW D Prepared Analyzed 02/18/16 11:10 02/18/16 13:16 Dil Fac 1 Lab Sample ID: 500-107612-24 Date Collected: 02/13/16 12:40 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier RL 0.50 22 MDL Unit 0.16 ug/L Client Sample ID: MPC47-B6-TAPCW DUP D Prepared Analyzed 02/18/16 11:10 02/18/16 13:31 Dil Fac 1 Lab Sample ID: 500-107612-25 Date Collected: 02/13/16 12:40 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier RL 0.50 14 MDL Unit 0.16 ug/L Client Sample ID: SHS48-1F117-TAPCW D Prepared Analyzed 02/18/16 11:10 02/18/16 13:35 Dil Fac 1 Lab Sample ID: 500-107612-26 Date Collected: 02/13/16 13:09 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier RL 0.50 2.3 MDL Unit 0.16 ug/L Client Sample ID: SHS48-1F117-TAPCW DUP D Prepared Analyzed 02/18/16 11:10 02/18/16 13:39 Dil Fac 1 Lab Sample ID: 500-107612-27 Date Collected: 02/13/16 13:09 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead Result Qualifier 0.82 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: MSC45-1F100N-BTTL FLL D Prepared Analyzed 02/18/16 11:10 02/18/16 13:42 Dil Fac 1 Lab Sample ID: 500-107612-28 Date Collected: 02/13/16 14:08 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead 5 6 7 8 Method: 200.8 - Metals (ICP/MS) Lead 3 4 Method: 200.8 - Metals (ICP/MS) Lead 1 Result Qualifier <0.16 RL 0.50 MDL Unit 0.16 ug/L D Prepared Analyzed 02/18/16 11:10 02/18/16 13:46 Dil Fac 1 TestAmerica Chicago Page 12 of 29 2/23/2016 9 10 11 12 13 14 Client Sample Results Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: MSC45-2F200C-BTTL FLL Lab Sample ID: 500-107612-29 Date Collected: 02/13/16 14:16 Date Received: 02/16/16 10:20 Matrix: Water Result Qualifier <0.16 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: SFC5-2F202-BTTL FLL D Prepared Analyzed 02/18/16 11:10 02/18/16 13:50 Dil Fac 1 Lab Sample ID: 500-107612-30 Date Collected: 02/13/16 14:32 Date Received: 02/16/16 10:20 Matrix: Water Result Qualifier <0.16 RL 0.50 MDL Unit 0.16 ug/L Client Sample ID: SFC5-1F28-BBTL FLL D Prepared Analyzed 02/18/16 11:10 02/18/16 14:01 Dil Fac 1 Lab Sample ID: 500-107612-31 Date Collected: 02/13/16 14:39 Date Received: 02/16/16 10:20 Matrix: Water Method: 200.8 - Metals (ICP/MS) Analyte Lead 5 6 7 8 Method: 200.8 - Metals (ICP/MS) Analyte Lead 3 4 Method: 200.8 - Metals (ICP/MS) Analyte Lead 1 Result Qualifier <0.16 RL 0.50 MDL Unit 0.16 ug/L D Prepared Analyzed 02/18/16 11:10 02/18/16 14:05 Dil Fac 1 9 10 11 12 13 14 TestAmerica Chicago Page 13 of 29 2/23/2016 Definitions/Glossary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Qualifiers 3 Metals Qualifier B F5 J 1 4 Qualifier Description Compound was found in the blank and sample. Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL. The data are considered valid because the absolute difference is less than the RL. Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. 5 6 7 Glossary Abbreviation ¤ %R CFL These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis Percent Recovery Contains Free Liquid CNF DER Contains no Free Liquid Duplicate error ratio (normalized absolute difference) Dil Fac DL, RA, RE, IN DLC MDA EDL MDC Dilution Factor Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample Decision level concentration Minimum detectable activity Estimated Detection Limit Minimum detectable concentration MDL ML NC ND PQL QC Method Detection Limit Minimum Level (Dioxin) Not Calculated Not detected at the reporting limit (or MDL or EDL if shown) Practical Quantitation Limit Quality Control RER RL RPD TEF TEQ Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent Difference, a measure of the relative difference between two points Toxicity Equivalent Factor (Dioxin) Toxicity Equivalent Quotient (Dioxin) 8 9 10 11 12 13 14 TestAmerica Chicago Page 14 of 29 2/23/2016 QC Association Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 1 2 Metals 3 Prep Batch: 323203 Lab Sample ID 500-107612-1 500-107612-2 500-107612-3 Client Sample ID HH10-4F400G-FNTN HH10-1F165-FNTN HH10-1F165-FNTN DUP Prep Type Total/NA Total/NA Total/NA Matrix Water Water Water Method 200.8 200.8 200.8 Prep Batch 500-107612-3 DU 500-107612-3 MS 500-107612-4 HH10-1F165-FNTN DUP HH10-1F165-FNTN DUP RSSL12-5F500-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 500-107612-5 500-107612-6 CFSC8-1F100-FNTN VR7-3F300A-FNTN Total/NA Total/NA Water Water 200.8 200.8 500-107612-7 AA19-3F300B-FNTN Total/NA Water 200.8 500-107612-8 500-107612-9 500-107612-10 MH17-2F201N-FNTN JT16A-2F201J-FNTN JHSA15-3F300J-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 500-107612-11 500-107612-12 500-107612-13 MLH11-3F300-FNTN JHSA16-3F300D-FNTN CT46-2F200K-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 500-107612-13 DU 500-107612-13 MS 500-107612-14 CT46-2F200K-FNTN CT46-2F200K-FNTN FH2-3F300B-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 500-107612-15 500-107612-16 500-107612-17 A18-3F301-FNTN MSC45-2F221-TAPHW MSC45-2F221-TAPHW DUP Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 500-107612-18 LCS 500-323203/2-A MSC45-2F221-TAPCW Lab Control Sample Total/NA Total/NA Water Water 200.8 200.8 MB 500-323203/1-A Method Blank Total/NA Water 200.8 Lab Sample ID 500-107612-1 500-107612-2 Client Sample ID HH10-4F400G-FNTN HH10-1F165-FNTN Prep Type Total/NA Total/NA Matrix Water Water Method 200.8 200.8 500-107612-3 HH10-1F165-FNTN DUP Total/NA Water 200.8 323203 500-107612-3 DU HH10-1F165-FNTN DUP Total/NA Water 200.8 323203 500-107612-3 MS 500-107612-4 HH10-1F165-FNTN DUP RSSL12-5F500-FNTN Total/NA Total/NA Water Water 200.8 200.8 323203 323203 500-107612-5 500-107612-6 500-107612-7 CFSC8-1F100-FNTN VR7-3F300A-FNTN AA19-3F300B-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323203 323203 323203 500-107612-8 500-107612-9 500-107612-10 MH17-2F201N-FNTN JT16A-2F201J-FNTN JHSA15-3F300J-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323203 323203 323203 500-107612-11 500-107612-12 500-107612-13 MLH11-3F300-FNTN JHSA16-3F300D-FNTN CT46-2F200K-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323203 323203 323203 500-107612-13 DU 500-107612-13 MS 500-107612-14 CT46-2F200K-FNTN CT46-2F200K-FNTN FH2-3F300B-FNTN Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323203 323203 323203 500-107612-15 500-107612-16 500-107612-17 A18-3F301-FNTN MSC45-2F221-TAPHW MSC45-2F221-TAPHW DUP Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323203 323203 323203 500-107612-18 LCS 500-323203/2-A MSC45-2F221-TAPCW Lab Control Sample Total/NA Total/NA Water Water 200.8 200.8 323203 323203 MB 500-323203/1-A Method Blank Total/NA Water 200.8 323203 5 6 7 8 9 10 11 12 13 14 Analysis Batch: 323267 Prep Batch 323203 323203 TestAmerica Chicago Page 15 of 29 4 2/23/2016 QC Association Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 1 2 Prep Batch: 323395 Prep Batch 3 Lab Sample ID 500-107612-19 500-107612-19 DU 500-107612-19 MS Client Sample ID MSC45-2F234-TAPCW MSC45-2F234-TAPCW MSC45-2F234-TAPCW Prep Type Total/NA Total/NA Total/NA Matrix Water Water Water Method 200.8 200.8 200.8 500-107612-20 500-107612-21 MPC47-2F220-TAPCW MPC47-2F208-TAPCW Total/NA Total/NA Water Water 200.8 200.8 500-107612-22 MPC47-2F220-TAPHW Total/NA Water 200.8 6 500-107612-23 500-107612-23 DU MPC47-2F208-TAPHW MPC47-2F208-TAPHW Total/NA Total/NA Water Water 200.8 200.8 7 500-107612-23 MS MPC47-2F208-TAPHW Total/NA Water 200.8 500-107612-24 500-107612-25 MPC47-B6-TAPCW MPC47-B6-TAPCW DUP Total/NA Total/NA Water Water 200.8 200.8 8 500-107612-26 SHS48-1F117-TAPCW Total/NA Water 200.8 500-107612-27 SHS48-1F117-TAPCW DUP Total/NA Water 200.8 9 500-107612-28 500-107612-29 MSC45-1F100N-BTTL FLL MSC45-2F200C-BTTL FLL Total/NA Total/NA Water Water 200.8 200.8 10 500-107612-30 500-107612-31 LCS 500-323395/2-A SFC5-2F202-BTTL FLL SFC5-1F28-BBTL FLL Lab Control Sample Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 11 MB 500-323395/1-A Method Blank Total/NA Water 200.8 4 5 12 13 Analysis Batch: 323537 Lab Sample ID 500-107612-19 500-107612-19 DU 500-107612-19 MS Client Sample ID MSC45-2F234-TAPCW MSC45-2F234-TAPCW MSC45-2F234-TAPCW Prep Type Total/NA Total/NA Total/NA Matrix Water Water Water Method 200.8 200.8 200.8 Prep Batch 323395 323395 323395 500-107612-20 500-107612-21 500-107612-22 MPC47-2F220-TAPCW MPC47-2F208-TAPCW MPC47-2F220-TAPHW Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323395 323395 323395 500-107612-23 500-107612-23 DU 500-107612-23 MS MPC47-2F208-TAPHW MPC47-2F208-TAPHW MPC47-2F208-TAPHW Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323395 323395 323395 500-107612-24 500-107612-25 500-107612-26 MPC47-B6-TAPCW MPC47-B6-TAPCW DUP SHS48-1F117-TAPCW Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323395 323395 323395 500-107612-27 500-107612-28 500-107612-29 SHS48-1F117-TAPCW DUP MSC45-1F100N-BTTL FLL MSC45-2F200C-BTTL FLL Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323395 323395 323395 500-107612-30 500-107612-31 LCS 500-323395/2-A SFC5-2F202-BTTL FLL SFC5-1F28-BBTL FLL Lab Control Sample Total/NA Total/NA Total/NA Water Water Water 200.8 200.8 200.8 323395 323395 323395 MB 500-323395/1-A Method Blank Total/NA Water 200.8 323395 TestAmerica Chicago Page 16 of 29 2/23/2016 14 QC Sample Results Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Method: 200.8 - Metals (ICP/MS) 3 Lab Sample ID: MB 500-323203/1-A Matrix: Water Analysis Batch: 323267 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 323203 MB MB Result Qualifier 0.173 J Analyte Lead RL 0.50 MDL Unit 0.16 ug/L Lab Sample ID: LCS 500-323203/2-A Matrix: Water Analysis Batch: 323267 Added 100 Result Qualifier 108 Sample Sample Result Qualifier 20 B Spike Added 100 MS MS Result Qualifier 125 Sample Sample Result Qualifier 0.66 B Spike Added 100 MS MS Result Qualifier 109 Unit ug/L D Unit ug/L D Unit ug/L D Sample Sample Result Qualifier 20 B DU DU Result Qualifier 19.5 Unit ug/L %Rec 105 %Rec 108 Sample Sample Result Qualifier 0.66 B DU DU Result Qualifier 0.534 F5 Unit ug/L %Rec. Limits 70 - 130 RPD 4 RPD Limit 20 RPD 21 RPD Limit 20 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 323395 MB MB Result Qualifier <0.16 RL 0.50 MDL Unit 0.16 ug/L D Prepared Analyzed 02/18/16 11:10 02/18/16 12:27 Dil Fac 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 323395 Spike Added 100 LCS LCS Result Qualifier 101 Unit ug/L D %Rec 101 %Rec. Limits 85 - 115 TestAmerica Chicago Page 17 of 29 5 6 7 8 10 11 12 %Rec. Limits 70 - 130 D 4 9 Client Sample ID: CT46-2F200K-FNTN Prep Type: Total/NA Prep Batch: 323203 Lab Sample ID: LCS 500-323395/2-A Matrix: Water Analysis Batch: 323537 Analyte Lead Limits 85 - 115 D Lab Sample ID: MB 500-323395/1-A Matrix: Water Analysis Batch: 323537 Analyte Lead %Rec 108 Client Sample ID: HH10-1F165-FNTN DUP Prep Type: Total/NA Prep Batch: 323203 Lab Sample ID: 500-107612-13 DU Matrix: Water Analysis Batch: 323267 Analyte Lead %Rec. Client Sample ID: CT46-2F200K-FNTN Prep Type: Total/NA Prep Batch: 323203 Lab Sample ID: 500-107612-3 DU Matrix: Water Analysis Batch: 323267 Analyte Lead Dil Fac 1 Client Sample ID: HH10-1F165-FNTN DUP Prep Type: Total/NA Prep Batch: 323203 Lab Sample ID: 500-107612-13 MS Matrix: Water Analysis Batch: 323267 Analyte Lead Prepared Analyzed 02/17/16 11:00 02/17/16 13:24 LCS LCS Lab Sample ID: 500-107612-3 MS Matrix: Water Analysis Batch: 323267 Analyte Lead D Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 323203 Spike Analyte Lead 1 2/23/2016 13 14 QC Sample Results Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Lab Sample ID: 500-107612-19 MS Matrix: Water Analysis Batch: 323537 Analyte Lead Sample Sample Result Qualifier 9.0 Client Sample ID: MSC45-2F234-TAPCW Prep Type: Total/NA Prep Batch: 323395 Spike Added 100 MS MS Result Qualifier 110 Lab Sample ID: 500-107612-23 MS Matrix: Water Analysis Batch: 323537 Analyte Lead Sample Sample Result Qualifier 14 Analyte Lead Spike Added 100 MS MS Result Qualifier 117 Sample Sample Result Qualifier 14 D %Rec 101 Unit ug/L D %Rec 103 DU DU Result Qualifier 8.87 Unit ug/L D %Rec. Limits 70 - 130 Unit ug/L D RPD 2 RPD Limit 20 RPD 0.09 RPD Limit 20 TestAmerica Chicago Page 18 of 29 4 6 7 8 Client Sample ID: MPC47-2F208-TAPHW Prep Type: Total/NA Prep Batch: 323395 DU DU Result Qualifier 13.8 3 5 Client Sample ID: MSC45-2F234-TAPCW Prep Type: Total/NA Prep Batch: 323395 Lab Sample ID: 500-107612-23 DU Matrix: Water Analysis Batch: 323537 Analyte Lead Unit ug/L %Rec. Limits 70 - 130 Client Sample ID: MPC47-2F208-TAPHW Prep Type: Total/NA Prep Batch: 323395 Lab Sample ID: 500-107612-19 DU Matrix: Water Analysis Batch: 323537 Sample Sample Result Qualifier 9.0 1 2/23/2016 9 10 11 12 13 14 Lab Chronicle Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: HH10-4F400G-FNTN Lab Sample ID: 500-107612-1 Date Collected: 02/13/16 09:20 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 13:35 PFK Client Sample ID: HH10-1F165-FNTN Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 13:39 PFK Client Sample ID: HH10-1F165-FNTN DUP Prep Type Total/NA Total/NA Batch Method 200.8 200.8 Batch Method 200.8 200.8 Run 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 13:43 PFK Batch Method 200.8 200.8 Lab Sample ID: 500-107612-4 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 13:58 PFK Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-5 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:09 PFK Client Sample ID: VR7-3F300A-FNTN Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-6 Date Collected: 02/13/16 10:25 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 14 Lab TAL CHI TAL CHI Date Collected: 02/13/16 10:09 Date Received: 02/16/16 10:20 Batch Type Prep Analysis 12 13 Dilution Factor Client Sample ID: CFSC8-1F100-FNTN Prep Type Total/NA Total/NA 11 Matrix: Water Date Collected: 02/13/16 09:52 Date Received: 02/16/16 10:20 Batch Type Prep Analysis 8 10 Lab Sample ID: 500-107612-3 Client Sample ID: RSSL12-5F500-FNTN Prep Type Total/NA Total/NA 7 9 Lab TAL CHI TAL CHI Date Collected: 02/13/16 09:37 Date Received: 02/16/16 10:20 Batch Type Prep Analysis 4 6 Lab Sample ID: 500-107612-2 Run 3 5 Lab TAL CHI TAL CHI Date Collected: 02/13/16 09:37 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA 1 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:13 PFK Lab TAL CHI TAL CHI TestAmerica Chicago Page 19 of 29 2/23/2016 Lab Chronicle Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: AA19-3F300B-FNTN Lab Sample ID: 500-107612-7 Date Collected: 02/13/16 08:32 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:17 PFK Batch Method 200.8 200.8 5 Lab TAL CHI TAL CHI 6 Lab Sample ID: 500-107612-8 Date Collected: 02/13/16 08:41 Date Received: 02/16/16 10:20 Batch Type Prep Analysis 3 4 Client Sample ID: MH17-2F201N-FNTN Prep Type Total/NA Total/NA 1 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:20 PFK 7 8 9 Lab TAL CHI TAL CHI 10 11 Client Sample ID: JT16A-2F201J-FNTN Lab Sample ID: 500-107612-9 Date Collected: 02/13/16 08:49 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:24 PFK Client Sample ID: JHSA15-3F300J-FNTN 13 Lab TAL CHI TAL CHI Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:28 PFK Client Sample ID: MLH11-3F300-FNTN Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-11 Date Collected: 02/13/16 10:37 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:32 PFK Client Sample ID: JHSA16-3F300D-FNTN Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-12 Date Collected: 02/13/16 09:00 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 14 Lab Sample ID: 500-107612-10 Date Collected: 02/13/16 09:06 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:35 PFK Lab TAL CHI TAL CHI TestAmerica Chicago Page 20 of 29 12 2/23/2016 Lab Chronicle Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: CT46-2F200K-FNTN Lab Sample ID: 500-107612-13 Date Collected: 02/13/16 10:47 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 14:39 PFK Batch Method 200.8 200.8 5 Lab TAL CHI TAL CHI 6 Lab Sample ID: 500-107612-14 Date Collected: 02/13/16 10:56 Date Received: 02/16/16 10:20 Batch Type Prep Analysis 3 4 Client Sample ID: FH2-3F300B-FNTN Prep Type Total/NA Total/NA 1 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 15:02 PFK 7 8 9 Lab TAL CHI TAL CHI 10 11 Client Sample ID: A18-3F301-FNTN Lab Sample ID: 500-107612-15 Date Collected: 02/13/16 11:13 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 15:05 PFK Client Sample ID: MSC45-2F221-TAPHW 13 Lab TAL CHI TAL CHI Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 15:09 PFK Client Sample ID: MSC45-2F221-TAPHW DUP Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-17 Date Collected: 02/13/16 11:32 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 15:13 PFK Client Sample ID: MSC45-2F221-TAPCW Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-18 Date Collected: 02/13/16 11:37 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 14 Lab Sample ID: 500-107612-16 Date Collected: 02/13/16 11:32 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323203 02/17/16 11:00 LWN 323267 02/17/16 15:17 PFK Lab TAL CHI TAL CHI TestAmerica Chicago Page 21 of 29 12 2/23/2016 Lab Chronicle Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: MSC45-2F234-TAPCW Lab Sample ID: 500-107612-19 Date Collected: 02/13/16 11:45 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 12:38 PFK Batch Method 200.8 200.8 5 Lab TAL CHI TAL CHI 6 Lab Sample ID: 500-107612-20 Date Collected: 02/13/16 12:07 Date Received: 02/16/16 10:20 Batch Type Prep Analysis 3 4 Client Sample ID: MPC47-2F220-TAPCW Prep Type Total/NA Total/NA 1 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 12:53 PFK 7 8 9 Lab TAL CHI TAL CHI 10 11 Client Sample ID: MPC47-2F208-TAPCW Lab Sample ID: 500-107612-21 Date Collected: 02/13/16 12:19 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 12:57 PFK Client Sample ID: MPC47-2F220-TAPHW 13 Lab TAL CHI TAL CHI Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:01 PFK Client Sample ID: MPC47-2F208-TAPHW Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-23 Date Collected: 02/13/16 12:20 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:16 PFK Client Sample ID: MPC47-B6-TAPCW Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-24 Date Collected: 02/13/16 12:40 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 14 Lab Sample ID: 500-107612-22 Date Collected: 02/13/16 12:10 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:31 PFK Lab TAL CHI TAL CHI TestAmerica Chicago Page 22 of 29 12 2/23/2016 Lab Chronicle Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: MPC47-B6-TAPCW DUP Lab Sample ID: 500-107612-25 Date Collected: 02/13/16 12:40 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:35 PFK Batch Method 200.8 200.8 5 Lab TAL CHI TAL CHI 6 Lab Sample ID: 500-107612-26 Date Collected: 02/13/16 13:09 Date Received: 02/16/16 10:20 Batch Type Prep Analysis 3 4 Client Sample ID: SHS48-1F117-TAPCW Prep Type Total/NA Total/NA 1 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:39 PFK 7 8 9 Lab TAL CHI TAL CHI 10 11 Client Sample ID: SHS48-1F117-TAPCW DUP Lab Sample ID: 500-107612-27 Date Collected: 02/13/16 13:09 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:42 PFK Client Sample ID: MSC45-1F100N-BTTL FLL 13 Lab TAL CHI TAL CHI Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:46 PFK Client Sample ID: MSC45-2F200C-BTTL FLL Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-29 Date Collected: 02/13/16 14:16 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 13:50 PFK Client Sample ID: SFC5-2F202-BTTL FLL Lab TAL CHI TAL CHI Lab Sample ID: 500-107612-30 Date Collected: 02/13/16 14:32 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 14 Lab Sample ID: 500-107612-28 Date Collected: 02/13/16 14:08 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Matrix: Water Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 14:01 PFK Lab TAL CHI TAL CHI TestAmerica Chicago Page 23 of 29 12 2/23/2016 Lab Chronicle Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Client Sample ID: SFC5-1F28-BBTL FLL Lab Sample ID: 500-107612-31 Date Collected: 02/13/16 14:39 Date Received: 02/16/16 10:20 Prep Type Total/NA Total/NA Batch Type Prep Analysis Batch Method 200.8 200.8 1 Matrix: Water 3 4 Run Dilution Factor 1 Batch Prepared Number or Analyzed Analyst 323395 02/18/16 11:10 LWN 323537 02/18/16 14:05 PFK 5 Lab TAL CHI TAL CHI 6 7 Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 8 9 10 11 12 13 14 TestAmerica Chicago Page 24 of 29 2/23/2016 Certification Summary Client: Short Elliott Hendrickson, Inc. dba SEH Project/Site: UW Stout - 136039 TestAmerica Job ID: 500-107612-1 2 Laboratory: TestAmerica Chicago 3 The certifications listed below are applicable to this report. Authority Wisconsin Program State Program 1 EPA Region 5 Certification ID 999580010 4 Expiration Date 08-31-16 5 6 7 8 9 10 11 12 13 14 TestAmerica Chicago Page 25 of 29 2/23/2016 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Page 26 of 29 2/23/2016 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Page 27 of 29 2/23/2016 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Page 28 of 29 2/23/2016 1 Login Sample Receipt Checklist Client: Short Elliott Hendrickson, Inc. dba SEH 2 Job Number: 500-107612-1 Login Number: 107612 List Number: 1 Creator: Scott, Sherri L List Source: TestAmerica Chicago 3 4 5 Question Answer Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. False Samples are received within Holding Time (excluding tests with immediate HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs Containers requiring zero headspace have no headspace or bubble is <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A 6 Comment 7 True 8 9 True 10 -1.4 11 12 13 Refer to Job Narrative for details. 14 True N/A True TestAmerica Chicago Page 29 of 29 2/23/2016