CHEMISTRY 131L GENERAL CHEMISTRY LABORATORY Fall 2015 Dr. Chris Adams, Room 302, Porter Hall Office Hours: MW 10-11, T 9-11, R 9-10 Telephone: 587-7716 E-mail: cladams@adams.edu Dr. Christina Miller, Room 304, Porter Hall Office Hours: TR 8-10, W 8-9 Telephone: 587-7506 E-mail: crmiller@adams.edu Dr. Renee Beeton, Room 303 Porter Hall Office Hours: MTF 10-11, MW 2-3 Telephone: 587-7383 E-mail: rbeeton@adams.edu Course Description Chemistry 131L is the laboratory course designed to accompany the general chemistry lecture course. Student Learning Outcomes (for students who are successful in the class) 1. Students will learn basic techniques associated with chemistry laboratories, including (but not limited to) measurement of solids and liquids, use of common equipment and instrumentation, and use of computer software. 2. Students will develop more thoroughly their skills in collaborative and individual efforts to solve problems and to design experiments. 3. Students will develop more thoroughly their abilities to collect and critically interpret experimental data, and to effectively communicate their results and interpretations. Text Lab manual is available on your lecture instructor’s Blackboard or Website. Supplies Safety goggles (these will be used in subsequent chemistry classes) Available at the bookstore or from the Adams Atoms Chemistry Club. A scientific calculator. Assignments, Evaluation Procedures and Grading Policy: 1. Attendance: Attendance is required for the laboratory and for the lab lecture on Wednesdays. Three points are deducted for each lab lecture missed and one point will be deducted if you are late for lab. If you are not present for an experiment, you will not get credit for the experiment. Dry-labbing will not be tolerated and will be treated as cheating. If you miss a lab for a documented, valid reason and you let the instructor know beforehand, your grade will be adjusted for that missed lab. Only one excused absence will be allowed. 2. Laboratory Groups: You will be assigned to a group of three or four students with whom you will work with for the laboratory experiments. This group will most likely be different from your lecture group. If you must miss an experiment, please contact at least one of your group members as well as the lab instructor. We plan to switch lab groups at mid-semester, to give you an opportunity to work with some new folks. 3. Safety and Standard Laboratory Procedures: You must listen to a safety lecture and sign a safety rules sheet before you may work in the lab. Strict rules regarding clothing and safety eyewear will be enforced for the lab. Unless otherwise instructed, you must always wear safety goggles (indirect ventilated) in the lab. Safety glasses are not permitted. These may be purchased at the bookstore or through the Adams Atoms Chemistry Club. If you refuse to wear eye protection, you will be asked to leave the lab without finishing the experiment and will receive a grade of zero for that experiment. You must provide your own safety eyewear. Wear appropriate clothing and footwear to the lab. Appropriate clothing includes long pants or other attire that covers legs to the ankle; short or long-sleeve tops that cover the shoulders, do not have deep-cut necklines, and do not leave exposed skin around the waist or the back (especially when bending over to conduct a routine lab technique); and shoes that cover the toes and heels (no sandals or clogs). In other words, wear old jeans, a long t-shirt, and tennis shoes! That way, you’ll be dressed to work safely (). Violation of any safety policy/procedure during the course of a single laboratory period will result in the following actions: 1st incident: Verbal Warning 2nd incident: Written Warning 3rd incident: Lose 10% of the value of the lab write-up for that experiment 4th incident: Removal from lab and earn a grade of 0 for that experiment 4. Cleanliness: Clean up all spills immediately, especially around balance areas. Replace all bottle lids and caps as soon as you are through. Clean your working area before leaving lab. 5. Equipment: The lab is organized with common items of equipment needed for experiments in certain drawers. Please make every effort to keep the equipment in good order. After cleaning the items used for an experiment, return them to their proper location(s) at the end of each laboratory period. 6. Preparation: Advance preparation for the laboratory will be necessary. This includes reading the experiment, attending the prelab lecture on Mondays, and answering the prelab exercise(s) included in the lab manual. Remember that a portion of your lab write-up grade will be determined by the answers to the prelab exercises. The lab instructor/assistant will check your lab report sheet when you first come to lab to ensure that you have finished the prelab exercise. 7. Grading: Your grade will be determined by the total points you accumulate in the lab, from your lab write-ups [70%] and lab practical exams [30%]. Lab report write-ups are due the week after the lab is finished at the start of lab. Late write-ups will not be accepted. Letter grades will not be assigned until the end of the semester. If you need to estimate your grade at any time, use the following scale: 100.0% – 93.0% = A; 92.9% – 90.0% = A-; 89.9% - 87.0% = B+; 86.9% - 83.0% = B; 82.9% - 80.0% = B-; 79.9% - 77.0% = C+; 76.9% - 73.0% = C; 72.9% - 70.0% = C-; 69.9% - 67.0% = D+; 66.9% - 60.0% = D 8. Cheating: Cheating of any sort, from copying someone else's answers on a lab quiz to working in a group when you are to be working individually, will not be tolerated. If you are caught intentionally cheating, you will receive as a minimum penalty a zero for that work. Repeated instances of cheating will result in an F for the course and may be subject to additional discipline from the College. 9. Adding, Withdrawing, and Incompletes: The last day to add class to your schedule is September 9. The last day to withdraw from this course and receive a grade of W is Friday October 30, 2015. After that date, a grade of W may only be given for documented medical reasons or extenuating circumstances, either of which must be determined by the instructor, the Department Chair, the Vice President for Student Affairs, and the Vice President of Academic Affairs. Poor performance in class is not an acceptable reason for an incomplete. 10. Special Consideration: If you require course adaptations or accommodations because of a documented disability, if you have emergency medical information to share with me, or if you need particular arrangements in case the building must be evacuated, please make an appointment with me as soon as possible. Office hours and location are given at the top of the first page of this syllabus. 11. Emergency Evacuation: In the event of an emergency, the entire lab section will exit out the appropriate stairwell (north or south, depending on the location of the emergency) and meet by the sign for the music building, on the east side of Porter Hall. Schedule Lab lectures will be given in class on Monday mornings. To get full credit for lab attendance, you must be present for the lab lecture and be on time. This schedule may be subject to change with advance notice. Date 8/25, 8/26, 8/27 9/1, 9/2, 9/3 9/8, 9/9, 9/10 9/15, 9/16, 9/17 9/22, 9/23, 9/24 9/29, 9/30, 10/1 10/6, 10/7, 10/8 10/13, 10/14, 10/15 10/22, 10/21, 10/22 10/27, 10/28, 10/29 11/3, 11/4, 11/5 11/10, 11/11, 11/12 11/17, 11/18, 11/19 11/24, 11/25, 11/26 12/1, 12/2, 12/3 12/8, 12/9, 12/10 Lab Safety Lab #1 - Pea Gravel Lab #2 – Nuclear Chemistry and Radioactivity Lab #3 – Periodic Trends Lab #4 – Light and the Structure of the Atom Lab #5 - Hydrates Fall Recess, no lab Lab Practical 1 Lab #6 - Molecular Modeling and Molecular Shapes Lab #7- Quality Assurance; Analysis by Titration Lab #8- Kidney Stones Lab #9 – A Copper Cycle Lab #10 – Coffee Cup Calorimetry No lab - Thanksgiving Break Lab # 11- Gas Laws Lab Practical 2