ME 388 – Applied Instrumentation Lab Spring 2012 Dave Bayless, PhD, PE, FASME Loehr Professor of Mechanical Engineering 248 Stocker Center e-mail: bayless@ohio.edu Office Hours: M,T,W,Th 15:30 – 16:30 Text • ME 388 Laboratory Manual can be found at http://www.ohio.edu/people/bayless/seniorlab • Experimental Methods for Engineers (Holman) may be useful, but is not required Grading Subject Unit Weight Total Five Experimental Lab Exercises @ 10% 50% Mastery level formal report @ 25% 25% CIM laboratory Project @ 5% 5% DOE Project @ 5% 5% Formal Lab Introductory material @ 5% 5% Final Exam @ 10% 10% Total 100% Purpose • Enhance fundamental engineering learning with lab experiments • Gain experience and improve experimental techniques • Improve data reduction and analysis skills • Improve written communication skills Outcomes • Mastery • Competence • Awareness Course Mastery Outcomes • Ability to perform curve-fitting of multivariate data sets • Ability to calculate the error/uncertainty propagation for calculations that include multiple terms with uncertainties. • Writing and editing clear and effective laboratory reports, including the creation of “professional quality” graphics for figures, tables, plots and charts. Course Competence Outcomes • Ability to use common measurement equipment • Ability to apply previously-learned engineering concepts to compare theoretical predictions with actual experimental results in diverse, practical mechanical engineering experiments. • Ability to program and use CNC machines to manufacture simple parts • An ability to interpret tensile test data Course Awareness Outcome • Awareness of Design of Experiments (DOE) statistical techniques • DOE Exercise will give you a chance to interpret a test matrix Spelling and Grammar • • • • • Write in the 3rd person Use spelling and grammar checker in Word Adopt the style of a textbook or journal article See formal report guidelines in lab notes “Write smart” – “Outlying data were rejected.” instead of “Bad data was thrown out.” – Edit your work to be concise!! Mullen Burst Strength (psi) Figure Example 600 500 400 300 200 Teflon - Reactive 275 Ryton B - Reactive 430 Ryton-Sulfuric 605 Omnisil-Sulfuric 550 100 0 0 100 200 300 400 500 Date of Sampling Figure 1. Burst strength as a function of time Table Example Table 4. Dependent process variables as a function of the DOE number. Dependent variables DOE No. Ram pressure (MPa) Specific pressure (MPa) 1 14.71 459.2 2 15.09 471.1 3 14.30 446.6 4 13.69 427.3 5 14.77 461.1 6 14.37 448.3 7 13.30 415.0 Use computer generated schematics tv p i p 1 i 3 tw Figure 5: Schematic of stressed multi-void tube due to pressure Equations • Use MS Word Equation editor • Number equations sequentially, right justified • See Lab notes Statistical Analysis Review • Mean • Standard Deviation • Sample Size Mean n x1 x2 x3 ... xn 1 x xi n n 1 Standard Deviation xi x Simple variance Sample variance 2 2 2 2 x x x2 x x3 x ... xi x 2 1 n 1 1 n 2 x x i n 1 1 Standard deviation of a sample x1 x x2 x x3 x 2 2 2 n 1 ... xi x 2 1 n xi x n 1 1 1 2 2 Histogram and normal distribution Standard deviation and data How many samples are enough? n 1 2 3 4 5 6 7 xi 90 89 91 87 80 90 92 xave --89.50 90.00 89.25 87.40 87.83 88.43 --0.707 1.000 1.708 4.393 4.070 4.036 Can “outlying” data be ignored? • Determine if there is a physical basis for the suspect data (i.e., the TC broke, etc.) • Chauvenet’s criteria for data rejection Chauvenet’s criteria 1. Calculate xave and for data set 2. Get dmax/ for the specific sample size from a table 3. Calculate dmax = (dmax/) × 4. Determine if the most “reject-able” data is larger than this value, d = |xave – xi| 5. Reject outlying data and then recalculate xave and for data set Chauvenet’s Example Chauvenet’s Example 4 2 3 17 5 (5 data points, n=5) Average = 6.2 Standard Deviation = 6.14 Which one to reject? Technically, examine at them all Realistically, focus on “17” d max 1.65 For n = 5, reject at d 17 6.2 6.14 1.76 ← REJECT 17 How sure are you of your data? • All measurement instruments have a degree of uncertainty when taking a reading • Uncertainty values for a particular instrument is usually given or can be determined • For calculated parameters, the uncertainty is a function of the uncertainties of the measured parameters. Uncertainty calculation Let x f (v, y, z ) 1 22 2 2 x x x Wx Wv W y Wz v y z • Report uncertainty as a % of calculated value Wx Uncerta int y 100% X Regression Analysis • Pertains to reporting of a “least-square” or other type of curve fit to your data • You must report the equation and the correlation coefficient (R) or the coefficient of determination (R2) • R-values should be presented with the equation and a graph of the data Formal Report • • • • • • Abstract Introduction Experimental Apparatus Results and Discussion Conclusions and Recommendations Appendices – Uncertainty analysis – Data Abstract (250 words) • • • • • Purpose What was done? Significant parameters measured or set Measurement results (summarized) Quantitative comparisons (i.e., to published values) Introduction • • • • Provide background information Establish significance of work Introduce work and motivation for experiment Introduce equations that are pertinent to data analysis and purpose of the lab Experimental Apparatus • Describe experimental equipment configuration using schematic diagrams • Explain test procedure • Present any calibration data • Show (tabulate) all uncertainty values measurements that were taken Results and Discussion • Present results (analyzed data) in graphical form • Discuss results and sources of error (explain why the data did what it did) • Develop logical and reasonable explanations with regard to data behavior • Make quantitative comparisons • Discuss uncertainty and if it accounts for any known or obvious discrepancies Conclusions and Recommendations • Summarize results quantitatively • Summarize any comparisons • Start with results of most importance or significance • Address all significant points • Make sound recommendations – Things that could be improved – Additional work that could be done