Experiment No.4: Grain size analysis Part II: Hydrometer analysis. -Hydrometer analysis is the procedure generally adopted for determination of the particle-size distribution in a soil for the fraction that is finer than No. 200 sieve size (0.075 mm). The lower limit of the particle-size determined by this procedure is about 0.001 mm. tools 1- Sensitive balance. 2- Hydrometer. 3- Control cylinder. 4- Sedimentation cylinder. 5- Thermometer. 6- Mixer. 7- Stop watch. Procedure • Dry the sample ( which passed sieve # 200 ) in an oven, then take ( 50 gram ) of it to do the hydrometer test on it . • Prepare two cups filled with 125 mL water , then add to one of them Sodium Hexametaphosphate substance ( so that the concentration become 4 % , so for this cup we need 5 gram of the substance ) . • Put one of the two cups in the control cylinder and add water to 1000ml. • Put the Hydrometer in the control cylinder and wait until it is rest at the water then tack its reading – this reading called Zero Condition - . • Put the soil in the other cup , then we have to mix it slurry – in a mixer for 5 minutes with adding water to the mixer till we fill half of the mixer . • Move the soil to the sedimentation cylinder and add water to 1000 ml. • Close the cylinder then we have to rotate it 30 times in a minute and wait a bit, then put the Thermometer and the Hydrometer in the sedimentation cylinder . • Record the value of the Temperature and take the reading of the Hydrometer after specific periods of time – these time periods depend on the specifications of the experiment (1,2,4 ,....) minutes – then keep recording the Hydrometer readings at the specific times till the Hydrometer reading reach the Zero Condition reading . • • • • • 1 min T=20 C Ra= 47mm 2 min T=20 C Ra= 42mm 4 min T=20 C Ra= 37mm 8 min T=20 C Ra= 32mm 16 min T=20 C Ra= 29mm 45 40 35 % passing 30 25 20 15 10 5 0 1 0.1 0.01 Grain Size ( mm ) 0.001