Department of Chemistry and Biochemistry Queens College of CUNY Laboratory Syllabus and Schedule for Chemistry 101.1 – Spring 2016 Required Text: Laboratory Experiments for Introduction to General, Organic, and Biochemistry, 8th Edition. by Bettelheim & Landesberg Week 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Experiment Check-in; Safety Video #1 – Laboratory Techniques/Measurements #2 – Density Determination #3 – The Separation of the Components of a Mixture #6 – Determination of the Formula of a Metal Oxide #15 – Water of Hydration #7 – Classes of Chemical Reactions (Part 1) #7 – Classes of Chemical Reactions (Part 2) #16 – Factors Affecting Rates of Reactions #17 – Equilibrium and LeChatelier’s Principle #11 – Charles’ Law #12 – Properties of Gases (Determining Molecular Weight) #19 – Analysis of Vinegar by Titration Check-out; No Experiments Performed SAFETY FIRST!!! The following safety guidelines must be followed at all times: • • • • • • • Goggles must be worn in the laboratory at all times, even if you have completed your experiment. Having and/or consuming food or drink in the laboratory is strictly prohibited. Never leave a flame unattended. Tie back long hair and secure all loose clothing before conducting any experiments. Feet must be completely covered during lab – no open toed shoes (sandals, flip=flops or the like). If an accident occurs, notify your lab instructor immediately. Do not run or throw anything in the laboratory. • • • Always listen carefully to your lab instructor for safety precautions and procedure modification. All chemical waste must be disposed of properly. Your instructor will provide you with specific instructions at the beginning of each lab regarding how to handle the chemical waste for that experiment. Failure to adhere to safety guidelines may result in your removal from the lab and an automatic failure for that experiment. Chemistry 101.1 Grading Rubric A quiz based on the previous lab experiment will be administered at the beginning of each lab session. NOTE: Tardiness will result in a grade of zero (0) for that day. Your quiz average is worth 25% of your overall grade. The lab reports comprise 75% of your overall grade. Included in your lab report is your pre-lab assignment, which must be completed and experimental lab procedures read before coming to class each day. The full lab report is required for each experiment and is due at the beginning of the next lab class following the completion of the lab experiment. For Laboratory Experiment #7 (Classes of Chemical Reactions) only one laboratory final report is required, upon completion of Part 2. Your lab report should include the pre-lab, data sheet(s), and answered post-lab questions stapled together. All pre-labs, data sheets, and post-lab questions are to be found in the laboratory textbook (Bettelheim & Landesberg). You may either cut from the text or use photocopies of those pages for your reports. Bring these to class (with the pre-lab portion already completed) when you are to do the experiment. Data measured in laboratory is to be recorded directly on your sheets. Read the background information and information from the textbook pages for that week’s experiment prior to coming to class. All laboratory experiments are to be performed individually (and evaluated by the instructor). There are no team experiments. Each person registered for lab is to perform each laboratory experiment individually. Chemistry Lab Attendance Policy • • • • ª Attendance in laboratory is mandatory. Students must report to laboratory on time. Late lab reports will be penalized two points (out of a total of 25 points for each report) per week. The first two-point penalty will be applied to lab reports that are submitted after the lab class time when they are due. Lab reports more than two (2) weeks late will not be accepted. A score of zero (0) will be reported for such. Failure to hand in a lab report will result in a grade of zero (0) for that lab, which will be averaged into your overall laboratory grade. A missed laboratory class (for a valid reason - illness, verified by a note from a registered physician; court appearance, verified by a note from an officer of the court; death in the family, preferably your own) can be made-up by following this procedure: (a) Obtain a lab make-up form from your regular lab instructor. (b) Attend an alternate Chem. 101.1 laboratory class that is working on the same experiment that you missed during the week the experiment is being performed. Get signed permission from the instructor of the section you hope to attend to make-up a missed laboratory experiment. (c) Follow the procedures for your missed laboratory experiment from your lab manual. (d) Complete the lab report. (e) Staple the make-up form to your lab report and submit it to your regular lab instructor the next time your class meets. Lab reports more than two (2) weeks late will not be accepted. Week # (Experiment) 1 (Check-in) 2 (#1) 3 (#2) 4 (#3) 5 (#6) 6 (#15) 7 (#7-Part 1) 8 (#7-Part 2) 9 (#16) 10 (#17) 11 (#11) 12 (#12) 13 (#19) 14 (Check-out) Monday 0915-1205 Feb 1 Feb 8 Feb 22 Feb 29 Mar 7 Mar 14 Mar 21 Mar 28 Apr 4 Apr 11 Apr 18 May 2 May 9 May 16 Monday 1340-1630 Feb 1 Feb 8 Feb 22 Feb 29 Mar 7 Mar 14 Mar 21 Mar 28 Apr 4 Apr 11 Apr 18 May 2 May 9 May 16 Tuesday 0940-1230 Feb 2 Feb 16 Feb 23 Mar 1 Mar 8 Mar 15 Mar 22 Mar 29 Apr 5 Apr 12 Apr 19 May 3 May 10 May 17 Tuesday 1830-2120 Feb 2 Feb 16 Feb 23 Mar 1 Mar 8 Mar 15 Mar 22 Mar 29 Apr 5 Apr 21 Apr 19 May 3 May 10 May 17 Wednesday 0915-1205 Feb 3 Feb 10 Feb 17 Feb 24 Mar 2 Mar 9 Mar 16 Mar 30 Apr 6 Apr 13 Apr 20 May 4 May 11 May 18 Thursday 0940-1230 Feb 4 Feb 11 Feb 18 Feb 25 Mar 3 Mar 10 Mar 17 Mar 24 Mar 31 Apr 7 Apr 14 Apr 21 May 5 May 12 Friday 0915-1205 Jan 29 Feb 5 Feb 9 Feb 19 Feb 26 Mar 4 Mar 11 Mar 18 Mar 23 Mar 25 Apr 1 Apr 8 Apr 15 May 6