Chem 115 Chemistry Laboratory Section 03 (Section ID 243973), Spring 2012 Dr. Wu Xu TR 1:00 – 3:50 pm MY 123 Syllabus ¾ ¾ ¾ ¾ ¾ ¾ ¾ ¾ ¾ ¾ ¾ Description/Objectives Requirements Grading/Evaluation Laboratory Report Contact with Instructor Office Hours Academic Misconduct Disability Accommodation Emergency Evacuation Procedures Tentative Lecture Schedule Laboratory Safety and Rules Description/Objectives Welcome to Chem 115! This course is designed to reinforce concepts learned in lecture of Chem 107 and Chem 108 and provides an introduction into basic laboratory techniques, the experimental methods, and the presentation of scientific data, as well as direct experiences with chemical principles and the properties and reactions of substances. Study hard and have a great semester! I will work hard too! Laboratory Manual for General Chemistry Chem 115: Department of Chemistry, University of Louisiana at Lafayette Requirements Prerequisites: Chem 107 Grading/Evaluation Students must attend all laboratory sessions and pre-lab lectures. There are no make-up labs. A score of ZERO will be assigned for each missed lab report. In the event, a student must miss a lab session for a valid excuse, the student must contact me at least 24 hours before or no later than 24 hours after the lab. A makeup pre-lab and/or a makeup quiz before or after the schedule lab will be decided at the discretion of the instructor. Makeup pre-labs and makeup quiz are generally more challenging. Chem 115 UL-Lafayette Spring 2012 Wu Xu Page 1 1/11/2012 Please be on time. Each lab period will begin with an important short lecture or a quiz or demonstration. Each pre-lab is due in the beginning of class. Each lab report is due in the beginning of next class. Tuesday lab reports will be due on Thursday and Thursday lab report will be due on Tuesday of the following week. The penalty for late assignments including pre-lab and lab report is two points per day. You need to purchase a notebook for keeping lab notes. The notebook is different from the written lab report. The purpose of the notebook is to allow someone to see exactly how the experiments were performed and what results were obtained. Twenty-three experiments are scheduled for this course. There will be twenty-two closed-book quizzes during the course of the semester. Each 15 minute quiz will cover the experiments, which you performed last time and will be worth 15 points. One quiz with the lowest score will be dropped. There will be twenty-three pre-labs and twenty-three lab reports during the course of the semester. One pre-lab with the lowest score and one lab report with the lowest score will be dropped. If you did not miss any of the twenty-three scheduled experiments for this course, you will obtain 30 bonus points. Final exam will be comprehensive and a study guide will be given to help you to prepare the final exam. Summary of Grading Scheme: (1) Pre-labs (5 points each): 110 points (2) Lab Reports (15 points each): 330 points (3) Quizzes (15 points each): 315 points (4) Final Exam 200 points Total: 955 points The grading will follow a standard percentile scale: 90 - 100% 80 – 89% 70 - 79% 60 - 69% 0 - 59% A B C D F Laboratory Reports Each experiment requires a written laboratory report, which contains: Title, Date, Objective, Results and Conclusions; Title and Date (1 point): a single sentence that states the experiment and write the date when the experiment was performed; Objective (1 point): one or more sentences that explain the purpose of the experiment and provide any relevant background information to help readers to follow the narrative of the report; Results (11 points): statements of fact regarding the data collected and your observations; appropriate tables or figures could be used; Conclusion (2 points): one or more sentences that summarize the results. Chem 115 UL-Lafayette Spring 2012 Wu Xu Page 2 1/11/2012 Contact with Instructor Dr. Wu Xu Office No. 138 Biochemistry Lab No. 221 and 236 Montgomery Hall Telephone: 337-482-5684 (Office) Email: wxx6941@louisiana.edu Office Hours Tuesday, 4:00pm - 5:00pm Thursday, 4:00pm - 5:00pm Please contact me if you have any questions. I will be very happy to help each of you. You are welcome to stop by my office any time. Academic Misconduct All acts of dishonesty in any work in this course will constitute academic misconduct. Exams and quizzes are an exercise in individuality. Any cheating on an exam or a quiz will result in an automatic score of ZERO point for that exam or quiz and may result in a grade of 'F' for the course. Disability Accommodation For more information about services available to UL Lafayette students with disabilities, contact Dr. Carol Landry at 482-5252. Emergency Evacuation Procedures A map of this floor is posted near the elevator marking the evacuation route and the Designated Rescue Area. This is an area where emergency service personnel will go first to look for individuals who need assistance in exiting the building. Students who may need assistance should identify themselves to the teaching faculty. Tentative Lab Schedule for Chem 115 Week of Jan 9 Day R Topics Introduction & Safety Jan 16 T R No lab Check In and Experiment 1. Inorganic Chemical Reactions Jan 23 T R Experiment 2. Measurement Experiment 3. Reactions of Copper & Use of Common Laboratory Techniques Jan 30 T R Experiment 4. Solubility of Potassium Nitrate Experiment 5. Stoichiometry - Hydrates Feb 6 T Experiment 6. Molar Mass of an Active Metal Chem 115 UL-Lafayette Spring 2012 Wu Xu Page 3 1/11/2012 R Experiment 7. Synthesis of Alum Feb 13 T R Experiment 8. Freezing Point Depression Experiment 9. Volumetric Analysis Feb 20 T R Mardi Gras Holiday No lab Feb 27 T R Experiment 10. Spectrophotometric Analysis Experiment 11. Indirect Analysis of Potassium Mar 5 T R Experiment 12. Kinetics I Experiment 13. Kinetics II Mar 12 T R Experiment 14. Heat, Temperature and Calorimetry Experiment 15. Thermochemistry Mar 19 T R Experiment 16. pH Measurement and pH Titration Curve Experiment 17. Buffers Mar 26 T R Experiment 18. Back Titration of Ammonium Experiment 19. Redox Titration Apr 2 T R Experiment 20. Paper Chromatography Experiment 21. Synthesis of Aspirin Apr 9 T R Easter Holidays Easter Holidays Apr 16 T R Experiment 22. Solubility Product Constant Experiment 23. Molar Mass of a Gas & Check Out Apr 24 T Final Exam at 1:00pm – 3:00pm in Room 123 Chem 115 UL-Lafayette Spring 2012 Wu Xu Page 4 1/11/2012