Go to page 2 for 2nd semester “Haste makes waste” “He/She who hesitates is lost” LABORATORY SCHEDULE FOR ORGANIC CHEMISTRY I - CHE2401 Fall 2004 (Wk) Date of Lab (1) Aug 19 (2) Aug 26 Lab Exercise TECH 700 Practicing Safety in Organic Lab1 Introduction to Infrared (IR) Spectroscopy TECH 702 Microscale Techniques2 (3) Sep 2 TECH 701 Measuring Melting Points2 (4) Sep 9 CA 16 Spectroscopy (5) Sep 16 TECH 710 Infrared Spectroscopy 2 (6) Sep 23 TECH 704 Separation … by Distillation3 (7) Sep 30 TECH 703 Purifying … by Recrystallization3 (8) Oct 7 TECH 705 Separating … by Solvent Extraction3 (9) Oct 14 REAC 712 Dehydrating Cyclohexanol2,3 (10) Oct 21 REAC 714 Studying SN1 & SN2 Reactions2,3 (11) Oct 28 REAC 734 Molecular Rearrangement Reactions3 (12) Nov 4 (13) Nov 11 SYNT 730 Dyes and Dyeing3 (14) Nov 18 ANAL 751 Enantiomeric Purity of Ibuprofen (15) Dec 2 Equipment Check In Must be completed prior to next week’s laboratory session. Ongoing…work on the tasks in subsequent weeks or outside of scheduled labs. 3 Laboratory report is required for this work. 1 2 533576204 March 8, 2016 “Haste makes waste” “He/She who hesitates is lost” LABORATORY SCHEDULE FOR ORGANIC CHEMISTRY II - CHE2403 Spring 2005 (Wk) Date of Lab Lab Exercise (1) Jan 20 SYNT 713 Preparing Isopentylacetate by the Fischer Esterification2,3 (2) Jan 27 Grignard Reaction–Carboxylic Acid3 (3) Feb 3 Finish IR spectroscopy on benzoic acid product (4) Feb 10 ANAL 729 Identifying an Unknown Alcohol (5) Feb 17 TECH 722 Isolating Clove Oil from Cloves Using Steam Distillation2,3 (6) Feb 24 Finish IR spectroscopy on Clove Oil product (7) Mar 3 KINE 733 The Kinetics of Solvolysis of 2Chloro-2-Methylpropane2 (8) Mar 10 KINE 733 The Kinetics of Solvolysis of 2Chloro-2-Methylpropane, Continued.3 (9) Mar 24 SYNT 720 Aldol Condensation: Synthesis of Dibenzalacetone3 (10) Mar 31 SYNT 724 Friedel-Craft Alkylation: Kinetic versus Thermodynamic Control2,3 (11) Apr 7 (12) Apr 14 SYNT 725 Oxidizing Methoxybenzyl Alcohol Using Phase-Transfer Catalysis2,3 (13) Apr 21 (14) Apr 28 SYNT 731 Luminol Synthesis and Chemiluminescence (15) May 5 Equipment Check In 2Ongoing… work on the tasks in subsequent weeks or outside of scheduled labs. 3Laboratory report is required for this work. 533576204 March 8, 2016