Radiation Safety Committee Margaret Telfer Building K07 Telephone +61 2 9351 7722 Facsimile +61 2 9351 5868 File Reference: 2006/2525 email howarda@usyd.edu.au 30 July 2008 INFORMATION SHEET No. 8 REMOVAL & DISPOSAL OF EQUIPMENT FROM RADIOISOTOPE LABORATORIES Introduction This information sheet outlines the procedure required for the removal of laboratory equipment from areas where radioisotopes have been used. The removal may be either for disposal as general waste, or for relocation to another laboratory. The aim of this procedure is to ensure that equipment: 1. Does not contain unwanted radioactive material 2. Is not contaminated with radioactive isotopes, Fridges and freezers are the most common items that fall into this category. In most cases they have been used to store radioactive stock solutions or contaminated research specimens. Responsibilities It is the responsibility of the chief investigator or laboratory manager to: Ensure that contaminated items are decontaminated prior to their removal from the radioisotope laboratory. Make arrangements for any unwanted sources to be removed from the equipment and appropriately stored or disposed of. 106745486 Page 1 of 6 Created on 13/11/2008 10:31:00 Radiation Safety Committee Margaret Telfer Building K07 Telephone +61 2 9351 7722 Facsimile +61 2 9351 5868 File Reference: 2006/2525 email howarda@usyd.edu.au 30 July 2008 1. Remaining Radioactive Sources The chief investigator or laboratory manager must conduct a thorough visual inspection of the inside of the fridge or freezer to confirm that no material is present. Particular attention should be paid to door compartments and trays in the bottom of the unit. 2. Contaminated Equipment In order to conduct an accurate assessment of any contamination, all isotopes previously used in the area must be known. List the isotopes used, their activities and the date last used in Attachment 1. After identifying what isotopes have been used in the area, select a suitable radiation contamination meter to check if there is any residual contamination. This direct monitoring method is appropriate for the detection of gamma emitting isotopes such as I-125 or the higher energy beta emitting isotopes such as P32 and P-33. Lower energy S-35 & C-14 can also be detected by this method if the monitor has the appropriate energy response. This direct survey method is however not appropriate for low energy beta emitting isotopes, such as tritium [H-3]. If H-3 has been used in the laboratory the equipment must be wipe-tested and counted in a liquid scintillation counter. If alpha emitting isotopes have been used contact the University Radiation Safety Officer before proceeding. Measurements using a contamination meter. Contamination measurements should be conducted at 10 mm above the equipment’s external & internal surfaces [fridges & freezers]. This will give a reading in counts per second [CPS]. Details of monitor used, who conducted the survey, the date of the survey and the CPS readings should be recorded on the Contamination Measurement Results form in Attachment 2. 106745486 Page 2 of 6 Created on 13/11/2008 10:31:00 Radiation Safety Committee Margaret Telfer Building K07 Telephone +61 2 9351 7722 Facsimile +61 2 9351 5868 File Reference: 2006/2525 email howarda@usyd.edu.au 30 July 2008 Wipe testing Monitors will not detect low energy beta. The most commonly used low energy beta source in the University is tritium [H-3]. The method used to confirm that there is no contamination on surfaces from H-3, is to wipe the surface and count the sample in a liquid scintillation counter. The method is as follows: Wipe surfaces for removable contamination by rubbing a moist 25 mm filter paper disc over approximately 100 cm 2 of the test area. Use a grid of approximately 1 meter2. Analyse wipe tests in a liquid scintillation counter [many counters will count for both H-3 & C-14]. Attach printout from counter! Remedial Action 1. Where radioactive sources are present they must be identified, and removed from the equipment. Where possible they should be disposed of through the waste system otherwise placed into long term storage. 2. Where surface contamination is detected the equipment must be decontaminated. The goal is to remove all contamination. This may require the monitoring/counting/decontamination process to be repeated several times. If detectable contamination remains after 3 such attempts, advice from the University Radiation Safety Officer should be sought. Equipment that is unable to be completely decontaminated may be able to be disposed of through the Hazardous Waste service. 106745486 Page 3 of 6 Created on 13/11/2008 10:31:00 Radiation Safety Committee Margaret Telfer Building K07 Telephone +61 2 9351 7722 Facsimile +61 2 9351 5868 File Reference: 2006/2525 email howarda@usyd.edu.au 30 July 2008 Clearance 1. Radioactive Sources The equipment was inspected and found: Not to contain a radioactive source OR Had any radioactive material removed The equipment is safe to dispose of as general waste. 2. Contaminated Equipment. Test Specification: All accessible external & internal surfaces of the equipment were monitored at 10 mm from surface using a contamination monitor OR wipe tested and counted if low energy sources were present. Acceptance Specification: Only equipment with no detectable surface activity is to be cleared for disposal as general waste There was no indication of any radioactive contamination by or emitting isotopes on any external or internal surfaces of the equipment. The equipment is safe to dispose of as general waste. Chief Investigator/Laboratory Manager: {insert name} University Radiation Safety Officer: Howard Ackland Report Date: 106745486 Page 4 of 6 Created on 13/11/2008 10:31:00 Radiation Safety Committee Margaret Telfer Building K07 Telephone +61 2 9351 7722 Facsimile +61 2 9351 5868 File Reference: 2006/2525 email howarda@usyd.edu.au 30 July 2008 ATTACHMENT 1 RADIATION SOURCES USED IN THAT AREA Laboratory: Building: EPA Registration Number: The following isotopes were used in this laboratory. Isotope 106745486 Maximum Activity [in MBq] Page 5 of 6 Date last used Created on 13/11/2008 10:31:00 Radiation Safety Committee Margaret Telfer Building K07 Telephone +61 2 9351 7722 Facsimile +61 2 9351 5868 File Reference: 2006/2525 email howarda@usyd.edu.au 30 July 2008 ATTACHMENT 2 CONTAMINATION MEASUREMENT RESULTS Equipment: Model No: Serial No: Surveyed by: Date: * POSITION MONITORED Monitor[s] used: CPS Background: ..………. cps ………... cps 106745486 Page 6 of 6 Created on 13/11/2008 10:31:00