ID-1559 AN EXPERIMENTAL INVESTIGATION OF THE BEARING FAILURE MECHANISMS IN BOLTED COMPOSITE JOINTS Yi Xiao and Takashi Ishikawa Structures Division, National Aerospace Laboratory 6-13-1, Osawa, Mitaka, Tokyo, 181-0015, Japan ABSTRACT: This paper presents an experimental investigation of the behavior in mechanically fastened composite structures. CF/PIXA and CF/Epoxy material systems were selected for the strength comparison, and a simple and highly functional measurement system using a non-contact Electro-Optical Extensometer was adopted to evaluate the bearing strength. A static tensile test for a double lap bolted joint was performed. During tests, the fracture process under the load-deformation response was monitored using the acoustic emission measurement. Some of the specimens were unloaded at different loading levels, in order to assess the damage progress and failure mechanisms using soft X-rays and SEM observation of the internal damage. Based on these experimental observations, it can be concluded that the kink band, delamination, fiber-matrix shearing, and fiber-matrix splitting failure formed the major failure modes of the shear cracks. The washer area and bolt clamping conditions should influence the damage progress. Keywords: CF/PIXA Composite, Bearing Strength, Failure Mechanism, Mechanically Fastened Joint, Out-of-plane Deformation, Microscopic Damage Behavior INTRODUCTION Degradation and failure of aircraft structures are frequently initiated at the joints, so that safety, durability and reparability are strongly influenced by the adequacy of joint design. The next generation supersonic transport (SST) aircraft make extensive use of advanced composite materials in both primary and secondary structure, and the mechanically fastened joints have been used. Mechanically fastened joints have generally been used for highly-loaded composite components, although the low bearing stiffness of composites can lead to problems of bolt bending and hole elongation under compressive loading. Significant research [1-4] has been carried out for fastener joints, depending on the specimen geometry and fiber orientation, the joint would be expected to eventually fail in a variety of modes, namely net-tension, shearing-out, and bearing. From the viewpoint of structural design, it is preferred that bearing failure in which a stable failure mode develops should occur. However, bearing failure is a local compressive failure mode due to contact and frictional forces acting on the surface of hole [5]. This fracture process is very complicated and is influenced by many parameters such as washer dimension and lateral clamping [6-9]. Eriksson [6] has shown that several important parameters influence the bearing strength including the lateral constraint condition and ply orientation. Wang et al. [7] examined the bearing failure mechanism as a function of the clamping pressure using the bearing response and bearing strength of bolted joints. In order to evaluate the bearing damage, a pin-loaded bearing (without lateral clamping) and a bolted bearing (with lateral clamping) test was conducted. Wu and Sun [8] investigated that the behavior of pin-contact failure in composite laminates and found fiber micro-buckling in the 0o-plies of the laminate to be an important role in the initiation of bearing damage. Camanho and Matthews [9] carried out a detailed experimental investigation into three basic failure modes of the joint, with the accumulation of delamination damage being the main mechanism of bearing failure. From the above literature, the damage phenomenon of bearing failure in a bolted composite joint would appear to be complicated. One of these complicated results is due to out-of-plane compressive deformation in the vicinity of the hole. Therefore, the fiber microbuckling, matrix cracks and delamination, etc. are easy to occur due to compressive load in laminate structures. An understanding of the occurrence and progress of the microscopic damage behavior is thus necessary to the evaluation of the damage allowable in structural designs. As a basic examination for optimizes joint design of CF/PIXA composites using polyimide resin PIXA with high fracture toughness in this study, a static tensile tests for a double lap bolted joint were performed. In addition, the experimental results of CF/Epoxy composites were also reported to compare with these results. During tests, in order to clarify the relationship between damage progress behavior and bearing strength, the fracture process under the load-deformation response was monitored using the AE (Acoustic emission) method. Some of the specimens were unloaded at different loading levels, in order to assess the damage progress and failure mechanisms using soft X-rays and SEM (Scanning Electron Microscope) observation of the internal damage. The accumulation of basic data for strength prediction on the bearing failure of bolted joints was attempted, whilst the mechanism of bearing failure was examined. EXPERIMENTAL DETAILS Material and specimen preparation In the present work, two types of material systems were selected for comparison: CF(IM-7)/PIXA (Mitsui Chemistry Co. Ltd.) and CF(IM600)/Epoxy (Q133) (Toho Rayon Co. Ltd.) materials [10]. These composites were a quasi-isotropic [45/0/-45/90]2S laminate with same layups, which was made using hot pressing of unidirectional prepreg for 16 layers. The geometrical configuration and testing setup of the joint specimens has been shown in Fig. 1. The double lap joining configurations were adopted so that the bolt fastener attached the CFRP specimen to a Chromium Molybdenum steel fixture (with lateral constrains). The tightening torque was adjusted at 12 ~ 13kgf-cm. All specimens were made with width-to-diameter ratio (W/d=8), edge-distance-to-diameter ratio (e/d=3). Experimental procedures To establish a simpler experimental technique for the bearing strength evaluation of bolted P 38.1 (w) Target Specimen CFRP specimen 4.8 (d) AE sensor 15 (e) Target Bolt ZIMMER camera INSTRON test machine Metal fixture Bolt HP A/D converter Loading steel plate Clamping head Thickness, t=2.24 UNIT: mm P Fig. 1 Geometrical configuration and testing setup of the joint specimens. PC computeri zed capture sysytem Control uni t 101B Fig. 2 Schematic of measurement system by non-contacting Electro-Optical Extensometer. composite joints, a simple and highly functional measurement system has been developed using a non-contact Electro-Optical Extensometer, which does not require special fixtures, and has been proposed as a practical test method [11,12]. In this study, the tests were carried out to evaluate the bearing strength of CFRP composite specimens, using a non-contacting electro-optical extensometer (ZIMMER Co. product MODEL-100B). The measurement system configuration is illustrated in Fig. 2. ZIMMER electro-optical extensometer converts the linear motion of a black-and-white edge (target) into a voltage proportional to displacement; that is to say, the optical image is converted into an electronic image using a special photo cathode. In the conventional contact form measuring method, metal fittings (yokes) have to be installed in which linked both side edges of the specimen with the pinhead [13,14]. In the present method, measurement of the pin relative displacement is possible only by bonding the black-and-white target. Tensile loading was applied using an INSTRON-8501 testing machine; the cross-head speed was 1.0 mm/min. During static tests, the load-displacement response and acoustic emission were recorded in order to understand the fracture process of joint specimens. A two-channel MISTRAS 2001 system (Physical and Acoustic Co.) was used in the AE test, and a sensor using resonant frequency type with 150kHz (PAC R15I) and the threshold was 55dB. Some of the specimens were unloaded at different loading levels, and the damage behavior was observed using soft X-rays and SEM. 1500 16 1250 Load, P (KN) Bearing load at P 1000 Ultimate failure strength 4%d 750 8 P CF/PIXA CF/Epoxy [45/0/-45/90] 4 500 2S 250 d=4.8 mm, e/d=3, W/d=8, t=2.24mm P Bearing strength (MPa) 12 0 0 0 0.5 4%d 1 1.5 2 2.5 3 Displacement, (mm) Fig. 3 Typical load-displacement curve of CF/PIXA and CF/Epoxy specimens. B-S-P6(MPa) Table 1. Experimental data of bearing strength obtained from each joint specimen. B-S-E07a(MPa) Specimens CF/PIXA P-S/N-03 P-S/N-04 P-S/N-07 P-S/N-08 P-S/N-09 Average CF/Epoxy E-S/N-04 E-S/N-06 E-S/N-07 Average 4%d Displacement (KN) (MPa) Ultimate Failure (KN) (MPa) Failure Mode 7.78 9.02 8.94 9.71 9.14 8.9 727.7 842.4 835.1 906.6 853.5 835 13.81 14.2 14.07 14.86 14.54 14.3 1289.1 1326.0 1314.2 1381.1 1357.1 1326 Bearing Bearing Bearing Bearing Bearing 8.63 8.8 8.49 8.6 809.67 825.62 796.46 808 15.85 15.9 15.71 15.82 1486.72 1491.74 1473.45 1485 Bearing Bearing Bearing RESULTS AND DISCUSSION Bearing strength A typical load-displacement curve (P-δcurve) of CF/PIXA and CF/Epoxy specimens is shown in Fig. 3. The bearing strength was obtained based on the bearing load at which the pin relative displacement was deformed by 4% of the pin diameter (4%D), and the ultimate failure load from the peak point of the load. An experimental data of bearing strength obtained from each specimen is shown in Table 1. It can be seen that the average bearing strength of CF/PIXA specimens is bigger at 4%D, but it is lower at ultimate failure strength. Bearing failures AE measurement results [15] To characterize the internal damage of the joint specimens, the result of monitoring by AE measurement is shown in Fig. 4. Two materials, it was more clearly shown in this case that damage behavior was associated with a load increase, with the AE count rate indicating the AE signal activity. When the applied load was increased to nearly the Knee point (about 10KN), a sharp change in the AE signal was observed. Significant nonlinear behavior was present on the load-displacement curve at the same time. At this stage, the microscopic damage of CF/Epoxy specimen was detected near bearing load of 4%D, and it can be seen that the tendency was easily deformed for compared with CF/PIXA specimen. Following this, the load response gradually was decreased. Furthermore, these progresses behavior appeared 16.0 16.0 2500 2500 Applied load 1500 AE Count 8.0 1000 4.0 2000 12.0 First peak point P 4%D Knee point AE Count 8.0 1500 1000 4.0 500 500 0.0 0 50 100 150 0 250 200 AE event count First peak point Knee point AE event count Load, P (KN) 2000 4%d Load, P (KN) P 12.0 Applied load 0.0 0 50 100 150 0 250 200 Time (sec) Time (sec) (b) CF/Epoxy (a) CF/PIXA Fig. 4 Comparison of loading response and AE event count vs. time for CF/PIXA and CF/Epoxy joint specimens. 1000 1000 CF/PIXA CF/Epoxy CF/PIXA CF/Epoxy 800 AE event count AE event count 800 600 400 600 400 200 200 0 0 60 70 80 90 100 Amplitude (dB) (a) Applied Load P=10-12 KN 110 60 70 80 90 100 110 Amplitude (dB) (b) Applied Load P=12-15 KN Fig. 5 Distributions of AE event count vs. amplitudes for load levels at 10-12KN and 12-15KN. 16 50 Applied load P 40 Load, P (KN) 12 Structural fracture 30 P 4%d 8 -- Local fracture 4 20 -- Damage growth 10 CF/Epoxy CF/PIXA -- Damage onset 0 0 50 100 150 200 Accumulative damage (%) max. 0 250 Time (sec) Fig. 6 Accumulative damage (AE energy) for CF/PIXA and CF/Epoxy joint specimens. at stage-by-stage as it can be clearly seen from the AE signal. It was considered that this PARA1 PARA1 corresponded to fiber-matrix splitting and delamination, together with out-of-plane shear PARA1 cracking. Fig. 5 shows AE amplitude distributions of each specimen in various loading stages. Both materials in loading range 10~12KN and 12~15KN, CF/PIXA specimen is manifest at the low or middle amplitude of 80dB, CF/Epoxy specimen at the high amplitude over 90dB is comparatively controlled. Based on the observation of SEM photographs after tested, it can be seen that the fiber micro buckling or matrix crack are correspondent to the AE signal of low or middle amplitude, and delamination or out-of-plane shear crack are correspondent to the AE signal of high amplitude. CF/PIAX 16 CF/Epoxy Stage Ult. P Max (100%) Stage... Applied load, P (KN) 12 Stage 3 (75%) Stage 2 (60%) P4%d 8 Stage 1 (50%) 4 0 0 0.5 1.0 1.5 2.0 Displacement, δ (mm) Fig. 7 X-radiographs for bearing damage under the various load conditions. The variation of accumulated damage rate (accumulated energy) that shows the total of damage production in the same load level is shown in Fig. 6. The AE signal of CF/PIXA and CF/Epoxy specimen was detected in 9KN and 7.8KN respectively. CF/Epoxy was lower than CF/PIXA. And it was observed that when the applied load was increased to 10~12KN range, the accumulated damage rate began to change in AE signal. Until the final fracture, the difference of accumulated damage rate is about 15% for two specimens. It was also accorded to the results of ultimate failure strength in Fig. 3, indicated that the fracture toughness of PIXA resin is high. X-radiographs results Fig. 7 shows X-radiographs for the bearing damage under various loading conditions. Corresponding with the AE results, it is possible to evaluate the damage state and scale of the damage production. In the initiation stage (50% max. load) prior to reaching the P4%D load, it can be seen that microscopic damage has occurred and this agrees well with the AE results. But this damage does not affect very much the response of load-displacement curve. It was also proven that the damage scale of CF/PIXA specimen is small. Upon increasing the load, the extent of damage became more extensive around the hole, significant nonlinear behavior was present on the load-displacement curve, and this tendency continued until reaching the final fracture. The damage scale of CF/Epoxy specimen is relatively large. SEM photographs results During the tests, in order to observe the internal damage of bearing some of the specimens 1 ○ 2 ○ 1 ○ 2 ○ Kink band band of of 00oo plies plies Kink Washer o Kink band of 0 plies CF/PIXA (Load: 60%Pmax) 1 ○ 2 ○ 1 ○ 2 ○ Kink band of 0o plies Washer CF/Epoxy (Load: 60%Pmax) Kink band of 0o plies Fig. 8 SEM photographs of the bearing damage at 60% of maximum load. Washer Washer CF/Epoxy (Load: 60%Pmax) CF/Epoxy (Load: 75%Pmax) Fig. 9 SEM photographs of the bearing damage at 75% of maximum load. CF/PIXA (Load: 100%Pmax) CF/Epoxy (Load: 100%Pmax) Fig. 10 SEM photographs of the bearing damage at 100% of maximum load. were unloaded at different load levels, and the tested specimens were cut along the centerline hole. Micrographs were made of these cross-sections using SEM. Fig. 8 to Fig. 10 shows SEM photographs of the bearing damage along the loading direction, loaded to 60%, 75%, and 100% of the maximum load. At 60% of the maximum load, the unusual kink band damage in the compressive failure can be clearly seen in the 0゜plies, whilst local matrix cracks and delamination also occurred under the washer area, CF/Epoxy specimen was more clearly. Next, the load was increased to 75% of the maximum load, with out-of-plane shear cracks occurring more frequently than the Crushing damage Contact surface (a) Washer -- Washer -- Loss of washer support Fixture -- (b) (c) Fig. 11 Schematic description of the bearing damage mechanisms in bolted joint specimens, (a) damage at contact surface, (b) damage within washer area, (c) damage under washer area. previous load level, and fiber-matrix splitting cracks can also be found in the 0゜plies. Such shear cracks that CF/PIXA occurred in the external surface layer, CF/Epoxy occur in full section of laminate, and the damage scale is also bigger than CF/PIXA. These damage patterns continued until reaching the final fracture, which can be understood from the case of the maximum load. In other words, it is conceivable that the load is reduced stage-by-stage on the P-δcurve due to the shear cracks which occurred intermittently. Summarization of damage pattern Based on the above SEM photograph observations, a schematic description of the damage pattern is shown in Fig. 11. The damage pattern features of bearing failure can be explained as following. (A) Damage at contact surface; it is crushing damage that occurred in contact surface between bolt/hole. This damage progress will be depending on the response of material stiffness and friction effect. (B) Damage within washer area; it is accumulated damage that occurred in washer area, and formation and accumulation of the damage are dependent on the clamping pressure. Since the out-of-plane deformation of laminate was suppressed by clamping pressure the compression failure behavior was mainly expanded along the in-plane direction, and the damage progress has been presented at stage-by-stage. (C) Damage under washer area; the damage such as the large-scale splitting cracks occurred under washer area due to the damage gradually reached the saturation state in washer area, and the joint response rapidly lowers. Based on these experimental observations, it can be concluded that the kink band, delamination, fiber-matrix shearing, and fiber-matrix splitting failure formed the major failure modes of the shear cracks. For the growth of shear cracks it can be concluded that the influence of the washer area and bolt clamping conditions is large. CONCLUSIONS In order to evaluate the bearing strength and damage behavior of the joint specimens, an experimental investigation of CF/PIXA and CF/Epoxy bolted composite joints was performed, and the relationship between load-displacement curve, AE characteristic and failure mechanism was also examined. There are correlations of the damage pattern and damage progress that the activity of the AE signal corresponds to the joint response. Furthermore, corresponding with results observed using X-rays and SEM photography, the bearing failure mechanisms were explained. Based on these, the following remarks can be made: 1. The kink band of 0゜plies and delamination appeared to be the dominant mode in the onset of damage. Out-of-plane shear cracks and fiber-matrix splitting cracks were the major reason for final failure. 2. Lateral constraint condition suppressed out-of-plane deformation, and it was recognized as an important parameter to improve the joint strength. 3. To evaluate the lateral clamping effect on the restrain of out-of-plane deformation, the construction of a 3-D damage model and development of analysis tools should be become a focus of further investigation. REFERENCES 1. Hart-Smith, L. J. “Bolted Joints in Graphite/Epoxy Composites”, NASA Langley Report CR-144899, 1976. 2. Matthews, F. L. “Joining Fiber-Reinforced Plastics”, New York: Elsevier Applied Science (1986). 3. AGARD Conference Proceedings CP-427, “Behaviour and analysis of mechanically fastened joints in composite structures”, North Atlantic Treaty Organization (1988). 4. AGARD Conference Proceedings CP-590, “Bolted/ Bonded Joints in Polymeric Composites”, North Atlantic Treaty Organization (1998). 5. Xiao, Y., Wang, W. X., Takao, Y. and Ishikawa, T. “The Effective Friction Coefficient of a Laminate Composite, and Analysis of Pin-Loaded Plates”, Journal of Composite Materials, Vol. 34, No. 1 (2000), pp. 69-87. 6. Eriksson, I. 1990. “On the Bearing Strength of Bolted Graphite/Epoxy Laminates,” Journal of Composite Materials, 24:1264-1269. 7. Wang, H. S., C. L. Hung and F. K. Chang. 1996. “Bearing Failure of Bolted Composite joints Part I: Experiments,” Journal of Composite Materials, 30(12): 1284-1313. 8. Wu, P. S. and Sun, C. T. April 1997. “Bearing failure in pin contact of composite laminates,” Proceedings of the 38th AIAA/ASME/ASCE/AHS/ASC Structures, Structural Dynamics and Materials Conference, pp.1974-1983. 9. Camanho, P. P., Bowron, S. and Matthews, F. L. “Failure mechanisms in bolted CFRP”, Journal of Reinforced Plastics and Composites, Vol. 17, 1998, pp.205-233. 10. Ishikawa, T. and Matsushima, M. Proceedings of 11th ICCM, Gold Cost, Australia, July 1997, Vol.II, pp. 1-9. 11. Xiao, Y., Hayashi, Y. and Ishikawa, T. “Consideration on Bearing Strength Evaluation Method in Composite Materials by Electro-Optical Extensometer”, April 1999. Proceedings of Annual Meeting of Japan Society for Composite Materials, pp.77-78. (in Japanese). 12. Xiao, Y. and Ishikawa, T. “Non-contact Measurement for Bearing Strength of Mechanically fastened Joints in CFRP Composites”, Journal of the Japan Society of Composite Materials, 26(6): pp.213-218. (in Japanese). 13. JIS K 7080, 1991. “Testing methods for bearing strength of carbon fiber reinforced plastics”, Japanese Industrial Standard. 14. ASTM D 953-95, “Standard Test Method for Bearing Strength of Plastics”, American Society for Testing and Materials (1995). 15. Xiao, Y., Hayashi, Y. and Ishikawa, T. “Examination of Acoustic Emission on Failure Processes of Bolted Composite Joints”, 2000-10. Proceedings of The 25th Symposium For Composite Materials (Japan-Korea Joint Session), pp.77-78.