Gulf of Mexico Shelf Region Waste Management Procedures Completion Fluids / Solids – (Calcium Bromide) Before you begin Description Fluid used to complete the well prior to first flow. Category E&P exempt if used downhole. Analysis To discharge subject to the water discharge permit, the following tests are required: Daily, during discharge – free oil static sheen test. Monthly – oil & grease test. Cannot exceed 29 mg/liter. Priority pollutants may be discharged only in trace amounts. Verify that no priority pollutants are present in the products used by: 1. Checking the manufacturer’s information, or 2. Testing effluent before discharge. A list of priority pollutants is in the glossary of these procedures. Accumulation Fluids that pass all tests above may be discharged Fluids that do not pass all tests above must be contained in portable tanks, cuttings boxes or drums and sent to a E & P waste disposal facility Waste Reduction Minimize wasteful usage practices. Avoid use with priority pollutants. Can be discharged (if it does not sheen) under NPDES permit. Disposal Return to vendor for credit. If used downhole liquids may be disposed of through the completion fluids discharge under the NPDES Permit. Slurried particles used in hydraulic fracturing, the accumulation of formation sands, and scale particles generated during production must be handled as produced sand [and solids]. Last choice, dispose of at a state permitted E&P waste facility. Identify waste as 04 Completion Fluids. Continued on next page Version 2, October 2011 Page 1 of 5 Gulf of Mexico Shelf Region Waste Management Procedures Completion Fluids / Solids – (Calcium Bromide) Before you begin, (continued) Recordkeeping Version 2, October 2011 For shipments to shorebases in Louisiana, prepare Non-hazardous Oilfield Waste Shipping Control Ticket Form UIC-28 (See Example). DO NOT SIGN THIS CONTROL TICKET. It is required to be signed in the presence of the truck driver. Dock personnel must sign. For shipments to shorebases in Alabama, prepare the State Oil and Gas Board of Alabama Waste Liquids Manifest. For shipments to shorebases in Texas, or Mississippi no state documents are required. Complete entry in General Cargo Section [Section II] of the Apache Shipping Manifest. (See example) Maintain a copy of manifest records at offshore and onshore facilities while active. Send original manifests with shipment. Retain records for three years. Page 2 of 5 Gulf of Mexico Shelf Region Waste Management Procedures Shipping Instructions: Completion Fluids / Solids – (Calcium Bromide) 1. Call or FAX Dock/Base to schedule shipment. 2. Package Fluid as follows: a. b. 3. 4. Non-Bulk Packaging: 1. Drum 1A1 or 1A2, 2. DOT Salvage Drum Bulk Packaging: 1. Marine Portable Tanks 2. Cutting Boxes Markings: a. Stencil Container-“Apache” and the generator's location (i.e. Eugene Island 158) Label Package: a. No labels required by DOT. 5. Prepare shipping papers: a. Complete entry in General Cargo Section [Section II] of the Shipping Manifest. (See example). b. For shipments to shorebases in Louisiana, Prepare Non-hazardous Oilfield Waste Shipping Control Ticket Form UIC-28 in Louisiana (See Example). DO NOT SIGN THIS CONTROL TICKET. Sign the ticket in the presence of the truck driver. Dock personnel must sign. c. For shipments to shorebases in Alabama, Prepare State Oil and Gas Board of Alabama Waste Liquids Manifest. d. For shipments to shorebases in Texas, or Mississippi no state documents are required. 6. Placard Vehicle/Vessel: a. No placard required 7. Load cargo in accordance with the following shipping limitations: AIR Passenger Aircraft Cargo Aircraft WATER Cargo and passenger vessels Other Requirements 8. RESTRICTIONS (49 CFR 172.101) No Restrictions No Restrictions RESTRICTIONS (49 CFR 172.101) No Restrictions None Include MSDS with shipment. Version 2, October 2011 Page 3 of 5 Gulf of Mexico Shelf Region Waste Management Procedures NONHAZARDOUS OILFIELD WASTE SHIPPING CONTROL TICKET STATE OF LOUISIANA OFFICE OF CONSERVATION P.O. BOX 94275 BATON ROUGE, LA 70804-9275 UIC - 28 1567899 Manifest No. CONSERVATION COPY ORIGINAL 1726545 1 END PART I TO BE COMPLETED BY GENERATOR Generator Apache Corporation 2014 W. Pinhook Road, Suite 800 Lafayette, LA, 70510 CODES 0152 ↔ Address City/State/Zip (337) 735-8210 Telephone No. ORIGINATION OF WASTE (see instructions on back) 999997 ↔ ↔ 5 OCS-G-1220 Eugene Island 175 Well Name & No. / Description LUW Type Field WASTE IDENTIFICATION AND AMOUNT (IN 42 GALLON BARRELS) 01 Salt Water 07 Prod. Sands/Solids 13 BS &W Waste 02 Oil Base Mud 08 Fresh Water 14 Pipeline Test Water 03 Water Base Mud 09 Rainwater 15 Com. Facility Waste 10 Washout Water 16 Oil Spill Waste 05 Prod. Pit Sludges 11 Washout Pit Water 50 Salvage Crude Oil 06 Prod Tank Sludges 12 Gas Plant Waste 99 Other 04 Completion Fluids 50 DESTINATION OF WASTE SITE CODE Commercial Facility (Company) Name 5101 ↔ CERTIFICATION: US Liquids Batemen Island 1200 Young’s Road, Morgan City, La. 70380 NOTE: MUST BE SIGNED IN THE PRESENCE OF THE TRANSPORTER! Site Name The waste described above was consigned to the carrier named below. I certify that the foregoing is true and correct to the best of my knowledge Sam Bourque am 0/1/11 Signature of Generator’s Authorized Agent pm Date and Time of Shipment PART II: TO BE COMPLETED BY TRANSPORTER IN PRESENCE OF GENERATOR Transporter Graham Gulf, Inc. P.O. Box 2291 PSC PERMIT 9997 ↔ Address City/State/Zip (985) 385-3475 Telephone No. Morgan City, LA, 70380 Truck License No. Trailer License No. If transported by barge, barge and tug identification Barge and Tug Id. CERTIFICATION: I certify that the waste in quantity above was received by me for shipment to the above destination. am pm Signature of Transporter’s Authorized Agent PART III Date and Time Received TO BE COMPLETED BY COMMERICAL FACILITY SITE CODE 5101 ↔ US Liquids Batemen Island 1200 Young’s Road, Morgan City, La. 70380 Facility (Company) Name Site Name CHEMICAL ANALYSIS Chloride (mg/l) CERTIFICATION: Conductivity (mmhos/cm) pH I certify that the waste described in Part I was received by me via the transporter described in Part II Signature of Facility Agent Version 2, October 2011 Date and Time Received Page 4 of 5 Gulf of Mexico Shelf Region Waste Management Procedures FORM OGB-26 5 / 00 STATE OIL AND GAS BOARD OF ALABAMA 420 Hackberry Lane P. O. Box 869999 Tuscaloosa, Alabama 35486-6999 (205) 349-2852 Fax (205) 349-2861 www.ogb.state.al.us To be filled in by Operator AP3 OCSG 5058 #001 Operator Code Manifest Number WASTES MANIFEST PART I: TO BE COMPLETED BY THE OPERATOR Operator Name: Apache Corporation (Mobile 821) 7778 Dauphin Island Parkway, Theodore, AL 36582 Address: (251) 449-7244 Origination of Waste Liquids Operator Name: Operator Type AP3 (337) 735-8220 NATURAL GAS Field County MOBILE 821 FIELD FEDERAL WATERS Description of Waste Calcium Bromide Completion Fluid Quantity of Waste 9.5 BARRELS Destination: Disposer’s Name Business Address Disposal Site Address Disposal Method US Liquids 1200 Young’s Road Morgan City, La. 70380 SEPARATION AND DEWATERING Certification: The waste described above was consigned to the carrier named below. I certify that the foregoing is true and correct to the best of my knowledge Sam Bourque 07 / 01 / 11 Signature of Operator’s Agent 2:30 p.m. Date and Time Shipped PART II: TO BE COMPLETED BY TRANSPORTER (Note: To be completed in presence of Operator) Transporter’s Name Code No. Gulf Glory Business Address Graham License Plate of Truck ALR000011247 Gulf Inc. P.O.Box 309, Bayou La Batre, AL 36509 (251) 824-1834 License of Trailer If Transported by Barge, Barge and Tug Identification Certification: I certify that the waste in the quantity above was received by me for shipment to the above destination Bill Jones 07 / 01 / 11 Signature of Transporter’s Agent 2:30 p.m. Date and Time Received PART III: TO BE COMPLETED BY DISPOSER Disposer’s Name US Liquids Disposal Site Address Louisiana Certification: I certify that the waste in the quantity and description above was received by me for proper disposal. Dennis Smith 07 / 03 / 11 Signature of Disposer’s Agent 1:30 p.m. Date and Time Received INSTRUCTIONS Read Carefully and Comply Fully 1. Every shipment of wastes liquids shall be accompanied by this form. 2. At the time of transport, the operator shall initiate the manifest by completing and signing Part I. The operator shall assi gn a sequential manifest number in the upper right corner. The number should be preceded by the operator code number provided by the State Oil and Gas Board. 3. The transporter shall complete and sign Part II. 4. The operator shall copy form and mail to the Board within ten (10) days. 5. The original shall accompany the wastes shipment. 6. Upon receipt of the wastes, the disposer shall complete and sign Part III. 7. The transporter shall retain a copy. 8. The disposer shall retain a copy and mail a copy to the operator and the original to the Board within ten (10) days. Version 2, October 2011 Page 5 of 5