Form 20
Version 3.0 (2007/2008)
Heriot-Watt University - Module Descriptor Template (RAY)
Module Title
Analytical Chemistry
School
Engineering and Physical Sciences
Module
Co-ordinator
Dr J.H. Cameron
SCQF
Level
9
Module
Code
1. Pre-requisites
Minimum D grade in Stage 2 core Chemistry modules, or the equivalent
2. Linked Modules
(specify if synoptic)
3. Excluded Modules
Forensic Analysis
4. Replacement Module
Code:
6. Degrees for which this
is a core module
7. Aims
5.
B19AC
Semester
2
On or OffCampus
Credits
On
15
Availability as an
Elective
Yes
No

Date Of Replacement:
MChem, BSc(Hons) and BSc(Ord) Chemistry; MChem Chemistry with a Year in North America ; MChem Chemistry with a Year in
Europe; MChem Chemistry with Industrial Experience
The module aims to provide :
 a general introduction to quantitative analytical methods
 an introduction to chemical separation techniques and to discuss the application and practice of various chromatographic methods in chemical analysis
 an introduction to the properties and reactions of gas phase ions and their use in the interpretation of spectra in analytical mass spectrometry
 an introduction to electrochemical methods of chemical analysis.
8. Syllabus




Quantitative Analysis – the use of calibration curves, standard addition and internal standards in analysis.
Separation Techniques – Introduction to chromatographic methods. Column efficiency, plate theory, band broadening (eddy diffusion, longitudinal diffusion and
resistance to mass transfer) and the Van Deemter equation. Application of gas chromatography, liquid chromatography, paper chromatography, ion exchange
chromatography and electrophoresis.
Mass Spectrometry – Batch, probe inlet systems, GC-MS, LC-MS, CZE-MS, MS-MS, with selected ion and selected reaction monitoring methods. Electron,
chemical, electrospray atmospheric pressure chemical ionization and inductively coupled plasma MS analyses. MALDI and double sector, quadrupolar, TOF and
ion-trap MS.
Electrochemical Analysis – Voltammetry, polarimetry, redox titrations, potentiometry and coulometry and their analytical applications.
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Form 20
Version 3.0 (2007/2008)
Heriot-Watt University - Module Descriptor Template (RAY)
Module Title
Analytical Chemistry
School
Engineering and Physical Sciences
Module
Co-ordinator
Dr J.H. Cameron
SCQF
Level
9
Module
Code
B19AC
Semester
2
On or OffCampus
Credits
On
15
9. Learning Outcomes (HWU Core Skills: Employability and Professional Career Readiness)
Subject Mastery
Understanding, Knowledge and Cognitive Skills
Scholarship, Enquiry and Research (Research-Informed Learning)
On completion of this module, the learner will be able to:
 Define and discuss the various contributions to chromatographic separation bandwidth
 Design the correct methods and experimental components required for chromatographic separation of a given mixture
 Interpret simple chromatographic data
 Predict the main mass spectral features expected for a molecule
 Use mass spectral data to determine the structure of a molecule
 Evaluate numerically the isotopomer intensity data for a molecule
 Display a critical understanding of the concepts, theories and principles discussed in the module
Personal Abilities Industrial, Commercial & Professional Practice
Autonomy, Accountability & Working with Others Communication, Numeracy & ICT
Personal abilities are embedded in the module. The module provides the opportunity to :
 Critically use mathematical methods to analyse isotope intensity and crystal diffraction data
 Interpret, use and evaluate a wide range of data to solve problems of both a familiar and unfamiliar nature
 Manage time effectively, work to deadlines and prioritise workloads
 Use ICT skills with on-line materials, assessments (formative and summative) and web links to support the learning process
 Exercise autonomy and initiative in carrying out defined activities
 Work with a group of peers to discuss problems in analytical chemistry, sometimes taking the lead role
10. Assessment Methods
11. Re-assessment Methods
Method
Duration of Exam
Weighting (%)
Synoptic modules?
Method
Duration of Exam
(if applicable)
Examination
Continuous Assessment
12. Date and Version
Date of Proposal
27 August, 2007
2h
Date of Approval by
School Committee
(if applicable)
70%
30%
Examination (100%)
Date of
Implementation
15 September, 2008
2h
Version
Number
1.0
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