Section 1:Table of Contents Version: 06 Page: 1 of 1 Issue Date: 17 January 2002 Authorised by: Marjorie Dickenson LABORATORY METHOD MANUAL TABLE OF CONTENTS ENVIRONMENTAL LABORATORY – INORGANIC Method No. 06-002 06-003 06-004 06-005 06-006 06-007 06-008 06-009 06-010 06-011 (Section Leader's Copy) Method Title Determination of pH. Measurement of Turbidity by a Nephelometric Method. Measurement of Conductivity. Determination of Total Suspended Solids. Determination Of Total Dissolved Solids. Determination Of Cyanide by Colorimetry. Determination Of Weak Acid Dissociable Cyanide In Soil, Sediment And Sludge Samples. Determination Of Oil And Grease In Soils, Sediments And Sludges By A Gravimetric Method. Determination Of Ammonia by Distillation and Colorimetry. Determination Of Anions In Water By Ion Chromatography. Current Version 03 02 03 01 01 05 04 01 02 05 ENVIRONMENTAL LABORATORY – METALS 06-047 06-048 06-050 06-051 06-054 06-057 06-058 06-063 06-075 06-078 06-079 06-083 06-085 06-096 Acid Digest of Sediments, Sludges and Soils (USEPA 3050). Digest Method for the Determination of Total Metals in Water Samples (USEPA 3030E). Digest method for the Determination of “Total Recoverable Metals” (USEPA 200.2). Digestion of Solid and Liquid Matrix Samples for the Determination of “Total” Antimony, Arsenic and Selenium (APHA 3114). Digest of Sediments, Sludges, Soils and Water Samples for the Determination of Mercury by Continuous Vapour AA. Toxic Characteristics Leaching Procedure (TCLP) – (USEPA 1311). Determination of Calcium in Waters by Flames AAS. Determination of Metals by Flame AAS. Determination Of Metals And Trace Elements By Inductively Coupled PlasmaAtomic Emission Spectrometry (USEPA 200.7). Determination Of Trace Elements In Waters And Wastes By Inductively Coupled Plasma - Mass Spectrometry (USEPA 200.8). Determination of Antimony, Arsenic and Selenium by Hydride AAS. Determination of Mercury by Hydride AAS. Determination of Lead in Blood by GFAAS. Determination of Hexavalent Chromium in Waters by a Colorimetric Method. 02 01 01 01 03 01 03 04 02 01 02 01 03 02 ENVIRONMENTAL LABORATORY - ORGANIC 06-130 06-131 06-133 06-134 06-155 06-167 06-181 06-182 The Determination of BTEX Compounds by GC/FID with Purge and Trap Concentration. The Determination of Monoaromatic Hydrocarbons (BTEX) in Soils, Sediments, Sludges and Waters by a Static Headspace/GC Method. Determination of Volatile Organics in Soils, Sludge and Waters by Static Headspace. Total Petroleum Hydrocarbons in Soil, Sediment, Sludge and Water Samples). The Determination of Polynuclear Aromatic Hydrocarbons by HPLC. The Determination of PAH’s in Soils, Solid Wastes and Groundwater by GC/MS in SIM mode. Operational Qualification of Howling Packett High Performance Liquid Chromatograph. The Determination of Organochlorine and Chlorinated Organophosphorus Pesticides and PCB’s by GC. 03 02 03 02 02 03 01 04 06-001