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CHEM 4432
Fall 2015
Inorganic Chemistry Laboratory
Time/Rm:
Lecture Fridays 12:00-1:00 JMH 626
Lab Fridays 2:30-5:00 JMH 218
Instructor: Dr. Robert H. Beer
Office:
642 JMH; x4430
Email:
HYPERLINK mailto:beer@fordham.edu
beer@fordham.edu
Course Requirements: General and Organic Chemistry, Inorganic Chemistry
(concurrent)
Text: Microscale Inorganic Chemistry by Szafran, Pike and Singh, J.
Wiley, 1991.
Grade Distribution: Written Final Exam (15%). Pre-lab Questions (25%)
and Post-lab Questions/ Lab Results (30%). Final Laboratory Report (15%).
Notebook and Laboratory Work (15%).
Course Description: Synthesis and physical characterization of main group
and transition metal inorganic compounds.
A separate one hour lecture
that presents the concepts of the laboratory experiment(s) will precede
the laboratory period(s) devoted to each experiment.
Topics Covered:
Safety in the Laboratory
Inert Atmosphere Techniques
Using the Inorganic Literature
Inorganic Syntheses and Reactions
Inorganic Physical Methods: nmr spectroscopy, vibrational spectroscopy,
electronic spectroscopy and magnetism
Laboratory Experiments/Assignments:
Experiment 20
Metal Complexes of Dimethyl Sulfoxide
Experiment 30
Preparation and Study of a Cobalt Dioxygen Complex
Experiment 8
Silicone Polymers: Preparation of Bouncing Putty
Chapter 4
Literature Searching and Use of the Inorganic Literature
Experiment 22A
Preparation of Tris(2,4-pentanedionato)Chromium(III)
Experiment 29
C r ( I I I )
Determination of
C o m p l e x e s
ð
Dðo
i n
C H E M
4 4 3 2
O r g a n o m e t a l l i c
G e n e r a l
C h e m i s t r y
L a b o r a t o r y
I n s t r u c t i o n s
L a b o r a t o r y
S a f e t y :
S a f e t y
a n d
w a s t e
d i s p o s a l
p r o c e d u r e s
w i l l
b e
a d d r e s s e d
i n
t h e
f i r s t
l a b o r a t o r y
m e e t i n g .
A t t e n d i n g
t h i s
m e e t i n g
i s
m a n d a t o ry. Please bring a Safety and Breakage Acknowledgement
Form to be completed and handed in at the end of the first class meeting.
Safety glasses and a laboratory coat must be worn at all times. You must
clean up your lab bench area and any general equipment used before
leaving the laboratory.
Laboratory Procedure: Do any assigned reading, pre-lab questions and
prepare your notebook ahead of time. Arrive at the laboratory prepared.
Bring all your data and your notebook to every lab period. A brief,
informal presentation on the laboratory procedure and safety precautions
will be discussed by the instructor before starting the lab. You must
attend this lecture. Your notebook will be checked periodically during
and at the conclusion of the laboratory period. After the experiment is
completed, store the product of a reaction in a vial labeled with the
formula, your initials and notebook page number.
Laboratory Notebooks: Follow the guidelines for keeping a notebook in
the text. A bound laboratory book is required; a composition notebook is
sufficient. Please number the pages of the notebook and include a table
of contents, which should be kept up to date. Please date all entries.
Any loose-leaf information (analyses, spectra) should be bound in a three
ring binder and labeled with the compound or reaction, conditions, e. g.
solvent, initials of the student and the notebook page that refers to the
experiment.
Laboratory Assignments: Pre-lab questions will be given out at the
lecture prior to the laboratory period.
Complete the questions prior to
the laboratory and turn them in at the beginning of the laboratory
period. Post-lab questions and instructions for reporting results will
be due at the subsequent class meeting, after the laboratory period. If
the experiment includes a synthetic procedure, please hand in your
labeled product and copied pages from your notebook related to that
experiment (which will be given a separate score) along with your postlab questions.
Laboratory Report: One full laboratory report and/or presentation on one
of the experiments will be due two weeks after the conclusion of the
assigned experiment. The long report/presentation should include an
abstract, introduction, experimental, results and discussion section
(using the guidelines in the text). Your discussion section should
include answers to questions posed in pre- and post-lab questions. In
order to properly search and cite literature, read Chapter 4; pay special
attention to 4.A.1 and 4.B. Use the library resources, Chemical
Abstracts/SciFinder Scholar or other electronic library resources to find
review articles and primary literature references. Please record and turn
in notes on your literature search methodology, including your electronic
search, when you turn in your assignment. The literature search will
receive a separate score.
CHEM 4432
Inorganic Chemistry Laboratory
Laboratory Safety and Breakage Policy Acknowledgement Form
(1) I understand and will carry out the practices described in the
laboratory safety lecture and demonstration as well as the laboratory and
safety procedures in Chapter 1 of the text. I agree to read and
understand the procedures and safety information regarding the chemicals
used in the laboratory assignment prior to the scheduled laboratory
period.
(2) Laboratory fees cover the expenses of chemicals I use in the
laboratory. I understand that since these fees do not cover my breakage
of laboratory glassware, equipment or instrumentation,
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