ACADEMIC PROCEDURES This document forms part of the Academic Procedures series Developed by the Directorate of Academic Planning COURSE SPECIFICATION Course code CHM 107 Course title Practical Chemistry I Department Chemistry/Biochemistry/Molecular Biology Credit unit 1 Level (UG) 100 Course leader Dr. R.C. Ehiri Official phone number and email Mobile-08037985949 richcee2003@yahoo.com address Email- richard.ehiri@funai.edu.ng Tuesday 10.00am – 2.00pm; by appointment Office Hours Other staff (if applicable) Mrs A. Nkwor; Mr. F.I. Offor, Official phone number and email Mr F.I. Offor -08063280098; address offorifeanyi@gmail.com Email: clement.ademola@funai.edu.ng Office Hours Thursday 9.00am – 2.00pm; by appointment Lecture Time Thursday 10 - 1pm; Friday 12.00noon - 3:00pm Lecture Venue Chemistry Laboratory For academic year 2013/2014 First Semester Contact hours for the semester Lectures [11 hours ] Labs/Seminars [33 hours] Assessment Method Proportion of marks Mid Semester Exams [15]% Coursework [15]% Examination [70]% This course is to be taken as part of the following programmes: B.Sc. Chemistry B.Sc. Biochemistry B.Sc. Molecular Biology B.Sc. Physics B.Sc. Geology B.Sc. Geophysics B.Sc. Mathematics B.Sc. Statistics B.Sc. Computer Science and Informatics B.Sc. Biology B.Sc. Microbiology B.Sc. Biotechnology B.Sc. Anatomy B.Sc. Physiology B.Sc. Medical Biochemistry Directorate of Academic Planning, FUNAI COURSE AIMS- ALIGNMENT WITH FUNAI VISION AND MISSION The course aims to produce very sharp and brilliant minds who will in the future participate actively in national and global discourse in the area of Chemical Science and Technology. This course is specifically designed to develop in the students the basic practical skills in quantitative analysis and also develop in them the manipulative skills in carrying titration experiments in chemistry. To this end, the various types of titrimetric analysis involving neutralization reactions, standardization of unknown solution, estimation of percentages and purity of compounds are key issues that help to form the content of the course. The main driver to the course lies in the need to equip students with a level of understanding (through practical skills) that will enable them to critically analyze issues based on methods, procedures and research developments at national, industry and workplace levels whilst simultaneously acknowledging increasingly influential, international contexts in relation to Nigerian environment. The incorporation of laboratory safety practices, precautions and first aid skills enables and also equips the students with the research skills and knowledge necessary for them to compete favourably with their counterparts locally and internationally in terms of labour and employment generation and also as key players in the chemical industry. INTENDED LEARNING OUTCOMES Having completed this course the student is expected to: 1 Understand key concepts, guiding principles, contemporary developments and current debates/issues in terms of modern knowledge about neutralization reactions. 2 Understand how and why the study of Chemistry is important and the abundant opportunities available in the chemical sciences sector. 3 Display appropriate knowledge and offer analytical insights that will make him or her employable locally or internationally in any sector. Knowledge of basic chemistry terms such as titration, equivalence point, mole concept and stoichiometry, standard solution, percentage purity, etc. 4 Demonstrate an awareness of the types of practical skills and knowledge vital for handling competently and confidently equipment and hence employment relations and HRM-linked matters arising in the field. 5 Be confident and willing to take up challenges. Be able to practice effectively laboratory safety rules, precautions and first aid. LEARNING AND TEACHING METHODS The unit employs a strategy based on lectures, tutorials and internet supported activities, group and individual activities. The mode of delivery differs and will be designed by individual lecturers following intended learning outcomes (ILOs). INDICATIVE CONTENT Lecture/seminar programme Directorate of Academic Planning, Federal University Ndufu-Alike, Ikwo (FUNAI) 2 FUN AI Wk 1 Lecture Session Topic/Reading for private study Tasks/Think points for private study Lecturers/Tech nologists Morning Strong acid versus strong base Concept of neutralization reaction, balancing reaction and titration Dr. Ehiri, Mrs Nkwor, Mr. Offor, Mr Jayeoye, Mr Semidara Miss Mgbenka Mr Ogbu Miss Ojo 10am12pm; Thursda ys. Afternoon 2 (13pm;Fri days) do 3 do Determination of relative atomic mass by acid base titration 4 do Determination of percentage purity of Na2CO3 5 do Determination of Na2CO3 content of washing soda 6 do 7 8 do Estimation of percentage of ammonia in a sample of ammonium chloride Mid –Semester Examination Standardization of KMnO4 solution by FeSO4(NH4)2SO4.6H2O 9 do Estimation of percentage purity of FeSO4.7H2O using standard KMnO4 10 do Standardization of Na2S2O3.5H2O using std KIO3 11 do Estimation of percentage of Cu in CuSO4.H2O crystals Revision Week Exams Exams 12 13 14 Miss Agha-Okoh Standardization of HCl using standard Na2CO3 Mole concept calculations by formula and /or first principles method Mole concept calculations by formula and /or first principles method Pure and impure compounds. Formula for % purity Mole concept calculations by formula and /or first principles method Moe concept calculation and percentages Mole concept calculations by formula and /or first principles method Pure and impure compounds. Formula for % purity Mole concept calculations by formula and /or first principles method Moe concept calculation and percentages Do Do Do Do Do All staff Do Do Do Do All staff All staff INDICATIVE KEY LEARNING RESOURCES Core reading list This course is in part based around notions and/or material that can be found in the core text(s) listed below. It is therefore likely that you will use, or refer to, in your lecture/seminar sessions the notions and/or material in the books listed here. You will likely be directed to study aspects of these texts in your out-of-classroom time, that is, in your private study. 1. Intermediate Practical Chemistry by C.W.L. Bevan, J. Redhead and A.J. Foley. Directorate of Academic Planning, Federal University Ndufu-Alike, Ikwo (FUNAI) 3 Supplementary reading 2. Basic Concepts of Analytical Chemistry by S.M. Khopkar, New Age Pub., New Delhi, 2009. 3. Analytical Chemistry by Gary D. Christian, 6th Ed., Wiley, 2009. 4. Practical Chemistry for School Certificate by W.K. Akonta and S.A. Afolayan, Macmillan Education, 1980. 5. Concise Chemistry by D. Garvie, J. Hughes, J. Reid and A. Robertson, Oxford University Press, 1979. In addition students are encouraged to explore relevant e-journals such as: Royal Society of Chemistry Review (e.g. www.rsc.org) Journal of Chemical Society of Nigeria CONTINIOUS ASSESSMENT The Intended Learning Outcomes are assessed through: Assessment Mid semester Exams Coursework Semester Exams Weight 15% 15% 70% Deliverables - important dates Ensure that you make a careful note of when the assessment tasks are due in for this course. Try not to leave working on these tasks until the last minute – this is stressful for you and tends to lead to poor quality work. Remember that you have several assessments (for different courses) due the same week and you will need to plan for this. Assessment Mid semester exam- Due date FUNAI week 7 Feedback & Result 14 days after the assessment FUNAI week 10 14 days after the assessment FUNAI weeks 13 and 14 14 days after the assessment To be held at the regular class time and place Coursework Semester Exam Feedback on your work The university is committed to providing you with written feedback for all assessed coursework within 14 days from the submission date. You will get feedback on your performance on a feedback form which will be returned to you. If you do not receive feedback within this time, then you should first contact the course leader. If it proves necessary, you should then contact the Head of Department. Submitted coursework, including your final year project, will not be returned to you. This is true for all coursework, in all courses and at all levels, and does not apply to only this course. We must keep the original copy of all coursework to provide the external examiners with a complete record of your work. Directorate of Academic Planning, Federal University Ndufu-Alike, Ikwo (FUNAI) 4 Late coursework It is the University policy to accept and grade all late items of coursework (up to the published latest date for submission). There is no such thing as 'an extension'. You cannot negotiate new deadlines, and you do not need to get agreement about handing in your work late from the course leader or any other member of staff. Late coursework submissions are, however, subject to penalties (capping) that determine the maximum grade that you can achieve depending upon how late the work is. The current penalty scale can be found below: The following caps to be uniformly applied, in the absence of relevant mitigating circumstances accepted by the BoE: Up to 1 working day late Up to 2 working days late Up to 5 working days late Up to 10 working days late Up to 15 working days late More than 15 working days late Mark capped at 70% Mark capped at 60%; Mark capped at 50%; Mark capped at 40%; Mark capped at 30%; Mark capped at 0%. A working day is here defined as Monday to Friday at any time of year, with the exception of Nigeria national holidays. Students with mitigating circumstances can apply to have penalties removed via submission of the appropriate form and evidence. How to do this is explained in the Student’s Handbook. Planning your time i. Students are expected to attend all classes including seminars and laboratory sessions for each course. It is mandatory for students to have a minimum attendance of 75% in this course to be eligible to take the final semester examination. ii. Learning Skills Development Week is a break from formal subject-specific teaching activities (lectures and seminars) and applies to all undergraduate courses in the University. During that week the university offers a number of very useful free sessions on topics such as essay and dissertation writing, exam technique and job applications. You are strongly encouraged to attend sessions relevant to your studies. iii. Note: Instructors are not required to provide mid semester examination make-up. Directorate of Academic Planning, Federal University Ndufu-Alike, Ikwo (FUNAI) 5