Analytical Chemistry I

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University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

Course Specification

Institution: University of Hail

College/Department: Faculty of Science / Department of Chemistry

A) Course Identification and General Information

1. Course title and code: CHEM 290 – Analytical Chemistry I

2. Credit hours: 4

3. Program(s) in which the course is offered (If general elective available in many programs indicate this rather than list programs): General Chemistry

4. Name of faculty member responsible for the course:

Dr. Osman Farghaly (Male branch)

Dr. Wafaa Yousef (Female branch)

5. Level/year at which this course is offered: 3 rd Level / 2 nd Year

6. Pre-requisites for this course (if any): CHEM 114 – General chemistry II

7. Co-requisites for this course (if any):

8. Location if not on main campus:

Page 1 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

B) Objectives

This course intends to introduce the bases of analytical chemistry for chemistry and biochemistry majors. The emphasis is put either on understanding the theoretical aspects of quantitative analysis or problem solving skills.

Students should:

Know the physical bases for analytical methods discussed during the course and understand them.

Be aware of the sources of errors and have knowledge how to -avoid them.

Know how to calculate the amount of analyte in the specific application of each method.

Know how to obtain calibration curve and how to use it for an analytical purpose.

Know the criteria, which are used for choosing the methods for a particular analysis.

1.

Briefly describe any plans for developing and improving the course that are being implemented (eg. increased use of IT or web based reference material, changes in content as a result of new research in the field):

The course will be mainly based on the interactive learning with computer application to digest the different theory applied on the course this will be achieved by:

1.

Create and design a website for the course.

2.

Completely correlate the course with new scientific application

The course will be modified and changes according the release of new application in the field.

C) Course Description (Note: General description in the form to be used for the Bulletin or

Handbook should be attached)

Analytical chemistry I is dealing with the determination of the absolute or relative abundance (often expressed as a concentration ) of one, several or all particular substance(s) present in a sample. We will start the course by studying basic principles and an intensive introduction to statistical data analysis. This

Page 2 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________ course will focus on the volumetric analytical chemistry. For the purpose of this course, the following material will be covered, Statistical Data Treatment and evaluation, Aqueous Solution and Chemical equilibria, Titrimetric Methods of

Analysis, Principle of Neutralization Titration, Application of Neutralization

Titration, Precipitation Titrimetry, Complexation reactions and titrations and

Application of Oxidation/Reduction Titration.

1. Topics to be covered:

List of Topics

1.

Calculation Used in analytical chemistry

2.

Introduction, Errors in Chem. Analysis, Random Errors in

Analysis

3.

Statistical Data Treatment and evaluation

No. of

Weeks

1

2

1

Contact

Hours

3

6

3

4.

Aqueous Solution and Chemical equilibria 2 6

5.

Titrimetric Methods of Analysis

6.

Principle of Neutralization Titration

2

2

6

6

7.

Application of Neutralization Titration

8.

Precipitation Titrimetry

9.

Complexation reactions and titrations

10.

Application of Oxidation/Reduction Titration

Total

2. Course components (total contact hours per semester): 30 hr

Lecture: 48 hr Tutorial:2.5hr Laboratory: 45 Practical/Field work/Internship:

0.0

2

1

1

1

15

Other: 0.0

6

3

6

3

48

Page 3 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

3. Additional private study/learning hours expected for students per week (This should be an average for the semester not a specific requirement in each week):

The student is expected to spent at least 3 hours per week in his own to fully control and understand the course.

4. Development of Learning Outcomes in Domains of Learning:

For each of the domains of learning shown below indicate:

A brief summary of the knowledge or skill the course is intended to develop.

Application of the scientific method to understand and solve problem

A description of the teaching strategies to be used in the course to develop that knowledge or skill.

It will be achieved through group learning and problem solving technique

The methods of student assessment to be used in the course to evaluate learning outcomes in the domain concerned.

Homework , quiz and General exams

4a. Knowledge

(i) Description of the knowledge to be acquired:

1.

The importance of the analytical chemistry in chemistry world.

2.

The physical bases for analytical methods discussed during the course and understand them.

3.

The sources of errors and how to avoid them.

4.

How to calculate the amount of analyte in the specific application of each method.

5.

The criteria, which are used for choosing the methods for a particular analysis.

(ii) Teaching strategies to be used to develop that knowledge:

1.

Lectures and tutorials

2.

Independent study assignment

3.

Website

Page 4 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

4.

Group learning

5.Self learning

(iii) Methods of assessment of knowledge acquired:

Homework , quiz , group project and General exams

4b. Cognitive Skills

(i) Description of cognitive skills to be developed:

How to use the scientific calculator

Problem solving

Minimizing the personal errors

The interaction between quantitative analysis and the other fields in science

- Choosing the methods for a particular analysis

(ii) Teaching strategies to be used to develop these cognitive skills:

Preparing the main outlines of topics

Homework assignments

Problem solving in the recitation sessions

 Discussing the application of quantitative analysis in our lives and industry

(iii)Methods of assessment of students cognitive skills:

In class short MCQs quizzes

Write report

Major and final exams

Checking the problems solved in the homework assignments

4c. Interpersonal Skills and Responsibility

(i) Description of the interpersonal skills and capacity to carry responsibility to be developed on completion of this course, students will be able to:

How to use the scientific calculator

Problem solving

Minimizing the personal errors

The interaction between quantitative analysis and the other fields in science

Page 5 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

- Choosing the methods for a particular analysis

(ii) Teaching strategies to be used to develop these skills and abilities:

Preparing the main outlines of topics

Homework assignments

Problem solving in the recitation sessions

Discussing the application of quantitative analysis in our lives and industry

(iii)Methods of assessment of students interpersonal skills and capacity to carry responsibility:

In class short MCQs quizzes

Write report

Major and final exams

Checking the problems solved in the homework assignments

4d. Communication, Information Technology and Numerical Skills

(i) Description of the skills to be developed in this domain:

Use Power point and software packages to solve and visualize the concepts

(ii) Teaching strategies to be used to develop these skills:

1.

Encourage team work

2.

Give the students tasks in: a) Problem solving b) Data representation

(iii)Methods of assessment of students numerical and communication skills:

1.

Design home work based on work team and evaluate it on this basis

2.

Writing reports on selected parts of the course

Page 6 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

3.

Exams, short quizzes

4e. Psychomotor Skills (if applicable)

(i) Description of the psychomotor skills to be developed and the level of performance required:

Not applicable

(ii) Teaching strategies to be used to develop these skills: Not applicable

(iii) Methods of assessment of students psychomotor skills: Not applicable

5. Schedule of Assessment Tasks for Students During the Semester

Assessment Assessment Task

(eg. essay, test, group project, examination, etc.)

1

Week

Due weekly

Proportion of

Final

Assessment

10%

2

3

4

5

6

Class activates ( in class quizzes, and homework)

Major exam I

Major exam II

Final comprehensive exam

Lab activates

Lab exam

6

12

16 weekly

15

15%

15%

30%

15%

15%

7 Total - 100%

D) Student Support

1. Arrangements for availability of teaching staff for individual student consultations and academic advice (include amount of time teaching staff are expected to be available each week):

There will be an office hour; at least one office hour daily in different

Page 7 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________ scheduled time for different day, Further more will be a regular meeting with students.

E) Learning Resources

1. Required Text(s): 8 th ed. by Skoog, D.A., West, D. M. Holler, F. J. and Crouch S.R

(2007) ISBN 0-03-020293-0

2. Essential References: Fundamentals of Analytical Chemistry, 8th edition by Skoog,

D.A.; West, D.M.; Holler, F.J. and Crouch S.R. Brooks Cole Publisher, 2004 .

3. Recommended Books and Reference Material - Journals, Reports, etc.(Attach a List if needed):

The Essential Guide to Analytical Chemistry, 2 nd edition by Georg Schwedt. Wiley publisher, 1997. ISBN-10: 0471974129, ISBN-13: 978-0471974123.

Analytical Chemistry, 5th Edition by Gary, D. Christian. John Wiley & Sons, 1993.

ISBN-10: 0471597619, ISBN-13: 978-0471597612.

4. Electronic Materials, Web Sites etc:

Websites on the internet that are relevant to the topics of the course

5.

Other learning material such as computer-based programs/CD, professional standards/ regulations:

CD of the text book - Power point presentation

F) Facilities Required

Indicate requirements for the course including size of classrooms and laboratories (ie. number of seats in classrooms and laboratories, extent of computer access etc.)

1. Accommodation (Lecture rooms, laboratories, etc.):

Lecture room with at least 25 seats and DATA SHOW

Page 8 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

 Chemical laboratory with at least 25 places

2. Computing resources:

Multi media associated with the text book and the relevant websites

 Origin Software

3. Other resources (specify - eg. If specific laboratory equipment is required, list requirements or attach list):

Availability of chemicals, glassware and equipment relevant to the course material

Safety facilities

G) Course Evaluation and Improvement Processes

1. Strategies for Obtaining Student Feedback on Effectiveness of Teaching:

Self evaluation and feedback report

2. Other Strategies for Evaluation of Teaching by the Instructor or by the Department:

1.

Self evaluation and feedback report

2.

Departmental council discussions

3.

Discussions within the group of faculty teaching the course

3. Processes for Improvement of Teaching:

1.

Self evaluation and feedback report will be adopted to improve the quality of the course in Regular basis

4. Processes for Verifying Standards of Student Achievement (eg. check marking by an independent faculty member of a sample of student work, periodic exchange and remarking of a sample of assignments with a faculty member in another institution):

NOT APPLICABLE

5. Describe the planning arrangements for periodically reviewing course effectiveness and planning for improvement:

Page 9 of 10

University of Hail

لـــــئاح ةــــعماج

Faculty of Science

Department of Chemistry

موـــــلعلا ةـــــيلك

ءايميكلا مسق

________________________________________________________________________________________________

Self evaluation and feedback report will be adopted to improve the quality of the course in regular basis

The course material and learning outcomes are periodically reviewed and the changes to be taken are approved in the departmental and higher councils.

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