Job Description Job title: Postgraduate Research Officer Department/School: Grade: Department of Chemistry and Department of Chemical Engineering 7 Location: Claverton Down Campus Contract: Fixed term 6 months Job purpose To carry out research at the University of Bath in the framework of a TSB project titled: “Innovative nanoporous carbon materials for energy storage applications” Reports to: Dr Janet L. Scott (CH), Dr Davide Mattia (CE) and Dr Laura Torrente (CE) Staff management responsibility No direct management responsibility, although some supervision of other staff, e.g. technical staff, or supervision of doctoral students may be required. Special conditions Will need to be available to travel to TSB project partners (MAST Carbon, Basingstoke; Johnson Matthey, Sonning Common; Axeon, Dundee; Sharp, Oxford) for quarterly project meetings and other ad hoc meetings, as required. Will be responsible for technology transfer to MAST Carbon and may be required to conduct experiments (with appropriate supervision) at MAST, or at other facilities, such as the Rutherford Appleton Laboratories at Harwell. Human Resources Page 1 Main duties and responsibilities 1 2 3 4 5 6 7 8 9 10 11 12 Conduct extensive review of the scientific and patent literature on designated topics pertaining to the research to be conducted and provide written summaries to the project partners. Design and conduct experiments on the dissolution and regeneration of cellulose from solutions containing ionic liquids to prepare particles of specific size and meso/microporosity as precursors to carbon materials for use in energy storage applications Design and test membrane reactors for the generation of the porous cellulose (or other biopolymer) particles and provide appropriate design parameters/diagrams to the project partners to facilitate scale-up. Design, assist in building and test a full experimental setup, with recycling for recovery/reuse of solvents and particle isolation units. Prepare and characterise samples of biopolymer particles suitable for carbonisation at project partner MAST Carbon, work alongside MAST personnel to carry out carbonisation experiments followed by characterisation of particles using appropriate microscopy and surface area techniques. Assist PI/CIs with project management (organising, attending meetings and corresponding with partners). Assist in publishing results in academic literature, and disseminating results as appropriate to the discipline, e.g. by presentations at conferences. Participate regularly in project meetings (quarterly minimum) and prepare and deliver high quality presentations to the project team and TSB monitoring officer. Participate in the supervision of graduate students and undergraduate project student and the assessment of student knowledge, where appropriate (under the supervision of the PI/CIs). Continually update knowledge and understanding in field or specialism to inform research activity Assist in the preparation of further funding proposals where appropriate and associated with this body of work. Provide a final, consolidated technical report to the TSB project team and assist with technology transfer to MAST Carbon. Human Resources Page 2 Person Specification Criteria Essential Desirable Assessed by A/F I/T R Qualifications √ A PhD degree already awarded, or PhD thesis submitted, in subject area of direct relevance for the project, or an equivalent professional qualification (or equivalent standard for overseas applicants) √ √ Membership of an appropriate professional body (e.g. IChemE, RSC, ACS) √ Experience/Knowledge A sound understanding of reactor design and principles of flow. √ √ √ √ √ √ √ √ √ √ √ √ √ √ √ √ √ Experience of working with porous particles, biopolymers or ionic liquids. Ability to collect and evaluate electron microscopy data and/or surface area and porosity data relevant to biopolymer particles. Experience in the design of experimental protocols and interpretation of results. Demonstrates depth and breadth of specialist knowledge of subject matter to contribute to the research programme. Demonstrates awareness of latest developments in the field of research. Demonstrates good publication record in high quality, peer reviewed journals pursuant to experience/opportunity. √ √ √ √ Skills A developing ability to conduct individual research work and to disseminate results √ √ √ Ability to organise own workload, with guidance from senior colleagues if required. Ability to write research reports and to effectively disseminate outcomes. Excellent verbal, interpersonal and written communication skills. Competent IT skills. √ √ √ √ √ √ √ √ √ √ √ √ √ Attributes Innovation and developing creative solutions √ √ √ Enthusiasm and self-motivation. √ √ √ Human Resources Page 3 Tenacity – working to achieve own objectives and overcoming obstacles Ability to be an effective team worker. √ √ √ √ √ √ Commitment to safe working practices and departmental procedures. √ √ √ √ Code: A/F – Application form, I/T – Interview/Test, R – References Further Particulars Synopsis of the Project Opportunity for career development The funded TSB project “Innovative nanoporous carbon materials for energy storage applications” runs for 36 months and it is envisaged that, at the completion of their 17 month contract, the PDRA candidate will be a very strong contender for a further 18 month contract position at SME MAST Carbon (Basingstoke, UK) to scale up the production of the carbon materials developed. Innovative nanoporous carbon materials for energy storage applications Nanoporous carbon materials are critical components in all energy storage devices - lithium-ion batteries, supercapacitors, flow batteries, and fuel cells. Currently these mainly derive from naturally occurring materials with relatively poor control over the key properties (porosity, surface chemistry, physical form). In this project we intend to build on a new technology for producing controlled structure porous polymers from renewable cellulosic precursors via ionic liquid solution/precipitation. These intermediates will then be converted to controlled structure carbons by adapting recently developed routes for converting viscose rayon precusors. The route should be capable of producing precisely controlled particle size distribution in the range 0.1 to 10 microns, a range critical for the production of storage electrodes, along with precise control of the pore structure in the 1 to 50 nm range. These products will be evaluated in the full range of strorage devices with end-users. Human Resources Page 4