SAFE WORK PROCEDURE LOCATION VMC WRITTEN BY: APPROVED BY: Science Team Solubility of Ammonia Gas Page 1 of 2 DATE CREATED WS&H LAST REVISION June 27, 2014 New PERSONAL PROTECTION EQUIPMENT (PPE) Safety glasses or face shield must be worn at all times in work areas. Long and loose hair must be tied back Appropriate footwear must be worn. Shoe must be fully enclosed. No open toed shoes. Close fitting/protective clothing must be worn. Remove strings hanging from pullovers/sweaters. Rings and jewelry (long necklaces / bracelets, etc.) must not be worn. HAZARDS PRESENT Chemical burns Absorption of Chemicals. Inhalation of Chemicals. Ingestion of Chemicals. Slips / trips & falls Chemical hazards Burns from the Bunsen burner ADDITIONAL REQUIREMENTS APPARATUS / MATERIALS Test tubes Ring stand Burner Bucket of water Rubber stopper and glass tubing Ammonia (liquid) Test tube clamps Equipment orientation WHMIS training SAFE WORK PROCEDURE 1. Don all personal protective equipment including: safety glasses, & protective nitrile gloves (where required). Ensure all loose clothing is either removed or tied back. Remove any jewelry and tie back long hair. 2. Half fill the lower test tube with ammonia. Be careful when pouring the ammonia. 3. Make sure the collecting tube (upside down test tube) is dry. 4. Gently heat the ammonia with the alcohol burner. If it is heated too fast, the ammonia gas will be driven off and then water vapor will start to be driven off into the collecting tube. To avoid burns, be careful when using the burner. 5. After the ammonia starts to gently bubble, heat for one more minute. 6. Remove the collecting tube slowly and carefully so as not to disturb the gas. 7. Place a stopper upside down over the mouth of the test tube. 8. Place the test tube upside down in a bucket of water and remove the stopper. Record your observations. SAFE WORK PROCEDURE 9. Clean up your workstation. REGULATORY REQUIREMENTS WS&H Act W210, Section 4, 5 Mb. Regulations 217/2006, Part 16, (Machines / Tools & Robots) Sections 16.1-16.18) Part 35, (WHMIS Application) Part 36, (Chemical & Biological Substances Application) Solubility of Ammonia Gas Page 2 of 2