GRADUATE STUDENT RESEARCH HIGHLIGHTS 2015 Spring Seminar Series Friday, January 23, 2015 307 SERF Building 2:00 – 2:15 Adam Lindsey (Zhuravleva’s Research Group) Dept. of Materials Science & Engineering The Development of a Cost Effective Multi-Ampoule Growth Station for Large Volume Bulk Production of Metal Halide Scintillator Crystals A significant portion of the cost of synthesizing bulk single crystals of metal halide scintillators can be attributed to the cost of the equipment in a typical Bridgman growth station comprised of a multi-zone furnace and translation components. In an effort to reduce these costs, the Multi-Ampoule Growth Station (MAGS) has been developed as a prototype to investigate the effectiveness of simultaneous growth of multiple crystals in a singular growth station. This experimental test bed was developed to minimize the cost of the furnace construction while exploring the advantages and potential challenges to growth of high quality crystals using multiple ampoule bays. The goal with this technology is to develop control, reproducibility, and maintainability of the growth station while maintaining an overall reduction in the equipment cost over conventional Bridgman furnace design. The objective of this research is to investigate the capability of this cost effective solution to the advanced manufacturing processes specifically required by single crystal synthesis of the metal halide class of materials. 2:20 – 2:35 Bilin Chen (Liaw’s Research Group) Dept. of Materials Science & Engineering Studying the Deformation Behavior of an X52 Pipeline Steel by Neutron-Diffraction Measurements In-situ neutron-diffraction experiments were performed to study the deformation behavior around the crack tip of an X52 [Fe-0.071C1.06Mn-0.24Si-0.026Nb, weight percent (wt. %)] pipeline steel sample, using the VULCAN Engineering Diffractometer at Spallation Neutron Source (SNS), Oak Ridge National Laboratory (ORNL). Compact-tension (CT) specimen was employed in the study. Samples were precracked to a certain crack length, and then they were divided into two groups. One group was hydrogen-charged in a high pressure hydrogen atmosphere, the other served as reference. Both samples were tested to detect the influence of hydrogen. Figures of Lattice parameter versus distance from the crack tip was plotted at various load levels during one fatigue (loading-unloading) cycle. It was shown that lattice parameters were expanded because of the presence of hydrogen, while they were expanded differently with locations and load levels. Join us for refreshments at 1:30 in 307 SERF 2:40 – 2:55 Haoyan Diao (Liaw’s Research Group) Dept. of Materials Science & Engineering Mechanical properties of 3 most-studied highentropy alloys (HEAs) High-entropy alloys (HEAs), a new class of materials, are equiatomic, multi-element systems that can crystallize as a single phase, despite containing multiple elements with different crystal structures. In this talk, I will review the mechanical properties of 3 representative and most-studied HEAs, CoCrFeMnNi, AlxCoCrCuFeNi, and refractory HEAs. The CoCrFeMnNi is confirmed to be consisted of a single face-centered cubic (FCC) solid-solution phase which solidifies dendritically. The elastic behavior studied by neutron diffraction, plastic behavior studied by tensile tests, and fracture toughness at low temperature are summarized to reveal the deformation mechanism of HEAs. The aluminum ratio effect on the structure type transition and fatigue properties of AlxCoCrCuFeNi are presented. The hightemperature mechanical properties of refractory HEAs are presented and compared with conventional alloys. All in all, even though the mechnical properties of HEAs scatter in a wide range, many properties are still promising.