Testing of Cyclone Sand Tailings at High Stresses Matthias Busslinger, PEng, MASc; Howard Plewes, PEng, MSc; Graham Parkinson, PGeo, BSc. Klohn Crippen Berger Ltd., Vancouver BC, Canada, mbusslinger@klohn.com ABSTRACT Over the past four decades, tailings dams have steadily increased in height with new proposed designs reaching close to 300 m. This paper describes research carried out for the pre-feasibility design of a centerline cyclone sand tailings dam for a Gold-Copper porphyry mine. Cyclone sand dams built by the centerline method require (a) sufficient shear strength and (b) free drainage in the cyclone sand. Shear strength is required for shell stability, whereas free drainage reduces liquefaction potential by lowering the phreatic surface. Behaviour of cyclone sands under high dam loads (up to 5,250 kPa) was examined in triaxial and oedometer tests to characterize material deformation, particle crushing effects, shear strength, and permeability. High shear strengths (effective stress friction angle 38º) were found despite observing net contractive behavior at higher stresses. The cyclone sand was found to crush (increase in fines) under elevated stresses, especially under shear deformations. RÉSUMÉ Durant les quarante dernières années, la hauteur des barrages de retenue des résidus miniers a progressivement augmenté pour atteindre environ 300 m dans les nouveaux projets. Cet article décrit la recherche entreprise pour l’étude de préfaisabilité d’une barrage à base de sable cyclone dans le cadre d’une mine de porphyre cuivre-or. Les barrages construites à base de sable cyclone avec la méthode de construction longitudinale nécessitent (a) suffisamment de résistance au cisaillement et (b) le drainage libre dans le sable cyclone; la résistance au cisaillement est requise pour la stabilité de l’enveloppe de la barrage, et le drainage libre permet de réduire le risque de liquéfaction en abaissant le nappe phréatique. Le comportement du sable cyclone sous haute pression (jusqu’à 5,250 kPa) a été étudié avec des essais triaxiaux et oedométriques pour caractériser sa déformation, l’effet du broyage des particules, sa résistance au cisaillement et sa perméabilité. Les résultats montrent que la résistance au cisaillement est élevée (angle de frottement effectif de 38°), malgré que le matériel soit sujet à contraction. A pression élevée, le sable cyclone a tendance à être broyé en fines particules, en particulier lorsque la déformation est cisaillant. 1 INTRODUCTION This paper assesses strength and permeability of cyclone sand for construction of the downstream shell of a 240 m high tailings dam. Owing to the high stresses occurring under this dam height, laboratory tests with stresses up to 5,250 kPa were carried out. The dam design requires sufficient shear strength of the cyclone sand shell, as well as free draining material properties keeping the phreatic surface in or near the drains at the base of the dam. Hence, this paper particularly emphasizes shear strength, deformation behavior, permeability and effects of particle crushing under elevated confining stresses. Flotation tailings for this project will have a gradation with d80 of 110 μm, and 56% fines passing the #200 sieve (i.e. < 74 µm). Cyclone sand is produced by feeding tailings to hydrocyclones, to classify the fines and produce sand suitable for dam fill. The cyclone sand has target fines content of 17% facilitating ease of compaction and providing a permeability of about kv = 5x10-6 m/s (initial compacted state). 2 TAILINGS DAM DESIGN Klohn Crippen Berger Ltd. (KCB) is currently designing a tailings management facility to store 2.3 billion tonnes of tailings for a mining project in British Columbia, Canada. Four tailings dams are proposed to provide staged storage over the mine life of which the tallest dam (240 m) is described here (Fig. 1). The starter dams, ranging up to 100 m high, will be earthfill embankments with shells of random fill supporting a central till core. The dams will be subsequently raised by the centerline method with a downstream shell of cyclone sand supporting the vertical till core along the centerline. No upstream shell will be built, as tailings are gradually raised with the dam, providing lateral confinement of the core. The ultimate dam crest will be 240 m above existing ground with a downstream slope of 3H:1V. Fig. 1 Cross Section Trough Tailings Dam. The sand shell will be constructed by hydraulic sluicing of the sand into cells oriented parallel to the dam crest. “Dykes” of sand pushed up by dozers confine the perimeter of the cells. The cells will be nominally 30 m to 50 m wide and 150 m to 300 m long. Cyclone underflow sand will be sluiced into the cells and compacted by dozer trafficking. For each year of construction, sand placement will start at the downstream toe and raise up to required crest elevation. Due to climatic constraints at the site, downstream cyclone sand will be placed during restricted periods: During the “summer” months of April to October, tailings will be routed to primary cyclones. Underflow from the primary cyclones will be pumped to secondary cyclone stations located along the dam crest. Secondary cyclone underflow sands will be conveyed in slurry pipelines to hydraulic fill cells on the downstream shell. Cyclone overflow, containing the fines, will discharge onto the upstream beach. During the “winter” months of November to March, flotation tailing will not be cycloned, but directly discharged into the impoundment via spigots located every 200 m along the crest of the dams. This will develop the beach and push the tailing pond towards the center of the cells. The deposition will also build up the tailing beach against the dam to support the construction of the central till core during the following summer. Because the final crest elevation will not be achieved until October at the end of each construction season, each year’s dam raise will provide the required storage needed until October of the following year. This ensures that adequate dam freeboard, tailing and flood storage capacity is available at all times. A system of finger drains will be installed at the base of the cyclone sand shell to keep the water level depressed within the dam. Main drains in the center of the valley floor will collect and convey seepage to the toe of the dam. Smaller secondary drains will convey water laterally into the main drains. Drains will comprise an inner core of highly pervious drain rock, surrounded by sand and gravel filter, to prevent piping of the cyclone sand or native foundation soils into the drain core. According to the Canadian Dam Safety Guidelines (CDA 2007) the dam falls under the “extreme” consequence classification. Therefore the dam is designed to withstand an earthquake with a 10,000-year return period, corresponding to design earthquake ground acceleration of 0.14 g. The dam provides enough storage to contain the operating pond and the probable maximum flood (i.e. 30 day flood with 100-year snowmelt) without discharge. Three stability scenarios were considered in design with the following factors of safety (FS) criteria: FSstatic > 1.5; FSpseudo-static > 1.0; and, FSpost-earthquake > 1.2 assuming all uncompacted tailings in the impoundment are liquefied during an extreme earthquake and with allowances for cyclic pore pressures induced in the cyclone sand and alluvium. 3 TESTING Metallurgical pilot plant tests were carried out during the ore processing plant feasibility study. Milling that simulated high pressure grinding rolling (HPGR) was used to crush drill core material for pilot plant tests. Tailings derived from these pilot plant tests were wet sieved to prepare samples matching the anticipated particle size distribution of cyclone sand. Laboratory tests were carried out characterizing the cyclone sand; including USCS soil classification, particle size distribution (PSD), relative density, and compaction. Mineralogy was assessed with quantitative x-ray diffraction (QXRD). Particle shape and angularity was visually characterized using scanning electron microscope (SEM). Uniaxial consolidation behaviour was tested with oedometers. Four consolidated, undrained triaxial test were carried out to measure shear strength and material behaviour. Results from PSD and SEM prior and after testing were compared to analyze particle breakage under static and shear stresses. 3.1 Sample Preparation To replicate the particle size distribution of cyclone sand produced from the tailings, samples of rougher flotation tailings were divided into separate parts by dry sieving (149 μm and 74 μm sieves) and washing. The cyclone sand sample was reconstituted by adding the separate components proportionally and gradation was tested again. Target fines content was 17% with an error margin of ±2%. The cyclone sand PSD is shown as dashed line in Fig. 6 (i.e. Cyclone Sand). Table 1. Cyclone Sand Properties. Property USCS Symbol Specific Gravity Gsa) Particle Size Distributionb) % Sand % Fines d85 Density Min. Dry Density ρmin,d Max. Dry Standard Proctor Density Max. Dry Density ρmax,d a) b) Description SM Silty Sand 2.75 83% 17% 0.208 mm 1280 kg/m3 1580 kg/m3 1640 kg/m3 whole tailings, prior cycloning prior testing 3.1 High Pressure Triaxial Shear Strength and Permeability Testing Samples for triaxial shear tests were prepared to an initial water content of 17% and compacted in a 63.5 mm diameter split mold with a height to diameter ratio of 2:1 after ASTM D4767-11.6.3. Samples were compacted in 7 lifts to a dry density of about 1630 kg/m3 which equates to 103% Standard Proctor density. The compaction procedure was carefully conducted to ensure soil density and permeability was consistent throughout the sample. De-aired water was used to saturate the samples. Four isotropically consolidated, undrained triaxial shear tests were conducted. During the sample consolidation, permeability tests were conducted at several confining stresses. Details of the triaxial testing program are given in Table 3. Table 3. Triaxial Testing Program. Relative Density Relative density of cyclone sand was tested according to BS1377-4:1990. In contrast to relative density testing following ASTM D-2049-69, this procedure does not require a shaking table. A saturated sample is compacted using a vibratory impact hammer into a confining cell to obtain maximum dry density ρmax,d. Minimum dry density ρmin,d is measured in graduated cylinders. Results are listed in Table 1. 3.2 3.3 Sample Mineralogy Quantitative X-Ray Diffraction (QXRD) analysis of cyclone sand material was conducted to quantify the relative proportions of the stronger quartz and K-spar minerals, compared with weaker micas and non-phyllosilicates. Three samples of cyclone sand were reduced to the optimum grain-size range (i.e. <10 μm) for QXRD analysis. Continuous-scan X-ray powder diffraction data were collected and analyzed using International Centre for Diffraction Database PDF-4. Results from QXRD analysis are listed in Table 2 and represent relative amounts of crystalline phases by weight, averaged for the three samples. Test Triax1 Triax2 Triax3 Triax4 p0' (kPa) 1000 2000 3000 4000 Permeability testing at p0' (kPa) 500, 1000 500, 1000, 2000 500, 1000, 2000, 3000 500, 1000, 2000, 3000, 4000 p0' = confining pressure Samples were sheared at 0.1%/min to axial strain εa of 31% to 34%. Fig. 2 shows deviator stress q and excess pore water pressure ue, versus axial strain εa. Net contractive pore pressure response was observed for all samples. All samples experienced strain softening after 20% strain, but this is partly attributed to sample distortion due to high strain. Table 2. Relative Percentage by Weight of Minerals in Cyclone Sand from Quantitative X-Ray Diffraction (QXRD). Mineral Calcite Clinochlore (chlorite) Illite-Muscovite Plagioclase K-Feldspar Quartz Pyrite Dolomite-Ankerite a) Ideal Formula CaCO3 (Mg,Fe2+)5Al(Si3Al)O10(OH)8 KAl2AlSi3O10(OH)2 NaAlSi3O8 – CaAl2Si2O8 KAlSi3O8 SiO2 FeS2 Ca(Mg,Fe2+, Mn)(CO3)2 %a) 5 5 32 6 4 47 0 1 average percentage by weight from 3 tests. Fig. 2. Deviator Stress and Excess Pore Pressure vs. Axial Strain for Triaxial Tests 1 to 4. Fig. 3. Permeability Measured During Consolidation Stages for Triaxial Tests 1 to 4. Fig. 3 illustrates vertical permeability kv as a function of effective confining stresses. Permeability reduces with increasing consolidation stress. Hydraulic conductivities measured during consolidation stages of triaxial tests ranged from 5·10-6 m/s to 5·10-7 m/s and decreased with increasing stress. 3.2 High Pressure Oedometer Tests Two oedometer tests were carried out to assess potential for particle breakage under static loads, by measuring particle size distribution prior and after testing. Samples for oedometer tests were prepared similar to triaxial test samples with moisture content of 17%. Test Oed 5 was carried out in a 63.5 mm diameter cell, while a 50.8 mm diameter cell was used for test Oed 6 to reach higher consolidation pressures. A height to diameter ratio of 1:4 was taken to mitigate side friction effects along oedometer wall. Samples were compacted in 2 lifts to a dry density of about 1510 kg/m3. Oed 5 was step-wise consolidated by doubling the load between each step from an initial vertical effective stress of 15 kPa to a vertical effective stress of 525 kPa, followed by unloading. Oed 6 was consolidated in the same manner as Oed 5. Subsequently, it was reloaded, by adding 1/3 of the previous load in each step to ultimate vertical effective stress of 5250 kPa, followed by unloading to 15 kPa. Results are presented in Fig. 4. The compression index Cc is 0.22 and the swelling index Cs for both unloading phases is approximately 0.02. 4 4.1 MATERIAL BEHAVIOUR STRESSES UNDER ELEVATED Stress Paths Fig. 5 plots the stress paths in terms of q = (σ1' – σ3')/2 versus p' = (σ1' + σ3')/2, where σ1' and σ3' are the effective major and minor principal stresses, respectively. Effective peak friction angle φ’peak is nominally 38º (i.e. sin1(0.6126)). Fig. 4. Void Ratio vs. Vertical Effective Stress for Oedometer Tests 5 and 6. Fig. 2 shows the failure deviator stress q f generally increased with the effective confining stress applied prior to shearing p0', with Triax 1 (p0' = 1000 kPa) being the exception, where qf was greater than in Triax 2 (p0' = 2000 kPa). Undrained shear strength ratio, s u/p0' (where su is undrained shear strength) are listed in Table 4. Since, initial densities for all triaxial tests were very similar, ranging between 1620 kg/m3 to 1630 kg/m3, the difference in su/p0' is attributed to the higher dilatancy of the sand at lower confining stresses. Fig. 5. Stress Paths in p’ vs. q Coordinates for Triaxial Tests 1 to 4. Table 4. Undrained Shear Strength Ratio from Triaxial Testing. p0' (kPa) 1000 2000 3000 4000 p0' = initial effective confining pressure su = undrained shear strength su/p0' 1.1 0.47 0.45 0.49 4.2 Stress Dependency of Permeability Fig. 3 shows decreasing permeability with increasing confinement for all samples (solid symbols in Fig. 3). Overall consolidation was observed to reduce permeability. Some variation exists and with values ranging from 5·10-6 m/s to 5·10-7 m/s, but overall the observed permeability decrease is up to one order of magnitude. 4.3 Particle Crushing Particle size distributions were measured prior and after triaxial and oedometer testing (Fig. 6). Particle size distributions measured after testing lie above the distribution measured prior testing (i.e. Cyclone Sand). Table 5 lists fines content measured with the #200 sieve. Triaxial samples show appreciable increases in fines content of 5% to 9% after testing, with the degree of fines generation increasing with stress level. Changes in fines content for one-dimensional consolidation tests was negligible at 525 kPa and 2.5% at 5250 kPa. Collectively, the results show that shearing plays a larger role in particle crushing than that contributed by confining stress. Table 5. Fines Content Measured Before and After Testing. Sampled Sample ID Before Test After Test After Test After Test After Test After Test After Test Cyclone Sand Triax 1 Triax 2 Triax 3 Triax 4 Oed 5 Oed 6 % Fines >74 µm 17.2 22.5 23.3 23.7 25.8 17.1 19.7 Δ % Fines >74 µm N/A 5.3 6.1 6.5 8.6 -0.1 2.5 Δ % Fines = (% Fines After Testing) – (% Fines Before Testing). Particle crushing due to high stresses on grain angularity were visually examined using trimmings from Oed 6 and Triax 4 samples. Prior to SEM analysis, the entire Oed 6 sample was wet sieved to allow for better assessment of separate grain size fractions, while only an approximately 1 mm thick layer of material was scraped from the shear plane of Triax 4 sample, this sample was not sieved. SEM micrographs of cyclone sand sampled before testing generally show varying degrees of angularity for fine sand size particles, typically with individual particles possessing many concavities (Figs. 7a and 7b). Material below sand size tends to be more elongated with very sharp asperities in a matrix of rock flour (Fig. 7c). This is consistent with the products of the milling process, whereby the larger particles tend to comprise the more crush-resistant minerals, whereas for example less resistant muscovites and calcites are expected to be subject to relatively high breakage. The asperities and relatively low numbers of inter-particle contacts in silt and clay size particles (Fig. 6c) cause high point loads, further contributing to particle crushing of these small particles. The larger sand particles have more inter-particle Fig. 6. Particle Size Distributions Before Testing (Cyclone Sand) and After Testing. contacts and experience less particle crushing. SEM micrographs of cyclone sand after loading up to 5250 kPa in the oedometer (Oed 6) are shown in Figs. 8a and 8b. Fig. 9 is an SEM micrograph for material sampled from the shear plane after consolidating the sample to 4000kPa and subsequent shearing (Triax 4). Post testing images show apparently ‘fresh’ particle breakage surfaces, however based on SEM analysis it cannot be determined whether these surfaces developed while testing, or already existed before. a) Sieved Particles > 149 μm (Micrograph 1c-2c); b) Passing 149 μm Sieve, but Retained on 74 μm Sieve (Micrograph 1a-1d); c) Sieved Particles < 74 μm (Micrograph 2a-2a); Fig. 7 Cyclone Sand Prior Testing: Scanning Electron Microscope Micrographs of Particles Sieved Into Three Fractions. a) Sieved Particles > 149 μm (Micrograph 1d-1c); b) Passing 149 μm Sieve, but Retained on 74 μm Sieve (Micrograph 1b-1e1); Fig. 8 Oed 6 Material After Testing: Scanning Electron Microscope Micrographs of Wet Sieved Particles. Fig. 9 Triax 4 Material from Shear Plane After Testing: Scanning Electron Microscope Micrograph (3-1c). 5 CONCLUSIONS Results from geotechnical laboratory tests to assess suitability of cyclone sand for construction of a 240 m high cyclone sand dam included: 1. Consolidated undrained triaxial tests. The effective stress friction angle of the cyclone sand is 38º. The sand displayed increasing contractive behavior with higher stress levels. The undrained strength ranged from a su/p0' of 1.10 at 500 kPa confining stress to 0.49 at 4000 kPa. 2. Hydraulic conductivities measured during consolidation stages of triaxial tests ranged from 5·10-6 m/s to 5·10-7 m/s and decreased with increasing stress. 3. Crushing of the sand under the confining stresses up to 5250 kPa in the oedometer tests was measured to contribute up to 2.5% increase in fines content. Particle crushing under shearing in the triaxial tests (confining pressure up to 4000 kPa) produced increased fines contents of 5% to 9%, and is consistent with the contractive response of the sand under shearing. 6 ACKNOWLEDGEMENT The authors thank Dr. Myles Lawler for his contribution to the coordination and interpretation of the testing program, Ms. Kate Lunney for preparing figures and tables, and Dr. Matthieu Sturzenegger for translating the abstract. REFERENCES Canadian Dam Association [2007]. “CDA Dam Safety Guidelines”. http://www.cda.ca.