COURSE INFORMATION FORM Course Code and Title GDM 212 INSTRUMENTAL FOOD ANALYSIS H+T/C 2+2/3 ECTS Credit 5 Year / Semester Sophomore Year / Fall Semester Course Level Undergraduate Course Type Compulsory Department Food Engineering Prerequisites None Teaching Method Theoretic-Practice Period (week-hour) 14 week-2 hours of lectures 2 hours of practical per week Course Language Turkish Course Objective To adopt the basic concepts underlying the major instrumental methods and to give the theoretical and experimental information about devices and applications because today, almost all laboratory analysis is implemented with small or large instruments Course Content Introduction to instrumental food analysis, techniques of instrumental analysis and basic principles, refractometry and polarimetry, UV-Vis absorption spectroscopy, fluorometry and chemiluminescence, infrared (IR) spectroscopy, atomic absorption spectroscopy, atomic emission spectroscopy, NMR spectroscopy, mass spectroscopy, X-ray spectroscopy, chromatographic techniques-1: HPLC-GC applications, chromatographic techniques-1: GC-MS applications, electrophoretic techniques. Assessment System Semester Requirements Number Contribution % 1 20 Midterm Exam Quiz Homework Attendance 14 20 Application 15 Total 40 Contribution to the Overall Success Contribution of the Final Exam to the Overall 60 Success Total 100 ECTS Workload Table Criteria Number Time Total Workload (hour) (hour) 14 4 56 Course Time Outside Classroom Study 14 5 70 Time Homework Presentation/Seminar Preparation Midterm Exam 1 1 1 Project Final Exam 1 2 2 Total Workload (hour) 129 Course ECTS Credit 5 Learning Outcomes The student who accomplishes the course successfully; 1.Learns the information about the instrumental food analyses and their basic principles. 2.Learns theoretical and practical information towards the instruments widely used in food analysis and operation of them. 3.Obtains the information about the selection of the appropriate instrument and method for determination of various components in food samples Course Stream Course Sources 4.Gains practical information about the application of food analysis by Refractometry an Polarimetry. 5.Gains practical information about the applications by Atomic Absorption and Atomic Emission Spectrometry for the analysis of mineral and trace elements in food samples. 6.Gains practical information about the applications of chromatographic techniques for analysis of organic species in food samples 7.Learns the information about IR and NMR techniques used for the disclosure of chemical structures. 8.Learns the comparative information about some other alternative techniques as well as instrumental techniques for food analysis. Week Education Modules Preliminary Documents Studies 1. Introduction to Instrumental Food Analysis Presentation Proposed Sources 2. Techniques of Instrumental Analysis and Presentation Proposed Basic Principles Sources 3. Refractometry and Polarimetry Presentation Proposed Practice Sources 4. UV-Vis Absorption Spectroscopy Presentation Proposed Practice Sources 5. Fluorometry and Chemiluminescence Presentation Proposed Sources 6. Infrared (IR) Spectroscopy Presentation Proposed Practice Sources 7. Atomic Absorption Spectroscopy Presentation Proposed Practice Sources 8. Mid-Term Exam 9. Atomic Emission Spectroscopy Presentation Proposed Practice Sources 10. NMR Spectroscopy Presentation Proposed Sources 11. Mass Spectroscopy Practice Proposed Sources 12. X-Ray Spectroscopy Presentation Proposed Sources 13. Chromatographic Techniques-1: HPLC-GC Presentation Proposed Applications Sources 14. Chromatographic Techniques-2: GC-MS Practice Proposed Applications Sources 15. Electrophoretic Techniques Presentation Proposed Practice Sources 1. D.A., Skoog; Holler, F.J. and Nieman, T.A. 2000; Principles of Instrumental Analysis (Trans. Ed. To Turkish: Kılıç, E.; Köseoğlu, F. and Yılmaz H.) Bilim Yayıncılık, Ankara. 2. Gündüz, T. 1993; Instrumental Analysis (In Turkish), Bilge Yayıncılık, 1993, Ankara. Contribution of the Course to Department Learning Outcomes Course Learning Outcomes Dep. Learn. Outcomes 1.Learns the information about the instrumental food analyses and 2, 3 their basic principles. 2.Learns theoretical and practical information towards the 2, 3 instruments widely used in food analysis and operation of them. 3.Obtains the information about the selection of the appropriate 2, 3 instrument and method for determination of various components in food samples 4.Gains practical information about the application of food analysis 2, 3 by Refractometry an Polarimetry. 5.Gains practical information about the applications by Atomic 2, 3 Absorption and Atomic Emission Spectrometry for the analysis of mineral and trace elements in food samples. 6.Gains practical information about the applications of 2, 3 chromatographic techniques for analysis of organic species in food samples 7.Learns the information about IR and NMR techniques used for the 2, 3 disclosure of chemical structures. 8.Learns the comparative information about some other alternative 2, 3 techniques as well as instrumental techniques for food analysis. Course Coordinator(s) Asst. Prof. Ali GUNDOGDU, Asst. Prof. Cemalettin BALTACI