1 Contribution of AMS measurements in understanding the migmatitic 2 terrains of Pointe Géologie, Terre Adélie (East-Antarctica) 3 Jérôme Bascou1, Bernard Henry2, René-Pierre Ménot1, Minoru Funaki3, Guilhem Barruol4 4 5 6 7 8 9 10 11 1 Université de Lyon, Université Jean Monnet and UMR-CNRS 6524, Laboratoire Magmas et Volcans, 23 rue du Dr Paul Michelon, 42023 Saint Etienne, France 2 Paléomagnétisme, Institut de Physique du Globe de Paris, Sorbonne Paris Cité, Univ ersité Paris Diderot and UMR-CNRS 7154, France 3 National Institute of Polar Research, 10-3 Midori-cho Tachikawa Tokyo 190-8518, Japan 4 Université de la Réunion, CNRS and Institut de Physique du Globe de Paris, Géosciences Réunion, 97715 Saint Denis cedex 9, La Réunion, France 12 13 14 15 16 17 18 1 19 Abstract 20 21 A detailed magnetic mapping using Anisotropy of Magnetic Susceptibility (AMS) technique 22 was carried out in Pointe Géologie archipelago (Terre Adélie, East Antarctica) that represents 23 a deep and hot crust that experienced a long-live anatectic event during Paleoproterozoic 24 times, 1.69 Ga ago. AMS measurements allowed to better characterize the tectonic structure 25 of the crystalline basement that is built up by rocks affected by various degrees of partial 26 melting and then devoid of clear markers of deformation. AMS sampling was performed from 27 main rocks types of Pointe Géologie: migmatites including leucosomes and melanosomes, 28 coarse-grained pink granites, anatexites and mylonitic gneisses. For melanosomes, the 29 magnetic foliation is dominantly in agreement with the observed field foliation, i.e. 30 dominantly sub-vertical N-S in shear zones and gently inclined in dome structures. AMS 31 technique reveals a sub-horizontal magnetic lineation in migmatites from shear zones and a 32 gently dipping one in dome structures. But in mylonitic gneisses, located in vertical shear 33 zones, magnetic lineation is highly dipping to sub-vertical that is could be the signature of 34 high-strained, late- to post-migmatisation deformation in transpressionnal regime. Magnetic 35 properties of leucosomes and dykes of coarse-pink granites contrast with melanosomes. The 36 bulk susceptibility and anisotropy degree are significantly lower in granitic magmas that in 37 melanosomes. In addition, in well-defined leucosomes, granitic dykes and anatexites, the 38 magnetic ellipsoid is characterized by a more dipping magnetic lineation, which tends to be 39 vertical. This is associated to a rheological contrast between the solid-state deformation 40 suffered by oxide grains in the melanosomes and their reorientation in a viscous flow during 41 the transfer of felsic melt in the granitic dikes. Magnetic structure of leucosomes, granitic 42 dykes and anatexites allows to highlight the role of the gravity-induced upwelling of a crust 43 undergoing high degree of partial melting. 44 45 Ces deux phrases , qui concernent les lineations magnétiques dans les SZ verticales, doivent être completées car elle paraissent contradictoires mes ajouts sont-ils suffisants ?? 46 47 48 49 50 51 Keywords: Migmatite, anatexite, AMS, Pointe Géologie, Antarctique 52 2 53 1. Introduction 54 55 Migmatites and anatexites result from progressive melting of rocks under high-grade 56 metamorphism conditions (Wimmenauer and Bryhni, 2007` and references therein). These 57 rocks are often the only key to determine the structural patterns in the deep crust. However, 58 the structural analysis of migmatites is often not very easy because of their complex and 59 multiphase evolution. Moreover, the products, leucosomes and melanosomes, from the 60 melting of an initial highly deformed rock acquire a fabric that mostly cannot be determined 61 by classical structural approaches. In partially melted gneisses, i.e. migmatites, this fabric can 62 differ from that of the initial parent rock. In dominantly melted rocks, the only visible fabric is 63 mostly related to the orientation of rafts of melanosomes or mesosomes, i.e. respectively 64 restites or protoliths, and therefore this fabric only offers an incomplete signature of the 65 tectonic events suffered by the rocks during melting. Melanosomes and mesosomes usually 66 exhibit features of metamorphic rocks whereas the leucosomes display an igneous-like 67 appearance. Therefore, one of the characteristics of the migmatite structures is their local 68 variability and then their analysis imply a statistical approach. To this aim, the field 69 observations are limited to (the few visible markers) part of the markers of the fabric and 70 generally not well-adapted to statistical analysis. 71 The anisotropy of magnetic susceptibility (AMS) technique (Graham, 1954); see 72 (Tarling and Hrouda, 1993; Borradaile and Henry, 1997; Borradaile and Jackson, 2004) and 73 references therein) has been widely used for structural applications. It offers several 74 advantages relatively to field observations: It gives not only foliation and lineation but also 75 intensity and shape of the fabric and it can be applied to a set of samples representative of a 76 significant area allowing simple statistical analysis. Ferré et al. (2003) and Kruckenberg et al. 77 (2010) applied the magnetic tool for migmatites studies. They showed that despite rheological 78 variations during deformation (solid-state deformation followed by viscous flow), AMS axes 79 were consistent with observed regional field structures and thus highlighting the interest of 80 the AMS data for the strain characterizations in high-temperature metamorphic rocks. In 81 paramagnetic migmatites, the biotite fabric can evidenced these two types of deformation 82 (Hasalovà et al., 2008). Others authors have shown that anatexites could have specific AMS 83 signature, associated with changes towards weak solid-state rheology and that AMS 84 characterizations could therefore help to better model the different stages of migmatitic 85 terranes (Charles et al., 2009; Schulmann et al., 2009; Kratinová et al., 2012). 3 86 The Pointe Géologie archipelago (Terre Adélie, East Antarctica) represents a deep and 87 hot crust that experienced a long-live anatectic event during Paleoproterozoic times, 1.69 Ga 88 ago (Ménot et al., 2007 and references therein). This archipelago is partially covered by the 89 ice cap and limited outcrops are key zones to constrain the Terre Adélie Craton tectonics. 90 Pelletier et al. (2002) and Gapais et al. (2008) proposed a detailed structural and kinematic 91 analyses of the area based on foliation and lineation measurements of migmatites. But we 92 believe these structural data may be supplemented by taking into account the magnetic fabric 93 of the leucosomes and anatexites, which correspond to more than 50% of the outcrops and 94 which are devoid of clear markers of deformation. This would greatly improve the knowledge 95 of the structural pattern of this region. 96 The first aims of this paper is thus to specify the deformation framework associated to 97 the Paleoproterozoic event in the Terre Adélie Craton from a large sampling in the Pointe 98 Géologie rocks. For this, a detailed AMS study was performed in the migmatites, the larger 99 granitic dykes and the anatexites observed on the field. Finally, we focus on various 100 migmatitic structures of centimetric to decametric size; they correspond to various phases of 101 segregation, extraction and transfer of melts. We discuss the relationships between these 102 different migmatitic habitus and their related AMS signature in order to constrain the 103 rheological evolution of the molten crust. 104 105 2. Geological setting 106 107 The Terre Adélie Craton (TAC) is located on the easternmost part of the East 108 Antarctic Shield. It crops out as islands and capes scattered along the coast between 135° and 109 145°E but most of the outcrops are located in three main archipelagos, from West to East: 110 around Pointe Géologie (66°50’S, 140°E), East of Port Martin (66°80’S, 142°25’E) and East 111 of Cape Denison (67°S, 142°25’E) up to the Mertz glacier. This crystalline basement consists 112 of Late Archean and Paleoproterozoic formations devoid of any significant reworking since 113 1.5 Ga and then it is considered as part of the Mawson block or Mawson continent (Fanning 114 et al., 1995; 2002). At the scale of the TAC, the Late Archean and Paleoproterozoic terrains 115 are distributed westwards and eastwards from Port Martin, respectively (Monnier et al., 1996; 116 Ménot et al., 2007), Figure 1. 117 This paper deals only with the Paleoproterozoic formations of the Pointe Géologie area, 118 i.e. close to the permanent French Polar Station Dumont d’Urville (DDU). As described by 119 (Bellair, 1961b, a), the main rock types are migmatitic to anatectic gneisses that are cross cut 4 120 by dykes of apparently isotropic coarse-grained pink granites. The detailed mapping, carried 121 on during the GEOLETA project, improves this previous description and points out some new 122 and significant features (Monnier et al., 1996; Peucat et al., 1999; Gapais et al., 2008). 123 Migmatitic gneisses and anatexites derived from a sedimentary sequence dominated by 124 aluminous pelites together with subordinate greywackes, quartzites and calc-silicates. 125 Metagreywakes appear as intercalations ranging from tens of centimetres to hundreds of 126 meters in thickness. Quartzites and calc-silicates form dismembered layers and enclaves of 127 mesosomes within the migmatites and they mark out a poorly preserved sedimentary layering 128 (Figure IIa). Amphibolitized dolerites and gabbros occur as dykes and sills and they are 129 coeval with the anatectic event as shown by magma mingling features between the mafic 130 intrusions and the granitic magmas. Isotopic data indicate Paleoproterozoic sources for both 131 sediments and magmas (Peucat et al., 1999 and references therein). According to Monnier et 132 al. (1996), mesosomes, neosomes and anatexites represent respectively 10%, 60% and 30% of 133 the rock types in the Pointe Géologie archipelago. 134 These migmatitic and anatectic formations underwent a polyphased tectonic and 135 metamorphic evolution with three phases of deformation leading to a composite sub vertical 136 regional S0-S1-S2 foliation (Monnier et al., 1996; Pelletier et al., 2002). Neosomes display two 137 successive parageneses related to both the S1 and S2 metamorphic foliations and bearing 138 comparable Sil+/-Kfs+/-Pl+/-Bt+/- Cd+/-Grt+/-Ilm+/-Qtz mineral assemblages. Moreover, 139 mineral chemistry of the S1 and S2 parageneses is similar and argues for a single continuous 140 LP-HT metamorphic event, the peak conditions of which reaching 750-700°C at 0.6-0.4 GPa. 141 Large amounts of anatectic melts have been produced all along the tectonic and metamorphic 142 evolution as suggested by the various habitus of the leucosomes. The oldest leucosomes 143 appear as mylonitic lenses isoclinally folded by the S1-S2 transposition, but most of them are 144 undeformed and concordant within the S2 foliation and the latest melts cross cut the S2 planes. 145 A retrograde imprint with Bt+/-Ms+/-And assemblages marks the later evolution to about 146 550-450°C and 0.5-0.4 GPa (Monnier et al., 1996;Pelletier et al. 2002, 2005; Gapais et al., 147 2008). 148 Bellair and Delbos (1962) assumed a 1.5 Ga age (Rb/Sr on micas) for the partial melting 149 event. More recently, new radiometric data (Peucat et al., 1999, U-Pb on zircons and 150 monazites, Sm-Nd and Rb-Sr on whole rocks and minerals) gave precise time constraints on 151 the geological evolution of the meta-volcano-sedimentary formations of Pointe Géologie. 152 Time of deposition is bracketed between the inherited zircon ages (1.72 -1.76 Ga) and the 153 peak metamorphism and partial melting age at 1.69 Ga. The later cooling path was 5 154 constrained by Nd garnet ages (650-600°C at 1.63-1.60 Ga) and Rb-Sr muscovite and biotite 155 ages (450-350°C at 1.5 Ga). 156 157 3. High temperature rocks types and regional structures 158 159 While the lithology is very homogeneous in the scale of the archipelago, field 160 relationships between different rock types are much more complex for the scale of outcrops. 161 Four main rocks types have been sampled for AMS measurements: migmatites including 162 leucosomes and melanosomes, coarse-grained pink granites, anatexites and strongly mylonitic 163 gneisses. 164 Migmatitic gneisses: they have been described previously as the K feldspar gneisses 165 (Monnier et al., 1996; Pelletier et al., 2005) and they are the dominant facies of the area, 166 especially on the Pétrels Island (Dumont d’Urville station, Figure I). We will discuss more 167 specifically the space and time relationships between leucosomes and melanosomes in the 168 migmatitic gneisses. As partial melting developed all along a polyphased tectonic and 169 metamorphic event, leucosomes display various habitus relative to the composite foliation, 170 which is marked on the field by melanosomes and septas of mesosomes. The melanosomes 171 defined continuous layers in migmatites (Figure IIa): 172 (i) The earliest leucosomes occur as mylonitized and elongated lenses, sometimes 173 affected by intrafolial folds within the foliation. They bear evidence of successive 174 segregation and deformation processes (Figure IIa). 175 (ii) The most common leucosomes are undeformed and concordant within the 176 migmatites foliation and they may be later folded together with the foliation. They 177 represent syn to late-foliation melts (Figure IIb). 178 (iii) The latest leucosomes form dykelets cross-cutting, and post-dating, the S1-2 179 foliation. They may be connected to the concordant leucosomes, tapping off and 180 transferring melts upwards (Figure IIa, c). 181 Coarse-grained pink granites: they appear as dykes of decimetric to decametric 182 thickness which cross cut the regional foliation (Figure IId). They are devoid of any visible 183 markers of orientation. Such dykes, collecting the dykelets, drain the more evolved melts 184 during the late- to post-tectonic stages of the partial melting and metamorphic event. 185 Anatexites: they outcrop widely on the W area of Pointe Géologie (e.g., Gouverneur, 186 Balance, Taureau and La Vierge islands, Figure IX). They derived from a higher degree of 187 partial melting than migmatitic gneisses and show a mineral assemblage comparable to that of 6 188 leucosomes but more enriched in Qtz and depleted in Crd. Anatexites display more isotropic 189 textures but a flow fabric or a palimpsest structure of the parent gneisses is often marked by 190 some oriented rafts of migmatitic gneisses or schlierens of biotite and oxides (Figure IIe). 191 Mylonitic gneisses: they outcrop in a restricted and narrow zone on the western flank of 192 the Pétrels Island (Rocher Jakobsen) and some islands of Pointe Géologie, i.e. along a major 193 shear zone (sites II and V, Figure X). They consist of Bt + Grt gneisses with only tiny Grt- 194 bearing leucosomes and are characterized by a vertical mylonitic foliation. They derive from 195 the K-feldspar migmatitic gneisses and then may be considered as late- to post-migmatisation 196 tectonites (Figure IIf). 197 As carefully described by Pelletier et al. (2002) and Gapais et al. (2008), the Pointe 198 Géologie archipelago shows two types of structural domains: NS to N340° striking vertical 199 shear zones and domes both of them developing during the metamorphic and anatectic event. 200 Between the vertical zones, foliation attitudes point out dome-shaped structures marked by 201 flat lying to gently dipping fabrics. Dome displays a mineral lineation outlined by a preferred 202 orientation of sillimanite crystals while such a lineation is almost invisible in the vertical 203 zones. The transition from flat lying to vertical foliation zones may be sharp, with 204 development of vertical foliation planes cutting across the horizontal foliation of domes, or 205 gradual when folds, with horizontal axes, induce vertical planes. Such a transition from dome 206 to vertical shear zone never exceeds five hundred meters in thickness. In both cases, vertical 207 structures seem to be later than flat lying ones. According Gapais et al. (2008), the kinematic 208 markers (lineations, boudinage, ...) suggest that shear zones reflect a dextral transpressive 209 movement while flat areas are the result of shortening combined with stretching parallel to the 210 shear zones. Such patterns might be explained in the frame of a regional convergence of a hot 211 and weak juvenile crust leading to horizontal crustal flow and strain partitioning with 212 localized deformation along transpressional shear zones. 213 214 4. Sampling and analyses procedures 215 216 Because of outcrops restrictions (areas non accessible because of ice cover or of birds 217 protection) and high variability of the visible deformation, sampling was often made in sites 218 relatively close one to another in the main island (Pétrels Island). Other sites were scattered in 219 different smaller islands (Figure IX). Most sampled sites correspond to a surface up to 50m2. 220 For magnetic fabric study, cores were sampled with a gasoline-powered portable drill. 221 All the cores were oriented only with a sun compass (Figure IIf) because of the immediate 7 222 proximity of the southern magnetic pole. That introduced a strong limitation for sampling 223 because of climatic conditions. The sampling was made during three different summer 224 fieldworks, in 1992, 2009 and 2011. As a whole, 819 rock cores were obtained in 33 sites, 225 including 20 on the Pétrels Island (Figure X). When possible, different facies (from gneiss to 226 anatexites) were sampled on the same site. The cores were cut in the laboratory in specimen 227 of standard paleomagnetic size. 228 Magnetic susceptibility and its anisotropy have been measured using Kappabridges 229 KLY3 and MKF1 (AGICO, Brno). Thermomagnetic experiments were performed on 230 representative samples by heating in argon or in air using the CSL equipment and the CS2-3 231 oven (AGICO, Brno) associated with the Kappabridges. Hysteresis loops were obtained for 232 small cores (cylindrical samples of about 3 cm3) using a laboratory-made translation 233 inductometer within an electromagnet capable of reaching 1.6 T. 234 235 5. Magnetic Mineralogy 236 237 5.1. Thin sections study 238 As the magnetic characteristics of the rocks are tightly controlled by their 239 mineralogical content, the various assemblages recorded in the different rock types need to be 240 specified. This is particularly important in the case of migmatitic gneisses where partial 241 melting induces a redistribution of refractory minerals from the mesosomes to both the 242 melanosomes and leucosomes. 243 Magnetite and ilmenite are the most abundant oxide minerals. They form discrete grains or 244 clusters with direct contact between magnetite and ilmenite. The larger grains (millimetric in 245 size) are generally found in the melanosomes and therefore in the foliation and they appear as 246 elongated parallel to the lineation defined by the sillimanite when the latter is present (Figure 247 III). For ilmenite crystals, deformation also induces a structural axes related lattice preferred 248 orientation (LPO), which is characterized by the c-axes strongly concentrated close to the 249 normal to the foliation, and by the poles of (2-1-10) and (10-10) prism planes concentrated 250 close to the lineation (Figure IV). Oxides are also present in the leucosomes but the fabric 251 (grains alignment) appears to be more scattered than in the melanosomes. At the melanosome- 252 leucosome boundary, elongated shape grains, may-be rotated, have been observed 253 perpendicular to the foliation. In the leucosomes these oxide grains become more discrete and 254 more rounded (Figure III). 8 255 Cordierite is also present in migmatitic gneisses and granitic dykes of Pointe Géologie. 256 This mineral that occurs mainly as grains of globular shape (up to a few millimetres in size) is 257 carefully watched because cordierite presents specific magnetic properties. This mineral 258 carries an inverse magnetic fabric (i.e. characterized by a switch between the principal 259 maximum K1 and minimum K3 axes of the AMS ellipsoid with respect to the grain shape 260 (Potter and Stephenson, 1988; Rochette et al., 1992)) that could lead to misinterpretation of 261 the measured magnetic fabrics. However the mean magnetic susceptibility (Km) for 262 magnetite, which is ubiquitous in studied thin sections, is significantly higher than for 263 cordierite (Km ratio > 1000). Therefore magnetite should be the main carrier of measured 264 AMS. For relatively large grains of magnetite, the K1 and K3 axes indicate the magnetic 265 lineation and magnetic foliation pole, respectively. 266 267 5.2. Rock-magnetism 268 The mean magnetic susceptibility Km (average 5.2 10-2) of the studied samples is 269 different according to the studied fraction of the migmatites (Figure V). The gneisses with 270 subordinate melted component and dominant melanosome fraction have very high 271 susceptibility (average?). Km values for dominant granitic fraction are lower (average?). 272 Migmatite samples including both leucosome and melanosome fractions present intermediate 273 Km values. This variability in leucosome versus melanosome content of gneissic specimens 274 largely explains the relatively large distribution of susceptibilities (Figure V). The anatexites 275 samples show the highest variation in Km values (from ? to ?). 276 All thermomagnetic KT curves (susceptibility K as a function of temperature T) show 277 a sharp susceptibility decrease around 580°C during heating (Figure VI), clearly indicating 278 the presence of magnetite. In addition low temperature experiments confirm the presence of 279 this mineral by a large susceptibility increase around -160°C (Figure VI). This variation 280 corresponds to the Verwey transition that is characteristic of pure magnetite. Few 281 thermomagnetic curves are perfectly reversible. Susceptibility values from the cooling curve 282 are mostly a little bit higher than the initial values, in air as in argon atmosphere (but 283 sometimes much higher as for the sample AP35). Partial cooling loops during heating 284 evidenced a weak mineral alteration due to heating around 300 to 400°C that probably reflects 285 transformation of a weak amount of maghemite in hematite. New magnetite is also often 286 formed at the highest temperatures. 287 Hysteresis loops show generally a full saturation of the magnetization for moderate 288 field (Figure VII). This saturation was partial only for the sample AP35, evidencing the 9 289 presence of another component of high coercivity. This component is probably hematite. In 290 most cases, ferrimagnetic minerals have a largely dominant effect for the susceptibility, but 291 two of the studied granite samples highlight also a strong contribution of the paramagnetic or 292 even diamagnetic minerals. Day plot (Day et al., 1977) for samples with mainly magnetite 293 clearly evidences a large size of the magnetite particles (Figure VIII). 294 Main magnetic mineral is therefore magnetite with a large size. Obtained AMS data 295 are then directly usable for a structural analysis (no inverse magnetic fabric due to small 296 Single Domain particles (Potter and Stephenson, 1988). 297 298 6 - Magnetic fabric 299 300 The AMS ellipsoid yields the three principal susceptibility axes defined as 301 K1 K2 K3. K1 is the magnetic lineation and K3 is perpendicular to the magnetic foliation. 302 The Jelinek (1981) parameters P' and T were used to describe the intensity and the shape of 303 the magnetic fabric, respectively. Data for a group of samples were analysed using normalized 304 tensor variability (Hext, 1963; Jelinek, 1978) statistics. 305 6.1 – Structures from AMS 306 Data for migmatitic gneiss and for granites are presented separately (migmatitic 307 gneisses included minor melted parts and "granitic" samples small amounts of melanosome 308 assemblage and this separation has been made then considering the dominant presence of one 309 of these component). Moreover, from the regional structural field pattern, two distinct zones 310 have been distinguished for the AMS analyse: the sub-vertical zones and the dome shaped- 311 zones (Figure IX and X). 312 6.1.1. In migmatitic gneisses of sub-vertical shear zones (sites T, R, D, O, XIII, A of 313 Pétrels Island, Figure X, melanosome layers show generally both well clustered magnetic 314 foliation pole (K3) and magnetic lineation (K1). The magnetic foliation is dominantly 315 subvertical N-S in accord with the observed field foliation and the magnetic lineation presents 316 a weak plunge and N-S trending. The granitic rich layers (site XIII) display more diffuse 317 fabric, in particular the K1 axes that tend to form a girdle perpendicular to K3. Well- 318 individualized leucosomes (e.g. Figure IIC) show a different magnetic fabric signature than 319 melanosome layers characterized by strongly inclined to sub-vertical magnetic lineation (site 320 XIII 321 horizontal plane with two dominant directions: N-S and E-W. . The K3 axes are more scattered than the K1 axes. They are in the 10 322 Xthe K3 In large coarse-grained pink granite dykes (sites A, E, D 323 axes are relatively well clustered defining a subvertical magnetic of strike close to that of 324 neighbouring gneisses (sites E, D 325 magnetic lineation pattern is characterized by the verticalization of K1-axes in comparison to 326 magnetic lineation measured in the melanosome layers of neighbouring gneisses. They form 327 girdle perpendicular to K3 (site E or strongly inclined to sub-vertical local maximum 328 (sitesD A a divergent strike (sites A). The 329 , Taureau, La Vierge, Balance Islands (sites 330 VIIXV, XIV XVIII, XIXFigure IX) and South of Pétrels Island (site 331 XX 332 Gouverneur anatexite (sites VII, XV 333 lies in the horizontal plane, relatively scatted or forms clusters at 90 degrees from each other 334 with the N-S and E-W directions that prevails for south Gouverneur Islands (site XV). 335 Sampling sites XIV, XVIII (Figure IX) show heterogeneities in the partial melting degree 336 that is expressed in the field by more or less regularly presence of migmatitic gneiss rafts in 337 the anatexites. For site XVIII 338 gneisses show distinct magnetic axes orientations characterized by K1 preferentially sub- 339 vertical and K3 horizontal N-S (i.e., magnetic foliation vertical E-W) in anatexites while K1 340 is horizontal to strongly plunging N-S and K3 is horizontal E-W (i.e., magnetic foliation 341 vertical N-S) in neighbouring gneisses. The N-S orientation of magnetic foliation in gneisses 342 fit quite well with the regional vertical shear zone structures. In opposite, the E-W vertical 343 magnetic foliation that appears in the larger dykes and anatexites is less well-constrained by 344 large-scale 345 XIV T 346 and the migmatitic gneisses was difficult to perform. That explains the relatively wide 347 confidence zones at 95% for K1 and K3. However the magnetic fabric is mainly oriented 348 vertical E-W for the foliation and strongly-inclined (westward) for the lineation. 349 K1max tends to have strong inclination or to be sub-vertical. For field anatexites and migmatitic structures (Figure IX). For site tinction on the field between the anatexites In mylonitic gneisses of Rocher Jakobsen (sites II, V, ) the magnetic 350 foliation (K1-K2) is dominantly subvertical N-S in accord with the observed field structures 351 (Figure IIf). On the contrary, the AMS measurement reveals uncommon highly dipping or 352 sub-vertical lineation. 353 11 354 6.1.2. In the migmatitic gneisses of the dome shaped-zones (sites J, VI, G, K, H, S, X) magnetic fabric 355 XVI, XVII, Figure IX; sites C, IV, Q, III, VIII, I, B, i, XII, F, 356 display a stronger variability of K1 and K3-axes orientations from one site to another one in 357 comparison to structured vertical shear zones. A relatively strong dip (about 45°) for the 358 magnetic foliation is frequently observed, in particular for the sites located in the flanks of 359 domes (sites H, K, Figure IX; sites IV, Q, III, Figure X) for the eastern flanks of the Pétrels- 360 Curies Islands dome). The magnetic foliations are generally in agreement with the field 361 measured strikes and dip of melanosome layers. The magnetic lineations show gently dip and 362 dominant NNW strike. The innermost zones of domes (sites XVI, XVII, Figure IX; sites VIII, 363 I, B, Figure X) show also a strong variability of AMS structure patterns correlated to the 364 complexity of migmatitic structures observed at the domes apex. In these areas are observed 365 the less well-defined magnetic directions (with the widest confidence zones at 95%: site XVI, 366 Figure IX; site I, Figure X). Sampling in a granitic dykelet of centimetric width crosscutting 367 flat-lying gneissic foliation was performed in site XVII (Figure IX). The related AMS pattern 368 is characterized by vertical N-S magnetic foliation and sub-vertical magnetic lineation and 369 then differs from that of gneiss. 370 Large dykes of coarse grained pink granites sampled in site F an XII (Figure X) are 371 characterized by vertical magnetic lineation when compared with the magnetic lineation from 372 the melanosomes of gneisses. This feature is similar to that observed in the granitic bodies 373 from the sub-vertical shear zones. The magnetic foliation in the granitic dykes is either 374 concordant with that of host gneisses (site F) or discordant (site XII). 375 376 6.2 – AMS parameters (P’ and T) 377 The Figure XI presents the characteristics of the susceptibility ellipsoid. The degree of 378 anisotropy P’ is very high in the migmatitic gneisses (mean 1.479; minimum 1.041; maximum 379 1.903). It is lower in granites (mean 1.222; minimum 1.040; maximum 1.413). The shape of 380 the susceptibility ellipsoid is dominantly oblate, in gneisses (for T value: mean 0.30; 381 minimum -0.08; maximum 0.66) as in granites (mean 0.25; minimum -0.10; maximum 0.62). 382 In granites, a clear relationship (Figure V, R2=0.70) between P’ (intensity of the fabric) and 383 Km (related to the concentration in ferrimagnetic minerals) highlights the dominant effect of 384 the magnetite in the AMS (Henry et al., 2004). Another relationship (R2=0.54) between T and 385 P’ in granites suggests that the most prolate fabrics correspond to the weakest anisotropy 12 386 Figure XI. In addition, for granite, the anatexites show the highest variability in P’ and T 387 values, including the extreme values Figure XI. 388 389 7 – Discussion 390 7.1 Mean susceptibility (Km) and anisotropy (P’) signature 391 The amount of magnetite is clearly different in migmatitic gneisses and in granites 392 (leucosomes and dyke), as shown by the susceptibility values (Figure V). This variation of 393 magnetic susceptibility between melanocratic and leucocratic layers is mainly due to the 394 variations in magnetite content. Magnetic studies suggest also mineralogical changes 395 affecting magnetite with formation of ferromagnetic oxides of lower susceptibility like 396 maghemite or hematite. Concerning this mineralogical change, gneiss sample AP35 (close to 397 site R, Figure X) is the only one with hematite; it also presents the strongest formation of a lot 398 of new magnetite at high temperature (susceptibility becomes 14 times higher on the cooling 399 curve). It is therefore probably due to a strong local mineralogical alteration (interaction with 400 deep fluids, weathering?) and remains an exception. 401 The intensity of magnetic anisotropy, illustrated by the P’ values, is lower in granites 402 than in gneisses (Figure XI). In granites, it presents a relationship with the Km values, 403 suggesting that this difference could be explained by the lower amount of magnetite in 404 granites, AMS then resulting mainly from strong magnetite anisotropy and weak anisotropy 405 of a low susceptibility component. Owing to its Km values, this last component is the 406 paramagnetic minerals and not the maghemite. The observed inverse correlation between T 407 and P’ in granites (Figure XI) shows that the AMS of this second component is less oblate 408 than the magnetite AMS. 409 Inversely to granitic magmas constituting leucosomes and dykes, a wide range in Km 410 values, according to samples within a single site, is observed in anatexites. It is due to the 411 presence of more refractory gneissic rafts with high concentration in oxides grains. 412 413 7.2 AMS in migmatitic gneisses and granites 414 In addition to the Km and P’ values, the main differences in magnetic fabric between 415 melanosome layers of gneisses and granitic magmas concern the orientation of the K1 axis 416 (Figures IX and X). K1 axis is dominantly close to the horizontal in melanosomes and close to 417 vertical in granites. In some granitic sites (e. g., sites E, XII, Figure IX), its orientation is 418 relatively scattered within a vertical plane, probably because of the presence of melanosome 419 fragments within the granite. Other difference in orientation of susceptibility axes concerns 13 420 K3. Whereas in melanosome the K3 orientation fits to the field structures, it appears in granite 421 a more complex magnetic orientation pattern with two dominant orientations. The first one 422 matches to the gneissic structures (for example, the magnetic foliation is vertical N-S in the 423 shear zone area) and the second is at 90 degrees of the first one. In some sites the two 424 clustering are present (e.g., site XV Figure IX and site XIII, Figure X). The first orientation 425 is associated to the strike-slip deformation, which is at the origin of the large-scale sub- 426 vertical corridors. The cause of the second orientation is less straightforward. In Pétrels 427 Island, the migmatitic layering is locally cut by vertical large granitic dykes of NE-SW to E- 428 W direction (Monnier, 1995). Then emplacement of such E-W trending dykes tectonically 429 controlled and consistent with a component of NNW-SSE to N-S dextral strike-slip (Gapais et 430 al., 2008). In the western area (Gouverneur island area, Figure IX) where rafts of melanocratic 431 restites are still packed in anatexites, E-W magnetite could correspond to inheritance of older 432 tectonic foliations. 433 The gneiss sites II and V, on the southwestern border of the Pétrels Island (Figure X) 434 also present mainly subvertical K1 axes. However, the gneisses of sites II and V (Rocher 435 Jakobsen) are intensely deformed, unlike the granitic leucosomes, dykes and anatexites that 436 have not recorded pervasive solid-state deformation. Thus, AMS fabric is interpreted as 437 resulting of high-strained, late- to post-migmatisation solid-state deformation. The strong K3 438 clustering indicating a N-S vertical magnetic foliation and the highly tilted to sub-vertical 439 magnetic lineation could be related to deformation in transpressionnal regime mainly 440 restricted to the N-S vertical shear zones. Narrow zones within the vertical SZ ?? 441 Thin section analyses show a change of orientation of magnetite grains from 442 melanosome to leucosome. In melanosome, the oxide grains are within the foliation and 443 elongated parallel to the lineation also marked by the sillimanite alignment. They are 444 interpreted as resulting from solid-state deformation that occurred during the Paleoproterozoic 445 metamorphic event (1.69 Ga ago). In addition, LPO of ilmenite, which strongly correlated 446 with the tectonic fabric, suggest dislocation glide on (0001) as main deformation mechanism. 447 The basal slip for hematite – ilmenite mineral could reflect high-temperature solid-state 448 deformation (e.g., Bascou et al., 2002; Siemes et al., 2003). Migmatitisation processes are 449 also associated with segregation and transfer of melts that lead to leucosomes, pink granitic 450 dykes and then anatexites when partial melting degree is higher. As discussed in Vigneresse 451 et al. (1996) and recently in Holtzman et al. (2012), the increase of melt fraction produce 452 changes in rheological behaviour. From plastic deformation evidenced by elongation of oxide 14 453 minerals, which are abundant in the melanosome to magma flow with transport of isolated 454 solid particles in leucosomes, dykes and anatexites. 455 Such different and successive regimes of deformation affecting magnetite grains first 456 deformed under solid-state conditions and then involved as passive rigid particles during 457 melting, have been already described in migmatitic terrains (e.g., Ferré et al., 2003). In Pointe 458 Géologie migmatites, these successive regimes generate distinctive AMS signatures. The 459 clearest difference concerns the K1 orientation, which tends to a vertical plunge during 460 segregation and circulation of felsic melt in agreement with the gravity-induced upwelling of 461 magmas. The K3 orientation in granitic layer appears more sensitive to the degree of partial 462 melting and the structuration of country rock. At lower degrees of partial melting, liquid 463 segregation remained strongly constrained by the framework of the unmelted gneissic 464 material. Then the felsic melt, forming dykelets and connected lenses, is concordant with the 465 foliation of gneisses. For higher degree of melting, the melt was injected as concordant or 466 cross-cutting large veins (Figure IIc,d) resulting in the various orientations of the magnetic 467 foliation. Then the dykes and veins intrude areas of lower stress, generally close to the 3 468 direction (e.g., Cooper, 1990; Hand and Dirks, 1992). 469 470 471 7.3 Methodological and regional-scale implications 472 All these observations evidence that the AMS study of migmatites cannot be 473 considered as a routine method. To be as reliable as possible, the AMS approach requires a 474 preliminary detailed observation of the various leucosomes habitus and then a large number 475 of magnetic measurements of rocks characterized by various degrees of melting. For low 476 degrees of partial melting, the leucocratic layers remain strongly constrained by the earlier 477 structure defined by the unmelted material. In that case, the AMS principal axes are 478 representative of the local and regional finite strain axes. This fits with the conclusions of 479 Ferré et al. (2003) for migmatites of the Superior Province in Minnesota. For more 480 pronounced partial melting degree, well-individualized leucocratic layers can developed 481 specific AMS patterns associated to flow regime. In the Pointe Géologie migmatites, the 482 difference with the local and regional finite strain axes is highlighted by the direction of K1- 483 axes. Large variations of the partial melting rates increase the probability to measure 484 composite AMS and the difficulty to isolate pre-melting and synmelting magnetic fabrics. 485 The strongest variations of AMS principal directions and parameters recorded in anatexites 15 486 are related to the heterogeneity of these rocks, which enclose number of schierens and 487 refractory material. 488 The structural pattern of Pointe Géologie consist of two domains with respectively 489 flat-lying and sub-vertical foliations related to a long-live tectonic, metamorphic and anatectic 490 event, both associated with partial melting (Monnier, 1995; Pelletier et al., 2002; Pelletier et 491 al., 2005). Commonly, stretching mineral lineations are not easy to observe within the 492 foliation, more specially within the sub-vertical shear zones. Combining structural field 493 evidences, determination of P-T-t metamorphic evolution and analogic simulations of the 494 mantle-crust ductile deformation Gapais et al. (2008) propose a model in which the 495 Paleaoproterozoic hot and weak lithosphere converges toward a cooler and more rigid craton 496 (Neoarchean in age). In this model, deformation of the Paleoproterozoic crust combines both 497 transpression and horizontal flow and/or lateral escape parallel to the Archean basement and 498 perpendicular to the shortening direction. 499 AMS structural pattern determination provides complementary structural information 500 such as magnetic lineations. They are mainly sub-horizontal in sub-vertical foliated gneisses. 501 It underlines the importance of the strike-slip component during the deformation. In mylonitic 502 gneisses, which are considered as late- to post-migmatisation tectonites nearly vertical 503 lineations are evidenced. This is considered as the effect of transpressionnal regime, which 504 combinates strike-slip and across-strike shortening. In migmatites with flat-lying foliation, the 505 magnetic lineation displays a moderate plunge and is commonly parallel to the mineral 506 stretching lineation. Such features are in good agreement with horizontal crustal flow 507 mechanism. 508 Increasing partial melting degree leads to a loss of the rock cohesion related to the 509 migration of the melt trough a solid-state made of previously deformed minerals. Thus the 510 former tectonic structures will be progressively erased. Melt segregation and transfer occur 511 under a viscous flow regime, mainly driven by gravity forces. In such a regime, the well- 512 defined leucosomes, dykes and anatexites will develop a magnetic fabric corresponding to the 513 upward transport of magmas. Then AMS measurements would allow to better map the mass 514 transfers associated with intensive melting at peak temperatures and to characterize the 515 general framework of a warm and buoyant lithosphere. 516 517 8 – Conclusion 518 Pointe Géologie archipelago in Terre Adélie represents a deep seated crustal section 519 affected by intensive anatectic processes during Paleoproterozoic times, 1.69 Ga ago. This 16 520 generated different HT rocks types such as: migmatites including leucosomes and 521 melanosomes, coarse-grained pink granites dyke and anatexites. Partial melting affects 522 indifferently the regional structures characterized by the juxtaposition of flat-lying and sub- 523 vertical deformation zones. 524 Magnetic mineralogy study shows that oxide minerals are mainly large grains of 525 magnetite. Ilmenite is also observed constituting clusters with magnetite, which are 526 particularly abundant in melanosome layers. The grains are intensely solid-state deformed and 527 aligned parallel to the lineation marked by sillimanite. In the leucosomes, oxides appear more 528 scattered than in the melanosomes and their rounded shape suggests rotation (and corrosion ?) 529 of the former elongated grain during melt segregation. La rotation ne suffit pas à expliquer la 530 forme arrondie ?? sauf à n’observer que des sections basales dans nos lames ?? 531 Melanocratic layers on the one hand and felsic leucosomes, dykes and anatexites on 532 the other hand develop contrasted AMS signatures. The mean magnetic susceptibility (Km) 533 and the anisotropy degree (P’) are higher in the gneisses and much lower in granitic samples. 534 Orientation of principal susceptibility axes also differs. In migmatitic gneisses, magnetic 535 foliations are coherent with the local and regional structural pattern. Nevertheless AMS 536 technique provides complementary information on the orientation of lineations when they are 537 difficult to observe in the field. They are subhorizontal in the shear zone, except in narrow 538 vertical late mylonitic zones where high plunge (dips ?) evidences the transpressionnal regime 539 of deformation. In well-defined leucosomes, granitic dykes and anatexites, the magnetic 540 ellipsoid is characterized by the vertical plunge of the magnetic lineation. Such a changing 541 orientation is related to a rheological contrast between the solid-state deformation suffered by 542 the oxide grains and their reorientation in a viscous flow during the aggregation of felsic melt. 543 Magnetic structure pattern do not disagree with the model of deformation of a hot and 544 weak lithosphere converging toward a cooler Archean craton proposed by Gapais et al. (2008) 545 from metamorphic and field structures analysis and analogic simulations. They explained the 546 structural pattern of the pointe Géologie and surrounding areas by horizontal, orogen-parallel, 547 subconstrictional flow that could result from oblique convergence and/or from particular 548 boundary conditions facilitating lateral escape. A comparable model was also assumed from 549 numerical modelling to image the deformation of the hot Neoarchean crust of the Eastern part 550 of the Terre Adélie Craton (Duclaux et al., 2007). The magnetic structures map allows to 551 highlight the role of the gravity-induced upwelling of a crust undergoing partial melting. 552 From methodological point of view, this work emphasizes on the importance of an 553 acute petrological characterization of sites to be selected for AMS measurements in order to 17 554 avoid pre- and syn-melting composite magnetic fabrics. Finally, it underlines the difficulty of 555 AMS analyses in anatectic rocks, which lead to a very large variability for AMS signature; 556 this mainly due by the preservation of refractory rafts and by the heterogeneity of such rocks. 557 558 Acknowledgements 559 We are very grateful to the "Institut polaire français Paul Emile Victor" for support of 560 the program ArLiTA (Architecture de la Lithosphere de Terre Adélie) and to the Japanese 561 "National Institute of Polar Research" for participation to the international exchange program 562 under the Antarctica Treaty and for invitation of BH in Tokyo. LPO were carried from EBSD 563 measurements using a SEM-JSM 5600 at the University of Montpellier (France) and ilmenite 564 pole figures were generate from software developed by D. 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Cambridge University Press, New York, pp. 43-45. 671 20 672 Figures captions 673 674 Figure I: Simplified geological map of the Terre Adélie Craton (after Ménot et al., 2007). 675 Studied zone (indicated by a star) is located in the 1.7 Ga domain, close to the French 676 Polar Dumont d’Urville station. Inset: location and limits of the Terre Adélie Craton 677 (TAC) in East Antarctica and of the Gawler Craton (GC) in South Australia. 678 679 Figure II : Example of high-temperature rock types outcropping in Pointe Géologie 680 archipelago. (a) Migmatitic gneiss structures illustrating the HT polyphased tectonic in 681 the Paleoproterozoic formation of the TAC: septas of mesosomes (1) and more 682 continuous layers of melanosomes (2) bearing foliation; successive generations of melt 683 with earliest elongated lenses (3) locally affected by intrafolial folds within the 684 foliation, undeformed leucosomes (4) concordant with the foliation and later thin 685 dykes (5) cross-cutting foliation. (b) Folded leucosomes with axial plane parallel to the 686 foliation. (c) Melt segregation and upwards transfer processes generating concordant 687 leucosomes feeding cross-cutting dykelets (Pétrel Island). (d) Coarse-grained pink 688 granites forming metric to decametric thickness dykes cross-cutting the regional 689 foliation (Pétrel Island). (e). Anatexite showing melanocratic schlierens and rafts 690 bearing the foliation (Balance Island). (f) Mylonitic gneisses characterized by vertical 691 foliation (Rocher Jackobsen, Pétrels Island). The solar compass used to determine the 692 geographical orientations of tectonic structures gives the photograph scale. 693 694 Figure III : Photomicrograph of migmatitic gneiss in the vertical shear zone (Lamarck Island). 695 Sillimanite (sil) and elongated oxide grains (mainly magnetite (mag) in this sample) 696 are parallel to foliation in the melanocratic layers. The shape of oxide grains tends to 697 be more rounded and perpendicular to the foliation in more leucocratic areas (see 698 arrows). 699 700 Figure IV: 701 Ilmenite LPO patterns of migmatitic gneiss in the vertical shear zone, Pétrel Island 702 (sample AP85). LPO are represented on equal area, lower hemisphere projection. 703 Foliation is marked by a black line and lineation is marked by the structural axis X. 704 The density contours are in Multiple Uniform Distribution (MUD); N is the number of 21 705 measured grains. 706 707 Figure V : P' parameter as a function of Km values: granitic dyke (open squares), mylonitic 708 gneisses (full triangles), gneisses (full squares) and anatexites (open diamonds). 709 710 711 Figure VI : Normalized susceptibility K/Ko as a function of the temperature T in gneisses (samples AP35 and AP85) and in granites (09cjb75, 11cjb41 and 11cjb71). 712 713 714 Figure VII : Hysteresis loops for gneisses (AP35 and AP85) and granite (11cjb108). Remanent coercive force (Hcr). 715 716 Figure VIII : Ratios of hysteresis parameters (Day et al., 1977): Jrs/Js (Jrs: remanence at 717 saturation; Js: magnetization at saturation) as a function of Hcr/Hc (Hcr: remanent 718 coercive force; Hc: coercive force). Areas for Multi-Domain (MD) and Pseudo Single 719 Domain (PSD) grain size for pure magnetite. 720 721 Figure IX: Projection of AMS data of each site of Pointe Géologie Archipelago. AMS 722 projections on Petrel Island (black frame) are illustrated in Figure X. Distribution of 723 maximum axes (K1; blue squares) and minimum axes (K3; violet circle) is in lower 724 hemisphere equal area projection along with confidence ellipses. White, yellow and 725 green colour of stereonets background represents the AMS projections of gneisses, 726 granitic dykes and anatexites, respectively. 727 728 729 Figure X : Projection of AMS data of each site of Petrel Island in Pointe Géologie 730 Archipelago. Distribution of maximum axes (K1; blue squares) and minimum axes 731 (K3; violet circle) is in lower hemisphere equal area projection along with confidence 732 ellipses. White, yellow and green colour of stereonets background represents the AMS 733 projections of gneisses, granitic dykes and anatexites, respectively. 734 735 Figure XI : T parameter as a function of P' values (Jelinek, 1981): granitic dyke (open 736 squares), mylonitic gneisses (full triangles), gneisses (full squares) and anatexites 737 (open diamonds). 738 22