1 Contribution of AMS characterization in understanding the migmatitic 2 terrains of Pointe Géologie, Terre Adélie (East-Antarctica) 3 Jérôme Bascou1, Bernard Henry2, René-Pierre Ménot1, Minoru Funaki3, Guilhem Barruol4 4 5 6 7 8 9 10 11 1 Université de Lyon, Université Jean Monnet and UMR-CNRS 6524, Laboratoire Magmas et Volcans, 23 rue du Dr Paul Michelon, 42023 Saint Etienne, France 2 Paléomagnétisme, Institut de Physique du Globe de Paris, Sorbonne Paris Cité, Univ ersité Paris Diderot and UMR-CNRS 7154, France 3 National Institute of Polar Research, 10-3 Midori-cho Tachikawa Tokyo 190-8518, Japan 4 Université de la Réunion, CNRS and Institut de Physique du Globe de Paris, Géosciences Réunion, 97715 Saint Denis cedex 9, La Réunion, France 12 13 14 15 16 17 18 19 20 Abstract 21 22 Keywords: Migmatite, anatexite, AMS, Pointe Géologie, Antarctique 23 1 24 1. Introduction 25 1er paragraphe, il me semble important de definer la terminologie utilise pour la 26 description des migmatites et anatexites, soit par une ou deux phrases préliminaires soit 27 comme ci dessous dans le fil du texte. A voir. (ref Wimmenauer and Bryhni, 2007 28 Migmatite and Anatexites result from progressive melting of rocks under high-grade 29 metamorphism conditions ref Wimmenauer and Bryhni, 2007. These rocks are often the only 30 key to determine the structural patterns in the deep crust. However, the structural analysis of 31 migmatites may be not very easy because of their complex and multiphase evolution. 32 Moreover, the products, leucosomes and melanosomes, from the melting of an initial highly 33 deformed rock acquire a fabric that mostly cannot be determined by classical structural 34 approaches. In partially melted gneisses, i.e. migmatites, this fabric can differ from that of the 35 initial parent rock. IIn dominantly melted rocks, the only visible fabric is mostly related to the 36 orientation of rafts of melanosomes or mesosomes, i.e. respectively restites or protoliths, and 37 therefore this fabric only offers an incomplete signature of the tectonic events suffered by the 38 rocks during melting. Melanosomes and mesosomes usually exhibit features of metamorphic 39 rocks whereas the leucosomes display an igneous-like appearance. Therefore, one of the 40 characteristics of the migmatite structures is their local variability and then their analysis 41 passes by a statistical approach. To this aim, the field observations are limited to part of the 42 elements (markers ?) of the fabric and generally not well-adapted. 43 The anisotropy of magnetic susceptibility (AMS) technique (Graham, 1954); see 44 (Tarling and Hrouda, 1993; Borradaile and Henry, 1997; Borradaile and Jackson, 2004) and 45 references therein) has been widely used for structural applications. It offers several 46 advantages relatively to field observations: It gives not only foliation and lineation but also 47 intensity and shape of the fabric and can be applied to a set of samples representative of a 48 significant area allowing simple statistical analysis. Ferré et al. (2003) and Kruckenberg et al. 49 (2010) applied the magnetic tool for migmatites studies. They showed that despite rheological 50 variations during deformation (solid-state deformation followed by viscous flow), AMS axes 51 were consistent with observed regional field structures and thus highlighting the interest of 52 the AMS data for the strain characterizations in high-temperature metamorphic rocks. In 53 paramagnetic migmatites, the biotite fabric can evidenced these two types of deformation 54 (Hasalovà et al., 2008). Others authors have shown that anatexites could have specific AMS 55 signature, associated with changes towards weak solid-state rheology and that AMS 56 characterizations could therefore help to better model the different stages of migmatitic 57 terranes (Charles et al., 2009; Schulmann et al., 2009). 2 58 The Pointe Géologie archipelago (Terre Adélie, East Antarctica) represents a deep and 59 hot crust that experienced a long-live anatectic event during Paleoproterozoic times, 1.69 Ga 60 ago (Ménot et al., 2007 and references therein). This archipelago is partially covered by the 61 ice cap and limited outcrops are key zones to constrain the Terre Adélie Craton tectonics. 62 Pelletier et al. (2002) and Gapais et al. (2008) proposed a detailed structural and kinematic 63 analyses of the area based on foliation and lineation measurements of migmatites. But we 64 believe these structural data may be supplemented by taking into account the magnetic fabric 65 of the leucosomes and anatexites, which correspond to more than 50% of the outcrops and 66 which are devoid of clear markers of deformation. This would greatly improve the knowledge 67 of the structural pattern of this region. 68 The first aims of this paper is thus to specify the deformation framework associated to 69 the Paleoproterozoic event in the Terre Adélie Craton from a large sampling in the Pointe 70 Géologie rocks. For this, a detailed AMS study was performed in the migmatites, the larger 71 granitic dykes and the anatexites observed on the field. Finally, we focus on various 72 migmatitic structures of centimetric to decametric size; they correspond to various phases of 73 segregation, extraction and transfer of melts. We discuss the relationships between these 74 different migmatitic habitus and their related AMS signature in order to constrain the 75 rheological evolution of the molten crust. 76 77 2. Geological setting 78 79 The Terre Adélie Craton (TAC) is located on the easternmost part of the East 80 Antarctic Shield. It crops out as islands and capes scattered along the coast between 135° and 81 145°E but most of the outcrops are located in three main archipelagos, from West to East: 82 around Pointe Géologie (66°50’S, 140°E), East of Port Martin (66°80’S, 142°25’E) and East 83 of Cape Denison (67°S, 142°25’E) up to the Mertz glacier. This crystalline basement consists 84 of Late Archean and Paleoproterozoic formations devoid of any significant reworking since 85 1.5 Ga and then it is considered as part of the Mawson block or Mawson continent (Fanning 86 et al., 1995; 2002). At the scale of the TAC, the Late Archean and Paleoproterozoic terrains 87 are distributed westwards and eastwards from Port Martin, respectively (Monnier et al., 1996; 88 Ménot et al., 2007), Figure 1. 89 This paper deals only with the Paleoproterozoic formations of the Pointe Géologie area, 90 i.e. close to the permanent French Polar Station Dumont d’Urville (DDU). As described by 91 (Bellair, 1961b, a), the main rock types are migmatitic to anatectic gneisses that are cross cut 3 92 by dykes of apparently isotropic coarse-grained pink granites. The detailed mapping, carried 93 on during the GEOLETA project, improves this previous description and points out some new 94 and significant features (Monnier et al., 1996; Peucat et al., 1999; Gapais et al., 2008). 95 Migmatitic gneisses and anatexites derived from a sedimentary sequence dominated by 96 aluminous pelites together with subordinate greywackes, quartzites and calc-silicates. 97 Metagreywakes appear as intercalations ranging from tens of centimetres to hundreds of 98 meters in thickness. Quartzites and calc-silicates form dismembered layers and enclaves of 99 mesosomes within the migmatites and they mark out a poorly preserved sedimentary layering 100 (Figure IIa). Amphibolitized dolerites and gabbros occur as dykes and sills and they are 101 coeval with the anatectic event as shown by magma mingling features between the mafic 102 intrusions and the granitic magmas. Isotopic data indicate Paleoproterozoic sources for both 103 sediments and magmas (Peucat et al., 1999 and references therein). According to Monnier et 104 al. (1996), mesosomes, neosomes and anatexites represent respectively 10%, 60% and 30% of 105 the rock types in the Pointe Géologie archipelago. 106 These migmatitic and anatectic formations underwent a polyphased tectonic and 107 metamorphic evolution with three phases of deformation leading to a composite sub vertical 108 regional S0-S1-S2 foliation {Monnier, 1996 #3766;Pelletier, 2002 #3923;Pelletier, 2005 109 #867}. Neosomes display two successive parageneses related to both the S 1 and S2 110 metamorphic foliations and bearing comparable Sil+/-Kfs+/-Pl+/-Bt+/- Cd+/-Grt+/-Ilm+/-Qtz 111 mineral assemblages. Moreover, mineral chemistry of the S1 and S2 parageneses is similar and 112 argues for a single continuous LP-HT metamorphic event, the peak conditions of which 113 reaching 750-700°C at 0.6-0.4 GPa. Large amounts of anatectic melts have been produced all 114 along the tectonic and metamorphic evolution as suggested by the various habitus of the 115 leucosomes. The oldest leucosomes appear as mylonitic lenses isoclinally folded by the S1-S2 116 transposition, but most of them are undeformed and concordant within the S2 foliation and the 117 latest melts cross cut the S2 planes. A retrograde imprint with Bt+/-Ms+/-And assemblages 118 marks the later evolution to about 550-450°C and 0.5-0.4 GPa (Monnier et al., 1996; Pelletier 119 et al., 2002; Gapais et al., 2008). 120 Bellair and Delbos (1962) assumed a 1.5 Ga age (Rb/Sr on micas) for the partial melting 121 event. More recently, new radiometric data (Peucat et al., 1999, U-Pb on zircons and 122 monazites, Sm-Nd and Rb-Sr on whole rocks and minerals) gave precise time constraints on 123 the geological evolution of the meta-volcano-sedimentary formations of Pointe Géologie. 124 Time of deposition is bracketed between the inherited zircon ages (1.72 -1.76 Ga) and the 125 peak metamorphism and partial melting age at 1.69 Ga. The later cooling path was 4 126 constrained by Nd garnet ages (650-600°C at 1.63-1.60 Ga) and Rb-Sr muscovite and biotite 127 ages (450-350°C at 1.5 Ga). 128 129 3. High temperature rocks types and regional structures 130 131 While the lithology is very homogeneous in the scale of the archipelago, field 132 relationships between different rock types are much more complex for the scale of outcrops. 133 Four main rocks types have been sampled for AMS measurements: migmatites including 134 leucosomes and melanosomes, coarse-grained pink granites, anatexites and strongly mylonitic 135 gneisses. 136 Migmatitic gneisses: They have been described previously as the K feldspar gneisses 137 {Pelletier et al 2005 #867}{Monnier et al., 1996 #764} and they are the dominant facies of 138 the area, especially on the Pétrels Island (Dumont d’Urville station, Figure I). We will discuss 139 more specifically the space and time relationships between leucosomes and melanosomes in 140 the migmatitic gneisses. As partial melting developed all along a polyphased tectonic and 141 metamorphic event, leucosomes display various habitus relative to the composite foliation, 142 which is marked on the field by melanosomes and septas of mesosomes. The melanosomes 143 defined continuous layers in migmatites (Figure IIa): 144 (i) The earliest leucosomes occur as mylonitized and elongated lenses, sometimes 145 affected by intrafolial folds within the foliation. They bear evidence of successive 146 segregation and deformation processes (Figure IIa). 147 (ii) The most common leucosomes are undeformed and concordant within the 148 migmatites foliation and they may be later folded together with the foliation. They 149 represent syn to late-foliation melts (Figure IIb). 150 (iii) The latest leucosomes form dykelets cross-cutting, and post-dating, the S1-2 151 foliation. They may be connected to the concordant leucosomes, tapping off and 152 transferring melts upwards (Figure IIa, c). 153 Coarse-grained pink granites: they appear as dykes of decimetric to decametric 154 thickness which cross cut the regional foliation (Figure IId). They are devoid of any visible 155 markers of orientation. Such dykes, collecting the dykelets, drain the more evolved melts 156 during the late- to post-tectonic stages of the partial melting and metamorphic event. 157 Anatexites: They outcrop widely on the W area of Pointe Géologie (e.g., Gouverneur, 158 Balance, Taureau and la Vierge islands, Figure VIII). They derived from a higher degree of 159 partial melting than migmatitic gneisses and show a mineral assemblage comparable to that of 5 160 leucosomes but more enriched in Qtz and depleted in Crd. Anatexites display more isotropic 161 textures but a flow fabric or a palimpsest structure of the parent gneisses is often marked by 162 some oriented rafts of migmatitic gneisses or schlierens of biotite and oxides (Figure IIe). 163 Mylonitic gneisses: they outcrop in a restricted and narrow zone on the western flank of 164 the Pétrels Island (Rocher Jakobsen) and some islands of Pointe Géologie, i.e. along a major 165 shear zone (sites II and V, Figure IX). They consist of Bt + Grt gneisses with only tiny Grt- 166 bearing leucosomes and are characterized by a vertical mylonitic foliation. They derive from 167 the K-feldspar migmatitic gneisses and then may be considered as late- to post-migmatisation 168 tectonites (Figure IIf). 169 As carefully described by Pelletier et al. (2002) and Gapais et al. (2008), the Pointe 170 Géologie archipelago show two types of structural domains: NS to N340° striking vertical 171 shear zones and domes both of them developing during the metamorphic and anatectic event. 172 Between the vertical zones, foliation attitudes point out dome-shaped structures marked by 173 flat lying to gently dipping fabrics. Dome displays a mineral lineation outlined by a preferred 174 orientation of sillimanite crystals while such a lineation is almost invisible in the vertical 175 zones. The transition from flat lying to vertical foliation zones may be sharp, with 176 development of vertical foliation planes cutting across the horizontal foliation of domes, or 177 gradual when folds, with horizontal axes, induce vertical planes. Such a transition from dome 178 to vertical shear zone never exceeds five hundred meters in thickness. In both cases, vertical 179 structures seem to be later than flat lying ones. According Gapais et al. (2008), the kinematic 180 markers (lineations, boudinage, ...) suggest that shear zones reflect a dextral transpressive 181 movement while flat areas are the result of shortening combined with stretching parallel to the 182 shear zones. Such patterns might be explained in the frame of a regional convergence of a hot 183 and weak juvenile crust leading to horizontal crustal flow and strain partitioning with 184 localized deformation along transpressional shear zones. 185 186 4. Sampling and analyses procedures 187 188 Because of outcrops restrictions (areas non accessible because of ice cover or of birds 189 protection) and high variability of the visible deformation, sampling was often made in sites 190 relatively close one to another in the main island (Pétrels Island). Other sites were scattered in 191 different smaller islands (Figure VIII). Most sampled sites correspond to a surface up to 50m2. 192 As a test, one site (site i, Figure IX) corresponds to a sampling made on a reduced surface 193 (about 0.5 m2) in gneisses showing visible foliation and lineation. 6 194 X large samples have been taken for petrographic and rock-magnetism studies. For 195 magnetic fabric study, cores were sampled with a gasoline-powered portable drill. All the 196 cores were oriented only with a sun compass (Figure IIf) because of the immediate proximity 197 of the southern magnetic pole. That introduced a strong limitation for sampling because of 198 climatic conditions. The sampling was made during three different summer fieldworks, in 199 1992, 2009 and 2011. As a whole, 819 rock cores were obtained in 33 sites, including 20 on 200 the Pétrels Island (Figure IX). When possible, different facies (from gneiss to anatexites) were 201 sampled on the same site. The cores were cut in the laboratory in specimen of standard 202 paleomagnetic size. 203 Magnetic susceptibility and its anisotropy have been measured using Kappabridges 204 KLY3 and MKF1 (AGICO, Brno). Thermomagnetic experiments were performed on 205 representative samples by heating in argon or in air using the CSL equipment and the CS2-3 206 oven (AGICO, Brno) associated with the Kappabridges. Hysteresis loops were obtained for 207 small cores (cylindrical samples of about 3 cm3) using a laboratory-made translation 208 inductometer within an electromagnet capable of reaching 1.6 T. 209 210 5. Magnetic Mineralogy 211 212 5.1. Thin sections study 213 As the magnetic characteristics of the rocks are tightly controlled by their 214 mineralogical content, the various assemblages recorded in the different rock types need to be 215 specified. This is particularly important in the case of migmatitic gneisses where partial 216 melting induces a redistribution of refractory minerals from the mesosomes to both the 217 melanosomes and leucosomes. 218 Magnetite and ilmenite are the most abundant oxide minerals. They form discrete grains or 219 clusters with direct contact between magnetite and ilmenite. The larger grains (millimetric in 220 size) are generally found in the melanosomes and therefore in the foliation and they appear as 221 elongated parallel to the lineation defined by the sillimanite when the latter is present (Figure 222 III). For ilmenite, deformation also induces a structural axes related lattice preferred 223 orientation (LPO), which is characterized by the c-axes strongly concentrated close to the 224 normal to the foliation, and by the poles of (2-1-10) and (10-10) prism planes 225 concentrated close to the lineation (Figure IIIbis). Oxides are also present in the leucosomes 226 but the fabric (grains alignment) appears more scattered (equant ?) than in the melanosomes. 227 At the melanosome-leucosome boundary, elongated shape grains, may-be rotated, have been 7 228 observed perpendicular to the foliation. In the leucosomes these oxide grains become more 229 discrete and more rounded (Figure III). 230 Cordierite is also present in migmatitic gneisses and granitic dykes of Pointe Géologie. 231 This mineral that occurs mainly as grains of globular shape (up to a few millimetres in size) is 232 carefully watched because cordierite presents specific magnetic properties. This mineral 233 carries an inverse magnetic fabric (i.e. characterized by a switch between the principal 234 maximum K1 and minimum K3 axes of the AMS ellipsoid with respect to the grain shape 235 (Potter and Stephenson, 1988; Rochette et al., 1992)) that could lead to misinterpretation of 236 the measured magnetic fabrics. However the mean magnetic susceptibility (Km) for 237 magnetite, which is ubiquitous in studied thin sections, is significantly higher than for 238 cordierite (Km ratio > 1000). Therefore magnetite should be the main carrier of measured 239 AMS. For relatively large grains of magnetite, the K1 and K3 axes indicate the magnetic 240 lineation and magnetic foliation pole, respectively. 241 242 5.2. Rock-magnetism 243 The mean magnetic susceptibility Km (average 5.2 10-2) of the studied samples is 244 different according to the studied fraction of the migmatites (Figure IV). The gneisses with 245 subordinate melted parts and dominant melanosome fraction have very high susceptibility 246 (average?). Km values for dominant granitic fraction are lower (average?). Migmatite samples 247 including both leucosome and melanosome fractions present intermediate Km values. This 248 variability in leucosome versus melanosome content of gneissic specimens largely explains 249 the relatively large distribution of susceptibilities (Figure IV). The anatexites samples show 250 the highest variation in Km values (from X to Y). 251 All thermomagnetic KT curves (susceptibility K as a function of temperature T) show 252 during heating a sharp susceptibility decrease around 580°C (Figure V), clearly indicating the 253 presence of magnetite. In addition low temperature experiments confirm the presence of this 254 mineral by a large susceptibility increase around -160°C (Figure V). This variation 255 corresponds to the Verwey transition that is characteristic of pure magnetite. Few 256 thermomagnetic curves are perfectly reversible. Susceptibility values from the cooling curve 257 are mostly a little bit higher than the initial values, in air as in argon atmosphere (but 258 sometimes much higher as for the sample AP35). Partial cooling loops during heating 259 evidenced a weak mineral alteration due to heating around 300 to 400°C that probably reflects 260 inversiontransformation of a weak amount of maghemite in hematite. New magnetite is also 261 often formed at the highest temperatures. 8 262 Hysteresis loops show generally a full saturation of the magnetization for moderate 263 field (Figure VI). This saturation was partial only for the sample AP35, evidencing the 264 presence of another component of high coercivity. This component is probably hematite. In 265 most cases, ferrimagnetic minerals have a largely dominant effect for the susceptibility, but 266 two of the studied granite samples highlight also a strong contribution of the paramagnetic or 267 even diamagnetic minerals. Day plot (Day et al., 1977) for samples with mainly magnetite 268 clearly evidences a large size of the magnetite particles (Figure VII). 269 Main magnetic mineral is therefore magnetite with a large size. Obtained AMS data 270 are then directly usable for a structural analysis (no inverse magnetic fabric due to small 271 Single Domain particles (Potter and Stephenson, 1988). 272 273 6 - Magnetic fabric 274 275 The AMS ellipsoid yields the three principal susceptibility axes defined as 276 K1 K2 K3. K1 is the magnetic lineation and K3 is perpendicular to the magnetic foliation. 277 The Jelinek (1981) parameters P' and T were used to describe the intensity and the shape of 278 the magnetic fabric, respectively. Data for a group of samples were analysed using normalized 279 tensor variability (Hext, 1963; Jelinek, 1978) statistics. 280 6.1 – Structures from AMS 281 Data for migmatitic gneiss and for granites are presented separately (migmatitic 282 gneisses included minor melted parts and "granitic" samples small amounts of melanosome 283 assemblage and this separation has been made then considering the dominant presence of one 284 of these components). Moreover, from the regional structural field pattern, two distinct zones 285 have been distinguished for the AMS analyse: the sub-vertical zones and the dome shaped- 286 zones (Figure VIII and IX). 287 6.1.1. In migmatitic gneisses of sub-vertical shear zones (sites T, R, D, O, XIII, A of 288 Pétrels Island, Figure IX, melanosome layers show generally both well clustered magnetic 289 foliation pole (K3) and magnetic lineation (K1). The magnetic foliation is dominantly 290 subvertical N-S in accord with the observed field foliation and the magnetic lineation presents 291 a weak plunge and N-S trending in agreement with the orientation of mineral lineation 292 outlined in few places by a preferred alignment of sillimanite crystals (je n’ai pas de souvenir 293 de lineation à sillimanite dans les SZ verticals, de plus le site I est assez marginal, voir 294 extérieur à la SZ majeure). The granitic rich layers (site XIII) display more diffuse fabric, in 295 particular the K1 axes that tend to form a girdle perpendicular to K3. Well-individualized 9 296 leucosomes (e.g. Figure IIC) show a different magnetic fabric signature than melanosome 297 layers characterized by strongly inclined to sub-vertical magnetic lineation (site 298 XIII 299 horizontal plane with two dominant directions: N-S and E-W. 300 . The K3 axes are more scattered than the K1 axes. They are in the IXthe K3 In large coarse-grained pink granite dykes (sites A, E, D 301 axes are relatively well clustered defining a subvertical magnetic of strike close to that of 302 neighbouring gneisses (sites E, D 303 magnetic lineation pattern is characterized by the verticalization of K1-axes in comparison to 304 magnetic lineation measured in the melanosome layers of neighbouring gneisses. They form 305 girdle perpendicular to K3 (site E or strongly inclined to sub-vertical local maximum 306 (sitesD A a divergent strike (sites A). The 307 , Taureau, la Vierge, Balance Islands (sites 308 VIIXV, XIV XVIII, XIXFigure VIII) and South of Pétrels Island (site 309 XX 310 Gouverneur anatexite (sites VII, XV 311 lies in the horizontal plane, relatively scatted or forms clusters at 90 degrees from each other 312 with the N-S and E-W directions that prevails for south Gouverneur Islands (site XV). 313 Sampling sites XIV, XVIII (Figure VIII) show heterogeneities in the partial melting degree 314 that is expressed in the field by more or less regularly presence of migmatitic gneiss rafts in 315 the anatexites. For site XVIII 316 gneisses show distinct magnetic axes orientations characterized by K1 preferentially sub- 317 vertical and K3 horizontal N-S (i.e., magnetic foliation vertical E-W) in anatexites while K1 318 is horizontal to strongly plunging N-S and K3 is horizontal E-W (i.e., magnetic foliation 319 vertical N-S) in neighbouring gneisses. The N-S orientation of magnetic foliation in gneisses 320 fit quite well with the regional vertical shear zone structures. In opposite, the E-W vertical 321 magnetic foliation that appears in the larger dykes and anatexites is less well-constrained by 322 large-scale 323 XIV T 324 and the migmatitic gneisses was difficult to perform. That explains the relatively wide 325 confidence zones at 95% for K1 and K3. However the magnetic fabric is mainly oriented 326 vertical E-W for the foliation and strongly-inclined (westward) for the lineation. 327 328 K1max tends to have strong inclination or to be sub-vertical. For field structures anatexites and migmatitic (Figure VIII). For site tinction on the field between the anatexites In mylonitic gneisses of Jakobsen (sites II, V, ) the magnetic foliation (K1-K2) is dominantly subvertical N-S in accord with the observed field structures (Figure 10 329 IIf). On the contrary, the AMS measurement reveals uncommon highly dipping or sub- 330 vertical lineation. 331 332 6.1.2. In the migmatitic gneisses of the dome shaped-zones (sites J, VI, G, K, H, S, 333 XVI, XVII, Figure VIII; sites C, IV, Q, III, VIII, I, B, i, XII, F, ) magnetic 334 fabric display a stronger variability of K1 and K3-axes orientations from one site to another 335 one in comparison to structured vertical shear zones. A relatively strong dip (about 45°) for 336 the magnetic foliation is frequently observed, in particular for the sites located in the flanks of 337 domes (sites H, K, Figure VIII; sites IV, Q, III, Figure IX) for the eastern flanks of the 338 Pétrels-Curies Islands dome). The magnetic foliations are generally in agreement with the 339 field measured strike and dip of melanosome layers. The magnetic lineations show gently dip 340 and dominant NNW strike. The innermost zones of domes (sites XVI, XVII, Figure VIII; sites 341 VIII, I, B, Figure IX) show also a strong variability of AMS structure patterns correlated to 342 the complexity of migmatitic structures observed at the domes apex. In these areas are 343 observed the less well-defined magnetic directions (with the widest confidence zones at 95%: 344 site XVI, Figure VIII; site I, Figure IX). Sampling in a granitic dykelet of centimetric width 345 crosscutting flat-lying gneissic foliation was performed in site XVII (Figure VIII). The 346 related AMS pattern is characterized by vertical N-S magnetic foliation and sub-vertical 347 magnetic lineation and then differs from that of gneiss. 348 Large homogénéiser dykes of coarse grained pink granites sampled in site F an XII 349 (Figure IX) are characterized by vertical magnetic lineation when compared with the 350 magnetic lineation from the melanosomes of gneisses. This feature is similar to that observed 351 in the granitic bodies from the sub-vertical shear zones. The magnetic foliation in the granitic 352 dykes is either concordant with that of host gneisses (site F) or discordant (site XII). Relire 353 les phrases avec attentiuon 354 355 6.2 – AMS parameters (P’ and T) 356 The Figure X presents the characteristics of the susceptibility ellipsoid. The degree of 357 anisotropy P’ is very high in the migmatitic gneisses (mean 1.479; minimum 1.041; maximum 358 1.903). It is lower in granites (mean 1.222; minimum 1.040; maximum 1.413). The shape of 359 the susceptibility ellipsoid is dominantly oblate, in gneisses (for T value: mean 0.30; 360 minimum -0.08; maximum 0.66) as in granites (mean 0.25; minimum -0.10; maximum 0.62). 361 In granites, a clear relationship (Figure IV, R2=0.70) between P’ (intensity of the fabric) and 11 362 Km (related to the concentration in ferrimagnetic minerals) highlights the dominant effect of 363 the magnetite in the AMS (Henry et al., 2004). Another relationship (R2=0.54) between T and 364 P’ in granites suggests that the most prolate fabrics correspond to the weakest anisotropy 365 Figure X. In addition, for granite, the anatexites show the highest variability in P’ and T 366 values, including the extreme values Figure X. 367 368 7 – Discussion 369 7.1 Mean susceptibility (Km) and anisotropy (P’) signature 370 The amount of magnetite is clearly different in migmatitic gneisses and in granites 371 (leucosomes and dyke), as shown by the susceptibility values (Figure IV). This variation of 372 magnetic susceptibility between melanocratic and leucocratic layers is mainly due to the 373 variations in magnetite content. Magnetic studies suggest also mineralogical changes 374 affecting magnetite with formation of ferromagnetic oxides of lower susceptibility like 375 maghemite or hematite. Concerning this mineralogical change, gneiss sample AP35 is the 376 only one with hematite; it also presents the strongest formation of a lot of new magnetite at 377 high temperature (susceptibility becomes 14 times higher on the cooling curve). It is therefore 378 probably due to a strong local mineralogical alteration (interaction with deep fluids, 379 weathering?) and remains an exception. 380 The intensity of magnetic anisotropy, illustrated by the P’ values, is lower in granites 381 than in gneisses (Figure X). In granites, it presents a relationship with the Km values, 382 suggesting that this difference could be explained by the lower amount of magnetite in 383 granites, AMS then resulting mainly from strong magnetite anisotropy and weak anisotropy 384 of a low susceptibility component. Owing to its Km values, this last component is the 385 paramagnetic minerals and not the maghemite. The observed inverse correlation between T 386 and P’ in granites (Figure X) shows that the AMS of this second component is less oblate than 387 the magnetite AMS. 388 Inversely to granitic magmas constituting leucosomes and dykes, a wide range in Km 389 values, according to samples within a single site, is observed in anatexites. It is due to the 390 presence of more refractory rafts of gneisses with high concentration in oxides grains. 391 392 7.2 AMS in migmatitic gneisses and granites 393 In addition to the Km and P’ values, the main differences in magnetic fabric between 394 melanosome layers of gneisses and granitic magmas concern the orientation of the K1 axis 395 (Figures VIII and IX). K1 axis is dominantly close to the horizontal in melanosomes and close 12 396 to vertical in granites. In some granitic sites (e. g., sites E, XII, Figure IX), its orientation is 397 relatively scattered within a vertical plane, probably because of the presence of melanosome 398 fragments within the granite. Other difference in orientation of susceptibility axes concerns 399 K3. Whereas in melanosome the K3 orientation fits to the field structures, it appears in granite 400 a more complex magnetic orientation pattern with two dominant orientations. The first one 401 matches to the gneissic structures (for example, the magnetic foliation is vertical N-S in the 402 shear zone area) and the second is at 90 degrees of the first one. In some sites the two 403 clustering are present (e.g., site XV Figure VIII and site XIII, Figure IX). The first 404 orientation is associated to the strike-slip deformation, which is at the origin of the large-scale 405 sub-vertical corridors. The cause of the second orientation is less straightforward. In Pétrels 406 Island, the migmatitic layering is locally cut by vertical large granitic dykes of NE—SW to E- 407 W direction (Monnier, 1995). Then emplacement of such E-W trending dykes is tectonically 408 controlled and consistent with a component of NNW-SSE to N-S dextral strike-slip (Gapais 409 et al., 2008). In the western area (Gouverneur island area, Figure VIII) where rafts of 410 melanocratic restites are still packed in anatexites, E-W magnetite could correspond to 411 inheritance of older tectonic foliations. 412 The gneiss sites II and V, on the southwestern border of the Pétrels Island (Figure IX) 413 also present mainly subvertical K1 axes. However, the gneisses of sites II and V (rocher 414 Jakobsen, voir aussi plus haut+carte pour nom) are intensely deformed, unlike the granitic 415 leucosomes, dykes and anatexites that have not recorded pervasive solid-state deformation,. 416 Thus, AMS fabric is interpreted as resulting of high-strained, late- to post-migmatisation 417 solid-state deformation. The strong K3 clustering indicating a N-S vertical magnetic foliation 418 and the highly tilted to sub-vertical magnetic lineation could be related to deformation in 419 transpressionnal regime mainly restricted to the N-S vertical shear zones. 420 Thin section analyses show a change of orientation of magnetite grains from 421 melanosome to leucosome. In melanosome, the oxide grains are within the foliation and 422 elongated parallel to the lineation also marked by the sillimanite alignment. They are 423 interpreted as resulting from solid-state deformation that occurred during the Paleoproterozoic 424 metamorphic event (1.69 Ga ago). In addition, LPO of ilmenite, which strongly correlated 425 with the tectonic fabric, suggest dislocation glide on (0001) as main deformation mechanism. 426 The basal slip for hematite – ilmenite mineral could reflect high-temperature solid-state 427 deformation (e.g., Bascou et al., 2002; Siemes et al., 2003). Migmatitisation processes are 428 also associated with segregation and transfer of melts that lead to leucosomes, pink granitic 429 dykes and then anatexites when partial melting degree is higher. As discussed in Vigneresse 13 430 et al. (1996), the increase of melt fraction produce changes in rheological behaviour. From 431 plastic deformation evidenced by elongation of oxide minerals, which are abundant in the 432 melanosome to magma flow with transport of isolated solid particles in leucosomes, dykes 433 and anatexites. 434 Such different and successive regimes of deformation affecting magnetite grains first 435 deformed under solid-state conditions and then involved as passive rigid particles during 436 melting, have been commonly observed in various migmatitic terrains voir labrousse 437 (scandinavie)Ferré et al., 2003). In Pointe Géologie migmatites, these successive regimes 438 generate distinctive AMS signatures. The clearest difference concerns the K1 orientation, 439 which tends (reaches) to a vertical orientation during segregation and circulation of felsic melt 440 in agreement with the gravity-induced upwelling of magmas. K3 orientation in granitic layer 441 appears more sensitive to the degree of partial melting and the structuration of country rock. 442 At lower degrees of partial melting, liquid segregation remained strongly constrained by the 443 framework of the unmelted gneissic material. Then the felsic melt formed dykelets and 444 connected lenses concordant with the foliation of gneisses. For higher degree of melting, the 445 melt was injected as concordant or cross-cutting large veins (Figure IIc,d) resulting in the 446 various orientations of the magnetic foliation. Then the dykes and veins intrude areas of lower 447 stress, generally close to the 3 direction (e.g., Cooper, 1990; Hand and Dirks, 1992). 448 449 450 7.3 Methodological and regional-scale implications 451 All these observations evidence that the AMS study of migmatites cannot be 452 considered as a routine method. To be as reliable as possible, the AMS approach requires a 453 preliminary detailed observation of the various leucosomes habitus and then a large number 454 of magnetic measurements of rocks characterized by various degrees of melting. For low 455 degrees of partial melting the leucocratic layers remain strongly constrained by the earlier 456 structure defined by the unmelted material. In that case, the AMS principal axes are 457 representative of the local and regional finite strain axes. This fits with the conclusions of 458 Ferré et al. (2003) for migmatites of the Superior Province in Minnesota. For more 459 pronounced partial melting degree, well-individualized leucocratic layers can developed 460 specific AMS patterns associated to flow regime. In the Pointe Géologie migmatites, the flow 461 regime differs from the local and regional finite strain axes by the direction of K1-axes. Large 462 variations of the partial melting rates increase the probability to measure composite AMS and 463 the difficulty to isolate pre-melting and synmelting magnetic fabrics.. The strongest variations 14 464 of AMS principal directions and parameters recorded in anatexites are related to the 465 heterogeneity of these rocks, that enclose number of schlierens and refractory material. 466 The structural pattern of Pointe Géologie consists of two structural domains with respectively 467 flat-lying and sub-vertical foliations related to a long-live tectonic, metamorphic and anatectic 468 event (Monnier, 1995; (Pelletier et al., 2002, 2005). Commonly, stretching mineral lineations 469 are not easy to observe within the foliation, more specially within the sub-vertical shear 470 zones. Combining structural field evidences, determination of P-T-t metamorphic evolution 471 and analogic simulations of the mantle-crust ductile deformation ,{Gapais, 2008 #437 and ref. 472 therein} propose a model in which the Paleoproterozoic hot and weak lithosphere converges 473 toward a cooler and more rigid craton (Neoarchean in age). In this model, deformation of the 474 Paleoproterozoic crust combines both transpression and horizontal flow and/or lateral escape 475 parallel to the Archean basement and perpendicular to the shortening direction. 476 AMS structural pattern determination provides complementary structural information 477 such as magnetic lineations. They are mainly sub-horizontal in sub-vertical foliated gneisses. 478 It underlines the importance of the strike-slip component during the deformation. In mylonitic 479 gneisses, which are considered as late- to post-migmatisation tectonites, nearly vertical 480 lineations are evidenced. This is considered as the effect of transpressionnal regime, which 481 combinates strike-slip and across-strike shortening. In migmatites with flat-lying foliation, the 482 magnetic lineation displays a moderate plunge and is commonly parallel to the mineral 483 stretching lineation. Such features are in good agreement with an horizontal crustal flow 484 mechanism. 485 Increasing partial melting degree leads to a loss of the rock cohesion related to the 486 migration of the melt trough a solid-state frame made of previously deformed minerals .Thus 487 the former tectonic structures will be progressively erased. Melt segregation and transfer 488 occur under a viscous flow regime, mainly driven by gravity forces. In such a regime, the 489 well-defined leucosomes, dykes and anatexites will develop a magnetic fabric corresponding 490 to the upwards transport of magmas. Then AMS measurements would allow to better map the 491 mass transfers associated to intensive melting at peak temperatures and to characterize the 492 general framework of a warm and buoyant lithosphere. 493 494 8 – Conclusion 495 Pointe Géologie archipelago in Terre Adélie represents a deep and hot crust affected 496 by intensive anatectic event during Paleoproterozoic times, 1.69 Ga ago. This generated 497 different HT rocks types such as: migmatites including leucosomes and melanosomes, coarse15 498 grained pink granites dyke and anatexites. Partial melting affects indifferently the regional 499 structures characterized by the juxtaposition of flat-lying and sub-vertical deformation zones. 500 Magnetic mineralogy study shows that oxide minerals are mainly large grains of 501 magnetite. Ilmenite is also observed constituting cluster with magnetite, which is particularly 502 abundant in melanosome layers. The grains are intensely solid-state deformed and aligned 503 parallel to the lineation marked by sillimanite. In the leucosomes, oxides appear more 504 scattered than in the melanosomes and their rounded shape suggests rotation of the former 505 elongated grain during melt segregation. 506 Melanocratic layers on the one hand and felsic leucosomes, dykes and anatexites on 507 the other hand develop contrasted AMS signatures. The mean magnetic susceptibility (Km) 508 and the anisotropy degree (P’) are high in the gneisses and lower in granitic samples. 509 Orientation of principal susceptibility axes also differs. In migmatitic gneisses, magnetic 510 foliations are coherent with the local and regional structural pattern. Nevertheless AMS 511 technique provides complementary information on the orientation of lineations, when they are 512 difficult to observe in the field. They are subhorizontal in the shear zones, (dans les domes 513 non ?) except in vertical mylonitic zone where high plunge evidences the transpressionnal 514 regime of deformation. In well-defined leucosomes, granitic dykes and anatexites, the 515 magnetic ellipsoid is characterized by the vertical orientation of the magnetic lineation. This 516 change of orientation is related to a rheological contrast between the solid-state deformation 517 suffered by the oxide grains and their reorientation in a viscous flow during the aggregation of 518 felsic melt. 519 Magnetic structure pattern do not disagree with the model of deformation of a hot and 520 weak lithosphere converging toward a cooler Archean craton proposed by Gapais et al. (2008) 521 from metamorphic and field structures analysis and analogic simulations. They explained the 522 structural pattern of the Pointe Géologie and surrounding areas by an horizontal, orogen- 523 parallel, subconstrictional flow that could result from oblique convergence and/or from 524 particular boundary conditions facilitating lateral escape. A comparable model was also 525 assumed from numerical modelling to image the deformation of the hot Neoarchean crust of 526 the Eastern part of the Terre Adélie Craton (Duclaux et al., 2007). The magnetic structures 527 map allows to highlight the role of the gravity-induced upwelling of a crust undergoing partial 528 melting. 529 From methodological point of view, this work emphasizes on the importance of an 530 acute petrological characterization of sites to be selected for AMS measurements in order to 531 avoid pre- and syn-melting composite magnetic fabrics. Finally, it underlines the difficulty of 16 532 AMS analyses in anatectic rocks, which lead to a very large variability for AMS signature; 533 this mainly cause by the preservation of refractory rafts and by the heterogeneity of such 534 rocks . . 535 536 Acknowledgements 537 We are very grateful to the "Institut polaire français Paul Emile Victor" for support of 538 the program ArLiTA (Architecture de la Lithosphere de Terre Adélie) and to the Japanese 539 "National Institute of Polar Research" for participation to the international exchange program 540 under the Antarctica Treaty and for invitation of BH in Tokyo. LPO were carried from EBSD 541 measurements using a SEM-JSM 5600 at the university of Montpellier (France) and ilmenite 542 pole figures were generate from software developed by D. 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Petrol. 57, 1579-1600. 642 19 643 Figures captions 644 645 Figure I : Simplified geological map of the Terre Adélie Craton (after Ménot et al. 2007). 646 Studied zone (red star) is located in the 1.7 Ga domain, close to the French Polar 647 Dumont d’Urville station. Inset: location and limits of the Terre Adélie Craton (TAC) 648 in East Antarctica and of the Gawler Craton (GC) in South Australia. 649 650 Figure II : Example of high-temperature rock types outcropping in Pointe Géologie 651 archipelago. (a) Migmatitic gneiss structures illustrating the HT polyphased tectonic in 652 the paleproterozoic formation of the TAC: septas of mesosomes and more continuous layers of 653 melanosomes bearing foliation (e.g., hammer area); successive generation of melt segregation 654 with earliest elongated lenses locally affected by intrafolial folds within the foliation, 655 undeformed and concordant leucosomes with the foliation and later thin dykes cross-cutting 656 foliation (arrowed). (b) Folded leucosomes with axial plane parallel to the foliation. (c) 657 Melt segregation process generating concordant leucosome that supplies “alimente” 658 cross-cutting dykelet transferring melts upward (Petrel Island). (d) Coarse-grained pink 659 granites forming metric to decametric thickness dykes cross-cutting the regional foliation 660 (Pétrel Island). (e). Anatexite showing melanocratic layers bearing foliation (Balance Island). 661 (f) Mylonitic gneisses characterized by vertical foliation (Rocher Jackobsen, Pétrels Island). 662 The solar compass used to determine the geographical orientations of tectonic structures gives 663 the photograph scale. 664 665 Figure III : Photomicrograph of migmatitic gneiss in the vertical shear zone (Petrels Island). 666 Sillimanite (sill) and elongated oxide grains (mainly magnetite (mt) and ilmenite) are 667 parallel to foliation in the melanocratic layers. The shape of oxide grains tends to be 668 more rounded and perpendicular to the foliation in more leucocratic areas (arrowed). 669 670 Figure IIIbis: 671 672 673 674 675 676 677 Ilmenite LPO patterns of migmatitic gneisses in the vertical shear zone, Pétrel Island (sample AP85). LPO are represented on equal area, lower hemisphere projection. Foliation is marked by a black line and lineation is marked by the structural axis X. The density contours are in Multiple Uniform Distribution (MUD); N is the number of measured grains. Figure IV : P' parameter as a function of Km values: granitic dyke (open squares), mylonitic 678 gneisses (full triangles), gneisses (full squares) and anatexites (open diamonds). 20 679 680 681 Figure V : Normalized susceptibility K/Ko as a function of the temperature T in gneisses (samples AP35 and AP85) and in granites (09cjb75, 11cjb41 and 11cjb71). 682 683 684 Figure VI : Hysteresis loops for gneisses (AP35 and AP85) and granite (11cjb108). Remanent coercive force (Hcr). 685 686 Figure VII : Ratios of hysteresis parameters (Day et al., 1977): Jrs/Js (Jrs: remanence at 687 saturation; Js: magnetization at saturation) as a function of Hcr/Hc (Hcr: remanent 688 coercive force; Hc: coercive force). Areas for Multi-Domain (MD) and Pseudo Single 689 Domain (PSD) grain size for pure magnetite. 690 691 Figure VIII : Projection of AMS data of each site of Pointe Géologie Archipelago. AMS 692 projections on Petrel Island (black square) are illustrated in Figure IX. Distribution of 693 maximum axes (K1; blue squares) and minimum axes (K3; violet circle) is in lower 694 hemisphere equal area projection along with confidence ellipses. White, yellow and 695 white colour of stereonets background represents the AMS projections of gneisses, 696 granitic dykes and anatexites, respectively. 697 698 699 Figure IX : Projection of AMS data of each site of Petrel Island in Pointe Géologie 700 Archipelago. Distribution of maximum axes (K1; blue squares) and minimum axes 701 (K3; violet circle) is in lower hemisphere equal area projection along with confidence 702 ellipses. White, yellow and white colour of stereonets background represents the AMS 703 projections of gneisses, granitic dykes and anatexites, respectively. 704 705 Figure X : T parameter as a function of P' values (Jelinek, 1981): granitic dyke (open 706 squares), mylonitic gneisses (full triangles), gneisses (full squares) and anatexites 707 (open diamonds). 708 21