CHEMPHOS 2 INTRODUCTION The use of zinc phosphate coatings as drawing lubricant carriers has become firmly established in the wire and tube drawing industries. The benefits of such coatings in facilitating higher drawing speeds, long tool life, and improved surface finish are now widely recognized. CHEMPHOS 2 is zinc phosphating chemical, ideally suited to meet the above requirements in wire and tube drawings and also in other jobs of cold mechanical deformation such as cold heading, cold extrusion etc. BENEFITS Single chemical process No iron build up. No need to add any external oxidizing agent Strongly adherent Lubricant absorbent zinc phosphate coating Excellent wear resistance Improved wire / tube drawing – higher speeds and greater reductions Increased tool life Smooth Drawing - no metal pick up or jarring Reduces friction – no breakups or scratching Corrosion protection – the fused film of zinc stearate formed by reaction during drawing, gives excellent protection Abusability - Being a single chemical process easy to control & stands a lot of shop abuse … P2 2 SUMMARY OF OPERATING DATA BATH MAKE UP For each 100 litres of bath, add to the water with stirring: CHEMPHOS 2 CONTROL POINTS 3 to 5 litres ( For Normal Operating Conditions ) POINTAGE 22 – 35 TEMPERATURE 65 – 70O C IMMERSION TIME 5 – 10 minutes PROCESS The work after thorough degreasing in CHEMLENE 1D must be pickled in Hcl or H 2So4 after pickling, it is rinsed twice - first with unheated water and then with hot (65-75oC) water. These rinses should be continuously overflowed to maintain cleanliness. The tanks should be drained and cleaned daily. When wire is treated in coils, a highpressure hose rinse is essential for thorough cleaning. BATH CONTROL The CHEMPHOS 2 bath is controlled by a POINTAGE TITRATION, using, the following method. POINTAGE TITRATION 1. 2. 3. 4. Pipette a 10 ml sample of the CHEMPHOS 2 bath into a beaker. Add 6-10 drops of Phenolphthalein indicator Fill the burette to the zero mark with 0.1N Sodium Hydroxide While stirring the sample, slowly run in 0.1N Sodium Hydroxide from the burette until a permanent pink color appears. 5. Record the number of milliliters of Sodium Hydroxide used as the POINTAGE. REPLENISHMENT Add 150ml of CHEMPHOS 2 per 100 litres of bah for each point lacking. should be kept within one point of the specified POINTAGE. The bath MAINTENANCE During processing, sludge is formed as a natural product of the coating reaction. This accumulates in the bottom of the tank and weekly desludging of the bath is recommended. To do this, allow the sludge to settle, decant the clear solution into the emptied rinse tank and discard the sludge. Wash out the CHEMPHOS 2 tank and return the solution. Restore the bath to its operating level by adding water and chemicals in the same proportion as used in the original bath. .. p 3 3 AFTER TREATMENT After the work has been coated with CHEMPHOS 2, it should be rinsed with water at room temperature. The rinse water should be overflowed sufficiently to keep it clean and uncontaminated. It should then be rinsed in a hot (70-90oC) NEUTRALIZER ( refer Tech Note ) rinse. The neutralizing rinse is made up with 0.1kg of NEUTRALIZER for 100 litres of rinse bath. The work is then dipped in the hot CHEMLUBE lubricant bath for 3 – 5 mts and dried thoroughly by hot air blow, before drawing NOTE The above recommendations are given in good faith and carries no warranty. The user will have to satisfy himself in all respects. Information regarding plant, equipment or materials not manufactured by THIN CHEMIE is based on experience and is provided by part of the Technical Service. THINCHEMIE accepts no responsibility for such plant, equipment and material. FURTHER INFORMATION For further information on Special Oils, Coolants, Rust Preventives, Chemical Processes for Pretreatment of Metal Surfaces and Prevention of Corrosion, apply to the following: CHENNAI OFFICE : THIN-CHEMIE FORMULATIONS ‘ BEJOYA ‘ 30, SCHOOL VIEW ROAD CHENNAI 600 028. PHONE : 2493 81 48 FAX NO : 2495 4012 E - MAIL : thinchem@yahoo.com Web : www.ThinChemie.com ***************