1. GENERAL SUBJECT DATA Universidad Politécnica de Valencia University: (Campus of Alcoy) Degree Course: Chemical engineering (3rd course) Departament: Ditexpa Subject: Environmental Analysis Code: 2047 ECTS credits: 4.8 Bachelors / Masters: Bachelors Academic year: 2008-2009 Semester 2 Duration: Optional Subject type: Lecturer/s: Antonio Arques Sanz José Antonio Bonastre Cano Tutorials: Timetable: Office: C2BD4 C2AD2 2. GENERAL DESCRIPTION OF THE SUBJECT This subject deals with the analysis of pollutants present in soils, water and air. The most important parameters are described, together with their significance and the methods that can be employed for their measurement. Aqueous effluents coming from different industries such as textile, paper or metal finishing are analysed in the laboratory classes. 3. OBJECTIVES (COMPETENCES) Introducing the students of technical careers into the main parameters used in environmental chemistry (water, air and soil examination). Studying the most important physical and chemical methods employed in analysis of pollutants Using the analytical methods in laboratory experiments using real effluents. Introducing the student into the most important instrumental devices employed in chemical analysis are explained and laboratory experiments are devoted to their use. 4. PREVIOUS KNOWLEDGE No previous knowledge is needed in order to follow this subject 5. CONTENTS: UNITS UNIT 1: Introduction. Contamination. Analytical methods Definition of contamination. Pollutants. Transport and dispersion of pollutants. Effects of contamination. Physical-chemical methods. Optical methods. Chromatographic methods. Biological methods. Sampling and preservation of samples. Characterisation of water: main parameters. UNIT 2: Determination of physical-chemical properties of water. Colour. Taste and smell. Solids. Conductivity. Temperature. Turbidity. Alcalinity and hardness. UNIT 3: Determination of organic matter in wastewaters: parameters and analytical methods Biological oxygen demand (BOD). Chemical oxygen demand (COD). Total organic carbon (TOC) UNIT 4: Specific analytical methods for important aqueous pollutants Nitrogenated species, metallic compounds, cyanides, phenols… UNIT 5: Biological analysis of water. Biodegradability and toxicity of wastewaters. Microbiological assays. Toxicity. Biodegradability of pollutants: respirometry. UNIT 6: Analysis of atmospheric pollutants. Polluted and non-polluted air. Pollutants. Effect of atmospheric contamination towards the environment. Diffusion and transport of pollutants. Sampling. Sulphur oxides. Carbon monoxide and dioxide. Nitrogen oxides. Ozone. Other inorganic pollutants. Hydrocarbons and other organic pollutants. Solid particles. UNIT 7: Contamination of soils. Different kinds of soils. Nutrients in solis. Interpretation of an analysis of a soil. Sampling. Conductivity and pH. C/N ratio and inorganic nitrogen. Phosphates. Potassium. Calcium and magnesium. Texture. Total nitrogen. Total organic carbon. Phosphor. Carbonate. Metals. Cations. Physical analysis of soils: humidity and particle size. 6. TEACHING-LEARNING METHODOLOGY CLASSROOM ACTIVITIES ACTIVITIES DESCRIPTION ECTS (hours) Theoretical clases Main contents are introduced by the professor 10 Practical classes and seminars Subjects are developed by presentation of real environmental problems 20 Laboratory classes Analysis of industrial efflents 30 ACTIVITIES AT HOME (AUTONOMOUS WORK) ACTIVITIES DESCRIPTION Theoretical study Preparation activities of Analysis of laboratory results ECTS (hours) The student reads the materials given by the professor 20 Computer and literature search 44 Treatment of data and explanation of the results obtained in the laboratory 20 7. EVALUATION The methodology employed in this subject is based in the active learning. Together with some “classical” sessions, the student is encouraged to work on selected parts of the program, and discuss about the results that are obtained. The global qualification of the subject is obtained from the evaluation of different factors: - Evaluation of the active work of the student (40%) - Tests carried out all along the course (30%) - Laboratory activities and practical work (30%) 8. BIBLIOGRAPHY Envirionmental Chemistry. 7th edition. S.E Manahan. Environmental Chemistry. 2nd edition. C. Baird. Standard Methods for the examination of water and wastewater. 20th edition. American Public Health Association, APHA, AWWA, WPCF.