A Perspective on Geotechnical Testing: The Details Matter John T. Germaine Massachusetts Institute of Technology Department of Civil and Environmental Engineering ASTM 2011 Workshop JTG.1 The Question How well are we doing as a profession with regards to the characterization of soils? ASTM 2011 Workshop JTG.2 Outline • Overview of soil testing industry • Establishing quality control • Some example industry data • • • • Specific gravity Shrinkage limit Compaction Hydraulic conductivity • Conclusions and recommendations ASTM 2011 Workshop JTG.3 Laboratory Testing Goals • Diversity in test type • Broad range of materials • Accurate results • Timely delivery • Profitability ASTM 2011 Workshop JTG.4 Testing Considerations • Test methods • Index Tests • Engineering Tests • No correct answer • Extreme variability of natural materials • Huge range in results • Quality control concerns ASTM 2011 Workshop JTG.5 Testing Organizations • Commercial companies • About 1200 • Commercial laboratories • In-house engineering consultants • Small independent laboratories • Government organizations • About 110 • Academic research laboratories • About 180 ASTM 2011 Workshop JTG.6 Distribution of Tests Laboratory B Laboratory A Total Index Strength Compaction Hydraulic Cond. Consolidation ASTM 2011 Workshop • • • • Laboratory C Laboratory D Very informal poll Three large commercial One in-house engineering Test numbers, not revenue JTG.7 Distribution Minus Index Laboratory A Compaction Hydraulic Cond. Consolidation Simple Strength Other Strength ASTM 2011 Workshop Laboratory B Laboratory C Laboratory D • Significantly different distributions • Large number of strength tests • In-house QC type testing JTG.8 Quality Control Tools • ISO Certification • Management, documentation and training • ASTM D3740 • Guidance for technical, documentation and training requirements • NICET • • • Certifies technician capabilties AMRL laboratory assessment • Certifies conformance to standard AMRL proficiency sample testing • Sends out uniform subsamples • Evaluates collective test results ASTM 2011 Workshop JTG.9 Documented Protocols • Facilitate communication • Product uniformity • Solidify professional practice • Expand domain of expertise • Formal Standards • ASTM • AASHTO • BS • In-house procedures • Improve product quality ASTM 2011 Workshop JTG.10 Quality of a Test Method • Precision and Bias • Bias: deviation relative to true value • Precision: variation for given test method • D18 standards have no Bias! • Quantities generally do not have a “correct” result • Use standard caveat statement in all standards ASTM 2011 Workshop JTG.11 Quantifying Precision • ASTM Standard E691 • Round Robin or Interlaboratory • Ruggedness testing • Impact of allowable variables • > 6 laboratories • Triplicate testing in each lab • Acceptable range • 2.8 x standard deviation • Repeatability for single operator • Reproducibility for between labs • Limited to independent observations ASTM 2011 Workshop JTG.12 l: Classification and Index • • • • • Simple equipment Considerable labor Technical skill and finesse Difficult to check results Rely on consistency and correlations ASTM 2011 Workshop JTG.13 Example: Specific Gravity Test • • • • • • AMRL proficiency program Method: ASTM D854 542 Laboratories Samples 157 and 158 Distributed uniform dry powder One test on each sample ASTM 2011 Workshop JTG.14 AMRL Sample Specifics • Sample 157 • • • • • • <200 < 2m Gs LL PI USCS 67 % 29 % 2.644 29 13 CL • Sample 158 • <200 • < 2m • Gs • LL • PI • USCS 62 % 27 % 2.645 28 13 CL 2008 Proficiency Testing Program ASTM 2011 Workshop JTG.15 Specific Gravity of Sample 157, (gm/cm3) Specific Gravity Results 3.2 3.0 2.8 2.6 2.4 2.2 2.0 2.0 2.2 2.4 2.6 2.8 3.0 3.2 • Huge range in results • Within laboratory correlation • Systematic error in procedure • 1995 study same variability Specific Gravity of Sample 158, (gm/cm3) ASTM 2011 Workshop JTG.16 Specific Gravity Results • Eliminate outliers • Wide distribution • Bias towards low values • Useful range 0.01 • ASTM 70 Number of Observations 60 50 40 Sample 157 Sample 158 30 20 10 0 2.50 2.55 2.60 2.65 Specific Gravity, (gm/cm3) 2.70 2.75 • Repeatability • 0.02 • Reproducibility • 0.06 ASTM 2011 Workshop JTG.17 Example: Shrinkage Limit Test • • • • • • • Comparison of Wax and Hg Method AMRL proficiency program Method: ASTM D4943 & D427 (old) About 50 Laboratories Samples 159 & 160 and 161 & 162 Distributed uniform dry powder One test on each sample ASTM 2011 Workshop JTG.18 AMRL Sample Specifics • Sample 159 / 160 – – – – – – <200 < 2m Gs LL PI USCS 89 / 83 % 39 / 37 % 2.704 / 2.699 43.0 / 43.2 20.8 / 20.9 CL • Sample 161 / 162 – – – – – – <200 < 2m Gs LL PI USCS 65 / 46 % 24 / 20 % 2.733 /2.694 24.8 / 23.7 10.2 / 10.1 CL 2009 & 2010 Proficiency Testing Program ASTM 2011 Workshop JTG.19 Shrinkage Limit: Wax Method • Huge range in results • Within laboratory correlation • Systematic error in procedure ASTM 2011 Workshop JTG.20 Shrinkage Limit: Wax Method • Wide distribution • Second year improvement • Distribution skewed to higher values ASTM 2011 Workshop JTG.21 Shrinkage Limit: Hg Method • About the same range as Wax method • Within laboratory correlation • Systematic error in procedure ASTM 2011 Workshop JTG.22 Shrinkage Limit: Hg Method • Clear difference between each year • Most labs in narrow range • Serious outliers ASTM 2011 Workshop JTG.23 Shrinkage Limit: Summary • Wax gives lower values • Wax method has more scatter • Average values capture subtle differences ASTM 2011 Workshop JTG.24 ll: Laboratory Compaction • Simple equipment • Calibration of automatic hammers • Energy transfer • Material processing very important • Technical skill • Interpretation of results ASTM 2011 Workshop JTG.25 Example: Standard Proctor • • • • • AMRL proficiency program Method: ASTM D698 Samples 157 and 158 963 Laboratories Report only wopt and gmax ASTM 2011 Workshop JTG.26 Compaction Results 158 Opt. Water Content, % 22 • Water Content 20 18 16 14 12 10 8 6 6 8 10 12 14 16 18 20 22 158 Max. Dry Unit Weight, lbf/ft3 157 Opt. Water Content, % • • • • Weak correlation Processing issues 157 higher Serious outliers 130 • Unit Weight 125 • Better correlation • Technique differences • 157 lower 120 115 110 105 100 100 105 110 115 120 157 Max. Dry Unit Weight, ASTM 2011 Workshop 125 130 lbf/ft3 JTG.27 Compaction Results Number of Observations 80 70 Sample 157 60 Sample 158 • Outliers Removed 50 40 • Water Content 30 20 10 0 9.0 9.5 10.0 10.5 11.0 11.5 12.0 12.5 13.0 Number of Observations Opt. Water Content, % • Broad distribution • Subtle difference 140 120 • Unit Weight Sample 157 100 Sample 158 • Narrow center band • Clear shift in average • Symmetrical tails 80 60 40 20 0 116 118 120 122 124 126 128 Max. Dry Unit Weight, lbf/ft3 ASTM 2011 Workshop JTG.28 Compaction Results • Considerable scatter • Clear outliers • No trend 130 Dry Unit Weight, lbf/ft3 125 120 115 110 158Measured Measureddata data 158 158 Measured data One lab with curve One curve Zerolabairwith voids 105 100 5 7 9 11 13 15 17 19 • Unlikely results • Impossible results Water Content, % ASTM 2011 Workshop JTG.29 Compaction Results • wopt =10.7 % • gmax =122.6 lbf/ft3 Dry Unit Weight, lbf/ft3 130 125 120 • Field specification • +/- 2 % wc 115 110 • 92 % R.C. 105 100 5 7 9 11 13 15 17 Water Content, % 19 • Field specification • Including 2 Std. Dev. AMRL Proficiency Sample 158 ASTM 2011 Workshop JTG.30 lll: Hydraulic Conductivity • • • • • • Widest range of any parameter Extreme equipment demands Little automation Expertise more than finesse Attention to detail QC equipment ASTM 2011 Workshop JTG.31 Example: Establishing Precision • • • • • • ASTM D5080 Craig Benson conducted study ISR ML, CL, and CH material Provided compacted test specimens 12 laboratories 3 tests per laboratory ASTM 2011 Workshop JTG.32 ISR Sample Specifics • ML Sample • CL Sample • CH Sample – <200 − − − − − − − − − − − − – – – – – 99 % < 2m 8% LL 27 PI 4 USCS ML Vicksburg silt <200 89 % < 2m 31 % LL 33 PI 14 USCS CL Annapolis clay ASTM ISR managed NSF, FHWA, and private sponsorship ASTM 2011 Workshop <200 96 % < 2m 46 % LL 60 PI 39 USCS CH Vicksburg clay 15,000 lbs of each soil Started 1993 7 Precision statements JTG.33 Hydraulic Conductivity, (cm/s) (10-6) Hydraulic Conductivity Results 3.0 • Variable Scatter with in labs Individual test ML Lab average Average +/- Std Dev Log Ave +/- Std Dev 2.5 2.0 • Two outlier labs 1.5 • Some labs very consistent 1.0 0.5 0.0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Laboratory Number ASTM 2011 Workshop • Log std. dev. fairly good JTG.34 Hydraulic Conductivity Results • ML (x10-6) 3.0 Individual test ML Lab average 2.5 Average +/- Std Dev Log Ave +/- Std Dev 2.0 natural Avg. • 1.2 S. D. • 0.8-1.6 Hydraulic Conductivity, cm/s 1.5 1.0 0.5 0.0 6.0 5.0 log 1.1 0.8-1.5 • CL (x10-8) 4.0 3.0 • 3.8 • 3.2-4.4 2.0 1.0 0.0 30 3.7 3.2-4.4 25 • CH (x10-9) 20 15 10 5 0 1 2 3 4 5 6 7 8 9 10 Laboratory Number ASTM 2011 Workshop 11 12 13 14 • 3.6 • <0-8.2 2.6 1.3-5.2 JTG.35 Hydraulic Conductivity Results Hydraulic Conductivity, (cm/s) 1.E-05 1.E-06 • Log provides better representation 1.E-07 • Equip. tuned to 10-7 1.E-08 • < one sign. digit 1.E-09 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Laboratory Number ASTM 2011 Workshop • Real problems for low permeability JTG.36 lV: Consolidation and Shear • • • • • • Significant advances in equipment Extensive automation Technical expertise Sample quality and handling Testing decisions based on soil behavior Essentially no precision data ASTM 2011 Workshop JTG.37 Conclusions • • • • • • QC tools are available Equipment adequate Too much scatter Causes of scatter are not obvious No data for consolidation or strength Substantial room for improvement ASTM 2011 Workshop JTG.38 Recommendations • • • • • • Formal protocols for every test Technician training Consistency evaluation of results Reference material testing In-house databases Participation in ASTM ASTM 2011 Workshop JTG.39 Acknowledgements • Friends associated with ASTM • Ron Holsinger; AMRL • Craig Benson; U of Wisconsin ASTM 2011 Workshop JTG.40