CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Course Information Sheet
Lecture
Room:
10:00 – 10:50 am MWF
CCIS L1-140
Dr. James Harynuk
Office Hours:
Chem W4-25A
492-8303
james.harynuk@ualberta.ca
Monday 1:00-2:30
Wednesday 1:00-2:30
or by appointment
Webpage: www.ualberta.ca/elearning
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Course Information Sheet
Labs
Dr. Greg Kiema
Chem W2–03A
gregory.kiema@ualberta.ca
Webpage:
http://www.chem.ualberta.ca/undergrad.html
then “Courses”
then “Chem 213”
Much of this info is/will be duplicated on the eClass site
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Course Information Sheet
Grading
Mid-term (in class Wed, Feb 29)
25%
Final (Monday, April 23 9:00 AM)
location TBD
37%
Laboratory
35%
Class/Laboratory Participation
3%
For some Participation points
Help Dr. Harynuk and the TAs get to know
you
Attach a photo of yourself to your Moodle
profile so that we can see who you are
when answering your questions
Please do this by January 20th
Analytical Chemistry seeks ever improved means
of measuring the chemical composition of natural
and artificial materials.
ACS
.
Instrumental Analysis
UV spectroscopy
IR spectroscopy
Raman spectroscopy
Flame atomic absorbance
Electrothermal AAS
Flame atomic emission
ICP-optical emission
ICP-Mass Spec
X-ray fluorescence
Fluorescence spectroscopy
Magnetic sector MS
Double focusing MS
Quadrupole MS
Ion trap MS
Time of flight MS
Electrospray MS
MALDI-TOFMS
Potentiometry
Coulometry
Voltammetry
Amperometry
Surface probe microscopy
Gas chromatography
HPLC
Ion chromatography
Capillary Electrophoresis
If you happened to have already
taken 313…
Why are you here???
You MAY NOT take this course for credit if you already
have credit for CHEM 313.
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Labs
Start Monday January 16
213 Lab Manual (2011-2012) (bookstore)
Lab notebook – black ‘Physics notes’ book
Safety glasses
Lab coat
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
How to do well in the 213 Lab ?
Read procedures BEFORE entering lab
Will preview labs in class (Hot Tips)
Hot Tip sheets are posted on Moodle
Talk to your friends
Take care in sample preparation
Take care in calculations/data handling
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Labs
Lockers 1 – 12 start with
Lockers 13 – 24
start with one of
Trace Iron by Spectrophotometry
Fluoride by Ion Selective Electrode
Benzene by Gas Chromatography
Nitroanilines Isomers by Liquid Chromatography
Sucrose and Glucose by Autoanalysis of Glucose
Quinine in Tonic Water by Fluorescence
Copper by Atomic Absorption Spectroscopy
Dextromethorphan in Cough Syrup by Solvent Extraction
Literature Search
Lab Notebook
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Lectures
Preview of Lab Experiments (5 lectures)
Ch. 4 Statistics (Sec. 4.7, 4.8)
Ch. 5 Calibration Methods (Sec. 5.3, 5.4)
Spectroscopy (12 lectures)
Ch. 18 Fundamentals of Spectrophotometry
Ch. 20 Spectrophotometers, UV-VIS, FTIR
Ch. 21 Atomic Spectroscopy
Midterm: (in class February 29)
25%
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Midterm
Based on:
lectures
suggested problems
assigned readings
experiments
Will include some:
Multiple choice/matching, Definitions, descriptions, diagrams,
calculations
~75% descriptive
~25% calculation
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Lectures (post midterm)
Separations
Ch. 23 Introduction to Analytical Separations
Ch. 24 Gas Chromatography
Ch. 25 High Performance Liquid Chromatography
Ch. 26 Other Chromatographic Methods
Mass Spectroscopy
Ch. 22 Mass spectrometry
Electrochemistry
Ch. 15 Potentiometry and Ion-Selective Electrodes (ISEs)
(Ch. 8 Activity)
Final (April 23, 9:00 AM, location TBD)
37%
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
Final
Semi-cumulative
~1/3 on material before midterm
~2/3 on material after midterm
Similar format to midterm
probably more choice and more calculations
CHEM 213 Quantitative Analysis II
Introduction to Instrumental Analysis
How to do well in 213 exams ?
• attend class
• read text
• do suggested problems
• will post answers for these problems
• do additional problems
• focus on descriptive
• ask questions
• online forum in Lecture section of course
website
Course Information Sheet
You have a set of handouts about academic integrity, plagiarism,
and ways to avoid plagiarism. It is understood that you will have
read them and be familiar with the Code of Student Behaviour.
This is your warning.
www.uofaweb.ualberta.ca/tie/