Cryogenic Yamamoto f2f (Aug2013)

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Report from sub-groups

Cryogenic

Kazuhiro Yamamoto

Institute for Cosmic Ray Research (ICRR) the University of Tokyo

KAGRA face to face meeting

University of Toyama, Toyama, Japan

1 August 2013

1

Contribution

R. Takahashi, K. Ono, T. Sekiguchi, Y. Sakakibara, C. Tokoku,

M. Kamiizumi, U. Iwasaki, E. Hirose, A. Khalaidovski, T. Uchiyama,

S. Miyoki, M. Ohashi, K. Kuroda, T. Akutsu A , H. Ishizaki A ,

F. E. Peña Arellano A , T. Suzuki B , N. Kimura B , S. Koike B , T. Kume B ,

K. Tsubono C , Y. Aso C , T. Ushiba C , K. Shibata C , D. Chen D , N. Ohmae E ,

K. Somiya F , R. DeSalvo G , E. Majorana H , L. Naticchioni H , W. Johnson I ,

A. Cumming J , R. Douglas J , K. Haughian J , I. Martin J , P. Murray J , S. Rowan J ,

G. Hofmann K , C. Schwarz K , D. Heinert K , R. Nawrodt K , S. Goto L , M. Tanaka L ,

S. Ioka M , K. Nakamoto M , H. Nezuka M , KAGRA collaboration

ICRR.UT, NAOJ A , KEK B , Phys.S.UT

C , Astro.S.UT

D , E.UT

E ,S.TIT

F ,

Sannio Univ.

G , INFN H , Louisiana State Univ.

I , University of Glasgow J ,

Friedrich-Schiller-Universitaet Jena K , Jecc Torisha L ,

Toshiba Keihin Product Operations M , KAGRA collaboration

2

0. Abstract

Although there are many topics , but here,

I will explain

(1)KAGRA cryostat

(2)Cryoduct

(2)1/4 cryostat

(3)Monolithic sapphire suspension

3

Contents

1. Introduction

2. KAGRA cryostat

3. Cryoduct

4. 1/4 cryostat

5. Sapphire suspension

6. Human resources

7. Summary

4

1. Introduction

Schematic view of KAGRA interferometer

Four mirrors of arm cavity will be cooled .

Mozumi

Y-end Sakonishi

X-end

Kamioka mine

(Underground site) Atotsu

Center

Vibration isolation system, Cryocooler unit, Cryostat,

Cryogenic payload

1. Introduction

Outline of vibration isolation and cryostat

14 m

Vibration

Isolation

Cryostat Cryogenic mirror

1. Introduction

Outline of cryostat to SAS

Cryogenic payload

Cryostat

Stainless steel t20mm

Diameter 2.6m

Height ~3.6m

M ~ 10 ton

Mirror

Cryo-coolers

Pulse tube, 60Hz

0.9 W at 4K (2nd)

36 W at 50K (1st)

S. Koike

4 Low vibration cryocooler unit

Remote valve unit

7

Outline of vibration isolation and cryostat Vacuum chamber

Inner shield

(300K)

(8K)

Outer shield

(80K)

Pulse tube cryocoolers

2 Pulse tube cryocoolers

Baffles Cryoduct

2 Pulse tube cryocoolers

Outline of vibration isolation and cryostat

Heat link (pure Al)

Pulse tube cryocoolers

Heat link (pure Al)

Pulse tube cryocoolers

Sapphire fiber

Sapphire mirror (About 20K)

Pulse tube cryocoolers

1. Introduction

Main topics

Experiment using KAGRA cryostat

Toshiba assembled four cryostats.

Cryoduct

Redution of 300K radiation propagation

1/4 cryostat

Performance test of cryogenic payload

Sapphire monolithic suspension

Key component of KAGRA

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2. KAGRA cryostat

KAGRA cryostats have already been assembled ! at Toshiba Keihin Product Operations

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2. KAGRA cryostat

Cooling test for all four KAGRA cryostats

January 2013 – April 2013

Three of them were move to a warehouse near

Kamioka on the 27 th and 28 th of July.

Cooling test for the 3rd cryostat

July 2013 – August 2013

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2. KAGRA cryostat

Three cryostats were move to a warehouse near

Kamioka on the 27 th and 28 th of July.

13

2. KAGRA cryostat

Three of cryostats were move to a warehouse near

Kamioka on the 27 th and 28 th of July.

14

2. KAGRA cryostat

Three of cryostats were move to a warehouse near

Kamioka on the 27 th and 28 th of July.

15

2. KAGRA cryostat

Cooling test of KAGRA cryostat in Toshiba

Test 1 : Initial cooling time of ratidation shield

How long does it take to cool shield ?

Test 2 : Heat load test

How much is temperature with extra heat load ?

C. Tokoku et al., Proceedings of CEC/ICMC 2013 (2EPoE1-03)

K. Yamamoto et al., Opening a new era for the astrophysics:

The future detectors of gravitational waves (19 April 2013) http://gwdoc.icrr.u-tokyo.ac.jp/cgibin/DocDB/ShowDocument?docid=1615

2. KAGRA cryostat

Cooling test of KAGRA cryostat in Toshiba

Test 1 : Initial cooling time

The result (2 weeks) is similar to our expectation .

There is no large unexpected heat invasion and resistance.

2. KAGRA cryostat

Experiments in cooling test of KAGRA cryostat

Experiment 1 : Initial cooling time of cryogenic payload

This initial cooling time should be short .

Yusuke Sakakibara will explain details later.

Experiment 2 : Measurement of shield vibration

This vibration causes motion of mirrors and scattered light noise .

Dan Chen will explain details later.

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3. Cryoduct

Two items for cryoduct

(1) 300K radiation though this cryo duct must be small .

(2) Scattered light noise by this duct should be small .

Not only scattered light itself but also vibration of cryo duct should be small.

Preparation for experiment is in progress .

Yusuke Sakakibara will explain details later.

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4. 1/4 cryostat

Cryogenic payload is not a simple system.

We need cryostat to test cryogenic payload performance.

KAGRA cryostat is not appropriate for test.

(1) Difficult access in mine

(2) Cleanness must be kept

1/4 cryostat will be prepared in Kashiwa campus .

1/4 means number of cryocooler, not size.

It will be delivered on the end of September .

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4. 1/4 cryostat

Construction is in progress (Jecc Torisha).

Vacuum chamber : 1.2 m in diameter, 1.6 m in height

Construction is in progress (Jecc Torisha).

Radiation shield

Construction is in progress (Jecc Torisha).

Support frame inside radiation shield

5. Sapphire suspension

Sapphire monolithic suspension

Sapphire mirror suspended by sapphire fibers.

Key component of KAGRA

We need

(a) Drilled sapphire mirror

(b)Sapphire fibers with nail heads

(c) Bonding between bulk and fibers

5. Sapphire suspension

Drilled sapphire bulk

We ordered Shinkosha ( test sample ).

It will be delivered on the 16 th of August.

KAGRA mirrors : 220 mm in diameter

5. Sapphire suspension

Drilled sapphire bulk

We ordered Shinkosha ( test sample ).

It will be delivered on the 16 th of August.

5. Sapphire suspension

Sapphire fibers with nail heads are necessary to suspend mirrors.

Test sample (T. Uchiyama)

5. Sapphire suspension

Sapphire fibers with nail heads

MolTech GmbH (Germany) and IMPEX HighTech

GmbH (Germany) have already delivered !

Although the size is similar to that of

KAGRA , quality check is necessary .

5. Sapphire suspension

Sapphire fibers with nail heads

Quality check under collaboration with ET ( ELiTES )

Q-value

Measurement in Glasgow , Jena , and Tokyo

Plan for measurement in Rome

Thermal conductivity

Measurement in Jena, Rome and Tokyo

Strength

Measurement preparation in Glasgow

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5. Sapphire suspension

Sapphire fibers with nail heads

Latest summary

Moltech IMPEX KAGRA requirement

Q-value 10 7 at 20K

Thermal

2*10 6 5*10

Conductivity 3000 5000 5000 at 20K [W/m/K] -10000

6

Although these results are promising , further investigation is necessary.

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5. Sapphire suspension

Bonding between sapphire fibers and sapphire mirror

Investigation of

Hydroxide Catalysis Bonding is in progress in Glasgow.

(Rebecca Douglas, GWADW2013).

Strength (about 60 MPa) measured by her is 10 times larger than those of previous papers.

T. Suzuki et al., Journal of Physics; Conference Series 32( 2006 )309.

A. Dari et al., Classical and Quantum Gravity 27( 2010 )045010.

Plan : Measurement of thermal resistance and so on.

5. Sapphire suspension

Assembled sapphire monolithic suspension

Performance of assembled monolithic sapphire pendulum must be checked .

Before that , sapphire bulk is suspended by sapphire fibers using indium as thermal and mechanical contact

(some kinds of “glue” instead of bonding) between sapphire bulk and fibers.

We will investigate performance and obtain expertise for the monolithic pendulum test as first step .

5. Sapphire suspension

Assembled sapphire monolithic suspension

A. Khalaidovski is designing the frame for this first step .

6. Human resources

Fresh persons

Dr. Aleksandr Khalaidovski from Hannover, June 2013-May 2014

Sapphire monolithic suspension

(Dr. Fabián Erasmo Peña Arellano from Birmingham, May 2013 – April 2016

Cryogenic sensor)

Dr. Rahul Kumar from Glasgow, October 2013 – September 2014

Simulation and development of payload

6. Human resources

ELiTES: ET-LCGT interferometric Telescope

Exchange of Scientists

Grant for collaboration about cryogenic between KAGRA and ET

European 7th Framework Programme

Marie Curie action (Mar. 2012 - Feb. 2016)

European people can visit Japan for KAGRA.

6. Human resources

Visitors supported by ELiTES in the last half year

Christian Schwarz, Gerd Hofmann, Ronny Nawrodt ( Jena )

Automatic systems to measure Q-values and thermal conductivity of sapphire fibers

Luca Naticchioni, Maurizio Perci, Ettore Majorana ( Rome )

Measurement of KAGRA radiation shield at cryogenic temperature

(Kieran Craig ( Glasgow )

Measurement of coating mechanical dissipation)

6. Human resources

Japanese graduate students visited (or will visit) Europe.

Yusuke Sakakibara (October 2012 – December 2012)

Investigation for coating and sapphire fibers

( Glasgow and Jena )

ET meeting, Hannover, December 2012 http://gwdoc.icrr.u-tokyo.ac.jp/cgi-bin/private/DocDB/ShowDocument?docid=1420 http://gwdoc.icrr.u-tokyo.ac.jp/cgi-bin/private/DocDB/ShowDocument?docid=1469

(Takanori Sekiguchi (January 2013 – March 2013)

Investigation for vibration isolation ( Amsterdam ) http://gwdoc.icrr.u-tokyo.ac.jp/cgi-bin/DocDB/ShowDocument?docid=1708

)

Dan Chen (September 2013 – October 2013)

Investigation for sapphire fiber ( Rome )

7. Summary

KAGRA cryostat

Three cryostats were transported to Kamika.

Test for KAGRA cryostat temselves

Experiment : Initial cooling time of payload

Radiation shield vibration

Yusuke Sakakibara and Dan Chen will explain details later.

Cryoduct

Preparation for experment

Yusuke Sakakibara will explain details later.

1/4 cryostat to check cryogenic payload will be delivered by the end of September .

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7. Summary

Sapphire monolithic suspension

Drilled bulk will be delivered on 16th of August .

Experiments for sapphire fiber and sapphire bonding are in progress but the results are promising .

We are preparing the first step experiment of monolithic sapphire suspension .

Human resources

Brilliant fresh persons

Strong support from ELiTES

Young Japanese researchers visit Europe.

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Thank you for your attention !

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7. For future

Some items for future research (not perfect list)

(a)Investigation material properties

(Q, thermal conductivity, strength etc.) of coating, fiber and so on.

(b)Sapphire bonding, Sapphire fiber clamp

(c)Control and damping scheme

Actuators and sensors at cryogenic temperature

(d) Mechanical and thermal simulation for payload

(e) Vertical spring in cryostat

(f) Reduction of initial cooling time

Thermal resistance of clamp ....

(g) Baffles for scattered light in radiation shield

(h) Assembly procedure

8. Summary

Cryostat : Assembly is in progress.

Cooling test is coming soon .

Cryogenic duct : Optimum position of 5 buffles

Cryocooler unit :

Future work : scattered light

Cooling test and vibration measurement : OK

Cryogenic payload

Preparation for 1/4 cryostat to check payload performance is in progress .

Current main R&D topics

Inital cooling time, Sapphire fiber with nail head,

Coating mechanical loss, Vibration of shield

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8. Summary

ELiTES has already started and supports the development of KAGRA cryogenic system .

If you want to join our mission, let us know.

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2. Issues

(1)How to assemble

Details of construction, clean room ….

(2)Strength

Tensile strength, development of clamp, sapphire bonding …

(3)Control and damping system to reduce fluctuation and instability

Actuators (what and where), resonant mode (frequency and Q) and so on

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2. Issues

(4)Cooling

Temperature of mirror (below 20 K), initial cooling time, heat resistance of clamp …

(5)Noise

Thermal noise, vibration via vibration isolation system and heat links …

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Cooling test in Toshiba

Test 2 : Heat load test

How much is temperature with extra heat load ?

We can derive extra heat load from temperature.

Examples for extra heat load

Scattered light by mirror

Heat absorption in mirror

300 K radiation through holes for main beam

Cooling test in Toshiba

Test 2 : Heat load test

Heater and thermometer

Pulse tube cryocoolers

Pulse tube cryocoolers

Sapphire mirror

Pulse tube cryocoolers

Cooling test in Toshiba

Test 2 : Heat load test

0 W

10 W

5 W

2 W

Scatted power is 5 W when scattered loss on the mirror surface is 10 ppm .

Cooling test in Toshiba

Test 2 : Heat load test

Heater and thermometer

Pulse tube cryocoolers

Pulse tube cryocoolers

Sapphire mirror

Pulse tube cryocoolers

Cooling test in Toshiba

Test 2 : Heat load test

0 W 10 W

4 W

According to our design, temperature should be below 8 K when heat absorption in mirror is 1 W .

2. 1/4 cryostat

Bid (for parts of 1/4 cryostat) was opened !

(Jecc Torisha)

Discussion for final design is in progress .

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4. Sapphire fibers

After Yusuke left …. Clamp for IMPEX fibers in Jena

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4. Sapphire fibers

Profile measurement in Glasgow

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5. Sapphire suspension

Sapphire fibers with nail heads

Q measurement in Jena

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5. Sapphire suspension

Sapphire fibers with nail heads

Thermal conductivity measurement in Jena

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5. Sapphire suspension

Sapphire fibers with nail heads

Latest summary

Crystal axis

Ribbon ?

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