3 Eddy Current NDE 3.1 Inspection Techniques 3.2 Instrumentation 3.3 Typical Applications 3.4 Special Example 3.1 Inspection Techniques Coil Configurations voltmeter voltmeter oscillator oscillator ~~ ~ excitation coil excitation coil voltmeter oscillator ~ Zo coil sensing coil testpiece Hall or GMR detector testpiece testpiece differential coils parallel coaxial rotated Remote-Field Eddy Current Inspection ferromagnetic pipe exciter coil Remote Field Near Field sensing coil Remote Field ln(Hz) low frequency operation (10-100 Hz) 1 f r 0 Exponentially decaying eddy currents propagating mainly on the outer surface cause a diffuse magnetic field that leaks both on the outside and the inside of the pipe. H z H z 0 e z / z Main Modes of Operation time-multiplexed multiple-frequency Signal Signal single-frequency Time Time frequency-multiplexed multiple-frequency Signal Signal pulsed Time Time D 2 excited signal (current) detected signal (voltage) Nonlinear Harmonic Analysis single frequency, linear response Signal ferromagnetic phase (ferrite, martensite, etc.) B Time nonlinear harmonic analysis Signal H Time 3.2 Eddy Current Instrumentation Single-Frequency Operation Vr low-pass filter A/D converter oscillator 90º phase shifter driver amplifier driver impedances + Vq low-pass filter Vm _ processor phase balance V-gain H-gain probe coil(s) Vm Vs cos(t s ), Vr Vo cos(t ), Vq Vo sin(t ) Vm Vr Vs cos(t s )Vo cos(t ) 1 Vs Vo cos(s ) cos(2t s ) 2 Vm Vq Vs cos(t s )Vo sin(t ) 1 Vs Vo sin(s ) sin(2t s ) 2 V Vm Vr o Vs cos(s ), 2 V Vm Vq o Vs sin(s ) 2 display Nonlinear Harmonic Operation Vr oscillator n divider 90º phase shifter driver amplifier driver impedances + Vq Vm _ low-pass filter A/D converter low-pass filter processor phase balance V-gain H-gain probe coil(s) Vm Vs1 cos(t s1) Vs2 cos(2t s2 ) Vs3 cos(3t s3) ... Vr Vo cos(nt ) V Vm Vr o Vsn cos(sn ) 2 Vq Vo sin(nt ) V Vm Vq o Vsn sin(sn ) 2 display Specialized versus General Purpose Nortec 2000S system Agilent 4294A system* frequency range* 0.1 – 10 MHz 0.1-80 MHz probe coil three pencil probes single spiral coil relative accuracy ≈ 0.1-0.2% ≈ 0.05-0.1% frequency scanning manual electronic measurement time ≈ 50 minutes for 21 points ≈ 3 minutes for 81 points *high-frequency application Probe Considerations sensitivity ferrite-core coil air-core coil high coupling low coupling high coupling high coupling flat air-core coil high coupling eddy current eddy current eddy current thermal stability I2 I1 I V ZI V Z i L* Rwire V1 V2 V1 Z11 Z12 V Z 2 12 Z 22 * Z12 i L12 11 12, 21 22 topology flexible, low self-capacitance, reproducible, interchangeable, economic, etc. I1 I 2 3.3 Eddy Current NDE Applications • conductivity measurement • permeability measurement • metal thickness measurement • coating thickness measurements • flaw detection 3.3.1 Conductivity Conductivity versus Probe Impedance constant frequency 1 Titanium, 6Al-4V Normalized Reactance 0.8 Inconel Stainless Steel, 304 0.6 Copper 70%, Nickel 30% 0.4 Lead Magnesium, A280 Nickel Aluminum, 7075-T6 0.2 Copper 0 0 0.1 0.2 0.3 Normalized Resistance 0.4 0.5 Conductivity versus Alloying and Temper IACS = International Annealed Copper Standard σIACS = 5.8107 Ω-1m-1 at 20 °C ρIACS = 1.724110-8 Ωm 60 Conductivity [% IACS] 2014 2024 6061 7075 50 T0 T0 T0 40 T0 T6 T73 T76 T72 T6 30 T6 T8 T4 T3 T4 T6 T3 T4 20 Various Aluminum Alloys Apparent Eddy Current Conductivity magnetic field probe coil specimen Normalized Reactance 1.0 0.8 lift-off curves 0.6 0.4 conductivity (frequency) curve 0.2 0 0 0.1 0.2 0.3 0.4 Normalized Resistance eddy currents • high accuracy ( 0.1 %) • controlled penetration depth Normalized Reactance 2 l=s 4 1 3 l=0 , l 2 1 Normalized Resistance 0.5 Lift-Off Curvature inductive (low frequency) lift-off ℓ =0 ℓ =s lift-off ℓ =0 σ2 σ2 conductivity σ σ1 “Vertical” Component. “Vertical” Component. ℓ =s capacitive (high frequency) conductivity σ σ1 “Horizontal” Component “Horizontal” Component Inductive Lift-Off Effect 4 mm diameter 8 mm diameter 2.0 2.0 1.5 %IACS 1.0 0.5 0.0 -0.5 -1.0 -0.5 -1.0 -2.0 100 0.1 80 80 70 70 60 60 AECL [μm] . . AECL [μm] . 0.0 -2.0 50 40 30 20 63.5 μm 50.8 μm 38.1 μm 25.4 μm 19.1 μm 12.7 μm 6.4 μm 0.0 μm 30 20 0 0 -10 -10 100 100 40 10 1 10 Frequency [MHz] 1 10 Frequency [MHz] 50 10 0.1 50.8 μm 38.1 μm 25.4 μm 19.1 μm 12.7 μm 6.4 μm 0.0 μm 0.5 -1.5 1 10 Frequency [MHz] 63.5 μm 1.0 -1.5 0.1 1.5 %IACS 1.5 Relative ΔAECC [%]. Relative ΔAECC [%] . 1.5 0.1 1 10 Frequency [MHz] 100 Instrument Calibration conductivity spectra comparison on IN718 specimens of different peening intensities 3.0 12A Nortec 8A Nortec 4A Nortec 12A Agilent 8A Agilent 4A Agilent 12A UniWest 8A UniWest 4A UniWest 12A Stanford 8A Stanford 4A Stanford 2.5 AECC Change [%] . 2.0 1.5 1.0 0.5 0.0 -0.5 0.1 1 10 100 Frequency [MHz] Nortec 2000S, Agilent 4294A, Stanford Research SR844, and UniWest US-450 3.3.2 Permeability Magnetic Susceptibility paramagnetic materials with small ferromagnetic phase content moderately high susceptibility low susceptibility 1.0 4 µr = 4 3 permeability 3 2 2 1 frequency (conductivity) 1 Normalized Reactance Normalized Reactance permeability 0.8 lift-off 0.6 frequency (conductivity) 0.4 0.2 0 0 0 0.2 0.4 0.6 0.8 1 Normalized Resistance 1.2 0 0.1 0.2 0.3 0.4 Normalized Resistance increasing magnetic susceptibility decreases the apparent eddy current conductivity (AECC) 0.5 Magnetic Susceptibility versus Cold Work cold work (plastic deformation at room temperature) causes martensitic (ferromagnetic) phase transformation in austenitic stainless steels Magnetic Susceptibility 101 SS304L SS302 SS304 100 10-1 10-2 SS305 10-3 IN718 IN625 IN276 10-4 0 10 20 30 Cold Work [%] 40 50 60 3.3.3 Metal Thickness Thickness versus Normalized Impedance scanning probe coil thickness loss due to corrosion, erosion, etc. 1 0.8 1 thinning 0.6 0.4 thick plate 0.2 f = 0.05 MHz f = 0.2 MHz f = 1 MHz 0.8 lift-off Re { F } Normalized Reactance aluminum (σ = 46 %IACS) 0.6 0.4 F ( x ) e x / e i x / 0.2 thin plate 0 -0.2 0 0 1 2 Depth [mm] 0 0.1 0.2 0.3 0.4 0.5 Normalized Resistance 0.6 3 Thickness Correction Vic-3D simulation, Inconel plates (σ = 1.33 %IACS) ao = 4.5 mm, ai = 2.25 mm, h = 2.25 mm Conductivity [%IACS] 1.4 1.3 thickness 1.0 mm 1.5 mm 2.0 mm 2.5 mm 3.0 mm 3.5 mm 4.0 mm 5.0 mm 6.0 mm 1.2 1.1 1.0 0.1 1 Frequency [MHz] 10 3.3.4 Coating Thickness Non-conducting Coating probe coil, ao non-conducting coating ℓ t d conducting substrate ao > t, d > δ, AECL = ℓ + t ao = 4 mm, simulated 63.5 μm 50.8 μm 38.1 μm 25.4 μm 19.1 μm 12.7 μm 6.4 μm 0 μm 1 10 100 Frequency [MHz] 80 70 60 50 40 30 20 10 0 -10 0.1 AECL [μm] lift-off: AECL [μm] 80 70 60 50 40 30 20 10 0 -10 0.1 ao = 4 mm, experimental 1 10 100 Frequency [MHz] Conducting Coating probe coil, ao conducting coating z = δe ℓ t Je d z conducting substrate (µs,σs) approximate: large transducer, weak perturbation equivalent depth: e s 2 1 AECC( f ) e 2 f s s 1 ( z ) AECC 4 z2 s s analytical: Fourier decomposition (Dodd and Deeds) numerical: finite element, finite difference, volume integral, etc. (Vic-3D, Opera 3D, etc.) Simplistic Inversion of AECC Spectra 0.254-mm-thick surface layer of 1% excess conductivity 1.2 uniform input profile 1 AECC Change [%] Conductivity Change [%] 1.2 0.8 0.6 inverted from AECC 0.4 0.2 1 0.8 0.6 0.4 0.2 0 0 -0.2 0.001 -0.2 0 0.2 0.4 0.6 0.8 1 Depth [mm] 10 1000 Frequency [MHz] 1.2 1.2 Gaussian input profile 1 AECC Change [%] Conductivity Change [%] 0.1 0.8 0.6 inverted from AECC 0.4 0.2 1 0.8 0.6 0.4 0.2 0 0 -0.2 0 0.2 0.4 0.6 Depth [mm] 0.8 1 -0.2 0.001 0.1 10 1000 Frequency [MHz] 3.3.5 Flaw Detection Impedance Diagram 1 Normalized Reactance 0.8 conductivity (frequency) lift-off 0.6 crack depth ω1 flawless material 0.4 ω2 0.2 0 0 0.1 0.2 0.3 0.4 Normalized Resistance apparent eddy current conductivity (AECC) decreases apparent eddy current lift-off (AECL) increases 0.5 Crack Contrast and Resolution Vic-3D simulation ao = 1 mm, ai = 0.75 mm, h = 1.5 mm probe coil austenitic stainless steel, σ = 2.5 %IACS, μr = 1 f = 5 MHz, δ 0.19 mm crack 1 -10% threshold Normalized AECC 0.8 0.6 0.4 0.2 detection threshold 0 0 semi-circular crack 1 2 3 Flaw Length [mm] 4 5 Eddy Current Images of Small Fatigue Cracks probe coil crack 0.5” 0.5”, 2 MHz, 0.060”-diameter coil Al2024, 0.025” crack Ti-6Al-4V, 0.026”-crack Crystallographic Texture J E generally anisotropic hexagonal (transversely isotropic) cubic (isotropic) 0 E1 J1 1 0 J 0 2 0 E2 2 J3 0 0 3 E3 0 E1 J1 1 0 J 0 0 E2 2 2 J3 0 0 2 E3 J1 1 0 0 E1 J 0 1 0 E2 2 J3 0 0 1 E3 x1 θ x3 σM σn σm basal plane x2 surface plane 1 2 σ1 conductivity normal to the basal plane n () 1 cos 2 2 sin 2 σ2 conductivity in the basal plane θ polar angle from the normal of the basal plane σm minimum conductivity in the surface plane σM maximum conductivity in the surface plane σa average conductivity in the surface plane m () 1 sin 2 2 cos 2 M 2 a () ½ [1 sin 2 2 (1 cos 2 )] Electric “Birefringence” Due to Texture 500 kHz, racetrack coil equiaxed GTD-111 1.05 1.40 1.04 1.38 Conductivity [%IACS] Conductivity [%IACS] highly textured Ti-6Al-4V plate 1.03 1.02 1.01 1.00 1.36 1.34 1.32 1.30 0 30 60 90 120 150 180 Azimuthal Angle [deg] 0 30 60 90 120 150 180 Azimuthal Angle [deg] Grain Noise in Ti-6Al-4V 1” 1”, 2 MHz, 0.060”-diameter coil as-received billet material solution treated and annealed heat-treated, coarse heat-treated, very coarse heat-treated, large colonies equiaxed beta annealed Eddy Current versus Acoustic Microscopy 1” 1”, coarse grained Ti-6Al-4V sample 5 MHz eddy current 40 MHz acoustic Inhomogeneity AECC Images of Waspaloy and IN100 Specimens inhomogeneous Waspaloy homogeneous IN100 4.2” 2.1”, 6 MHz 2.2” 1.1”, 6 MHz conductivity range 1.38-1.47 %IACS conductivity range 1.33-1.34 %IACS ±3 % relative variation ±0.4 % relative variation Conductivity Material Noise as-forged Waspaloy 1.50 1.48 1.46 AECC [%IACS] 1.44 1.42 1.40 1.38 1.36 Spot 1 (1.441 %IACS) 1.34 Spot 2 (1.428 %IACS) Spot 3 (1.395 %IACS) 1.32 Spot 4 (1.382% IACS) 1.30 0.1 1 Frequency [MHz] no (average) frequency dependence 10 Magnetic Susceptibility Material Noise 1” 1”, stainless steel 304 intact 0.51×0.26×0.03 mm3 edm notch f = 0.1 MHz, ΔAECC 6.4 % f = 0.1 MHz, ΔAECC 8.6 % f = 5 MHz, ΔAECC 0.8 % f = 5 MHz, ΔAECC 1.2 % 3.4 Special Example Residual Stress Assessment Alternating Stress [MPa] 1500 1000 with opposite residual stress service load 500 intact (no residual stress) natural life time 0 10 2 endurance limit increased life time 10 4 10 6 Fatigue Life [cycles] 108 Residual stresses have numerous origins that are highly variable. Residual stresses relax at service temperatures. Surface-Enhancement Techniques Laser Shock Peening (LSP) 200 50 0 40 Cold Work [%] Residual Stress [MPa] Shot Peening (SP) -200 -400 Ti-6Al-4V SP Almen 4A SP Almen 12A LSP LPB -600 -800 -1000 0 0.2 0.4 0.6 Depth [mm] Low-Plasticity Burnishing (LPB) Ti-6Al-4V SP Almen 4A SP Almen 12A LSP LPB 30 20 10 0 1.0 1.2 0 0.2 0.4 0.6 Depth [mm] 1.0 1.2 Piezoresistive Effect parallel, normal, circular F Electroelastic Tensor: 12 11 12 12 12 11 1 / E / E 2 3 / E Axial Stress [ksi] 1 / 0 11 / 2 0 12 3 / 0 12 Isotropic Plane-Stress ( 1 2 ip and 3 0 ) : a / 0 11 12 ip / E Adiabatic Electroelastic Coefficients: * 11 11 th * 12 12 th 80 60 40 20 0 -20 -40 Time [1 s/div] Conductivity [%IACS] ip F 1.403 1.402 1.401 1.4 1.399 1.398 1.397 IN 718, parallel Time [1 s/div] Material Types Al 2024 Ti-6Al-4V 0 0 parallel normal 0 -0.002 -0.002 -0.002 -0.004 -0.002 -0.004 -0.001 -0.004 -0.001 0 0.002 0.004 ua / E 0.002 0.004 parallel normal 0.002 / 0 0.004 0 0 0.001 0.002 ua / E IN718 Waspaloy / 0 0.002 / 0 0.002 0.004 parallel normal 0.004 parallel normal 0 0.002 parallel normal 0 -0.002 -0.002 -0.002 -0.004 -0.002 -0.004 -0.002 -0.004 -0.001 0 0.002 0.004 ua / E 0 0.002 0.004 ua / E 0 0.001 0.002 ua / E Copper / 0 / 0 0.002 0.004 parallel normal / 0 0.004 Al 7075 0 0.001 0.002 ua / E XRD and AECC Measurements Waspaloy 50 40 -500 Almen 4A Almen 8A Almen 12A Almen 16A -1000 -1500 30 Almen 4A Almen 8A Almen 12A Almen 16A 20 10 -2000 0 0 0.2 0.4 0.6 Depth [mm] 0.8 0 0.2 0.4 0.6 Depth [mm] Conductivity Change [%] Cold Work [%] -500 Almen 4A Almen 8A Almen 12A Almen 16A -1000 -1500 30 Almen 4A Almen 8A Almen 12A Almen 16A 20 10 0 -2000 0 0.2 0.4 0.6 Depth [mm] 0.8 Almen 4A Almen 8A Almen 12A Almen 16A 1 0 1 Frequency [MHz] 10 3 40 0 2 -1 0.1 0.8 50 500 Residual Stress [MPa] 3 Conductivity Change [%] 0 Cold Work [%] Residual Stress [MPa] 500 0 0.2 0.4 0.6 Depth [mm] 0.8 2 Almen 4A Almen 8A Almen 12A Almen 16A 1 0 -1 0.1 1 Frequency [MHz] before (solid circles) and after full relaxation for 24 hrs at 900 °C (empty circles) 10 Thermal Stress Relaxation in Waspaloy Waspaloy, Almen 8A, repeated 24-hour heat treatments at increasing temperatures Apparent Conductivity Change [% ] 0.6 intact 300 °C 350 °C 400 °C 450 °C 500 °C 550 °C 600 °C 650 °C 700 °C 750 °C 800 °C 850 °C 900 °C 0.5 0.4 0.3 0.2 0.1 0 0.1 0.16 0.25 0.4 0.63 1 1.6 2.5 4 6.3 Frequency [MHz] The excess apparent conductivity gradually vanishes during thermal relaxation! 10 XRD versus Eddy Current inversion of measured AECC in low-plasticity burnished Waspaloy 20 1.2 200 eddy current XRD 0 . . Residual Stress [MPa] 15 0.8 Cold Work [%] AECC Change [%] 1.0 0.6 0.4 0.2 10 5 0.0 -0.2 0.01 -200 -400 -600 -800 -1000 XRD eddy current -1200 0.1 1 Frequency [MHz] 10 0 0.0 -1400 0.5 1.0 Depth [mm] 1.5 0.0 0.5 1.0 Depth [mm] 1.5 XRD versus High-Frequency Eddy Current shot peened IN100 specimens of Almen 4A, 8A and 12A peening intensity levels 40 200 Almen 8A (XRD) . 30 0 -200 Almen 12A (XRD) Residual Stress [MPa] Cold Work [%] . Almen 4A (XRD) -400 20 10 -600 Almen 4A (AECC) -800 Almen 8A (AECC) -1000 Almen 12A (AECC) -1200 Almen 4A (XRD) -1400 Almen 8A (XRD) -1600 Almen 12A (XRD) -1800 0 0 0.1 0.2 0.3 0.4 Depth [mm] 0.5 0.6 0.7 0 0.1 50 MHz 0.2 0.3 0.4 Depth [mm] 0.5 0.6 0.7