Statistical Analysis Professor Lynne Stokes Department of Statistical Science Lecture 5 Complete Factorial Experiments, Completely Randomized Designs, Main Effects & Interactions 1 Complete Factorial Experiments All combinations of the factor levels appear in the design at least once Does not require that each combination occur an equal number of times Does not state what type of statistical design is being used “Factorial Design” is not a correct statistical term 2 Completely Randomized Design Randomize the sequence of test runs, assignment to experimental units Can be any type of complete or fractional factorial experiment 3 Randomization Inexpensive Insurance Bias due to changes in uncontrollable Factors or in experimental conditions Bias due to premature termination of the experiment Bias due to machine drift, fatigue, wear Validates key assumptions (Independence, Randomization Distributions) 4 Changes in Experimental Conditions : Oil Viscosity Tests Experiment : Two Oils One Test Run Per Day Six Test Runs Per Week Day 1 2 3 4 5 6 Average Week #1 56.4 (A) 44.7 (A) 67.5 (A) 76.6 (A) 71.3 (A) 72.8 (A) 64.9 Week #2 60.6 54.5 62.8 65.2 78.6 80.3 67.0 t-Test: averages are not significantly different (B) (B) (B) (B) (B) (B) 5 Changes in Experimental Conditions : Oil Viscosity Tests Environmental or equipment change between weeks : add 5 unit bias to all measurements in Week #2 Day 1 2 3 4 5 6 Average Week #1 56.4 (A) 44.7 (A) 67.5 (A) 76.6 (A) 71.3 (A) 72.8 (A) 64.9 Week #2 65.6 59.5 67.8 70.2 83.6 85.3 72.0 (B) (B) (B) (B) (B) (B) Average viscosity for Oil B is significantly greater than for Oil A 6 Changes in Experimental Conditions : Oil Viscosity Tests Randomize the test sequence, 3 oils each week, add 5 unit bias to all measurements in Week #2 Day 1 2 3 4 5 6 Average Week #1 80.3 (B) 67.5 (A) 56.4 (A) 54.5 (B) 76.6 (A) 78.6 (B) 67.4 Oil B - Oil A Original 2.1 Week #2 67.8 77.8 70.2 76.3 65.6 49.7 69.5 Biased 7.1 (B) (A) (B) (A) (B) (A) Randomized 2.1 7 Premature Termination : Oil Viscosity Tests Oil Type A B Lubricant #1 #2 #3 #4 #1 #2 #3 #4 Viscosity 54.6 54.3 44.7 47.0 67.5 67.2 76.6 77.4 60.6 Equipment Failure 8 Response Drift 50 Gallon Drum of Chemicals Background Noise Time Test Runs Figure 4.7 Influence of machine drift; test runs indicated by arrows. 9 Torque Study Goal : Investigate the effects of three factors on torque forces on rotating shafts Factor Shaft Alloy Sleeve Metal Lubricant Type Rotating Shaft Levels Steel, Aluminum Porous, Nonporous Lub 1, Lub 2, Lub 3, Lub 4 Stationary Sleeve Lay Out the Design MGH Figure 10 5.1 Construction of Completely Randomized Designs List the factor-level combinations All combinations, if complete factorial; only those to be tested, if a fractional factorial Include repeat tests, if any Number the combinations (including repeats) from 1 to N Obtain one or more random number sequences of numbers from 1 to N Randomize the test run sequence, if testing is performed sequentially (one after another) Randomize the assignment of factor-level combinations to experimental units, if any 11 Completely Randomized Design for Torque Study Combination 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Alloy Steel Steel Steel Steel Steel Steel Steel Steel Aluminum Aluminum Aluminum Aluminum Aluminum Aluminum Aluminum Aluminum Sleeve Porous Porous Porous Porous Nonporous Nonporous Nonporous Nonporous Porous Porous Porous Porous Nonporous Nonporous Nonporous Nonporous Lubricant Lub 1 Lub 2 Lub 3 Lub 4 Lub 1 Lub 2 Lub 3 Lub 4 Lub 1 Lub 2 Lub 3 Lub 4 Lub 1 Lub 2 Lub 3 Lub 4 Random Number Sequence : 8, 13, 4, 7, 5, 1, 11, 15 9, 3, 12, 10, 6, 14, 16, 2 MGH Table 5.1 12 Completely Randomized Design for Torque Study Run No. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Combination 8 13 4 7 5 1 11 15 9 3 12 10 6 14 16 2 Alloy Steel Aluminum Steel Steel Steel Steel Aluminum Aluminum Aluminum Steel Aluminum Aluminum Steel Aluminum Aluminum Steel Sleeve Nonporous Nonporous Porous Nonporous Nonporous Porous Porous Nonporous Porous Porous Porous Porous Nonporous Nonporous Nonporous Porous Repeats : Same Procedure Lubricant Lub 4 Lub 1 Lub 4 Lub 3 Lub 1 Lub 1 Lub 3 Lub 3 Lub 1 Lub 3 Lub 4 Lub 2 Lub 2 Lub 2 Lub 4 Lub 2 MGH Table 5.213 Completely Randomized Design for Torque Study cf. Table 5.3 CRD with 2 Repeats Combination 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 2 3 5 9 10 12 13 16 Alloy Steel Steel Steel Steel Steel Steel Steel Steel Aluminum Aluminum Aluminum Aluminum Aluminum Aluminum Aluminum Aluminum Steel Steel Steel Aluminum Aluminum Aluminum Aluminum Aluminum Sleeve Porous Porous Porous Porous Nonporous Nonporous Nonporous Nonporous Porous Porous Porous Porous Nonporous Nonporous Nonporous Nonporous Porous Porous Nonporous Porous Porous Porous Nonporous Nonporous Lubricant Lub 1 Lub 2 Lub 3 Lub 4 Lub 1 Lub 2 Lub 3 Lub 4 Lub 1 Lub 2 Lub 3 Lub 4 Lub 1 Lub 2 Lub 3 Lub 4 Lub 2 Lub 3 Lub 1 Lub 1 Lub 2 Lub 4 Lub 1 Lub 4 Randomly Selected Repeat Tests 14 Lubricant Deposit Study Lubricant Repeats 1 9 2 9 3 9 4 9 5 9 6 9 7 9 8 9 Overall Pooled Average Std. Dev. 24.89 20.11 78.11 37.96 64.94 23.95 72.50 29.15 88.61 29.46 78.94 26.48 61.94 12.95 51.50 33.52 65.18 27.68 15 ? What are the Main Factor Effects Notation (One-Factor Experiment) Factor Level Average 1 2 3 ... k Overall Average y1 y2 y3 ... yk y Data: yij i = Factor Level j = Repeat 16 Factor Main Effects Change in the average response due to changes in levels of one factor Factor Level 1 2 ... k Mean m1 m2 ... mk Average y1 y2 ... yk 17 Factor Main Effects Fixed Effects : Constant (mean) changes (Pre-selected levels, systematic changes) Random Effects : Random changes (Standard Deviation > 0) (Effects sampled from a probability distribution) 18 Factor Main Effects Models One factor model yij mi eij m a i eij Averages yi . mi ei . m a i ei . Cell Means Model Effects Model Assumption E(eij) = 0 Conventions mi = m + ai S ai = 0 19 Factor Main Effects Models Main Effects yi . - y j. mi - m j (ei . - e j.) a i - a j (ei . - e j.) yi . y.. mi m (ei . e.. ) a i (ei . e.. ) Note: mi = mj ai = aj Note: mi = m ai = 0 Main Effects Theoretical: changes in factor-level means Empirical : changes in factor-level averages 20 Pilot Plant Experiment 45 80 C2 Catalyst 52 83 54 68 C1 40 60 160 Concentration 72 Temperature 180 20 MGH Figure 5.3 21 Pilot Plant Experiment 45 80 C2 Catalyst 52 83 54 68 C1 40 60 160 Concentration 72 Temperature 180 20 22 Pilot Plant Experiment 45 80 C2 Catalyst 52 83 54 68 C1 40 60 160 Concentration 72 Temperature 180 20 23 Pilot Plant Experiment 45 80 C2 Catalyst 52 83 54 68 C1 40 60 160 Concentration 72 Temperature 180 20 24 Pilot Plant Experiment Main Effects Change in the average response due to changes in levels of one factor Temperature Concentration Catalyst Low 52.75 66.75 63.50 High 75.75 61.75 65.00 (High – Low) Main Effect 23.0 -5.0 1.5 Main effects do not measure joint factor effects Main effects are averaged across levels of the other factors 25 Interactions Effects of the levels of one factor on the response depend on the levels of one or more other factors 26 No Interaction Response Factor #2 Change in average response for factor #1 is constant for all levels of factor #2 Factor #1 27 Pilot Plant Experiment 45 52 62.5 Change with concentration roughly the same for each catalyst C2 Catalyst 67.5 54 80 83 68 61 C1 40 60 160 66 Temperature Concentration 72 180 20 28 Pilot Plant Experiment 45 80 C2 81.5 48.5 Catalyst Change with temperature greater for catalyst C2 than for catalyst C1 52 83 54 57 60 160 68 C1 40 70 Concentration 72 Temperature 180 20 29 Average Chemical Yield, Conditioned on Catalyst and Concentration (%). 160 165 C2 20 170 175 180 C2 40 80 Average yield (%) 70 60 50 C1 20 C1 40 80 70 60 50 160 165 170 175 180 Temperature (deg C) 30 Pilot Plant Experiment Interaction Plot No Interaction 75 70 Average Yield (%) Catalyst C2 65 60 Catalyst C1 55 50 20 40 Concentration (%) 31 MGH Figure 5.4 Pilot Plant Experiment Interaction Plot 80 Catalyst C2 Interaction 75 70 Average Yield (%) 65 Catalyst C1 60 55 50 160 180 Temperature (deg C) 32 MGH Figure 5.4 Cutting Tool Life 50 No Interaction 40 Tool Life (hrs) Tool Type B 30 } 20 10 Tool Type A 15 Hours 0 500 600 700 800 Lathe Speed (rpm) 900 1000 MGH Figure 5.2 33 Plasticity Study Purpose : Study “Plastic-Like” Properties of Friction-Reducing Lubricants and Additives Moveable Test Sample Stationary Platform Lubricant + Additive Responses: Plastic Viscosity Gel 34 Plasticity Experiment Design Factors Lubricant Additive Acme XLT, Monarch1, Standard None, 1%, 5% Design Factorial Experiment 2 Repeat Tests / Combination Completely Randomized Design 35 Factor Effects on Plastic Viscosity Effects of Lubricants Acme XLT - Standard : Monarch 1 - Standard : 6.22 - 4.81 = 1.41 4.79 - 4.81 = -0.02 Main Effects for Lubricants Effects of Additives 1% - None : 5% - None : Lubricant Acme XLT Monarch 1 Standard Average Average Viscosity 6.22 4.79 4.81 5.27 Main Effects for Additives 4.04 - 5.39 = -1.35 6.39 - 5.39 = 1.00 Main Effect 0.95 -0.48 -0.46 0.00 Additive None 1% 5% Average Viscosity 5.39 4.04 6.39 5.27 Main Effect 0.12 -1.23 1.12 0.00 36 Factor Effects on Plastic Viscosity Primary Conclusion Acme XLT has a greater mean plastic viscosity, especially with 5% concentration If Verified by statistical analysis Weak, if any, interaction effects Average Plastic Viscosity 8 Acme XLT 6 Monarch1 Standard 4 2 0 None 1% 5% 37 Additive Amount Factor Effects on Gel Effects of Lubricants Acme XLT - Standard : Monarch 1 - Standard : 11.45 - 10.01 = 1.44 10.10 - 10.01 = 0.09 Main Effects for Lubricants Effects of Additives 1% - None : 5% - None : 8.49 - 15.70 = -7.21 7.37 - 15.70 = -8.33 Main Effects for Additives 38 Factor Effects on Gel Primary Conclusion Acme XLT has a lower mean gel with no additive, greater with additives If verified by statistical analysis Strong Interaction Effects 20 Average Gel 15 Acme XLT 10 Monarch1 Standard 5 0 None 1% 5% 39 Additive Amount Completely Randomized Design for Torque Study Run No. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Alloy Steel Aluminum Steel Steel Steel Steel Aluminum Aluminum Aluminum Steel Aluminum Aluminum Steel Aluminum Aluminum Steel Sleeve Nonporous Nonporous Porous Nonporous Nonporous Porous Porous Nonporous Porous Porous Porous Porous Nonporous Nonporous Nonporous Porous Lubricant Lub 4 Lub 1 Lub 4 Lub 3 Lub 1 Lub 1 Lub 3 Lub 3 Lub 1 Lub 3 Lub 4 Lub 2 Lub 2 Lub 2 Lub 4 Lub 2 Average Torque 79.0 69.5 74.5 77.5 78.5 79.0 78.5 69.0 78.0 77.0 73.5 2.0 67.0 70.5 70.0 77.5 40 Interaction Effects : Torque Study Aluminum Shaft 85 Porous Sleeve 80 Average Torque (in-oz) 75 70 65 60 1 2 3 4 Lubricant Type 41 Interaction Effects : Torque Study Aluminum Shaft 85 Porous Sleeve 80 Average Torque (in-oz) 75 70 65 Nonporous Sleeve 60 1 2 3 4 Lubricant Type 42 Interaction Effects : Torque Study Average Torque (in-oz) Average Torque (in-oz) Aluminum Shaft 85 Steel Shaft 85 Porous Sleeve 80 75 75 70 70 65 Porous Sleeve 80 Nonporous Sleeve 60 65 Nonporous Sleeve 60 1 2 3 Lubricant Type 4 1 2 3 4 Lubricant Type 43 Interaction Effects Interaction effects cannot be properly evaluated if the design does not permit their estimation Complete factorials permit the evaluation of all main effects and all interaction effects 44