IMD series Iljin Metal bond Diamond ILJIN DIAMOND Co., Ltd. Diamond IMD series IMD-G IMD-F IMD-D Sawing of granite & ceramic tiles Core drill of glass Rough polishing of granite Crystal & glass decorating groove Reinforced glass edge Ferrite motor core CMP pad conditioner Silicon nitride OD grinding Middle stage grinding of Crystal & granite IMD-B Glass (Normal, TFT-LCD, Motor) edge Cut-off wheel for crystal or glass Final polishing of granite IMD-A Fired tungsten carbide Dental burrs Beveling of glass and mirror Cut-off wheel for glass & quartz Ferrite grinding Diamond Toughness Index 80 Toughness Index 70 60 G F 50 D 40 B 30 20 10 A TP IGD II 80/100 100/120 120/140 140/170 170/200 200/230 230/270 270/325 325/400 400/500 Mesh Size Diamond Grades equivalent IMD-G IMD-F IMD-D IMD-B IMD-A MBG-660 MBS-640 MBG-620 MBG-610 PDA-999 PDA-989 PDA-878 PDA-P768 Diamond Shape comparison As-grown Product IMD-TP Crushed Products IGD-II IGD-V Diamond Ti coating MESH Weight Percent Spec. 80/100 2wt% ±0.5 100/120 3wt% ±0.5 120/140 4wt% ±0.5 140/170 5wt% ±0.5 170/200 6wt% ±0.5 200/230 7wt% ±0.5 230/270 8wt% ±0.5 270/325 9wt% ±0.5 325/400 10wt% ±0.5 400/500 11wt% ±0.5 Diamond Ferrite Motor Core Grinding C Test Condition Area : Wheel Type : Bond : Workpiece Material : Mesh Size : Concentration : Peripheral Speed : DOC : Feed rate : Japan N/A Electroplated Ferrite motor core 100/120 N/A N/A N/A N/A A EA B 20000 IMD-F MBG-660 D Company 15000 10000 5000 0 A B C Diamond Glass Grinding Test Condition 15000 Area : Japan Wheel Type : N/A Bond Material : Bronze (Cu-Sn) Work piece Material : Glass Mesh Size : 170/200 Concentration : N/A Peripheral Speed : N/A DOC : N/A Feed rate : N/A IMD-F IMD-F Ti 9700 9500 5500 G-ratio Power Consumption Diamond Safety Glass Grinding Korea Industry Automotive Part Name Safety Glass Operation Glass Edge Grinding (Bando) Workpiece Material Glass Wheel Specific Metal Bond Φ200 x 4w x 75H x 11t Diamond & cBN IMD-F Ti (Ti Coating) Process Parameters Metal Bond Wheel Vs : 1600m/min Feed rate : 10~20m/min Results Part/hr (ea) Remark 250 14000 200 Wheel Life (m/wheel) Area 150 100 50 0 STD IMD-FTi 12000 10000 8000 6000 4000 2000 0 STD IMD-FTi Diamond Ti coated wheel grit ILJIN DIAMOND Co., Ltd. Grit Business Unit Diamond 1. 코팅 광학 형상 기존 IMD-Fti 170/200 신규 IMD-Fti 170/200 • 광학사진에서 기존 방식은 상당히 어두운 색을 띄고 표면이 거칠어 보임. • 신규 샘플은 기존 방식의 제품과 비교하여 광택을 띄고 표면이 매끄러움. Diamond 2. 코팅 SEM 형상 기존 IMD-Fti 170/200 신규 IMD-Fti 170/200 • 기존 제품은 edge가 벗겨지거나 코팅층이 불균일하게 형성되었음. • 신규 제품은 코팅층이 일관성있게 형성되어 있음. Diamond 2. 코팅 SEM 형상 기존 IMD-Fti 170/200 신규 sputtering IMD-Fti 170/200 • 고배율 관찰에서도 기존 제품에 비해 치밀한 코팅층을 유지하고 있고, edge부분도 손상이 없음. Diamond 3. TRS test result Kg/mm2 As-is New coating #1 1.72 1.32 #2 1.96 1.47 #3 1.75 1.43 #4 1.61 1.50 #5 1.66 1.60 Avg 1.74 1.46 2 Sintering Condition Bond system: 50%Cu-20%Sn30%Fe Sintering Temp: 700℃/2min TRS Test-Kgf/mm 3.0 1.74 Transverse Rupture Strength Test Dia grade/size: IMD-FTi 170/200 mesh Concentration: 100 Segment size: 6.4*6.4*40mm TRS M/C: ZWICK Z050 Test condition: ISO B Type 1.46 0 New coating As-is Diamond 4. 소결 후 본드와의 결합 상태 기존 IMD-Fti 170/200 신규 IMD-Fti 170/200 • SEM 관찰 시 신규 제품이 본드층과의 접합성이 기존 제품에 비해 우수한 것으로 관찰됨. Diamond 5. 소결 후 TIP 파단면 상태 New Coating As-is • SEM 관찰 결과 다이아몬드 표면은 모두 Ti 코팅층으로 형성되어 있음. • 기존 제품과 신규 제품과의 소결 후 탈락된 부분을 비교 관찰한 결과 신규 제품에 비해 기존 제품이 약 20% 가 탈락율 이 높은 것으로 분석됨. Diamond Diamond for CMP Pad conditioner ILJIN DIAMOND Co., Ltd. Diamond Trend of CMP Process Metal vs. Oxide CMP : Million $ CMP growth by material Metal CMP의 성장속도가 높으며, 이 중 Cu CMP의 성장율이 높음. Cu CMP에서 scratching issue 및 고집적화에 의한 diamond의 fine, narrow 경향 심화 Metal CMP에서 Diamond의 Shape, Narrow PSD, Diamond purity의 중요성이 강조 Diamond CMP Process Logic Memory Memory Semiconductor와 Logic 간에 가공하는 피삭재의 차이에 따라 적용되는 Diamond는 틀리게 적용 Diamond Tech. Trend of CMP Conditioner Typical Type of CMP Conditioner Sintering Electroplating Blazing Pattern, Narrow Size, Special Shape • CMP Conditioner에서 요구되는 Cutting Rate가 높아지고, 고 집적화 되면서 Diamond는 fine, narrow한 PSD가 요구됨. • Conditioning 효과를 높이기 위하여 pattern 및 diamond의 돌출높이는 높이기 위한 개발, 적용 진행 중 Diamond Tech. trend of diamond for CMP As was Coarse size 80/90 90/100 Blocky shape IMD – F,D PDA 999 MBG 660 As is Increased number of particles (High Density) Higher Cutting Rate (CR) Medium / fine size 100/120 140/170 170/200 200/230 Angular shape IMD – B,A,TP PDA 878 MBG 620 Diamond Special process for CMP only PSD Shape Impurity Special Treatment – I Special Treatment – II Narrow PSD (Double size → Single mesh → Micron size) Over size particle removing process (3 stage sieving at clean room) Precision heating control (HPHT) Perfect shape sorting and consistency Minimized metal inclusions using high magnetic field Suitable for electroplating and vacuum brazing process Removing the twin, sharp needles and weak crystal No damage of normal crystal’s sharp edge To prevent the Ni over plating and nodules on diamond crystal Perfectly clean and non electric conductivity on the surface of diamond De-magnetizing Diamond Pressure (GPa) Shape – HPHT technology 6.5 (100) (111)+(100) (111) 6.0 (110) 5.5 1300 1400 1500 Temp (0C) A B C D E F G H I Diamond Shape – HPHT technology IMD-F IMD-T Diamond Shape – Sorting technology IMD-G IMD-F IMD-D IMD-B IMD-A IMD-TP Diamond Special treatment I IMD-NB1 IMD-NA1 IMD-NB2 IMD-NA2 Diamond Special treatment II Diamond Special treatment II Metal impurities on the surface of diamond grit for CMP Element ILJIN 2hrs 4hrs DI 8hrs 2hrs (unit : ppb) E6 4hrs 8hrs 2hrs 4hrs 8hrs Li - - 0.00 0.01 0.01 0.01 0.00 0.01 0.01 Na 1.54 1.28 1.22 1.79 3.37 3.76 13.34 12.39 14.53 Mg 0.80 0.89 1.00 0.13 0.21 0.20 6.66 6.02 6.61 Al 0.42 0.39 0.47 0.34 0.64 0.61 0.33 0.43 0.50 K 0.04 - - 0.15 - - 2.17 2.25 2.36 Ca 1.22 1.83 1.94 1.47 2.01 2.12 55.72 54.72 58.23 Cr 0.12 0.36 0.35 0.35 4.71 4.58 0.52 9.80 10.52 Mn 0.21 0.27 0.25 0.10 0.41 0.44 0.07 1.14 1.42 Fe 7.25 23.02 30.47 5.19 31.41 44.57 14.38 97.34 135.27 Co - - - 0.01 0.03 0.04 0.01 0.13 0.15 Ni 1.08 4.30 6.82 1.39 5.79 9.25 4.78 20.64 31.59 Cu 0.92 0.93 0.83 1.96 2.23 2.39 0.28 0.38 0.44 Zn 0.80 1.10 1.29 0.67 0.90 1.15 0.52 1.36 1.92 As 0.01 0.01 0.01 - - - 0.01 0.02 0.02 Sr 0.03 0.03 0.03 0.01 0.03 0.03 0.17 0.18 0.18 Cd 0.01 0.01 0.00 0.00 0.00 0.01 0.00 0.05 0.02 Ba 0.03 0.03 0.03 0.01 0.04 0.05 1.05 1.17 1.20 Pb 0.81 0.77 0.69 0.06 0.13 0.14 0.35 0.43 0.48 Diamond Special treatment II Metal impurities on the surface of diamond grit ILJIN DI E6 150 135.27 100 58.23 (ppb) 50 44.57 31.59 30.47 14.53 10.52 10 9.25 6.82 4.58 3.76 2 1.94 2.39 2.12 1.22 0.83 0.35 0.44 0 Na Ca Cr Cu Fe Ni Diamond End of documents Thank you ! 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