Advanced UV System P-PTD120 1 Advanced UV System P-PTD 120 Peltier controlled optical transparent base plate Can be combined with Peltier hood (H-PTD 200) Temperature range 0 – 120°C Has a holder for a UV light guide underneath External UV-source can be connected P-PTD 120 / UV: Not just for UV-Curing ! Can be used for: Flow visualization and microscopy 2 Advanced UV System P-PTD 120 Features: Fast data acquisition with DSO Software controlled shutter Sample is protected against external light sources and day light Closed system, purging with inert gas possible Temperature calibration routine with certified temperature probe Sensitive normal force control (auto shrinkage compensation) Auto gap control (compensation for thermal expansion of geometries) Compliance correction UV curing in combination with fast, accurate and gradient reduced temperature control Perfect system for applications where the sample first is stabilized (Gel) with UV and then cured with temperature 3 Viscoelastic Behavior Time - dependent UV Curing coatings polymers UV – reactive resin, fast curing reaction 1010 rigid finally since G' > 1 GPa (already after t = 10 s) Pa 10 lg G' lg G'' 106 1 104 0.1 102 0.01 curing 0.01 0.1 1 time t 4 lg tan 10 s 100 MS - PP 08 g = 0.02 % ω = 63 rad/s ( = 10 Hz) tan = G'' / G' Viscoelastic Behavior Time - dependent UV Curing printing inks polymers 108 Pa UV printing ink at variable UV - intensities 106 lg G' curing process 104 I = 50 / 40 / 30 / 20 / 10 / 5 / 4 / 3 / 2 / 1 % 102 0 20 40 60 80 time t 5 100 120 s 140 Summary: Faster curing process with increasing UV light intensity I (here for I = 1 to 50%) Advanced UV System P-PTD 120 coatings curing G' > G'' UV resin 105 „soft touch“, since finally G' = 0.1 MPa gel point G' = G'' Pa 103 lg G' lg G'' 50 T 45 101 °C G'' > G' bottom: plate of quartz-glass 40 35 10-1 g = 0.1 %, ω = 10 rad/s, T = +23°C 0 400 800 time t 6 polymers 1200 1600 s 30 2000 temperature peak: end of the exothermic crosslinking reaction Advanced UV System P-PTD 120 Application: Flow Visualization I 7 Surfactant solution with air bubbles Advanced UV System P-PTD 120 Application: Flow Visualization II 8 Tooth Paste