Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, June 2004 / Copyright © 2004 Japan Concrete Institute 141 Invited Paper State-of-the-Art Report on Control of Cracking in Early Age Concrete Hirozo Mihashi1 and João Paulo de B. Leite2 Received 25 December 2003, revised 30 April 2004 Abstracts Durability of concrete structures is seriously compromised by cracking in early age concrete, particularly in high-strength or massive concrete structures. Since early age cracking is influenced by various highly interrelated factors that affect the hydration process and stress/strain development, its behavior is highly complex and no rational methodologies for its control have yet been established. On the other hand, demands for high strength and massive concrete structures in modern cities are ever growing, regardless of the many durability problems. More comprehensive methodologies for the control are therefore essential to ensure sustainability of such structures. This report reviews state-of-the-art research on mechanisms that cause complex cracking phenomena and newly developed methodologies to control early age cracking. 1. Introduction Cracking of concrete structures often seriously compromises not only structural integrity, but also durability and long-term service life. Early age cracking of concrete is a constant problem that arises from the fact that concrete interacts with its environment and experiences complex physical and chemical changes. Early age cracking has thus been subject of extensive research, yet due to the large number of contributing factors and the complex nature of the interacting phenomena, designers have purely relied on empirical rules based on well-confined and idealized assumptions for experimental conditions. In recent years, more realistic insights have been gained through various research efforts in related fields, as for example, on thermal cracking of concrete, including research on thermal cracking of early age concrete by a RILEM technical committee and on mass concrete by a Japan Concrete Institute (JCI) research committee. On the other hand, the ever-growing number of applications of high-strength concrete and massive concrete structures makes essential the establishment of comprehensive methodology to prevent cracking of early age concrete. Basically, concrete structures often present volumetrical changes particularly due to thermal and moisture related shrinkage. Volumetric instability is detrimental to performance and durability of concrete structures because structural elements are usually restrained. When the concrete is prevented from shrinking freely, tensile 1 Professor, Department of Architecture and Building Science, School of Engineering, Tohoku University, Japan. E-mail: mihashi@timos.str.archi.tohoku.ac.jp 2 Lecturer, Department of Architecture and Building Science, School of Engineering, Tohoku University, Japan. stresses are developed, which in combination with the low fracture resistance of concrete, often results in cracking. Given this, cracking control measures should be devised based on consideration of several factors including age-dependent material property development, free shrinkage and shrinkage rate, creep relaxation and degree of restraint, as well as external environmental conditions. Free-shrinkage measurements may provide useful information yet not sufficient to determine whether concrete will crack in service. On the other hand, constant refinements in restrained shrinkage testing techniques have revealed contradicting results when compared with existing data. Suitable evaluation and modeling of material properties and accurate numerical analysis techniques are necessary to be employed in combination with refined shrinkage testing techniques for solid understanding and effective control of early age cracking. Under these circumstances, a noticeable trend has been the reviewing of past research data to determine future paths of research. For example, the Japan Society of Civil Engineers (JSCE 2000) published a report entitled “Creep and Drying Shrinkage of Concrete II” and nearly at the same time the JCI (2001) published the “Report of Committee on Time-Dependent Deformation of Concrete Structures Due to Creep and Shrinkage”. The Architectural Institute of Japan (AIJ 2001) also published a “State-of-the-Art Report on Mass Concrete” as well as a revised version of “Recommendations for Practice of Crack Control in Reinforced Concrete Structures - Design and Construction (2002)”. The most recent publication by the AIJ (2003) on this subject is “Shrinkage Cracking in Reinforced Concrete Structures Mechanisms and Practice of Crack Control”. The RILEM has set a technical committee (TC 181-EAS) exclusively to deal with “Early Age Shrinkage and Cracking in Cementitious Materials” and hosted recently the International Conference on Early Age Cracking in Cementitious Systems (Kovler & Bentur 2001). Shortly before that, Tohoku University and JCI jointly organized 142 H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 2. Mechanisms driving cracking in early age concrete Stress which arises in early age concrete leading cracking is mainly associated to three types of deformation: autogenous shrinkage, induced by water absorption during hydration of cement particles, drying shrinkage, induced by evaporation of water along concrete curing and thermal shrinkage, owing to a poor dissipation of heat evolved by cement hydration and cooling of the hot concrete. The definition of autogenous shrinkage is still subject of debate, owing to the ambiguous understanding of the phenomenon. According to the JCI Committee on Autogenous Shrinkage of Concrete (JCI 2002), “autogenous shrinkage” is defined as a “reduction in the global volume of the cementitious material, caused by hydration of cement during and after the setting process” (Fig. 1). On the other hand, drying shrinkage is well accepted as being a volume deformation induced by evaporation of water from hardened concrete to the surrounding atmosphere. Considering the differences in shrinkage mechanism, high-strength concretes with low water-cement ratios (w/c) are prone to significant autogenous shrinkage, while ordinary concretes with high w/c are likely to incur in drying shrinkage. However, when water evaporates from the surface of early age concrete along desiccation during the hydration reaction process, it is impossible to separate drying shrinkage from autogenous shrinkage that may simultaneously occur. Autogenous shrinkage and drying shrinkage share similar characteristics in that they are volume reductions induced by decrease of relative humidity during concrete hardening, yet they are very different in timing of stress development, as well as in mechanisms as mentioned before. While autogenous shrinkage may occur from few hours after setting has started through several days until the hydration is completed, drying shrinkage may occur only after the surface is eventually exposed to environmental conditions, few days after setting starts, to the end of the curing process. Other important difference is that autogenous shrinkage is a uniform deformation with no in-plane strain gradient unless the hydration heat distributes non-homogenously inside the section or deformation is locally restrained. On the other hand, since drying shrinkage is induced by the loss of water inside concrete through the member surface, resulting in non-homogenously distribution of humidity within the member, strain gradients are always observed within the member sections (Fig. 2). As the surface dries and attempts to shrink, it is restrained by the core volume. Consequently, cracking caused by drying shrinkage initiates from the surface area. Then as the core volume dries, it undergoes shrinkage deformation, which when subjected to restraint, induces tensile stress leading to the development of cracks throughout the section. Note that initial cracking due to autogenous shrinkage may already exist. Around 5 to 10 hours after hydration starts, at the time when the concrete microstructure starts to form, autogenous shrinkage deformation, if free, increases as hydration further progresses. Yet if it is restrained, significant tensile stress may arise inducing cracking. Thermal shrinkage differs from the two former in the Drying (a) Water Water (b) Depth Autogeneous Subsidence shrinkage Bleeding chemical water shrinkage Pore tn 1.0 Cement (c) Setting (d) Depth Hydration products 0.0 Unrestrained deformations 0.0 Restrained deformations Cracks 0.0 Stress Hydration products Placing 0.5 Stress Cement Cement h Stress Water Depth Chemical shrinkage Hardening Fig. 1 Definition of autogeneous shrinkage (JCI 2002). hext=0.5 t1 Depth another conference to provide a forum of exchange of ideas particularly focused in controlling fracture mechanics of early age of concrete, the “International Workshop on Control of Cracking in Early Age Concrete” (Mihashi & Wittmann 2002). Meanwhile, the JCI Committee on Autogenous Shrinkage of Concrete completed its 2-year research project, begun in 2000, and published a comprehensive report on the latest findings (JCI 2002). This paper gives an overview, specifically from the mechanical aspect, of the status of current research on cracking of early age concrete and its control, topics that are drawing increasing attention as mentioned above. The objective is to provide experts with awareness of state-of-art research and advances fracture mechanics and control of cracking of early age concrete. Restrained deformations with crack formation Fig. 2 Stress distribution and crack formation in a drying concrete element (Martinola et al. 1998 © by Aedificat reprinted with permission). H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 fact that it is not related to moisture movements but with fluctuations in internal and external temperatures. Thermal shrinkage includes the effects of diurnal temperature changes (Mohamed & Hansen 1996), as well as the response of massive concrete structures to the heat generated during hydration (Springenschmid et al. 1985). As cement hydrates in an exothermic reaction, a large quantity of heat is generated. Dissipation of such heat in large structures is relatively slow. The excessive rise of heat accelerates the hydration process and causes the concrete set in an expansive condition. Then as the concrete cools, shrinkage occurs, which often leads to cracking. Recently, several works have focused on calculation of thermal stresses and their potential to induce cracking (Springenschmid 1995). In some cases of practice, concrete members are subjected to loading during early age, given rise to creep strains, which are gradual increase in strain over time under sustained loads. Creep in concrete differs from the creep observed in other structural materials in the fact that it occurs at room temperature. When the concrete member is restrained, the reverse phenomenon may be observed as stresses gradually relax. Stress relaxation not only occurs in the instance of external loading but also in the case of shrinkage stresses, adding further complexity to the matter. Note that while creep and relaxation are separated in conventional mechanics literature to properly distinguish stress and strain states, they are often used interchangeably to describe the same phenomenon in concrete literature, as they are viewed as same phenomenon. Hence early age cracking mechanism is a complex interplay among development or growth of strength, progress of autogenous and/or drying shrinkage, creep deformation and stress relaxation. When examining this mechanism, it is important to consider the strain component of each causal factor separately. Thus, the total strain at time t may be defined by equation (1) as proposed by the CEB-FIP (1991): εT (t ) = εelastic (t ) + εcreep (t ) + εshrinkage (t ) + εthermal (t ) (1) The sum of εelastic and εcreep represents the material’s mechanical response to stresses, i.e. stress dependent strains, while εshrinkage and εthermal are stress independent volumetric changes caused by moisture movements and thermal variations. Hence the stresses that cause cracking of early age concrete are, in case of absence of external loading, induced by restraint of deformations. There may be different types of restraints at work in structural concrete. Restraining may be imposed by alien bodies acting on the concrete material, such as reinforcing bars inside a member; by concrete joints connecting a member to an adjoining member with high stiffness; and even by the core concrete of a member when non-homogenous strain distributions are created internally according to the temperature and humidity distributions, as explained in the case of drying shrinkage. In practice, restraints are nearly always, and to a considerable extent, at work in 143 concrete structures, yet hardly detaining completely the movements of concrete members. Therefore, it is usually difficult but essential to evaluate the effective level of restraint, which depends on the ratio between the local stiffness of the concrete and that of the surrounding concrete or adjoining structural elements. According to the parametric studies by Weiss et al. (1999), reduction in the restraint level delays the crack initiation, suggesting that the restraint level λ is a key factor for predicting crack initiation in concrete. The latter study also draws attention to the influence of the shrinkage rate on the stress development and age of cracking. For high restraint levels, a faster shrinkage rate will result in earlier arising of cracks. On the other hand, when the restraint level is low, cracks develop slower as the shrinkage rate increases. This means that high restraint levels are more concerning in concrete with a low w/b, since the decrease in w/b accelerates the rate and intensity of autogenous shrinkage. 3. Material properties of early age concrete The accuracy of stress analysis of restrained shrinkage depends primarily on how the required mechanical properties are described. Most mechanical properties are rapidly changing at early age, particularly in the period when the concrete changes from liquid to solid state. The key mechanical properties required for analysis at early age are modulus of elasticity, tensile strength and those governing the viscoelastic behavior of the material. In principle, every material property contributing to the shrinkage behavior and early age cracking is dependent on the progress of cement hydration or the hydration product, and varies significantly according to concrete age, component materials, mixture proportions and curing environment. This section focuses on recent research findings with regard to the creep characteristics under tensile stress causing cracking, the unavoidable rise in hydration heat during the hydration process of high-strength concrete that undergoes especially significant autogenous shrinkage, and the linear expansion coefficient associated with thermal expansion accompanying the rise in hydration heat. 3.1 Elastic modulus and strength Around the time when a microstructure starts to form as the result of the cross-linking and consolidation of hydration products, yielded in accordance with the progress of the hydration reaction of cement particles, the early age concrete starts to gain strength and stiffness, which increase with time. Berggstrom et al. (1980) pointed out that at the age of 3 to 4 hours, concrete has very inelastic components even under low stress and most deformations are permanent. At the ages of 8 to 10 hours, it starts to develop clearly defined elastic and inelastic regions, and at the age of 14 to 18 hours, begins to show similar characteristics to those of hardened concrete. In particular, the elastic modulus of high-strength concrete 144 H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 tends to exhibit a high elastic modulus at an early stage as compared with normal-weight concrete, which is illustrated by the fact that the elastic modulus on the second day is approximately 80% or more of that at age of 28 days (JCI 2002). The rate at which a high elastic modulus is gained is higher than that of compressive strength development. Elastic modulus is usually measured based on the pattern of increase of strain versus stress, but according to Hagiwara et al. (2002), values of tensile elastic modulus are approximately 1.1 to 1.2 times greater than values of compressive elastic modulus. Fukasawa et al. (2002) demonstrated the influence of the hydration heat into the development of strength and elastic modulus, comparing potential estimators. In addition, drew attention to the fact that component materials may affect substantially the development of these mechanical properties. experimental data has been reported with regard to the linear expansion coefficient of early age concrete (AIJ 2003). Among various efforts to devise better measurement techniques, Yan et al. (2000) proposed a method for isolating the strain induced by temperature changes and managed to measure the linear expansion coefficient by keeping the specimen temperature within a low range between -1 and 5 degrees centigrade to restrain the progress of the hydration reaction and control autogenous shrinkage. Based also on other research findings, it gradually became clear that the linear expansion coefficient is usually larger for early age concrete than hardened concrete and that it is largely time-dependent (AIJ 2003). 3.2 Tensile creep characteristics The tensile creep and compressive creep of concrete had long been considered equal to each other. However, because tensile creep greatly affects the development of thermal and shrinkage cracks, an increasing amount of research has recently focused on this issue, and as a result, a number of enlightening experimental findings have been reported (JCI 2001, 2002, AIJ 2003). Iriya et al. (1998, 2002) reported that compressive creep is more prominent than tensile creep under same stress-strength ratio, and that the older the concrete at time of loading, the smaller the difference between the two creep types. According to Hagiwara et al. (2002), the specific tensile creep (creep strain per unit stress) is approximately 75% of the specific compressive creep, regardless of the age at which loading is applied or the loading duration. On the other hand, Yoshitake et al. (2000) performed creep tests under environment conditions in which the hydration reaction was restricted and reported that specific tensile creep was considerably larger than specific compressive creep. They pointed out that the progress of the hydration reaction had a great effect on tensile creep and on compressive creep, though there was clear difference between the two development mechanisms. However complex the phenomena may be, it is usually possible to identify the determining material properties through experiments, as long as they can be broken down into independent behaviors. Nonetheless, as mentioned earlier, hydration is a constantly progressing reaction accompanied by nonlinear temperature rises and thermal expansion, as well as the concurrent changes in microstructure and autogenous shrinkage behavior. All such processes occur simultaneous and are affected by diverse interacting factors. Hence, it seems hardly conceivable to solely rely on experiments to identify material time-depending properties of the early age concrete. The determining material properties can still be identified, though complex and highly nonlinear may be the phenomena, if carefully performed experiments are used in conjunction with appropriate analytical models. In recent years, remarkable progress on analytical models of hydration process has been achieved (Sakai & Daimon 1998). Analytical models for simulating the cement hydration process can broadly be classified into three categories according to the scale at which the hydration process is described (Mihashi 1998). The first type, categorized as a microscopic model, can simulate point by point the random hydration of each chemical component constituting the cement particles. The second type, referred to as meso-model, directly simulates the growth of cement particles as the hydration process evolves to form a skeleton (mesoscopic) structure of the hardened cement paste. The third type projects the influence of the hydration reaction onto the material variances of macroscopic element models without considering individual particle as explicit. This model is known as macro-model. Bentz et al. (1996) developed a method for directly representing the chemical components constituting the cement microstructure as image data and relating them to each image element, thereby simulating the random hydration reaction occurring at each image element point by point. Since this model allows study of the hydration process and the subsequent formation of microstructure 3.3 Linear expansion coefficient of early age concrete The linear expansion coefficient of concrete as in other solid materials is generally obtained from the temperature-strain relationship, which is derived from the measurement of changes in length brought about by temperature change. However, in the case of just-placed high-strength concrete, it is extremely difficult to isolate the temperature-strain relationship because, for example, temperature increases in accordance with the progress of the hydration reaction and is thus difficult to control, and autogenous shrinkage is induced as the microstructure is constantly changing in response to the progress of the hydration reaction. It was not until recently that reliable 4. Numerical models for simulation and analysis of creep and shrinkage behaviors 145 H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 in a very precise way, as well as representation of the growth behavior of void structures, the modeling results can also be used to simulate the strength development process and shrinkage. Breugel (1992) developed a meso-model for numerical analysis that directly represents the cement particles, considering the random distribution of particles of various sizes. Among the group of cement particles whose arrangements depend on the w/c and particle size distributions, Breugel isolated a unit space around a larger cement particle, which is the core of the hydration reaction. He considered that a hydration product is formed and expanded within the unit space, which then takes in smaller particles along with their hydration products, creates hydration clusters and consolidates them. The cross-linked particles represent the level of consolidation inside the cement paste, which has close correlation with the stress transfer mechanism, such as the development of strength and elastic moduli. Lokhorst & Breugel (1997) expanded this model to represent the change in the cement paste composition during the hydration process (Fig. 3) and managed to describe the behavior of early age creep. Later, Navi et al. (2002) further developed Breugel’s hydration model into a three-dimensional system to discuss void structures and stiffness changes, as well as the development of thermal stress and the potential risk of crack initiation in a manner that more closely reflects reality. Several rheological models can be cited as examples of macro-models, in which material properties influencing the creep behavior are associated to elastic (spring) and viscous (dashpot) elements placed together in a series and/or parallel coupling. In most cases, such models give a phenomenological description of the response of the concrete based on empirical analyses, but say nothing about the actual mechanism of creep. The age-dependent aspects of basic creep is mathematically handled by considering the material parameters involved in the creep model as empirical functions of the age. On the other hand, the experimental data on creep characteristics is substantially controversial and such predictive models may introduce substantial inaccuracies. Pioneering theories to model creep taking into account micromechanics of the solidifying process, associated to the 1-r r q p α + ∆α σ Burgers 1-p-q α cement hydration reaction, were independently proposed by Bažant (1977) and Kawasumi et al. (1982). Hence, it was obvious that the age-dependency of overall macroscopic creep was attributable to changes in the microstructure composition. Bažant & Prasannan (1989) succeeded later in simplifying the mathematical treatment of age effects on creep by considering the progress of hydration reaction not as a process of change in the material properties of hydration products themselves, but as a production/accumulation process of individual layer materials with age-independent characteristics. The basic hypothesis illustrated by this model is that the volume fractions of the volume dv(t) solidified at various times are all subjected to a same strain εv(t). The most significant advantage in this solidification theory is that load-bearing matter are age-independent. Adopting the concept of a unit element represented by the so-called Zener model, in which an elastic spring and the Voigt (Kelvin) model are connected in series, Mabrouk et al. (2002) proposed a parallel spring-dashpot model, where the number of unit elements is increased in accordance with the progress of hydration. The parameters of this dashpot were determined based on a pore structure that was presumed using the hydration reaction model by Maekawa et al. (1999). On the other hand, using Burger’s model, in which the Maxwell and Voigt models are connected in series, Nakamura et al. (2002) simulated the rapid change in material properties in accordance with the progress of the early-age hydration reaction, on the assumption that each parameter of the spring and dashpot elements changes with age. One of the special characteristics of this model is that it allows adjusting each model component’s function to the actual creep behavior of early age concrete (Fig. 4). In specific terms, Maxwell’s spring element and Maxwell’s dashpot element bear the reversible instant elastic deformation and irreversible delayed elastic deformation, respectively. The reversible delayed elastic deformation is born by the Voigt model, in which the spring and dashpot elements are connected in series. Thus, it is possible to quantify each model parameter by performing inverse-analysis on experimental results (Hagihara et al. 2002). Recent advances in restrained shrinkage testing has Unhydrated cement Cement gel Air + water Fig. 3 Meso-level modeling of cement hydration (Lokhorst and Breugel 1997 © by Elsevier - reprinted with permission). Maxwell εc εd α: constant Voigt εv t ε εd EV(t) EM(t) ηM(t) εv η V(t) Elastic Creep strain strain t0 εc t1 t Fig. 4 Schematic representation of Burgers model (Nakamura et al. 2002). 146 H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 made more fashionable to experimentally determine the effects on early age cracking behavior. Little work has been performed to theoretically predict the age at first cracking. Consideration is given here to some works as examples of different approaches. Gilbert (1992) used a strength-based approach along with the effect of continuous reinforcement to investigate the behavior of concrete containing steel reinforcement. Strength of materials approach has been widely used, but it has clear limitations since it cannot account for energy absorbing mechanisms such as fiber reinforcement. Several studies have been conducted to investigate shrinkage-cracking behavior using finite element modeling (Thelanderson et al. 1989, Wittman et al. 2002) to simulate the behavior of slabs and rings. Gryzbowski & Shah (1989) proposed a model based on damage mechanics and found a favorably comparison between the experiments behavior and the simulations. However, this approach relies on substantial information on material parameters and the implementation of the model is somehow cumbersome. Weiss et al. (1998, 1999) carried out a series of simulations of ring-type and slab-type specimens undergoing restrained shrinkage to evaluate the potential of cracking. A fracture mechanics approach was used to predict failure and the residual stresses were estimated using the following equation: ⎡ 1 φ(t , t ') ⎤ dε T (t , t ') = dσ (t ') ⎢ + ⎥ + dε shrinkage (t ') E ( t ') E28d ⎦ ⎣ (2) where dεT(t,t’) is the total differential strain at an age t, E(t’) is the elastic modulus and dσ(t’) is the acting stress at the time of loading t’, E28d is the elastic modulus at 28 days, ø(t, t’) is the creep coefficient, and dεshrinkage(t’) is the sum of autogenous shrinkage, drying shrinkage and thermal shrinkage at t’, assuming absence of restraint. Thereafter, assuming an effective restraint level λ, Equation (2) can be rearranged as follows. ⎡ 1 φ(t , t ') ⎤ d σ(t ') ⎢ + ⎥ = λ ⋅ d ε shrinkage (t ') E ( t ') E28d ⎦ ⎣ (3) with λ = ⎡⎣dε T (t , t ') − dε shrinkage (t ') ⎤⎦ / dε shrinkage (t ') (0≤λ≤1) concrete is extremely complex, it can be simulated by numerical analysis when its mechanism is described by a consistent analytical model and pertinent constitutive equations are established. Thus, simulating shrinkage behavior through numerical analysis is extremely important in that it can shed light on what factors have a more immediate impact on the development of shrinkage cracking and make it easier to develop fundamental crack control measures, providing that the analytical model properly represents the actual mechanism and that the material property values used in the analysis more or less represent reality. A flowchart outlining requirements for analysis of shrinkage-crack behavior of early age concrete is presented in Fig. 5. Noted that temperature effects are not included in the flowchart, and hence when analyzing concrete members in which the rise in hydration heat cannot be neglected, such as high-strength concrete members, the changes in temperature distributions and their effects must be introduced onto the material property under consideration (AIJ 2003). In analyzing the behavior of cracking induced by autogenous or drying shrinkage, it is necessary to calculate the stress at appropriate time intervals while judging whether the calculated stress satisfies the crack initiation or transmission conditions. However, to calculate such shrinkage stresses it is necessary primarily to quantitatively define the driving forces, which cause them. Hence as mentioned before, such stresses are resulting from the inhibition of free shrinkage deformation under certain restraining conditions working on the concrete member. On the other hand, shrinkage is induced by moisture gradients resulting by water movements towards the surface. Therefore, to calculate such stresses is necessary accurate knowledge of the moisture content acting at different times or the rate of moisture diffusion and moisture distribution along the concrete element. Wittmann et al. (2002) performed finite element analyses on drying shrinkage cracking of ring-restrained (4) Equation (3) above though relatively simples, casts perfectly the complexity of problems involved in shrinkage cracking of early-age concrete. 5. Analysis of shrinkage-cracking behavior of early age concrete Analytical models are essential to characterize the iteration between tensile creep and shrinkage, since a technique for direct experimental measurement is not yet available. Though the deformation behavior of early age Setting initial conditions Modeling of hydration reaction and microstructure. Clarification of boundary (restraint) conditions. Calculation of water content distributions inside the member section (Water movement analysis including self-desiccation) Non-linear water diffusion theory of porous media. Quantification of the relationship between water content and diffusion coefficient. Calculation of unrestrained shrinkage strain distributions inside the member section Quantification of the relationship between the shrinkage strain and water content Calculation of restrained shrinkage and stress distributions Tensile creep characteristics and elastic modulus of early age concrete Crack analysis Crack initiation-propagation conditions / tensile softening Fig. 5 Flowchart of numerical analysis of shrinkage cracking. 147 H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 Steel ring 508 mm Radial drying 1.0 Crack opening (mm) Diffusion coeff.(cm2/d) 11 mm Mortar 0.8 0.6 0.4 0.2 0 0.5 D=α0 •exp(b.h) D=α0/2•exp(b.h) D=α0/4•exp(b.h) 0.6 0.7 1.0 0.8 0.6 0.4 =α 0 20 0 (b ) .h 0 D= 0.2 0.9 1.0 0.8 D xp •e ex / 2• α0 α D= p( b .h /4 • 0 ex ) p(b 80 60 40 .h) 100 Humidity (-) Drying time (d) Fig. 7 Water diffusion and crack propagation (Wittmann et al. 2002). 46 mm α ( h) = d ε ∞ ( h) dh Figure 8 then shows that the drier the concrete, the larger the shrinkage strain. It also demonstrates, by referring to a maximum amplitude α0, that the peak value of the shrinkage strain coefficient α(h) exert substantial influence on shrinkage-cracking behavior. Finally, α(h) was set alternatively to two amplitude levels (α0 and α0/2) while the elastic modulus E was also varied at three different values (15, 25 and 35 GPa). It was reported that as the elastic modulus increased, easier the cracking occurred and also greater was the rate in which the crack width increased. This tendency even was more pronounced when α(h) was set to the lower amplitude α0/2. Furthermore, it was found that changing the crack resistance performance (tensile softening curve and fracture energy GF) delayed the development of visible cracking and restricted the tendency of the crack width to increase. In addition, it was demonstrated that for α(h) = α0/2, the development of visible cracking can be relatively controlled by increasing the GF value (Fig. 9). An important conclusion was drawn from the series of analyses using the fracture mechanics models, which showed that the tensile strength of concrete affected the development of microcracking cracking but had little impact on the subsequent increase in crack width, i.e. the development and growth of macrocracking cracking. An important finding derived from this analytical work is that retaining α=α0/2 1.5 1.0 0.5 0 0.4 0.6 0.8 0.6 0 2.0 0.8 0.4 α= α 2.5 /2 α=α 0 0.2 1.0 0 Humidity (-) α=α0/4 0 20 40 60 80 Drying time (d) 100 Fig. 8 Shrinkage coefficient and crack propagation (Wittmann et al. 2002). 5 4 3 (5) α=α0 Crack opening (mm) specimens (Fig. 6) to study the effect of material properties on the shrinkage behavior. First analyses to investigate the influence of the moisture diffusivity on the cracking development/growth showed that the diffusion coefficient of concrete plays an important role in the crack formation. Figure 7 shows that the faster is the rate of water evaporation from the concrete, earlier the crack initiates and larger becomes the crack width. Subsequently, the influence of the moisture-dependent coefficient of shrinkage α(h), given as a first derivative of the final curve with respect to the humidity potential h, was investigated with respect to the risk of cracking. 3.0 G 11 =350 N/m 2 G10=97.5 N/m 1 0 0 0.1 0.2 0.3 0.4 0.5 Crack opening (mm) Fig. 6 Specimen of the ring-restrained shrinkage cracking (Wittmann et al. 2002). Coeff. shrinkage (10 -3) 200 mm Crack opening (mm) 0.8 0.6 :α G 11 =α 0 G 10:α=α0/2 0.4 0.2 G11:α=α0/2 0 0 20 40 60 80 100 Drying time (d) Fig. 9 Strain softening and crack propagation (Wittmann et al. 2002). the rapid rate of water evaporation and associated shrinkage strain is the most efficient course for controlling shrinkage. This may be more effectively obtained if crack resistance performance is kept as high as possible and stiffness as low as possible. These insights provide many useful pointers regarding the technology of controlling shrinkage cracking in early age concrete (JCI 2002, AIJ 2003), as well as laid theoretical and analytical basis to support recently developed experimental research and optimize newly developed techniques. For example, shrinkage reducing agent and/or expansive additive can help restricting the growth of shrinkage strain and by adding wet lightweight aggregates to high-strength concrete the rate of water evaporation can be restricted (Schwesinger & Sickert 2002). Also, the inclusion of fibers in concrete can enhance crack resistance performance and assist to control growth and expansion of cracking (Paillère et al. 1989). 148 H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 Analytical methods are therefore essential to achieve optimum reduction of shrinkage rate by selecting mix parameters and contents/proportions, including types of cement, aggregates and admixtures, as well as to estimate effects of member size changes on shrinkage-cracking development and use of crack-inducing joints on the reduction of the restraint degree. 6. Recent developments on early age shrinkage crack testing Generally speaking, tests on early age concrete can be categorized into the following four types according to the purpose of testing (AIJ 2003): 1) tests to obtain physical property values; 2) tests to understand a behavior under the actual conditions of the structure/members tested; 3) tests to draw a relative comparison between characteristics and performance; and 4) tests for quality control and inspection. Hence, the test method that should be adopted when trying to control shrinkage cracking of early age concrete depends on the aim of the test. For the shrinkage cracking of concrete, the test method that is most widely used in Japan is the Test Method for Drying Shrinkage Cracking in Restrained Concrete, which has recently been designated as JIS-A-1151 according to the Japanese Industrial Standard (AIJ 2002). For the measurement of stress induced by volume changes as a result of autogenous shrinkage, a parameter required for the prediction of crack initiation in high-strength concrete, a revised test method, the Draft of Stress Test Method for Autogenous Shrinkage in Concrete (JCI 2002). These two methods are both uniaxial restraint type. The first method uses steel forms to give an external restraint to the concrete specimen (“form type”). On the other hand, the second method uses deformed bars embedded at the center of a concrete specimen to provide an internal restraint (“rebar type”). In the first method (form type), what is actually being measured is the average tensile stress working on the member section, because restraint stress is measured with a strain gauge attached to the parallel side of the restraint device. On the other hand, in the second method (rebar type), there is a difference between strain near the rebar at the center, to which a strain gauge is attached, and strain at the edge of the specimen. Therefore, a strain gradient is obviously created inside the section. Thus, evaluating the measured restraint stress based on rebar strain, as the average tensile stress working on the concrete would produce a major error (Nakamura et al. 2002). In either case, these testing methods are designed to draw a relative comparison of the crack resistance performance of concrete but not to obtain physical property values. As described before, the physical properties of a specimen undergo great changes with age in accordance with drying and hydration progress, and there are creep and relaxation deformations occurring at the same time. Thus, the restraint level changes over time and it is not possible to accurately evaluate restraint stress and shrinkage stress. The “Cracking Frame Method”, originally developed in Germany in the 1960s for thermal stress measurements, has been employed as method for controlling early age concrete cracking, particularly thermal cracking. In this apparatus, though stiff longitudinal bars at the side of the restraining frame separate the crossheads, the degree of restraint was still much lower than 100% restraint. The restraining force is measured by strain gauges attached to the frame. Also in Germany, Springenschmid et al. (1985) improved the frame to provide 100% restraint, for thermal crack control purposes. The new frame, as described in Fig. 10, has been named as “Temperature-Stress Testing Machine” (TSTM). In the new frame an actuator was attached to an adjustable crosshead to control the distance between gauge marks at the center of specimens having the same section to keep the distance constant (Springenschmid et al. 1994). The length measurements were performed using deformation transducers on carbon fiber bars at both sides. Elsewhere, other researchers have devised testing apparatus based on the frame with movable crossheads, specifically for early age concrete. Paillère et al. (1976, 1989) developed alternative solution to control the restraint level, by gripping the ends of the specimen inside of a restraint frame, with one movable end attached to a air pressure device. The cracking-test bench was laid horizontally for pouring the concrete and set vertically after the mould has been removed. Twin specimens were used, yet one of them was restrained and the other free to shrink. The idea behind this test setup was that the stress induced due to restrained deformation is recorded, while the strain in the other specimen undergoing free shrinkage is also measured. Hence, creep data can also be obtained when free shrinkage strain of a specimen having the same mixture proportions is recorded at the same time. A possible 8 6a 4 5 6b 2 9 7 3 1 6a 6b 7 Specimen: section 150x150, length 1500 mm Adjustable cross-head 3 Fixed cross-head 4 Stepping motor: accuracy of advancement 1µm 5 Load cell 6 a Measurement of cross-head movement 6 b Length measurement with carbon fiber bars 7 Formwork with heating/cooling system 8 PC for controlling and recording 9 Cryostat for heating/cooling of the formwork 1 2 Fig. 10 Outline of TSTM apparatus (Springenschmid et al. 1994). H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 Total strain Shrinkage+strain Elastic strain εthreshold Time (a) Total deformation of the specimen Stress Theoretical stress under permanent full restraint φσ i φσ 1 Incremental loading (b) Applied stress Time Fig. 11 Principle of the discretized restrained shrinkage test (Bissonnette et al. 2001. Reprinted with permission of The American Ceramic Society, www.ceramics.org. Copyright 2004. All rights reserved). Degree of restraint: 1.0 Stress (N/mm2) drawback in this test setup is the fact the test is carried at vertical position, which induces rupture in the upper part due to the influence of the self-weight of the specimen. Bloom & Bentur (1994) modified the test setup, in ways that allow the test was carried out in the horizontal position. The adjustable end was monitored by displacement gauge and periodically recovered by applied tensile load manually. Kovler (1994) developed a system with a closed-loop computer control, in order to improve accuracy of the measurements. As the shrinkage grows to a given strain level, the specimen is pulled by force so that the strain returns to zero (Fig. 11a). At each step when this is repeated, the stress needed for the forceful deformation is recorded and then plotted onto a time-stress correlation chart to obtain the history of shrinkage stress (Fig. 11b). Test methods as such, resetting strains to zero in stepwise manner, are sometimes referred to as “discretized restrained shrinkage” (DRS) testing (Bissonnette et al. 2001). Owing to such advances, valuable experimental data on the influence of component materials, mixture proportions and degrees of restraint on shrinkage stress have been made available. Figure 11 shows the basic concept of shrinkage strain control adopted for these testing methods. Figure 12 shows example of results of autogenous shrinkage testing on early age concrete using such type of 100% strain control technique. The tendency of shrinkage stress to increase is shown to be affected at considerable extent by the restraint level. In the case of conventional creep testing methods, creep strain is reported to reduce in accordance with the decrease in w/c. However, the DRS test has been reported to yield quite different results. In the DRS testing on early age concrete, it is the mechanism of relaxation, rather than that of creep, that is at work. It has nonetheless been pointed out by some researchers that it is necessary to study the creep 149 Degree of restraint: 0.5 Degree of restraint: 0.2 Ordinary portland cement Age (day) Fig. 12 Changes in shrinkage stress according to restraint revels (Mizobuchi et al. 2002). characteristics of early age concrete without being held captive by knowledge about concrete that has completed the hydration process, which has been accumulated through a vast amount of past research (Bissonnette et al. 2001). 7. Criteria of shrinkage-crack initiation Once shrinkage stress induced by the restraining effect of drying or autogenous shrinkage deformation has been predicted, appropriate criteria are necessary to judge whether the shrinkage stress will lead to crack initiation. Figure 5 outlines general requirements for criterion of crack initiation, yet no generally accepted criterion is currently available. Such a possibility is now within sight, however, due to advances in accuracy of evaluation techniques for physical properties, such as the development of TSTM and DRS testing, as well as analytical techniques for the behavior of highly non-linear shrinkage deformations. Two recently proposed alternative approaches for crack initiation criteria are worthy to be mentioned. Breugel & Lokhorst (2001) performed both shrinkage crack and direct tensile testing using the TSTM and reported that the tensile stress at time of crack initiation was approximately 75% of the splitting tensile strength, regardless of the differences between the two cement types used (four different mixture proportions) and also regardless of the degree of hydration of each concrete. They also reported that the uniaxial tensile strength of the rectangular column specimen employed in the tests was approximately 88% of the splitting tensile strength. Based on these results, and assuming both tensile strength and stress of a sample of shrinking specimens described by normal distributions, the variation coefficient V, which is the ratio of standard deviation σ to average value µ, is assumed to be 10% and 8% of the shrinkage stress and splitting tensile strength, respectively. Assuming R - S = Z, where R is the splitting tensile strength and S is the shrinkage stress, the probability of failure (cracking), Pf is given as follows. Pf {Z < 0} = Pf {−β} where β is the safety performance index given by (6) 150 (7) Hence, assuming maintenance of a reliability limit of 5% and imposing safety coefficient γ, defined as ratio between characteristic values of strength Rchar and stress Schar, often a standard procedure in engineering problems, the following equation is obtained: γ= Rchar µR − 1.64σ R (1 − 1.64VR ) µ R = = ⋅ µS + 1.64σ S (1 + 1.64VS ) µS Schar (8) Therefore, safety coefficient γ of early age concrete under tensile stress is given by γ= f char σ char = ( 0.75 f ctmspl 1 − 1.64V f σ (1 + 1.64Vσ ) ) 1.6 1.4 Coefficient of variation V V(σ)=10 % V(f ctm, spl)=8 % σ<η•fctm, spl γ (-) µz µ − µS = R σz σ R2 + σ S2 Safety factor (-) β= H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 1.2 1.0 0.8 0.6 10-1 10-2 10-3 10-4 10-5 Probability of fracture Pf (-) 0.3 0.4 0.5 0.6 0.7 0.8 Allowable stress /strength ratio η (-) Fig. 13 Design graph for the allowable stress/ strength ratio, safety factor and probability of fracture (Breugel et al. 2002). (9) where fctmspl is the average value of the splitting tensile strength and the value of 0.75fctmspl is assumed as strength criterion conforming above mentioned empirical observations that the average stress at the time of shrinkage-crack initiation is 75% of the splitting tensile strength. The term σ represents the average value of shrinkage stress. Thus the allowable stress ratio η, which corresponds to the safety coefficient γ, is given as follows. σ f ctmspl = 0.75 (1 − 1.64Vf ) (1 + 1.64Vσ ) γ (10) The diagrams in Fig. 13 represent the relationships between the safety coefficient γ, failure probability Pf and allowable stress ratio η. Such diagrams allow the determination of permissible stress ratio η corresponding to crack initiation probability Pf associated to the design requirement for the structure performance. Permissible η values may also be compared against the values of each part and member obtained through numerical analysis of shrinkage stress. If the value estimated in the analysis is greater than the permissible η value, the probability of crack initiation is higher than the pre-determined value and thus changes are necessary to reduce the risk of inducing shrinkage stress. Alternatively, using the aforementioned ring-restrained specimen (Fig. 6), Martinolla (2001) performed a parametric study and proved that crack initiation criteria could be represented by three-dimensional functions, the parameters being the shrinkage strain coefficient α(h), fracture energy GF and elastic modulus E (Fig. 14). Thus, performing tests in advance to obtain these three material properties of the concrete to be used makes it possible to evaluate the possibility of crack initiation. When the concrete is found to be in the crack initiation range, the material design need pertinent changes to make the material fall into non-cracking range (Fig. 15). Fig. 14 Risk of crack formation as a function of fracture energy, coefficient of shrinkage and Young's modulus (Wittmann et al. 2002). Mean coeffi. of shrinkage α (‰, 1/h) η= 2.8 2.4 Cracking 2.0 A1 1.6 1.2 Pa 5G 1 E = 25G Pa E= A3 = 35GPa E No cracking 0.4 1.0 0.8 0.4 0.2 0 0 1.2 0.6 A2 0.8 1.4 100 200 300 400 500 0 Fracture energy (N/m) Fig. 15 Crack control by materials design (Martinola 2001). H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 8. Smart materials for preventing shrinkage cracking Smart materials have been thoroughly developed in this decade in various fields including civil engineering. In a quite loose definition, smart materials are equipped with functions such as sensing (detecting presence of matter or problem), processing (judging which and/or when an action should be taken) and actuating (putting planned operations into action). According to such concepts, some concrete composites have been designed for self-controlling shrinkage problems and prevent cracking in early age concrete. An example of “smart” concrete was developed by Mihashi et al. (2002) for controlling the hydration heat, in order to prevent problems of thermal cracking (Fig. 16). Paraffin microcapsule containing a hydration retarder agent was mixed in the concrete composition. Once the temperature of concrete rises up to a certain value, which is specified by using types of paraffin with different melting temperatures, the microcapsules melt releasing the hydration retarder agent. Hence, the temperature of concrete may be controlled under the specified value and thermal stress may be neglected. The new material proved to be efficient in controlling the temperature under a certain level suitable for the steady hydration and to mitigate the rapid increase and decrease of temperature in concrete. Note that the outcome is quite different from techniques in which hydration retarder products are directly introduced in the mixture. In the latter though the hydration heat is reduced, depending on the size of the element, thermal gradients may still arise from the core to the surface. The results obtained in the experiments using former controlling technology large specimens prove that it can be applicable to practical uses in concrete technology. It was suggested also that if microcapsules made with different 1 Concrete Hydration Retarder Agent (HRA) Capsule Capsule detects hydration heat (Sensing) 2 Capsule melts at a designed temperature (Processing) 3 Capsule releases the HRA to delay hydration process (Actuating) Fig. 16 Schematic description of the smart concrete mechanism. 151 types of paraffin are blended, the melting temperatures may be varied to further moderate the increasing and decreasing rates of temperature. A study on the effects of using a cocktail of microcapsules with different melting temperatures is currently under development. Dhir et al. (1994) investigated the development of another new material also obtained through chemical intervention in the hydration process, which shows promising capabilities to control drying shrinkage. The concept involves tailoring the concrete composite by adding water-soluble chemicals during mixing to reduce water evaporation as the concrete is exposed to air-drying. In this way, the “self-curing” concrete would dispense any externally applied curing. The researchers tested six different chemicals, five of which were synthetic water-soluble polymers and one was a natural chemical and showed that some chemicals have a positive self-curing effect. The research was conducted on ordinary concrete; however, the concept may warrant further study to determine its applicability to HPC. Dhir et al. (1996) performed additional research on the influence of microstructure on the physical properties of self-curing concrete. Standard compressive tests as well as initial surface absorption tests (ISAT) were carried out on concrete specimens of the new material, whose results suggested the chemicals produce some alterations in the microstructure. Results revealed that the new material shows significant improvement in surface quality and compressive strength when compared with air-stored concrete. Although further investigation is required on the feasibility of formulating self-curing concrete, particularly as it relates to high-performance concrete, these studies appear to offer encouraging results. Another material tailoring technique that showed promising results to control autogenous shrinkage consists of the introduction of soaked lightweight aggregate to enhance the curing of high-strength concrete. Some research in Germany focused on the replacement of a portion of normal weight aggregate by lightweight aggregate to provide a supply of water within the concrete to sustain the curing process (Weber & Reinhardt 1996). This technique has proven to be effective in offsetting some of the effects of self-desiccation in low water-cement ratio concrete. The concept is relatively simple - to store water for curing inside the concrete by using lightweight aggregate with high moisture content. This research investigated the trade off between the benefits of additional moist curing versus the potential strength loss from using lightweight aggregate. The insensitivity of the high-strength concrete with lightweight aggregate to the type of curing was a significant benefit when compared with the concrete with normal weight aggregate. This can be attributed to the availability of internal moisture from the lightweight aggregate for the continuation of curing, which was independent of the external curing method. Within the lightweight aggregate concrete, curing can continue even after the surface becomes impervious, thus reducing the need for additional 152 H. Mihashi and J. P. de B. Leite / Journal of Advanced Concrete Technology Vol. 2, No. 2, 141-154, 2004 moist curing. Similar research was developed by Schwesinger & Sickert (2002) using a lightweight aggregate (Liapor 9.5) consisting of expanded clay with a spherical geometry and a pore volume of approximately 55 %. The spherical shape and the relatively dense outer shell of the lightweight aggregate make reliable its use for the production of High-Performance Concrete. Thus, the internal moisture conditions were able to reduce or eliminate autogenous shrinkage. 9. Concluding remarks As many complex and interacting factors affect shrinkage cracking of early age concrete, experiments used to yield contradicting results. Consequently, developing a crack control measure used not to be seen as feasible task. However, remarkable advances in research have gradually shed light on the dominant factors involved in these phenomena. It is now then possible to, at certain extent, properly evaluate the physical properties that determine the phenomena in question and predict shrinkage behavior by performing numerical analysis using the physical properties obtained. Further advances in research, as well as broad application and deployment of the findings to actual design and construction are in our doorstep. 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