Fractura y Falla. Introducción a la mecánica de fractura 1 FRACTURE • How do cracks that lead to failure form? • How is fracture resistance quantified? How do the fracture resistances of the different material classes compare? • How do we estimate the stress to fracture? • How do loading rate, loading history, and temperature affect the failure behavior of materials? Ship-cyclic loading from waves. Adapted from chapter-opening photograph, Chapter 8, Callister & Rethwisch 8e. (by Neil Boenzi, The New York Times.) Computer chip-cyclic thermal loading. Adapted from Fig. 22.30(b), Callister 7e. (Fig. 22.30(b) is courtesy of National Semiconductor Corporation.) Hip implant-cyclic loading from walking. Adapted from Fig. 22.26(b), Callister 7e. 3 Failure: Fracture, Fatigue and Creep Temperature, Stress, Cyclic and Loading Effect Ship-cyclic loading - waves and cargo. It is important to understand the mechanisms for failure, especially to prevent in-service failures via design. This can be accomplished via - Materials selection. - Processing (e.g. strengthening). - Design Safety. From Callister, photo Neal Noenzi (NYTimes) Objective: Understand how flaws in a material initiate failure. • describe crack propagation for ductile and brittle materials. • explain why brittle materials fail well below theoretical expectations. • define and use Fracture Toughness. • define fatigue and creep and specify conditions in which they are operative. • what is steady-state creep and fatigue lifetime? 5 Casting Porosity: Influence of Hot Isostatic Pressing 8 Fracture •Fracture: separation of a body into pieces due to stress, at temperatures below the melting point. Steps in fracture: crack formation crack propagation Depending on the ability of material to undergo plastic deformation before the fracture two fracture modes can be defined - ductile or brittle • Ductile fracture - most metals (not too cold): Extensive plastic deformation ahead of crack Crack is “stable”: resists further extension unless applied stress is increased • Brittle fracture - ceramics, ice, cold metals: Relatively little plastic deformation Crack is “unstable”: propagates rapidly without increase in applied stress Ductile fracture is preferred in most applications 9 Fracture mechanisms Ductile fracture • Accompanied by significant plastic deformation • Brittle fracture – Little or no plastic deformation – Catastrophic 10 Ductile vs Brittle Failure • Classification: Fracture behavior: Very Ductile Moderately Ductile Brittle Large Moderate Small Adapted from Fig. 8.1, Callister & Rethwisch 8e. %AR or %EL • Ductile fracture is usually more desirable than brittle fracture! Ductile: Warning before fracture Brittle: No warning 11 Example – Failure of a Pipe Ductile failure one piece large deformation Brittle failure many pieces small deformation Figures from V.J. Colangelo and F.A. Heiser, Analysis of Metallurgical Failures (2nd ed.), Fig. 4.1(a) and (b), p. 66 John Wiley and Sons, Inc., 1987. Used with permission. 12 13 Brittle vs. Ductile Fracture Brittle materials little plastic deformation and low energy absorption before fracture Ductile materials extensive plastic deformation and energy absorption (“toughness”) before fracture 14 Brittle vs. Ductile Fracture A. Very ductile Soft metals (e.g. Pb, Au) at room temperature, other metals, polymers, glasses at high temperature. B. Moderately ductile fracture typical for ductile metals C. Brittle fracture cold metals, ceramics. 15 Ductile Fracture Dislocation Mediated Necking Cavity Formation Crack propagation Cavity coalescence to form a crack Fracture 16 Moderately Ductile Failure Evolution to failure necking void nucleation void growth and linkage shearing at surface fracture Resulting fracture surfaces (steel) Particles serve as void nucleation sites. 50 mm From V.J. Colangelo and F.A. Heiser, Analysis of Metallurgical Failures (2nd ed.), Fig. 11.28, p. 294, John Wiley and Sons, Inc., 1987. (Orig. source: P. Thornton, J. Mater. Sci., Vol. 6, 1971, pp. 347-56.) 100 mm Fracture surface of tire cord wire loaded in tension. Courtesy of F. Roehrig, CC Technologies, Dublin, OH. Used with permission. 17 Ductile Fracture Cap-and-cone fracture in Al Scanning Electron Microscopy: Fractographic studies at high resolution. Spherical “dimples” correspond to micro-cavities that initiate crack formation. 18 Brittle Fracture (Limited Dislocation Mobility) No appreciable plastic deformation Crack propagation is very fast Crack propagates nearly perpendicular to the direction of the applied stress Crack often propagates by cleavage – breaking of atomic bonds along specific crystallographic planes (cleavage planes). Brittle fracture in a mild steel 19 Microstructural Features of Fracture in Metallic Materials Transgranular Meaning across the grains (e.g., a transgranular fracture would be fracture in which cracks would go through the grains). Intergranular In between grains or along the grain boundaries. Microvoids Development of small holes in a material. 20 Brittle Fracture A. Transgranular fracture: Fracture cracks pass through grains. Fracture surface have faceted texture because of different orientation of cleavage planes in grains. B. Intergranular fracture: Fracture crack propagation is along grain boundaries (grain boundaries are weakened or embrittled by impurities segregation etc.) 21 Transgranular Fracture 22 Intergranular Fracture 23 Brittle Fracture Surfaces (between grains) 304 S. Steel (metal) Intragranular, Transgranular (within grains) 304 S. Steel (metal) Al Oxide(ceramic) Reprinted w/ permission from "Failure Analysis of Brittle Materials", p. 78. Copyright 1990, The American Ceramic Society, Westerville, OH. (Micrograph by R.M. Gruver and H. Kirchner.) 3mm 1 mm 160mm Reprinted w/ permission from R.W. Hertzberg, "Defor-mation and Fracture Mechanics of Engineering Materials", (4th ed.) Fig. 7.35(d), p. 303, John Wiley and Sons, Inc., 1996. Intergranular Polypropylene (polymer) Reprinted w/permission from "Metals Handbook", 9th ed, Fig. 633, p. 650. Copyright 1985, ASM International, Materials Park, OH. (Micrograph by J.R. Keiser and A.R. Olsen, Oak Ridge National Lab.) 4 mm (Orig. source: K. Friedrick, Fracture 1977, Vol. 3, ICF4, Waterloo, CA, 1977, p. 1119.) 24 25 26 27 Fracture Mechanics Fracture mechanics The study of a material’s ability to withstand stress in the presence of a flaw. Fracture toughness The resistance of a material to failure in the presence of a flaw. 28 Ideal vs Real Materials • Stress-strain behavior (Room T): E/10 perfect mat’l-no flaws TSengineering << TS perfect carefully produced glass fiber E/100 typical ceramic 0.1 materials materials typical strengthened metal typical polymer e • DaVinci (500 yrs ago!) observed... -- the longer the wire, the smaller the load for failure. • Reasons: -- flaws cause premature failure. -- larger samples contain longer flaws! Reprinted w/ permission from R.W. Hertzberg, "Deformation and Fracture Mechanics of Engineering Materials", (4th ed.) Fig. 7.4. John Wiley and Sons, Inc., 1996. 29 Stress Concentration Figure by N. Bernstein & D. Hess, NRL Fracture strength of a brittle solid is related to the cohesive forces between atoms. One can estimate that the theoretical cohesive strength of a brittle material should be ~ E/10. But experimental fracture strength is normally E/100 - E/10,000. This much lower fracture strength is explained by the effect of stress concentration at microscopic flaws. The applied stress is amplified at the tips of micro-cracks, voids, notches, surface scratches, corners, etc. that are called stress raisers. The magnitude of this amplification depends on micro-crack orientations, geometry and dimensions. 30 Flaws are Stress Concentrators! Griffith Crack 1/ 2 a m 2o t t Kt o where t = radius of curvature o = applied stress m = stress at crack tip Adapted from Fig. 8.8(a), Callister & Rethwisch 8e. 31 Flaws and Fracture Actual fracture strength in most materials are significantly lower than expected from bond strengths. Flaw/cracks can amplify or concentrate stress! Max stress at the crack tip: For long microcracks: Stress concentration factor: Kt m a 2 o t Large Kt promotes failure Avoid sharp corners! Minimize crack size (a) and maximize radius of curvature (rt) if crack is unavoidable 32 Engineering Fracture Design • Avoid sharp corners! max Stress Conc. Factor, K t = 0 w max r, fillet radius 2.5 h Adapted from Fig. 8.2W(c), Callister 6e. (Fig. 8.2W(c) is from G.H. Neugebauer, Prod. Eng. (NY), Vol. 14, pp. 82-87 1943.) 2.0 increasing w/h 1.5 1.0 0 0.5 1.0 sharper fillet radius r/h 33 34 Crack Propagation Cracks having sharp tips propagate easier than cracks having blunt tips • A plastic material deforms at a crack tip, which “blunts” the crack. deformed region brittle ductile Energy balance on the crack • Elastic strain energy• energy stored in material as it is elastically deformed • this energy is released when the crack propagates • creation of new surfaces requires energy 35 Impact Testing • Impact loading: (Charpy) -- severe testing case -- makes material more brittle -- decreases toughness Adapted from Fig. 8.12(b), Callister & Rethwisch 8e. (Fig. 8.12(b) is adapted from H.W. Hayden, W.G. Moffatt, and J. Wulff, The Structure and Properties of Materials, Vol. III, Mechanical Behavior, John Wiley and Sons, Inc. (1965) p. 13.) final height initial height 36 Influence of Temperature on Impact Energy • Ductile-to-Brittle Transition Temperature (DBTT)... Impact Energy FCC metals (e.g., Cu, Ni) BCC metals (e.g., iron at T < 914ºC) polymers Brittle More Ductile High strength materials ( y > E/150) Temperature Ductile-to-brittle transition temperature Adapted from Fig. 8.15, Callister & Rethwisch 8e. 37 Criterion for Crack Propagation Crack propagates if crack-tip stress (m) exceeds a critical stress (c) 1/ 2 i.e., m > c 2E s c a where – E = modulus of elasticity – s = specific surface energy – a = one half length of internal crack For ductile materials => replace s with s + p where p is plastic deformation energy 38 Critical Stress for Crack Propagation Stress at which crack propagates E = elastic modulus gs = specific surface energy gp = plastic deformation energy i.e. For crack to propagate, enough stress must be applied to overcome energy needed to create surface and cause plastic deformation. Highly ductile Brittle 39 40 41 Fracture Toughness Measure of material’s resistance to brittle fracture. In the presence of a crack, it’s related to critical stress for crack propagation and depends on 1) material size & geometry, 2) crack dimension & orientation, 3) manner in which the load is applied. Gc = 2(gs+gp) Fast-Fracture Condition: K = c a0 EGc = constant!! Units of MPam “stress intensity Hard to measure factor” Internal flaws Measureable (fixed) materials properties • fast fracture will occur when (in a material subjected to stress (s) a crack reaches some critical size “a”; or, when a material contains cracks of size “a” is subjected to some critical stress s. • Point is that the critical combination of stress and crack length at which fast fracture occurs is a MATERIAL CONSTANT! Fracture Toughness: Kc Y c a Relates to how the load is applied, crack orientation etc. 42 Geometry, Load, & Material Condition for crack propagation: K ≥ Kc Stress Intensity Factor: Depends on load & geometry. Fracture Toughness: Depends on the material, temperature, environment, & rate of loading. Values of K for some standard loads & geometries: K 1.1 a K a Units of K: MPa(m)0.5 or ksi(in)0.5 a Adapted from Fig. 8.8, Callister 6e. 43 44 45 increasing Fracture Toughness Based on data in Table B5, Callister 6e. Composite reinforcement geometry is: f = fibers; sf = short fibers; w = whiskers; p = particles. Addition data as noted (vol. fraction of reinforcement): 1. (55vol%) ASM Handbook, Vol. 21, ASM Int., Materials Park, OH (2001) p. 606. 2. (55 vol%) Courtesy J. Cornie, MMC, Inc., Waltham, MA. 3. (30 vol%) P.F. Becher et al., Fracture Mechanics of Ceramics, Vol. 7, Plenum Press (1986). pp. 61-73. 4. Courtesy CoorsTek, Golden, CO. 5. (30 vol%) S.T. Buljan et al., "Development of Ceramic Matrix Composites for Application in Technology for Advanced Engines Program", ORNL/Sub/85-22011/2, ORNL, 1992. 6. (20vol%) F.D. Gace et al., Ceram. Eng. Sci. Proc., Vol. 7 (1986) pp. 978-82. 46 Impact Behavior Impact test Measures the ability of a material to absorb the sudden application of a load without breaking. Impact energy The energy required to fracture a standard specimen when the load is applied suddenly. Impact toughness Energy absorbed by a material, usually notched, during fracture, under the conditions of impact test. Fracture toughness The resistance of a material to failure in the presence of a flaw. 47 Properties Obtained from the Impact Test Ductile to brittle transition temperature (DBTT) The temperature below which a material behaves in a brittle manner in an impact test. Notch sensitivity Measures the effect of a notch, scratch, or other imperfection on a material’s properties, such as toughness or fatigue life. 48 (c)2003 Brooks/Cole, a division of Thomson Learning, Inc. Thomson Learning ™ is a trademark used herein under license. Ductile to Brittle Transition Temperature Results from a series of Izod impact tests for a super-tough nylon thermoplastic polymer 49 Ductile to Brittle Transition As temperature decreases a ductile material can become brittle-ductile-to-brittle transition. Alloying usually increases the ductile-to-brittle transition temperature. FCC metals remain ductile down to very low temperatures. For ceramics, this type of transition occurs at much higher temperatures than for metals. The ductile-to-brittle transition can be measured by impact testing: the impact energy needed for fracture drops suddenly over a relatively narrow temperature range – temperature of the ductile-to-brittle transition. 50 Effects of Temperature Increasing temperature increases %EL and Kc Adapted from C. Barrett, W. Nix, and A.Tetelman, The Principles of Engineering Materials, Fig. 6-21, p. 220, Prentice-Hall, 1973. Electronically reproduced by permission of Pearson Education, Inc., Upper Saddle River, New Jersey. 1551 (c)2003 Brooks/Cole, a division of Thomson Learning, Inc. Thomson Learning ™ is a trademark used herein under license. Charpy V-Notch Properties The Charpy V-notch properties for a BCC carbon steel and a FCC stainless steel. The FCC crystal structure typically leads top higher absorbed energies and no transition temperature 52 53 Famous example failures: Liberty ships USS Esso Manhattan, 3/29/43 Fracture at entrance to NY harbor. John P. Gaines, 11/43 Vessel broke in two off the Aleutians (10 killed). http://www.uh.edu/liberty/photos/liberty_summary.html USS Schenectady, 1/16/43 Liberty tanker split in two while moored in calm water at the outfitting dock at Swan Island, OR. Coast Guard Report: USS Schenectady Without warning and with a report which was heard for at least a mile, the deck and sides of the vessel fractured just aft of the bridge superstructure. The fracture extended almost instantaneously to the turn of the bilge port and starboard. The deck side shell, longitudinal bulkhead and bottom girders fractured. Only the bottom plating held. The vessel jack-knifed and the center portion rose so that no water entered. The bow and stern settled into the silt of the river bottom. The ship was 24 hours old. Official CG Report attributed fracture to welds in critical seams that “were found to be defective”. Adapted from D. Johnson 54 Design Strategy: Stay above the DBTT! Pre-WWII: The Titanic Reprinted w/ permission from R.W. Hertzberg, "Deformation and Fracture Mechanics of Engineering Materials", (4th ed.) Fig. 7.1(a), p. 262, John Wiley and Sons, Inc., 1996. (Orig. source: Dr. Robert D. Ballard, The Discovery of the Titanic.) WWII: Liberty ships Reprinted w/ permission from R.W. Hertzberg, "Deformation and Fracture Mechanics of Engineering Materials", (4th ed.) Fig. 7.1(b), p. 262, John Wiley and Sons, Inc., 1996. (Orig. source: Earl R. Parker, "Behavior of Engineering Structures", Nat. Acad. Sci., Nat. Res. Council, John Wiley and Sons, Inc., NY, 1957.) Problem: Used a type of steel with a DBTT ~ Room temp. 1655 The Importance of Fracture Mechanics Selection of a Material Design of a Component Design of a Manufacturing or Testing Method Griffith flaw - A crack or flaw in a material that concentrates and magnifies the applied stress. 56 Homework 57 Fatigue (Failure under fluctuating / cyclic stresses) Under fluctuating / cyclic stresses, failure can occur at loads considerably lower than tensile or yield strengths of material under a static load: Fatigue Estimated to causes 90% of all failures of metallic structures (bridges, aircraft, machine components, etc.) Fatigue failure is brittle-like (relatively little plastic deformation) - even in normally ductile materials. Thus sudden and catastrophic! Applied stresses causing fatigue may be axial (tension or compression), flextural (bending) or torsional (twisting). Fatigue failure proceeds in three distinct stages: crack initiation in the areas of stress concentration (near stress raisers), incremental crack propagation, final catastrophic failure. 58 Fatigue: S-N curves (stress-number of cycles to failure) Fatigue properties of a material (S-N curves) are tested in rotating-bending tests in fatigue testing apparatus: Result is commonly plotted as S (stress) vs. N (number of cycles to failure) Low cycle fatigue: high loads, plastic and elastic deformation High cycle fatigue: low loads, elastic deformation (N >105) 59 FATIGUE TEST METHODOLOGIES Fatigue Fatigue = failure under cyclic stress. specimen bearing compression on top bearing motor counter flex coupling tension on bottom Adapted from Fig. 8.16, Callister 6e. (Fig. 8.16 is from Materials Science in Engineering, 4/E by Carl. A. Keyser, Pearson Education, Inc., Upper Saddle River, NJ.) Stress varies with time. key parameters are S and sm Key points: Fatigue... can cause part failure, even though smax < sc. causes ~ 90% of mechanical engineering failures. 1761 Cyclic Stress and Strain Fatigue Results of the Fatigue Test Endurance limit - An older concept that defined a stress below which a material will not fail in a fatigue test. Fatigue life - The number of cycles permitted at a particular stress before a material fails by fatigue. Fatigue strength - The stress required to cause failure by fatigue in a given number of cycles, such as 500 million cycles. Notch sensitivity - Measures the effect of a notch, scratch, or other imperfection on a material’s properties, such as toughness or fatigue life. 63 Fatigue: Cyclic Stresses Periodic and symmetrical about zero stress Periodic and asymmetrical about zero stress Random stress fluctuations 64 Fatigue: Cyclic Stresses Cyclic stresses are characterized by maximum, minimum and mean stress, the range of stress, the stress amplitude, and the stress ratio Remember the convention that tensile stresses are positive, compressive stresses are negative 65 Fatigue: S—N curves Fatigue limit (endurance limit) occurs for some materials (some Fe and Ti allows). In this case, the S—N curve becomes horizontal at large N. The fatigue limit is a maximum stress amplitude below which the material never fails, no matter how large the number of cycles is. 66 Fatigue: S—N curves In most alloys, S decreases continuously with N. In these cases the fatigue properties are described by: Fatigue strength: stress at which fracture occurs after specified number of cycles (e.g. 107) Fatigue life: Number of cycles to fail at specified stress level 67 Fatigue Design Parameters Fatigue limit, Sfat: no fatigue if S < Sfat Sometimes, the fatigue limit is zero! S = stress amplitude unsafe case for Al (typ.) safe 103 105 107 109 N = Cycles to failure Adapted from Fig. 8.17(a), Callister 6e. Adapted from Fig. 8.17(b), Callister 6e. 68 S-N Graph The stress-number of cycles to failure (S-N) curves for a tool steel and an aluminum alloy (c)2003 Brooks/Cole, a division of Thomson Learning, Inc. Thomson Learning ™ is a trademark used herein under license. 69 Fatigue Behavior of BCC versus FCC Metals Fractographic Evidence of Crack Growth fatigue striations 10 mm 71 Ni-base ALLOY TURBINE BLADE FATIGUE FAILURE Fatigue clam shell marker–band color changes due to differences in service-related oxide layer thickness Design and Safety Factors Design uncertainties mean we do not push the limit. Factor of safety, N Often N is between y working 1.2 and 4 N Example: Calculate a diameter, d, to ensure that yield does not occur in the 1045 carbon steel rod below. Use a factor of safety of 5. working 220,000N d 2 / 4 y N 5 73 Fatigue Crack Growth Once a crack is present in a material, it will tend to grow under the influence of cyclic loading. The crack may be initiated by fatigue, or may be preexisting from manufacture, or may be caused by an impact, or similar event (e.g., a thermal shock.) The crack will grow to a critical length then fracture of the component will occur. 74 Fatigue: Crack Initiation and Propagation Three stages of fatigue failure: 1. Crack initiation in the areas of stress concentration (near stress raisers) 2. Incremental crack propagation 3. Final rapid crack propagation after crack reaches critical size 75 Fatigue: Crack Initiation and Propagation Crack initiation at the sites of stress concentration (microcracks, scratches, indents, interior corners, dislocation slip steps, etc.). Quality of surface is important. Crack propagation Stage I: initial slow propagation along crystal planes with high resolved shear stress. Involves just a few grains, and has flat facture surface. Stage II: faster propagation perpendicular to the applied stress. Crack grows by repetitive blunting and sharpening process at crack tip. Rough fracture surface. Crack eventually reaches critical dimension and propagates very rapidly. 76 Crack Growth Mechanisms Load reduced No Load Loaded Slip No Load Max Load Loaded again77 Fatigue Fracture Surface Schematic representation of a fatigue fracture surface in a steel shaft, showing the initiation region, the propagation of fatigue crack (with beam markings), and catastrophic rupture when the crack length exceeds a critical value at the applied stress (c)2003 Brooks/Cole, a division of Thomson Learning, Inc. Thomson Learning ™ is a trademark used herein under license. 78 Cyclic Stress-Controlled Fatigue Total Fatigue Life (NT) is the Sum of the Number of Cycles Require to Initiate a Crack (Ni) plus the Number of Cycles to Propagate the Crack (NP) Factors That Affect Fatigue Life Magnitude of stress (mean, amplitude..) Quality of surface (scratches, sharp transitions and edges) Solutions: Polishing (removes machining flaws etc.) Introducing compressive stresses (compensate for applied tensile stresses) into thin surface layer by “Shot Peening” – firing small shot surface to be treated. High-tech solution- ion implantation, laser peening. Case Hardening – create C or N rich outer layer in steels by atomic diffusion from the surface. Makes harder outer layer and also introduces compressive stresses. Optimizing geometry – avoid internal corners, notches etc. 80 Improving Fatigue Life Impose a compressive surface stress (to suppress surface cracks from growing) Method 1: Shot Peening Method 2: Carburizing shot put surface into compression Remove stress concentrators. C-rich gas Adapted from Fig. 8.22, Callister 6e. Adapted from Fig. 8.23, Callister 6e. bad better bad better 81 Surface Treatment to Improve Fatigue Resistance SHOT–PEENED SURFACE in STEEL Residual Stress Pattern after Shot Peening Influence of Grinding & Shot–Peening on Overall Fatigue Limetime Laser Shot Peening Applied to Jet Engine Components Factors That Affect Fatigue Life: Environmental Effects Thermal fatigue: Thermal cycling causes expansion and contraction, hence thermal stress, if component is restrained. Solutions: Eliminate restraint by design Use materials with low thermal expansion coefficients Corrosion fatigue: Chemical reactions induce pits which act as stress raisers. Corrosion also enhances crack propagations. Solutions: Decrease corrosiveness of medium, if possible Add protective surface coating Add residual compressive stresses 86 Surprising Fatigue Failures Creep Creep is a time-dependent and permanent deformation of materials when subjected to a constant load at a high temperature (> 0.4 Tm). Examples: turbine blades, steam generators. 88 Elevated Temperature Effects on Materials Standard Tensile Test • Strain Rate Controlled Deformation • Monitor Load versus Displacement to Yield Stress versus Strain Standard Creep Test • Stress or Load Controlled Deformation • Monitor Displacement versus Time to Yield Strain versus Time Data Stages of Creep 1. Instantaneous deformation, mainly elastic. 2. Primary/transient creep. Slope of strain vs. time decreases with time: work-hardening 3. Secondary/steady-state creep. Rate of straining is constant: balance of work-hardening and recovery. 4. Tertiary. Rapidly accelerating strain rate up to failure: formation of internal cracks, voids, grain boundary separation, necking, etc. 91 Creep Test Data Analysis Region I: Primary Creep Region II: Secondary (Steady-State) Creep Region III: Tertiary Creep Deformation Mechanisms: Region I: Strain Hardening mechanisms associated with dislocation-obstacle interactions. Strain rate decreasing. Region II: Dynamic balance between hardening and recovery mechanisms. Dislocation-obstacle interactions versus dislocation-dislocation annihilation. Constant strain rate. Region III: Prior to fracture, void growth, cavitation, sample necking. Strain rate increasing. Mostly interested in Region II: Steady State As this region represents the major portion of component life. Parameters of Creep Behavior The stage secondary/steady-state creep is of longest duration and the steady-state creep rate is the most important parameter of the creep behavior in long-life applications. Another parameter, especially important in short-life creep situations, is time to rupture, or the rupture lifetime, tr. 93 Creep: Strain Time Plot (c)2003 Brooks/Cole, a division of Thomson Learning, Inc. Thomson Learning ™ is a trademark used herein under license. A typical creep curve showing the strain produced as a function of time for a constant stress and temperature 94 Creep Behavior Occurs at elevated temperature, T > 0.4 Tmelt Deformation changes with time. Adapted from Figs. 8.26 and 8.27, Callister 6e. 2195 Creep: Stress and Temperature Effects With increasing stress or temperature The instantaneous strain increases The steady-state creep rate increases The time to rupture decreases 96 Creep Stress and Temperature Effects The effect of temperature or applied stress on the creep curve (c)2003 Brooks/Cole, a division of Thomson Learning, Inc. Thomson Learning ™ is a trademark used herein under license. 97 Creep Stress and Temperature Effects The stress/temperature dependence of the steady-state creep rate can be described by where Qc is the activation energy for creep, K2 and n are material constants. (Remember the Arrhenius dependence on temperature for thermally activated processes that we discussed for diffusion?) 98 Secondary Creep stress exponent (material parameter) Q c . n es K 2 exp activation energy for creep RT (material parameter) Most of component life spent here. Strain rate is constant at a given T, s strain hardening is balanced by recovery Strain rate increases for larger T, s applied stress 200 100 40 20 10 Stress (MPa) 427C 538C 649C Adapted from Fig. 8.29, Callister 6e.(Fig. 8.29 is from Metals Handbook: Properties and Selection: Stainless Steels, Tool Materials, and Special Purpose Metals, Vol. 3, 9th ed., D. Benjamin (Senior Ed.), American Society for Metals, 1980, p. 131.) strain rate material const. 1 10-2 10-1 Steady state creep rate es (%/1000hr) 22 99 Mechanisms of Creep Different mechanisms are responsible for creep in different materials and under different loading and temperature conditions. The mechanisms include Stress-assisted vacancy diffusion Grain boundary diffusion Grain boundary sliding Dislocation motion Different mechanisms result in different values of n, Qc. 100 Creep Mechanisms 101 Alloys for High-Temperature Use (turbines in jet engine, hypersonic airplanes, nuclear reactors, etc.) Creep is generally minimized in materials with: High melting temperature High elastic modulus Large grain sizes (inhibits grain boundary sliding) Following materials are excellent resilient to creep: Stainless steel Refractory metals (containing elements of high melting point, like Nb, Mo, W, Ta) Superalloys (Co, Ni based alloys) 102 High Temperature Structural Materials 103 Creep: Engineering Applications 104 Practical Implications for Engineering Applications Negative or Limiting Implications: Time dependent deformation means component part shapes, sizes, properties vary over time. Critical Applications: • Turbine blades in Jet Engines and Gas Turbine Engines • Nuclear Fuel Elements (Both in-service and Long Term Storage) Practical Implications for Engineering Applications Negative or Limiting Implications: Time dependent deformation means component part shapes, sizes, properties vary over time. Critical Applications: • Turbine blades in Jet Engines and Gas Turbine Engines • Nuclear Fuel Elements (Both in-service and Long Term Storage) 107 Summary Make sure you understand language and concepts: Brittle fracture Charpy test Corrosion fatigue Creep Ductile fracture Ductile-to-brittle transition Fatigue Fatigue life Fatigue limit Fatigue strength Fracture toughness Impact energy Intergranular fracture Izod test Stress raiser Thermal fatigue Transgranular fracture 108